CN106619266A - Natural cherry blossom petal and hydrolat thereof - Google Patents
Natural cherry blossom petal and hydrolat thereof Download PDFInfo
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- CN106619266A CN106619266A CN201610887110.3A CN201610887110A CN106619266A CN 106619266 A CN106619266 A CN 106619266A CN 201610887110 A CN201610887110 A CN 201610887110A CN 106619266 A CN106619266 A CN 106619266A
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- oriental cherry
- picked
- hydrosol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
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- Biotechnology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Engineering & Computer Science (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses natural cherry blossom petal and hydrolat thereof. The hydrolat mainly comprises manually picked natural cherry blossom petals and cherry blossom extract and the like. The hydrolat has effects of preserving moisture, whitening skin and delaying skin aging and the like, and the smell is aromatic and pleasant.
Description
Technical field
The present invention relates to daily necessities field, specially a kind of to be rich in natural oriental cherry petal and its hydrosol.
Background technology
Shower cream be it is a kind of formed by surfactant and conditioner modulation, usual only clean result, single function,
With the raising of human living standard, the effect having to shower cream is also constantly increasing, such as antibacterial, anti-ageing work(of waiting for a long time
Effect is increasingly welcome by consumers in general.《A kind of whitening and skin-protecting shower cream》(application number：CN201010245208.1), it is public
A kind of shower cream containing compositions such as apricot kernel oil, folium isatidis, light-coloured vinegar, the bighead atractylodes rhizome, the root of Dahurain angelica, Folium Isatidis extracts is opened, with decontamination, has been protected
Wet, whitening function, but it has been short of at anti-oxidant aspect；《A kind of shower cream》(application number：CN201410516847.5),
Disclose one kind and contain the compositions such as sodium laureth sulfate, flavoring rose essence, vegetable protein, neopelex, citric acid
Shower cream, the effect with whitening and moistening skin equally, has been short of in terms of delay skin aging.
The content of the invention
To make up problems and shortcomings present in existing shower cream, the invention discloses a kind of rich in the natural of picked by hand
Oriental cherry petal and its hydrosol.Fragrant odour, foam is fine and smooth abundant easily to be rinsed, moderate performance, skin whitening, moisturizing, deep layer cleaning it is same
When, delay skin aging makes skin recover delicate.
The present invention is achieved by the following scheme：
A kind of natural oriental cherry petal rich in picked by hand and its hydrosol, mainly including following component：
Further, the surfactant is laureth sodium sulfovinate, Cocoamidopropyl betaine, laruyl alcohol
The mixture of sodium sulfovinate, coconut oleoyl amine DEA.
Further, the preservative is methylisothiazolinone, the mixture of iodine propilolic alcohol butyl mephenesin Carbamate.
Further, the chelating agent is methacrylaldehyde/acrylic copolymer, the mixture of EDETATE SODIUM.
Further, the PH conditioning agents are potassium hydroxide, the mixture of citric acid.
Further, the pigment is CI 19140, the mixture of CI 10020.
Wherein, described oriental cherry extract is prepared by the following method and forms：
(1) the natural oriental cherry petal of 1 part of picked by hand is weighed, by 1:10 solid-liquid ratio, by the petal 80% second is immersed
Alcohol soaks 30min；
(2) mixed liquor of step (1) is placed in into heating and refluxing extraction 1.5h in water-bath, is filtered, collect filtrate, filter residue uses 8
Again 80% ethanol of amount repeats to extract once, merges filtrate twice；
(3) by the filtrate reduced in volume in step (2) to without alcohol taste, concentrate is inhaled by AB-8 macroporous resin columns
It is attached, first with distillation water elution, then 60% ethanol elution is used, 60% ethanol eluate is collected, oriental cherry extraction is obtained after reduced pressure concentration
Thing.
Further, the preparation method of the hydrosol is as follows：
(1) deionized water in formula is weighed, 75-80 DEG C is heated to, surfactant, chela is added under stirring condition according to this
Mixture, glycine, polyethylene glycol -90M, dipropylene glycol, homogeneous, to being completely dissolved；
(2) addition essence, UVNUL MS-40, oriental cherry extract, pigment, preservative when being cooled to 40-45 DEG C, stirring, homogeneous,
PH is adjusted, addition oriental cherry petal after room temperature is down to.
Cherry petal extract has oxidation resistant effect, removes the free radical of skin surface, and delaying skin aging keeps U.S. flesh
State (《The antioxidation in vitro function of oriental cherry extract and safety research》, Zhang Yunqing, Yin Songchao)；Simultaneously black can also be suppressed
The generation of element, skin whitening；And the fragrance of oriental cherry can make one to loosen, prevent from being still drank after a night.
Selected petal of the invention gets in morning band dew picked by hand, tender flower is especially selected, per piece
Petal thickness is uniform, and frivolous softness farthest remains the beneficiating ingredient in oriental cherry petal.
The invention has the advantages that：The oriental cherry petal of natural picked by hand is added in the shower cream of the present invention,
Tenderness massage of the natural aromatic and petal of oriental cherry to skin surface, can make whole bathing experience full of temperament and interest, the heart of releiving
Feelings, discharge pressure, and are conducive to the further removal of skin dirt；Further, add in formula and carried by fresh oriental cherry
The oriental cherry extract for taking, has good inhibition to the free radical of human body surface, while melanic formation can be suppressed,
This product is made while with good cleaning effect, moreover it is possible to slow down the daily aging course of skin, skin whitening allows skin
Gradually recover young vigor.
Description of the drawings
Fig. 1 is impact figure of the test sample to pathogen growth curve.
Specific embodiment
The integral production method of shower cream of the present invention is as follows：
(1) deionized water in formula is weighed, 75-80 DEG C is heated to, surfactant, chela is added under stirring condition according to this
Mixture, glycine, polyethylene glycol -90M, dipropylene glycol, homogeneous, to being completely dissolved；
(2) addition essence, UVNUL MS-40, oriental cherry extract, pigment, preservative when being cooled to 40-45 DEG C, stirring, homogeneous,
PH is adjusted, addition oriental cherry petal after room temperature is down to.
Finally, according in the preparation method, the difference of each component content can specifically be divided into following 5 embodiments：
Embodiment 1
| Component | Weight portion/part |
| Natural oriental cherry petal | 2 |
| Oriental cherry extract | 5 |
| Laureth sodium sulfovinate | 5 |
| Cocoamidopropyl betaine | 3 |
| Laruyl alcohol sodium sulfovinate | 3 |
| Coconut oleoyl amine DEA | 0.5 |
| Methylisothiazolinone | 0.002 |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.02 |
| Methacrylaldehyde/acrylic copolymer | 0.05 |
| EDETATE SODIUM | 0.05 |
| Potassium hydroxide | 0.02 |
| Citric acid | 0.03 |
| Dipropylene glycol | 5 |
| Polyethylene glycol -90M | 0.2 |
| UVNUL MS-40 | 0.02 |
| Glycine | 0.05 |
| Essence | 0.1 |
| CI 19140 | 0.02 |
| CI 10020 | 0.03 |
| Deionized water | 75 |
Embodiment 2
| Component | Weight portion/part |
| Natural oriental cherry petal | 5 |
| Oriental cherry extract | 10 |
| Laureth sodium sulfovinate | 10 |
| Cocoamidopropyl betaine | 5 |
| Laruyl alcohol sodium sulfovinate | 8 |
| Coconut oleoyl amine DEA | 2 |
| Methylisothiazolinone | 0.008 |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.05 |
| Methacrylaldehyde/acrylic copolymer | 0.1 |
| EDETATE SODIUM | 0.1 |
| Potassium hydroxide | 0.04 |
| Citric acid | 0.06 |
| Dipropylene glycol | 10 |
| Polyethylene glycol -90M | 1.5 |
| UVNUL MS-40 | 0.07 |
| Glycine | 0.1 |
| Essence | 0.2 |
| CI 19140 | 0.04 |
| CI 10020 | 0.06 |
| Deionized water | 48 |
Embodiment 3
Embodiment 4
| Component | Weight portion/part |
| Natural oriental cherry petal | 3 |
| Oriental cherry extract | 6.25 |
| Laureth sodium sulfovinate | 6.25 |
| Cocoamidopropyl betaine | 3.5 |
| Laruyl alcohol sodium sulfovinate | 4.25 |
| Coconut oleoyl amine DEA | 0.875 |
| Methylisothiazolinone | 0.0035 |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.0275 |
| Methacrylaldehyde/acrylic copolymer | 0.0625 |
| EDETATE SODIUM | 0.0625 |
| Potassium hydroxide | 0.025 |
| Citric acid | 0.0375 |
| Dipropylene glycol | 6.25 |
| Polyethylene glycol -90M | 0.525 |
| UVNUL MS-40 | 0.035 |
| Glycine | 0.0625 |
| Essence | 0.125 |
| CI 19140 | 0.0215 |
| CI 10020 | 0.041 |
| Deionized water | 69 |
Embodiment 5
Comparative example 1
| Component | Weight portion/part |
| Oriental cherry extract | 7.5 |
| Laureth sodium sulfovinate | 5.5 |
| Cocoamidopropyl betaine | 4 |
| Laruyl alcohol sodium sulfovinate | 5.5 |
| Coconut oleoyl amine DEA | 1.25 |
| Methylisothiazolinone | 0.005 |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.035 |
| Methacrylaldehyde/acrylic copolymer | 0.075 |
| EDETATE SODIUM | 0.075 |
| Potassium hydroxide | 0.03 |
| Citric acid | 0.045 |
| Dipropylene glycol | 7.5 |
| Polyethylene glycol -90M | 1.5 |
| UVNUL MS-40 | 0.045 |
| Glycine | 0.075 |
| Essence | 0.15 |
| CI 19140 | 0.035 |
| CI 10020 | 0.04 |
| Deionized water | 68 |
Comparative example 2
Efficacy validation
1) performance of keeping humidity test
The each 10g of following formulation samples of experimental design table 1 is weighed respectively, and uniform application is 40* in 6cm adhesive plasters, size is stained with
In 25 measuring cup, do not add a cover, be placed in 29 DEG C, during relative humidity (RH) is for 40% ± 5% constant temperature and humidity plant incubator, often
Took out every 3 hours and weigh, as shown in Table 1, parallel test 3 times calculates according to the following formula average percentage of water loss to weighing results：
Percentage of water loss %=W1-W2/W1-W × 100%；
Wherein, W1 is the measuring cup weight of sample before experiment, gram；
W2 is sample machine measuring cup weight after specific time interval, gram；
W is measuring cup weight, gram.
Table 1：Shower cream and the performance of keeping humidity test and comparison of like product prepared by embodiment, comparative example
The moistening effect that can be seen that shower cream of the present invention by the experimental data table of embodiment is good, and moistening effect will
Better than certain brand shower cream of same type；Lack the shower cream product of fresh oriental cherry petal and oriental cherry extract, its moisturizing respectively
Property will be less than comparative example made by shower cream finished product.And in the complete embodiment of two kinds of compositions, oriental cherry extract with it is fresh
Petal composition Synergistic, making the moistening effect of shower cream of the present invention has and is obviously improved.
2) antioxygenic property test：
Represent that it is eliminated to organic free radical with spectrophotometer method measure, plus the decline that OD514 absorbs after antioxidant
Ability.DPPH is first dissolved with a small amount of ethanol solution, and is configured to 1 × 10-4mol/L with 10% ethanol, is kept in dark place.Take
2molDPPH solution, adds 2mL shower creams to be sufficiently mixed, and it is determined in 514nm (maximum absorption wave strong point) after 30 minutes
OD514, shower cream amount is as non-oxidizability index needed for remove DPPH50% i.e. IC50.Clearance rate P calculates available following formula：
P=[A0- (Ai-Aj)]/A0
In formula, the absorbance of A0=2mLDPPH solution+2mL solution；Ai=2mLDPPH solution+2mL the present embodiment 1-5 and
The absorbance of comparative example 1-4 shower cream；The absorbance of Aj=2mL the present embodiment shower cream+2mL solvents.
Test result indicate that, the external each embodiment for removing DPPH free radicals (1 × 10-4mol/L) 50% i.e. needed for IC50
And the shower cream amount needed for comparative example is as shown in the table：
Table 2：Antioxygenic property table
As can be seen that compared with comparative example and certain shower cream, shower cream of the present invention has prominent external removing free radical
Ability, the performance with good anti-oxidant delay skin aging.
3) fungistatic effect test
In order to study inhibition of the shower cream product of the present invention that with the addition of oriental cherry extract to body surface bacterium, take
Same amount of embodiment 3, comparative example 1, the sample of comparative example 2, test identical bacterium colony sample, bacterium in analysis each group
The growth curve for falling, as shown in Figure 1.
The result shown from Fig. 1 can be seen that the shower cream fungistatic effect of the present invention is good, and extract while adding oriental cherry
Due to both Synergistics after thing and fresh oriental cherry petal, its fungistatic effect will be obviously improved.
4) using effect：
Respectively choosing 25-35 year for embodiment 1-5, comparative example 1-2 and certain brand shower cream has different degrees of skin mistake
Quick, itch women is each 100.
Usage cycles 2 months, take a shower use above-mentioned shower cream product every time, are tied as follows after observation using effect
Really：
The using effect of table 3 is counted
Shown using result, skin smooth moistens after the shower cream bath prepared by the present invention, and Long-Time Service can suppress skin
Aging makes it recover elasticity in the past, while the bacterium of body surface can be suppressed, builds the skin environment of health, and using effect is excellent
Certain brand shower cream on market；And under conditions of oriental cherry extract or oriental cherry petal is lacked, two kinds of compositions cannot be assisted
Same synergy so as to which beneficial effect is substantially reduced.
Embodiment described above only expresses the several embodiments of the present invention, and its description is more concrete and detailed, but not
Therefore the restriction to the scope of the claims of the present invention can be interpreted as.It should be pointed out that for the person of ordinary skill of the art,
Without departing from the inventive concept of the premise, some deformations and improvement can also be made, these belong to protection scope of the present invention.
Claims (9)
1. a kind of natural oriental cherry hydrosol rich in picked by hand, the hydrosol is mainly including the natural oriental cherry petal 2- of picked by hand
5 parts, oriental cherry extract 5-10 parts.
2. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 1, it is characterised in that the hydrosol is also
Including the composition of following weight portion：
。
3. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 2, it is characterised in that live on the surface
Property agent be laureth sodium sulfovinate, Cocoamidopropyl betaine, laruyl alcohol sodium sulfovinate, the mixing of coconut oleoyl amine DEA
Thing.
4. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 2, it is characterised in that the preservative
For methylisothiazolinone, the mixture of iodine propilolic alcohol butyl mephenesin Carbamate.
5. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 2, it is characterised in that the chelating
Agent is methacrylaldehyde/acrylic copolymer, the mixture of EDETATE SODIUM.
6. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 2, it is characterised in that the PH is adjusted
Agent is potassium hydroxide, the mixture of citric acid.
7. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 2, it is characterised in that the pigment is
The mixture of CI 19140, CI 10020.
8. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 1, it is characterised in that the oriental cherry is carried
Take thing and be prepared by the following method and form：
(1) the natural oriental cherry petal of 1 part of picked by hand is weighed, by 1:10 solid-liquid ratio, by the petal leaching of 80% ethanol is immersed
Bubble 30min；
(2) mixed liquor of step (1) is placed in into heating and refluxing extraction 1.5h in water-bath, is filtered, collect filtrate, filter residue is measured with 8 times
80% ethanol repeats to extract once, merges filtrate twice；
(3) by the filtrate reduced in volume of step (2) to without alcohol taste, concentrate is adsorbed by AB-8 macroporous resin columns, is first used
Distillation water elution, then 60% ethanol elution is used, 60% ethanol eluate is collected, oriental cherry extract is obtained after reduced pressure concentration.
9. a kind of natural oriental cherry hydrosol rich in picked by hand according to claim 1-8, it is characterised in that its preparation side
Method is as follows：
(1) deionized water in formula is weighed, 75-80 DEG C is heated to, surfactant, chelating is added under stirring condition according to this
Agent, glycine, polyethylene glycol -90M, dipropylene glycol, homogeneous, to being completely dissolved；
(2) essence, UVNUL MS-40, oriental cherry extract, pigment, preservative are added when being cooled to 40-45 DEG C, stirring, homogeneous are adjusted
PH, is down to addition oriental cherry petal after room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610887110.3A CN106619266A (en) | 2016-10-11 | 2016-10-11 | Natural cherry blossom petal and hydrolat thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610887110.3A CN106619266A (en) | 2016-10-11 | 2016-10-11 | Natural cherry blossom petal and hydrolat thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106619266A true CN106619266A (en) | 2017-05-10 |
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ID=58855264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610887110.3A Pending CN106619266A (en) | 2016-10-11 | 2016-10-11 | Natural cherry blossom petal and hydrolat thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106619266A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108498411A (en) * | 2018-06-28 | 2018-09-07 | 厦门柔丝丽生物科技有限公司 | A kind of petal shower cream and preparation method thereof |
| CN111714423A (en) * | 2020-07-31 | 2020-09-29 | 广州环亚化妆品科技有限公司 | Traditional Chinese medicine composition extract with effects of resisting aging and relieving allergy, and preparation method and application thereof |
-
2016
- 2016-10-11 CN CN201610887110.3A patent/CN106619266A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108498411A (en) * | 2018-06-28 | 2018-09-07 | 厦门柔丝丽生物科技有限公司 | A kind of petal shower cream and preparation method thereof |
| CN111714423A (en) * | 2020-07-31 | 2020-09-29 | 广州环亚化妆品科技有限公司 | Traditional Chinese medicine composition extract with effects of resisting aging and relieving allergy, and preparation method and application thereof |
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