CN105062731A - Fermented-shea-butter amino acid transparent soap - Google Patents
Fermented-shea-butter amino acid transparent soap Download PDFInfo
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Abstract
The invention discloses fermented-shea-butter amino acid transparent soap. The fermented-shea-butter amino acid transparent soap comprises, by weight, 25% to 45% of amino acid surfactants, 10% to 30% of triethanolamine, 5% to 15% of ethanol, 5% to 15% of polyhydric alcohol, 1% to 10% of fermented shea butter, 0.5% to 1.5% of urea, 0.5% to 3% of plant extract, 1% to 5% of monocrystal rock sugar, 0.1% to 0.3% of EDTA-disodium and the balance water. According to the amino acid transparent soap, as the water-soluble fermented shea butter is added, the amino acid transparent soap can have the advantages of being resistant to ultraviolet light, oxidation and aging, capable of achieving deep moistening, skin regenerating and moisture preserving and the like, is easy to absorb, mild and free of stimulation. The amino acid transparent soap is high in hardness, good in transparency, low in price, high in dirt removing capacity, free of pigment, preservatives, chlorine, phosphorus and the like, environmentally friendly and suitable for large-scale production, the amount of the added amino acid surfactants is small, long-short-chain cooperation is avoided, the production technology is simple, and the broad market prospects are achieved.
Description
Technical field
The present invention relates to a kind of fermentation shea butter amino acid transparent soap.
Background technology
Traditional soap is the general name of fatty acid metal salt, soap many employings grease in the market and alkaline matter obtain, meta-alkalescence, degreasing power are too strong, pungency large, foam is abundant not, product use after xerosis cutis, tight pungency is strong, peculiar smell is comparatively large, therefore must add a large amount of wetting Agent for Printing Inkss, grease to relax the stimulation to skin.
Grease is the natural high moleculer eompound by fat and glycerine chemical combination, has skin care, soft and smooth, moist, multiple efficacies such as solidification figuration and moisturizing etc., is widely used in makeup.Wherein, shea butter is called as from ancient times " gold of woman ", and its application in skin care product can trace back to the ancient Egypt Ke Liao Petra epoch, and shea butter contains the not saponification compositions such as abundant plant sterol and vitamin-E.Not saponification composition has moist moisturizing, resists ultraviolet effect, also has splendid maintenance, anti-inflammatory function, can promote wound healing.
Amino acid type surfactant is mainly used as the sanitas in medicine and makeup, and before its research starts from more than 40 year, research finds that it has good antiviral property, good security and skin-friendly, pungency are little.The amino acid soap soil removability utilizing amino acid surfactant to make is strong, and amino acid surfactant slant acidity, human body skin is also weakly acidic, thus its gentle, few stimulation.Meanwhile, also have that peculiar smell is little, environmental friendliness, security be high, readily biodegradable, with the consistency of other various tensio-active agent better, bacteriostasis property and the feature such as bactericidal property is good, there are wide market outlook.But the cost of amino acid type surfactant is high, general only as senior washing product.The market price of amino acid transparent soap is more than 150 yuan/block, and price comparison is expensive.
At present, mainly there is following problem in commercially available amino acid transparent soap: 1) addition of amino acid surfactant is very high, have also need by length chain amino acid tensio-active agent with the use of, formula is complicated, technique is loaded down with trivial details, this just makes the expensive of amino acid transparent soap, and application is very restricted; 2) with Viscotrol C and trolamine saponification, then add glucose and carry out crystallization to obtain certain degree of hardness, the amino acid transparent soap hardness obtained is less, and Viscotrol C itself has certain toxicity, not only harmful, also pollutes the environment; 3) because amino acid transparent soap is water miscible, and common grease belongs to oil soluble, immiscible with amino acid transparent soap system, muddiness can be produced, affect transparency and the hardness of amino acid transparent soap, cause system unstable and then affect the stability of amino acid soap simultaneously, therefore, do not occur the amino acid transparent soap containing Vegetable oil lipoprotein in the market.
Summary of the invention
The object of the present invention is to provide a kind of fermentation shea butter amino acid transparent soap.
The technical solution used in the present invention is: a kind of fermentation shea butter amino acid transparent soap, is made up of the raw material of following weight percentage:
Amino acid surfactant: 25 ~ 45%;
Trolamine: 10 ~ 30%;
Ethanol: 5 ~ 15%;
Polyvalent alcohol: 5 ~ 15%;
Fermentation shea butter: 1 ~ 10%;
Urea: 0.5 ~ 1.5%;
Plant milk extract: 0.5 ~ 3%;
Monocrystal rock sugar: 1 ~ 5%;
EDTA-disodium: 0.1 ~ 0.3%;
Surplus is water.
Described amino acid surfactant is at least one in sodium lauroyl glutamate, cocoyl propyl group glutaminate, cocounut oil acyl disodium glutamate, sodium cocoyl glutamate.
Described plant milk extract is at least one in green tea extract, camomile extract, Herba Saussureae Involueratae extract, Aloe extract, hamamelis extract, oat extract, Rhizoma Zingiberis Recens extract, rose extract, Radix Angelicae Sinensis extract, Radix Ginseng extract, Herba Lysimachiae foenumgraeci extract, Fructus Cucumidis sativi extract, Seaweed Extract.
Described polyvalent alcohol is at least one in ethylene glycol, propylene glycol, dipropylene glycol, butyleneglycol, glycerine, tetramethylolmethane, Xylitol, sorbyl alcohol.
Corresponding above-mentioned formula system, the preparation method of this kind of fermentation shea butter amino acid transparent soap comprises the following steps:
1) amino acid surfactant, ethanol, polyvalent alcohol, urea and water are mixed, be stirred and heated to 60 ~ 75 DEG C, dissolve completely to material;
2) add EDTA-disodium, stir;
3) fermentation shea butter is added, homogeneous 5 ~ 10 minutes;
4) slowly trolamine is added, regulation system pH value to 5.5 ~ 6.5;
5) add monocrystal rock sugar, stir, be incubated 10 ~ 15 minutes, froth breaking;
6) add plant milk extract, after stirring, pour mould into, cooling, shaping.
The invention has the beneficial effects as follows:
1) the fermentation shea butter of the present invention's employing, obtained through bio-fermentation process by missible oil wood and water, shea butter is converted to water-soluble through biological fermentation by oil soluble, can dissolve each other with formula system well.The laurate contained in fermentation shea butter has the effect of good antiultraviolet, vitamin-E and catechin have the anti-aging and skin repair effect of antioxygen, plant sterol has the effect of conditioning, and fermentation shea butter and human secretory grease index is very close, easily absorbs, non-stimulated, deep layer moist;
2) addition of amino acid surfactant is low, and without the need to length chain amino acid tensio-active agent with the use of, simplify formula, reduce cost;
3) adopt amino acid surfactant and trolamine saponification, then add monocrystal rock sugar and carry out crystallization, β type crystallization proportion is high, and the transparency of the amino acid transparent soap obtained is good, hardness is high;
4) plant milk extract added, can play Shu Min, balanced fat secretion, anti-inflammatory, antibacterial, effect such as maintenance skin gloss and elasticity etc.;
5) amino acid transparent soap of the present invention is weakly acidic, close with the pH value of skin, and gentle non-stimulated, comfort level is high;
6) do not add pigment and sanitas, the environmental pollutant such as not chloride, phosphorus, production technique is simple, and be suitable for scale operation, price is low, has wide market outlook.
Embodiment
The technical solution used in the present invention is: a kind of fermentation shea butter amino acid transparent soap, is made up of the raw material of following weight percentage:
Amino acid surfactant: 25 ~ 45%;
Trolamine: 10 ~ 30%;
Ethanol: 5 ~ 15%;
Polyvalent alcohol: 5 ~ 15%;
Fermentation shea butter: 1 ~ 10%;
Urea: 0.5 ~ 1.5%;
Plant milk extract: 0.5 ~ 3%;
Monocrystal rock sugar: 1 ~ 5%;
EDTA-disodium: 0.1 ~ 0.3%;
Surplus is water.
Preferably, described fermentation shea butter is obtained through bio-fermentation process by missible oil wood and water, during the fermentation, yeast can produce a kind of glycolipid bio-surfactant: mannosylerythritol lipid (as shown in the formula 1), the oil-soluble ingredients of this tensio-active agent in shea butter is combined, make it soluble in water, oil-soluble shea butter is converted to water miscible fermentation shea butter.
Wherein, n is the integer of 6 ~ 10.
Preferred further, described fermentation shea butter is the SheaButterST of DAMY Chemical Co., Ltd..
Preferably, described amino acid surfactant is at least one in sodium lauroyl glutamate, cocoyl propyl group glutaminate, cocounut oil acyl disodium glutamate, sodium cocoyl glutamate.
Preferably, described plant milk extract is at least one in green tea extract, camomile extract, Herba Saussureae Involueratae extract, Aloe extract, hamamelis extract, oat extract, Rhizoma Zingiberis Recens extract, rose extract, Radix Angelicae Sinensis extract, Radix Ginseng extract, Herba Lysimachiae foenumgraeci extract, Fructus Cucumidis sativi extract, Seaweed Extract.
Preferably, described polyvalent alcohol is at least one in ethylene glycol, propylene glycol, dipropylene glycol, butyleneglycol, glycerine, tetramethylolmethane, Xylitol, sorbyl alcohol.
Preferred further, described polyvalent alcohol is glycerine.
Corresponding above-mentioned formula system, the preparation method of this kind of fermentation shea butter amino acid transparent soap comprises the following steps:
1) amino acid surfactant, ethanol, polyvalent alcohol, urea and water are mixed, be stirred and heated to 60 ~ 75 DEG C, dissolve completely to material;
2) add EDTA-disodium, stir;
3) fermentation shea butter is added, homogeneous 5 ~ 10 minutes;
4) slowly trolamine is added, regulation system pH value to 5.5 ~ 6.5;
5) add monocrystal rock sugar, stir, be incubated 10 ~ 15 minutes, froth breaking;
6) add plant milk extract, after stirring, pour mould into, cooling, shaping.
Below in conjunction with embodiment, the present invention is further illustrated.
One fermentation shea butter amino acid transparent soap of the present invention, its preparation technology is as follows: amino acid surfactant, ethanol, polyvalent alcohol, urea and water are mixed, be stirred and heated to 60 ~ 75 DEG C, and insulation is to dissolving completely; Add with appropriate water-soluble EDTA-disodium, stir; Add fermentation shea butter, homogeneous 5 ~ 10 minutes; Slowly add with appropriate water-soluble trolamine, reconcile pH value to 5.5 ~ 6.5 of system; Add monocrystal rock sugar, stir, be incubated 10 ~ 15 minutes, froth breaking; Add plant milk extract, stir, pour mould into, cooling, shaping, namely obtain fermentation shea butter amino acid transparent soap.
Embodiment 1:
A kind of fermentation shea butter amino acid transparent soap, its raw material table 1 composed as follows:
Table 1 ferment shea butter amino acid transparent soap raw material composition
Raw material | Mass content (%) |
Sodium lauroyl glutamate | 17 |
Cocoyl propyl group glutaminate | 8 |
Trolamine | 30 |
Fermentation shea butter (Shea Butter ST) | 5 |
Ethanol | 5 |
Glycerine | 15 |
Herba Saussureae Involueratae extract | 0.5 |
Urea | 0.5 |
Monocrystal rock sugar | 5 |
EDTA-disodium | 0.1 |
Water | 13.9 |
Embodiment 2:
A kind of fermentation shea butter amino acid transparent soap, its raw material table 2 composed as follows:
Table 2 ferment shea butter amino acid transparent soap raw material composition
Raw material | Mass content (%) |
Sodium lauroyl glutamate | 23 |
Sodium cocoyl glutamate | 12 |
Trolamine | 20 |
Fermentation shea butter (Shea Butter ST) | 10 |
Ethanol | 11 |
Glycerine | 5 |
Aloe extract | 3 |
Urea | 1 |
Monocrystal rock sugar | 1 |
EDTA-disodium | 0.2 |
Water | 13.8 |
Embodiment 3:
A kind of fermentation shea butter amino acid transparent soap, its raw material table 3 composed as follows:
Table 3 ferment shea butter amino acid transparent soap raw material composition
Raw material | Mass content (%) |
Sodium lauroyl glutamate | 45 |
Trolamine | 10 |
Fermentation shea butter (Shea Butter ST) | 1 |
Ethanol | 15 |
Glycerine | 10 |
Oat extract | 1 |
Fructus Cucumidis sativi extract | 1 |
Urea | 1.5 |
Monocrystal rock sugar | 5 |
EDTA-disodium | 0.3 |
Water | 10.2 |
Test case 1:
Carry out performance test to amino acid transparent soap prepared by embodiment 1 ~ 3, the performance test data obtained is as following table 4:
The performance test data of the amino acid transparent soap of table 4 embodiment 1 ~ 3
Table 4 is the performance test data of the amino acid transparent soap of embodiment 1 ~ 3, and the standard index of institute's foundation is the physical and chemical index (QBT2485-2008) of soap.As can be seen from Table 4, amino acid transparent soap of the present invention is without dry soap (namely without saponification fat), and system is slightly acidic, and close to the normal ph of skin, and conventional toilet soaps is in alkalescence.Amino acid transparent soap alkali-free material of the present invention, chlorine and phosphorus, gentleer, environmental protection, has skin-care effect concurrently while decontamination, and life-time service security is high, skin effect good.Amino acid transparent soap foaming abundancy of the present invention, meets or exceeds other amino acid transparent soap on market.Amino acid transparent soap hardness of the present invention is high, the transparency good, inhibited from yellowing, free from extraneous odour suitable, cold-resistant, heat-resisting with the hardness of common soap.
Test case 2:
This test case is crowd's test result, to choose on market certain common clean facial soap and certain amino acid transparent soap in contrast.
Testing method: choose 14 volunteers, between 20 ~ 30 years old age, M-F is 1:1, and position on probation face, uses according to usually using the method for clean facial soap.
Table 5 organoleptic conditions:
As shown in Table 5: 1) satisfactory degree of the color and luster of amino acid transparent soap of the present invention, smell and hardness is obviously better than certain amino acid transparent soap on the market; 2) without under essence condition, amino acid transparent soap of the present invention does not have the soap base taste of common clean facial soap, and smell satisfactory degree is apparently higher than common clean facial soap; 3) satisfactory degree of amino acid transparent soap hardness of the present invention is basic maintains an equal level with common clean facial soap, is significantly better than certain amino acid transparent soap on the market.
Table 6 foam situation:
As shown in Table 6: amino acid transparent soap foaming abundancy of the present invention, durable lather, reach the level of common clean facial soap, certain amino acid transparent soap on market is better than.
Table 7 soil removability and the complexity rinsed well:
As shown in Table 7: amino acid transparent soap of the present invention, soil removability is significantly higher than common clean facial soap, and certain amino acid transparent soap is suitable on the market.Amino acid transparent soap of the present invention easily rinses, and crowd tests satisfactory degree higher than common clean facial soap.
Table 8 rinses tight sense and the stimulation degree of rear skin:
As shown in Table 8: amino acid transparent soap of the present invention has necessarily good moisture-keeping efficacy, the satisfactory degree of the tight sense of skin after rinsing is higher than common clean facial soap and certain amino acid transparent soap on the market.Amino acid transparent soap of the present invention, gentle non-stimulated, stimulate satisfactory degree apparently higher than common clean facial soap after rinsing, be slightly better than certain amino acid transparent soap on the market.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from spirit of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (5)
1. ferment a shea butter amino acid transparent soap, it is characterized in that: be made up of the raw material of following weight percentage:
Amino acid surfactant: 25 ~ 45%;
Trolamine: 10 ~ 30%;
Ethanol: 5 ~ 15%;
Polyvalent alcohol: 5 ~ 15%;
Fermentation shea butter: 1 ~ 10%;
Urea: 0.5 ~ 1.5%;
Plant milk extract: 0.5 ~ 3%;
Monocrystal rock sugar: 1 ~ 5%;
EDTA-disodium: 0.1 ~ 0.3%;
Surplus is water.
2. one fermentation shea butter amino acid transparent soap according to claim 1, it is characterized in that, described amino acid surfactant is at least one in sodium lauroyl glutamate, cocoyl propyl group glutaminate, cocounut oil acyl disodium glutamate, sodium cocoyl glutamate.
3. one fermentation shea butter amino acid transparent soap according to claim 1, it is characterized in that, described plant milk extract is at least one in green tea extract, camomile extract, Herba Saussureae Involueratae extract, Aloe extract, hamamelis extract, oat extract, Rhizoma Zingiberis Recens extract, rose extract, Radix Angelicae Sinensis extract, Radix Ginseng extract, Herba Lysimachiae foenumgraeci extract, Fructus Cucumidis sativi extract, Seaweed Extract.
4. one fermentation shea butter amino acid transparent soap according to claim 1, it is characterized in that, described polyvalent alcohol is at least one in ethylene glycol, propylene glycol, dipropylene glycol, butyleneglycol, glycerol, tetramethylolmethane, Xylitol, sorbyl alcohol.
5. the preparation method of a kind of shea butter amino acid transparent soap that ferments according to claim 1, is characterized in that: comprise the following steps:
1) amino acid surfactant, ethanol, polyvalent alcohol, urea and water are mixed, be stirred and heated to 60 ~ 75 DEG C, and keep constant temperature, material is dissolved completely;
2) add EDTA-disodium, stir;
3) fermentation shea butter is added, homogeneous 5 ~ 10 minutes;
4) slowly trolamine is added, regulation system pH value to 5.5 ~ 6.5;
5) add monocrystal rock sugar, stir, be incubated 10 ~ 15 minutes, froth breaking;
6) add plant milk extract, after stirring, pour mould into, cooling, shaping.
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Denomination of invention: Fermented-shea-butter amino acid transparent soap Effective date of registration: 20191226 Granted publication date: 20180213 Pledgee: China Co truction Bank Corp Guangzhou green finance reform and innovation pilot area Huadu Branch Pledgor: GUANGDONG ESSENCE BIOTECHNOLOGY CO., LTD. Registration number: Y2019440000320 |
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