CN104434644A - Facial cleanser containing cucumber extraction - Google Patents
Facial cleanser containing cucumber extraction Download PDFInfo
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- CN104434644A CN104434644A CN201410650627.1A CN201410650627A CN104434644A CN 104434644 A CN104434644 A CN 104434644A CN 201410650627 A CN201410650627 A CN 201410650627A CN 104434644 A CN104434644 A CN 104434644A
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Abstract
The invention provides a facial cleanser containing cucumber extraction; the facial cleanser provided by the invention contains the cucumber extraction, an amino acid type surface active agent and a thickening agent; and the content of the cucumber extraction is 1-10%w/w. According to the invention, cucumber juice is extracted in a flash manner, so that the active ingredients of plants are reserved to the most extent and cannot be destroyed after being heated; the use amount of a solvent is low; the extraction time is short; water-soluble functional components in cucumber juice can be extracted sufficiently; after being effectively compatible with the amino acid type surface active agent, the weakly acidic facial cleanser close to human skin (the pH of human skin is 4.2-6.5) can be prepared; and the facial cleanser containing cucumber extraction disclosed by the invention has the characteristics of being moderate, low in irritation and abundant in foam.
Description
Technical field
The present invention relates to cosmetic field, specifically, relate to a kind of Cleansing Foam containing cucumber extract.
Background technology
Cleansing Foam day by day accept by consumers in general, shortcomings such as using skinfeel after soap dry, puckery, tight can be overcome.Compared with traditional soap, Cleansing Foam foam is fine and smooth, abundant, thoroughly can remove cosmetics residual organic matter, come off horny layer, dredges the pore got clogged, and carries out the multiple efficacies such as moisturizing to skin, and skinfeel exquisiteness lubrication, experiences splendid.Cleansing Foam detergency mechanism, is the effect such as moistening, foaming by surfactant, the surface tension of dirt is declined, and is easy to rinse.
In Cleansing Foam, surfactant is divided into soap base type and non-soap fundamental mode two class, soap base class surfactant, and as dodecyl sodium sulfate, Polyoxyethylene Lauryl Ether, cost is low, but this kind of material is in alkalescence, and comparatively large to skin irritation, life-time service can destroy skin lipid layer.Amino acid type surfactant is lactate, and close to human body skin pH, skin-friendly is splendid, is suitable for life-time service.
Fructus Cucumidis sativi moisture, up to 96%-98%, containing the abundant many kinds of substance such as oligosaccharide, vitamin, polysaccharide, glycoprotein, chlorogenic acid, is the favorite of personage of liking to be beautiful, cucumber slice is directly spread on face, can play the multiple efficacies such as whitening, reduce wrinkle, moisturizing.The people such as Wang Changtao research shows that Fructus Cucumidis sativi has restraint of tyrosinase activity, antioxidation, SOD enzyme activity (Wang Changtao, Dong Yinmao, analogy sea is flourish, Beijing daily use chemicals, the fourth phase in 2007, P6-8) demonstrate Fructus Cucumidis sativi beauty functions further.
Cucumber extract is added Cleansing Foam, undoubtedly can organically in conjunction with cleaning action and Fructus Cucumidis sativi skin moistening effect of Cleansing Foam, but the preparation process of existing cucumber extract (Sucus Cucumidis sativi), if publication number is the Chinese patent application of CN103637936A, disclose a kind of preparation method of cucumber extract, comprise the steps: 1, choose fresh Gherkin, mince; 2, Sucus Cucumidis sativi is filtered; 3, the Sucus Cucumidis sativi of filtration is carried out upper pot and steam 2 minutes; 4, again Sucus Cucumidis sativi is filtered; 5, inside Sucus Cucumidis sativi, antiseptic is put into; 6, inside Sucus Cucumidis sativi, put into vitamin C, complete making.The method only relates to the separating steps such as squeezing, filtration, does not extract fully functional component.
For another example publication number is the patent application of CN103393584A, disclose a kind of Fructus Cucumidis sativi moisture retention liquid, be made up of the raw material of following weight percents: cucumber extract 25 ~ 35%, Mel 5%, amino acid humectant 1%, carbomer 2%, methyl parahydroxybenzoate 0.1%, all the other are for deionized water; Wherein, the preparation method of cucumber extract is: to squeeze the juice pulverizing after 1) being cleaned by Fructus Cucumidis sativi, adds the alcohol steep 2 hours of Cucumber weight 30%, gets filtrate; Add the ethanol lixiviate 2 hours of equivalent in filtering residue, get filtrate, merging filtrate; 2) filtrate reduced in volume, reclaims ethanol, obtains cucumber extract.The method introduces ethanol extraction step, but in Fructus Cucumidis sativi, aqueous soluble active constituent is present in cell, cannot reach effective extraction by means of only pulverizing, 30% alcohol steep.
Summary of the invention
In order to solve problems of the prior art, the object of this invention is to provide a kind of Cleansing Foam containing cucumber extract, homogenate extraction method is utilized fully to extract water solublity functional component in Fructus Cucumidis sativi, and obtained cucumber extract is combined with amino acid type surfactant and thickening agent compatibility, develop a foaming abundancy, bland skin moistening Cleansing Foam.
In order to realize the object of the invention, technical scheme of the present invention is as follows:
Containing a Cleansing Foam for cucumber extract, it is characterized in that, described Cleansing Foam contains cucumber extract, amino acid type surfactant and thickening agent, and the content of described cucumber extract is 1 ~ 10%w/w; Be preferably 3 ~ 7%w/w.
The pH value of described Cleansing Foam is 4.5 ~ 6.5.
Cleansing Foam of the present invention, controls its pH value in above-mentioned scope by adding known conventional pH adjusting agent where necessary.The selection of concrete pH adjusting agent and feed postition, for the routine of this area is selected, the present invention is not limited this.
Further, the preparation method of described cucumber extract is: by Fructus Cucumidis sativi stripping and slicing, squeeze the juice, gained Sucus Cucumidis sativi utilizes flash extracter at 0 ~ 4 DEG C, under 8000 ~ 12000rpm condition, extracts 0.5 ~ 3min, products therefrom adds the chitosan of 0.01 ~ 0.1%w/v, after ambient temperatare puts 2h, the centrifugal 15min of 5000rpm, gets supernatant, through 0.22 μm of filtration, to obtain final product.
Further, in described Cleansing Foam, the content of amino acid type surfactant is 5 ~ 25%w/w; Be preferably 8 ~ 15%w/w.
Further, in described Cleansing Foam, the content of thickening agent is 0.2 ~ 3%w/w.
Further, described amino acid type surfactant is selected from one or more in hydration sodium lauroyl sarcosine, sodium lauroyl glutamate, Disodium N-Coco acy-L-Glutamate, cocos nucifera oil acyl glycine potassium, cocos nucifera oil acyl glutamic acid, sodium cocoyl glutamate, cocos nucifera oil acyl Kaglutam, sodium cocoyl glycinate, cocoyl glutamic acid triethanolamine salt;
Preferably, described amino acid type surfactant is selected from one or more in hydration sodium lauroyl sarcosine, sodium lauroyl glutamate, Disodium N-Coco acy-L-Glutamate, cocos nucifera oil acyl Kaglutam.
Further, described thickening agent is selected from one or more in PEG-120 methyl dioleate (DOE120), acrylate copolymer (SF-1), Carbopol ETD 2020, CarbopolUltrez 20, hydroxyethyl-cellulose;
Preferably, described thickening agent is selected from one or both in acrylate copolymer, PEG-120 methyl dioleate, Carbopol ETD 2020.
Further, the invention provides a kind of concrete formula of the Cleansing Foam containing cucumber extract:
Further, the present invention provides a more preferred formula in the ratio range of above-mentioned formula, specifically composed as follows:
Further, the invention provides the concrete formula of the another kind of Cleansing Foam containing cucumber extract:
Further, the present invention provides a more preferred formula in the ratio range of above-mentioned formula, specifically composed as follows:
Cleansing milk of the present invention, wherein the consumption of water is as the criterion finally to make the total consumption of each component in cleansing milk formula reach 100%.
The present invention is except cucumber extract, and other used compositions are commercially available known product.
Beneficial effect of the present invention is:
The present invention is by carrying out homogenate extraction to Sucus Cucumidis sativi, retain effective ingredients in plant to greatest extent, heat damage can not be subject to, solvent load is little, extraction time is short, fully can extract water solublity functional component wherein, by itself and the effective compatibility of amino acid type surfactant, the faintly acid Cleansing Foam close to people's skin (people's skin pH4.2 ~ 6.5) can be prepared.Product of the present invention, has gentle zest little, fizzy feature.
In addition, the present invention utilize chitosan have good hydrophilic, parent Proteinaceous, to skin without irritated, non-stimulated, non-toxic reaction, make Cleansing Foam and contact skin sense obviously soft so obviously increase the affinity of skin.And chitosan has immunoregulatory activity, human body causes infection immunity to antibacterial, fungus can be increased, hinder former bacteria growing, not only can not cause infection to the skin of breakage, it also can be impelled to heal, eliminate facial dermatosis.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but it will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting scope of the present invention.Unreceipted actual conditions person in embodiment, the condition of conveniently conditioned disjunction manufacturer suggestion is carried out.Agents useful for same or the unreceipted production firm person of instrument, being can by the conventional products of commercial acquisition.
Prepared by embodiment 1 cucumber extract
Get 1kg and clean Fructus Cucumidis sativi, after stripping and slicing is squeezed the juice according to a conventional method, utilize flash extracter at 0 DEG C gained Sucus Cucumidis sativi, 8000rpm extracts 1min, gained juice adds after 0.025% chitosan ambient temperatare puts 2h, and the centrifugal 15min of 5000rpm, gets supernatant, through 0.22 μm of filtration, obtain cucumber extract.
By free radical scavenging test and MTT activity test, study above-mentioned cucumber extract, common Sucus Cucumidis sativi (extract without mishap, other step is same as embodiment 1) and the preparation method of cucumber extract prepares disclosed in CN103637936A and CN103393584A cucumber extract.
Concrete process of the test is as follows:
1) free radical scavenging test:
Test principle: DPPH is a kind of stable free radical in organic solvent, and its lone pair electrons have strong absorption (aobvious darkviolet) near 517nm.When organic scavenger exists, lone pair electrons are paired, and absorb and disappear or weaken, and by measuring the degree absorbing and weaken, can evaluate the activity of free radical scavenger.
Test method: extracting sample solution 2mL and concentration are that the DPPH solution 2mL of 100 μm of oL/L successively adds in same tool plug test tube, shake up; Left at room temperature 30min, working sample absorbance under 517nm wavelength.
Suppression ratio: K%=[1-(Ai-Aj)/Ac] × 100%
The absorbance of Ai:2mLDPPH solution+2mL product to be tested solution
The absorbance of Aj:2mL product to be tested solution+2mL solvent
The absorbance of Ac:2mLDPPH solution+2mL solvent
During test, product to be tested being unified diluted concentration is 0.1% (w/v)
2) MTT activity test
Take the logarithm the human epidermal cell HEK-n of trophophase, according to 1 × 10
5the concentration of cells/mL inoculates 96 orifice plates, every pore volume 200 μ L, after normal cultivation 24h, in protection group cell culture fluid, adds trial target respectively, after 5min, adopts 1mM H respectively
2o
2carry out oxidative damage process 6h.After oxidative damage process terminates, take out 96 well culture plates, abandon supernatant, after carefully rushing 2-3 time with PBS, then add the fresh medium of 200 μ L containing 0.5mg/mL MTT, continue at 37 DEG C, 5%CO
24h is cultivated under condition.After cultivation terminates, discard MTT solution, every hole adds 100 μ L DMSO, vibration mixing, surveys each hole absorbance (A490) that wavelength is 490nm, calculates cell survival rate.
Result of the test is in table 1.
The different Coupon Testing Results of table 1
| Title | The present invention | Carry without flash | CN103637936A | CN103393584A |
| Cucumber extract | The Sucus Cucumidis sativi got | Middle cucumber extract | Middle cucumber extract | |
| Clearance rate (%) | 85 | 53 | 35 | 48 |
| Cell survival rate (%) | 62 | 37 | 33 | 22 |
As shown in Table 1, the cucumber extract after mishap is extracted, its oxidation resistance (DPPH clearance rate can embody) and cell survival rate comparatively other groups have clear superiority; Without the Sucus Cucumidis sativi of homogenate extraction, because intracellular functional components is not discharged, therefore effect is undesirable; Cucumber extract in prior art CN103637936A, after extracting, carried out high-temperature process, its functional components is destroyed, and the actual constituent playing antioxidation is the vitamin C of follow-up interpolation; Cucumber extract in prior art CN103393584A, owing to using ethanol extraction, can not Ex-all completely in distillation is except the step of alcohol, residual ethanol produces to strengthen on cell survival rate to be affected.
Embodiment 2 cucumber extract Cleansing Foam
1, form
2, preparation method:
By above-mentioned prescription, prepare B, component C respectively, by two component mixing under 75 DEG C of conditions, and stir 30min under 300rpm condition, when being down to 40 DEG C, add component A, continue to stir 10min, be down to room temperature and get final product, product pH value is 5.8.
Embodiment 3 cucumber extract Cleansing Foam
1, form
2, preparation method:
Preparation method is with embodiment 2, and product pH value is 6.0.
Embodiment 4 cucumber extract Cleansing Foam
1, form
2, preparation method:
Preparation method is with embodiment 2, and product pH value is 6.5.
Embodiment 5 cucumber extract Cleansing Foam
1, form
2, preparation method:
Preparation method is with embodiment 2, and product pH value is 4.5.
Experimental example 1 irritation test
Experimental technique: choose 48 Cavia porcelluss of body weight between 350 ~ 450g, be divided into 8 groups at random, irritation test is carried out to following trial target.In test, guinea pig back is shaved hair, respectively about 0.2 gram of trial target is smeared to 1cm × 1cm region.Observe after 18h and smear Cleansing Foam area skin situation.
Trial target is as follows:
The product of sample 1-2 prepared by embodiment of the present invention 2-3;
Reference substance 11: the composition of reference example 2 and preparation method, unlike, will wherein hydration sodium lauroyl sarcosine remove, the content of Disodium N-Coco acy-L-Glutamate is brought up to 12.5%, all the other prescriptions and preparation method constant.
Reference substance 12: the composition of reference example 2 and preparation method, unlike, hydration sodium lauroyl sarcosine is changed to sodium dodecyl aminopropionitrile (amino acid type amphoteric surface active agent is commonly used in this area), other components and content constant.
Reference substance 13: the composition of reference example 2 and preparation method, unlike, Disodium N-Coco acy-L-Glutamate is changed to the amino sodium diformate (amino acid type amphoteric surface active agent is commonly used in this area) of dodecyl dimethylene, other components and content constant.
Reference substance 21: the composition of reference example 3 and preparation method, unlike, will wherein sodium lauroyl glutamate remove, the content of cocos nucifera oil acyl Kaglutam is brought up to 14%, all the other prescriptions and preparation method constant.
Reference substance 22: the composition of reference example 3 and preparation method, unlike, sodium lauroyl glutamate is changed to sodium dodecyl aminopropionitrile (amino acid type amphoteric surface active agent is commonly used in this area), other components and content constant.
Reference substance 23: the composition of reference example 3 and preparation method, unlike, cocos nucifera oil acyl Kaglutam is changed to the amino sodium diformate (amino acid type amphoteric surface active agent is commonly used in this area) of dodecyl dimethylene, other components and content constant.
The results are shown in Table shown in 2:
Guinea pig back change of skin after Cleansing Foam smeared by table 2
| Quantity | No change | Erythema, infiltration or pimple | Edematous erythema, pimple | Remarkable redness, companion's bulla |
| Sample 1 | 6 | 0 | 0 | 0 |
| Reference substance 11 | 6 | 0 | 0 | 0 |
| Reference substance 12 | 3 | 2 | 1 | 0 |
| Reference substance 13 | 3 | 2 | 1 | 0 |
| Sample 2 | 6 | 0 | 0 | 0 |
| Reference substance 21 | 6 | 0 | 0 | 0 |
| Reference substance 22 | 3 | 1 | 2 | 0 |
| Reference substance 23 | 3 | 2 | 1 | 0 |
As shown in Table 2, the present invention, by the selection to amino acid surfactant, makes Cleansing Foam product relative to the Cleansing Foam adopting other conventional amino acid surfactants, more gentle safe and non-stimulating.
Experimental example 2 foaming power and foaming stability test
Respectively by trial target described in embodiment 1, be mixed with 10% (percentage by weight) newborn solution, get 3mL and be placed in 50mL tool plug graduated cylinder, adding distil water is diluted to 15mL, add a cover, concuss 10 times, immediate record foam volume (mL), again record foam volume after 10min, the results are shown in Table 3:
Table 3 foaming power and foam stability result (ml)
| Title | Instant foam volume | Foam volume after 10min |
| Sample 1 | 35.2 | 34.3 |
| Reference substance 11 | 33.1 | 32.7 |
| Reference substance 12 | 25.4 | 16.4 |
| Reference substance 13 | 22.7 | 14.5 |
| Sample 2 | 38.5 | 36.4 |
| Reference substance 21 | 35.4 | 34.1 |
| Reference substance 22 | 26.9 | 17.2 |
| Reference substance 23 | 23.8 | 15.4 |
As shown in Table 3, the present invention is by the selection to amino acid surfactant, and make Cleansing Foam product relative to the Cleansing Foam adopting other conventional amino acid surfactants, foam is abundanter, and stability is better.
In order to verify the ageing of Cleansing Foam of the present invention, after each sample above-mentioned is placed 6 months and 12 months respectively, repeat above-mentioned identical test method, detect foaming power and the foam stability of each sample, experimental result is in table 4:
Table 4 foaming power and foam stability result (ml)
| Title | Instant foam volume | Foam volume after 10min |
| Sample 1 | 34.1 | 33.2 |
| Reference substance 11 | 32.5 | 31.4 |
| Reference substance 12 | 18.4 | 13.9 |
| Reference substance 13 | 16.8 | 8.5 |
| Sample 2 | 35.4 | 34.1 |
| Reference substance 21 | 33.6 | 31.8 |
| Reference substance 22 | 19.8 | 14.5 |
| Reference substance 23 | 17.7 | 10.2 |
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (10)
1., containing a Cleansing Foam for cucumber extract, it is characterized in that, described Cleansing Foam contains cucumber extract, amino acid type surfactant and thickening agent, and the content of described cucumber extract is 1 ~ 10%w/w, and the pH value of described Cleansing Foam is 4.5 ~ 6.5.
2. Cleansing Foam according to claim 1, it is characterized in that, the preparation method of described cucumber extract is: by Fructus Cucumidis sativi stripping and slicing, squeeze the juice, and gained Sucus Cucumidis sativi utilizes flash extracter at 0 ~ 4 DEG C, under 8000 ~ 12000rpm condition, extract 0.5 ~ 3min, products therefrom adds the chitosan of 0.01 ~ 0.1%w/v, after ambient temperatare puts 2h, the centrifugal 15min of 5000rpm, get supernatant, through 0.22 μm of filtration, to obtain final product.
3. Cleansing Foam according to claim 1 and 2, is characterized in that, in described Cleansing Foam, the content of amino acid type surfactant is 5 ~ 25%w/w; Be preferably 8 ~ 15%w/w.
4. Cleansing Foam according to claim 3, is characterized in that, in described Cleansing Foam, the content of thickening agent is 0.2 ~ 3%w/w.
5. Cleansing Foam according to claim 3, it is characterized in that, described amino acid type surfactant be selected from hydration sodium lauroyl sarcosine, sodium lauroyl glutamate, cocos nucifera oil acyl glutamic acid, sodium cocoyl glutamate, Disodium N-Coco acy-L-Glutamate, cocos nucifera oil acyl Kaglutam, sodium cocoyl glycinate, cocos nucifera oil acyl glycine potassium, cocoyl glutamic acid triethanolamine salt one or more;
Preferably, described amino acid type surfactant is selected from one or more in hydration sodium lauroyl sarcosine, sodium lauroyl glutamate, Disodium N-Coco acy-L-Glutamate, cocos nucifera oil acyl Kaglutam.
6. Cleansing Foam according to claim 4, it is characterized in that, described thickening agent be selected from PEG-120 methyl dioleate, acrylate copolymer, Carbopol ETD 2020, Carbopol Ultrez 20, hydroxyethyl-cellulose one or more;
Preferably, described thickening agent is selected from one or both in acrylate copolymer, PEG-120 methyl dioleate, Carbopol ETD 2020.
7. Cleansing Foam according to claim 1 and 2, is characterized in that, it is composed as follows:
8. Cleansing Foam according to claim 7, is characterized in that, it is composed as follows:
9. Cleansing Foam according to claim 1 and 2, is characterized in that, it is composed as follows:
10. Cleansing Foam according to claim 9, is characterized in that, it is composed as follows:
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| CN201410650627.1A CN104434644A (en) | 2014-11-14 | 2014-11-14 | Facial cleanser containing cucumber extraction |
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| CN104814887A (en) * | 2015-04-09 | 2015-08-05 | 兰柳生 | Cucumber facial cleanser |
| CN106491387A (en) * | 2016-12-06 | 2017-03-15 | 广州聚禅现代农业研究院有限公司 | A kind of skin Caring facial milk cleanser containing chive polysaccharide |
| CN107669574A (en) * | 2017-09-22 | 2018-02-09 | 广西巧恩茶业有限公司 | A kind of Jasmine Cleansing Foam |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104814887A (en) * | 2015-04-09 | 2015-08-05 | 兰柳生 | Cucumber facial cleanser |
| CN106491387A (en) * | 2016-12-06 | 2017-03-15 | 广州聚禅现代农业研究院有限公司 | A kind of skin Caring facial milk cleanser containing chive polysaccharide |
| CN107669574A (en) * | 2017-09-22 | 2018-02-09 | 广西巧恩茶业有限公司 | A kind of Jasmine Cleansing Foam |
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Application publication date: 20150325 |