CN110251428A - A kind of solid amino acid cleansing product and preparation method thereof - Google Patents
A kind of solid amino acid cleansing product and preparation method thereof Download PDFInfo
- Publication number
- CN110251428A CN110251428A CN201910494964.9A CN201910494964A CN110251428A CN 110251428 A CN110251428 A CN 110251428A CN 201910494964 A CN201910494964 A CN 201910494964A CN 110251428 A CN110251428 A CN 110251428A
- Authority
- CN
- China
- Prior art keywords
- amino acid
- acid
- solid amino
- face cleaning
- cleaning product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Abstract
The invention belongs to cosmetic technical fields, specifically disclose a kind of face cleaning product and preparation method thereof of solid amino acid.The present invention aiming at the shortcomings in the prior art, by the compounding of special ratios between pure amino acid surfactant, had not only solved the small defect of solid amino acid cleansing product itself hardness, but also solve the problems, such as that foam number is relatively fewer to a certain extent.Solid amino acid cleansing product of the invention can reach best in terms of foaming power, foam stability, foam exquisiteness degree, transparency, hardness comprehensive performance, and product is faintly acid, pH value and human skin are close, and skin does not have tight feeling after cleaning or false sliding sense, comfort level are high.
Description
Technical field
The present invention relates to daily chemical product fields, and the present invention relates to a kind of solid amino acid cleansing products and preparation method thereof.
Background technique
Surfactant is widely used in many industrial circles as important chemical products, and social required quantity
It is being continuously increased always.The application of conventional surfactant is while meeting people to life and production, also because it largely makes
With waste water after, for waste sludge discharge into water body and soil, bring environmental problem is also increasingly severe.Therefore in recent years, low toxicity,
The development and application of degradable green surfactant attracts attention.Amino acid surfactant is not only to environment
Highly-safe with organism, and, irritation is small, and low toxicity, biological degradability is good to hair and skin action temperature, and and other
The compatibility of various surfactants is preferable.Presently commercially available amino acid cleansing product specifically includes that liquid or cream shape product,
Such as Freeplus amino acid cleansing frost, II washing cream of SK, Avene cleansing mousse and solid amino acid cleansing product, such as DHC
Crystal soap.Relative to liquid or cream shape product, solid amino acid cleansing product can save preservative ingredient, therefore safer nothing
Stimulation, and its shape can carry out personalized customization according to the hobby of consumer.But for solid amino acid cleansing product
Speech, there is also some defects, such as foaming power are relatively fewer, hardness and transparency are not perfect, especially hardness, shaping packaging
Difficulty, and soften in the moist easy moisture absorption of environment, cause product not to be durable.Therefore, develop that a kind of foam exquisiteness is abundant, hardness
The solid pure amino acid face cleaning product all good with transparency is very important.
Summary of the invention
It is an object of the invention in view of the above problems, provide a kind of abundant foam exquisiteness, hardness and transparent
Spend the face cleaning product of all good solid pure amino acid compounding.
The purpose of the present invention is achieved through the following technical solutions: both can be with using the compounding between amino acid surfactant
The comprehensive performance of amino acid surfactant is improved, and the surfactant after compounding is with more excellent than single surfactant
Performance more, the face cleaning that can obtain the solid pure amino acid compounding that a kind of foam exquisiteness is abundant, hardness and transparency are all good produce
Product.
The present invention is achieved through the following technical solutions: a kind of face cleaning product of solid amino acid, and raw material includes such as the following group
Point:
N~acylamino acid: 30~38%；
Triethanolamine: 18~28%；
Ethyl alcohol: 5~13%；
Polyalcohol: 5~15%；
Surplus is water；
N~the acylamino acid is that cocoyl glutamic acid and lauroyl glutamate mix, its ratio be 1.5:1~
2:1。
N~the acylamino acid is that cocoyl glutamic acid and myristoyl glutamic acid mix, its ratio be
4:3~1:1.
N~the acylamino acid is that lauroyl glutamate and myristoyl glutamic acid mix, its ratio be
5:2~5:3.
N~the acylamino acid is that cocoyl glutamic acid, lauroyl glutamate and myristoyl glutamic acid are mixed
It closes, its ratio be 1:1:1~5:5:4.
N~the acylamino acid is cocoyl glutamic acid, lauroyl glutamate, myristoyl glutamic acid, the moon
Osmanthus acylglycine ratio is 2:2:1:1~6:4:3:2.
The polyalcohol is ethylene glycol, propylene glycol, dipropylene glycol, butanediol, glycerine, pentaerythrite, xylitol, sorb
At least one of alcohol.
The face cleaning product of the solid amino acid further includes the plant extracts of 1~5 parts by weight.
The plant extracts is green-tea extract, camomile extract, Herba Saussureae Involueratae extract, aloe extract, dent
Amaranth extract, mulberry root bark extract, ginseng extract, Herba Lysimachiae foenumgraeci extract, gadol extract, Astragalus Root P.E, seaweed mention
Take at least one of object.
The face cleaning product of the solid amino acid further includes urea, trehalose, glycine betaine, the EDTA- of 1~5 parts by weight
At least one of 2Na, Etidronic Acid.
The face cleaning product of the solid amino acid further includes the skin conditioning agent of 1~5 parts by weight, the skin conditioning agent
For at least one of shea butter, olive fruit oil, white pond flower seed oil, wheat-germ oil.
A kind of preparation method of the face cleaning product of solid amino acid is claimed in the present invention simultaneously, comprising the following steps:
(1) materials such as N- acylamino acid, water, ethyl alcohol, polyalcohol are mixed and is used as material, be stirred and heated to 70~75 DEG C, and
Constant temperature is kept, material is completely dissolved；
(2) 55~65 DEG C are heated to using triethanolamine as second material, constant temperature, for use；
(3) second material is slowly added into material, is slowly stirred, 70~75 DEG C of constant temperature are saponified 15~20 minutes, obtain soap lye；
(4) soap lye for obtaining step (3) sprays a small amount of ethyl alcohol and defoams, and is then injected into silica gel mould, demoulds after cooled and solidified,
Packaging is made to obtain the face cleaning product of solid amino acid after finishing.
Beneficial effects of the present invention:
1. the face cleaning product preparation process of solid amino acid of the invention is simple, the pure amino acid compounding face cleaning prepared is produced
The low stimulation of product, no anti-corrosion are free of petroleum resources surfactant.While its maximum feature is exactly high-efficiency cleaning, mild parent
Skin, low stimulation, pregnant woman, infant and sensitive skin can use.
2. pure amino acid compounding face cleaning product of the invention is faintly acid, pH value and human skin are close, in addition amino acid
It is the base substance for constituting protein, so mild pro-skin, can add different effects and play its different purposes.Skin after cleaning
Skin does not have tight feeling or false sliding sense, comfort level are high.
3. overcoming the deficiencies in the prior art, solid amino acid cleansing product of the invention is by pure amino acid surface-active
Compounding is made between agent, has not only solved the small defect of solid amino acid cleansing product itself hardness, but also solve to a certain extent
Foam number relatively fewer problem.Solid amino acid cleansing product of the invention is fine and smooth in foaming power, foam stability, foam
Degree, transparency, hardness comprehensive performance can reach best.
Specific embodiment
Below with reference to embodiment, the invention will be further described.
Comparative example 1-4 and the commercially available amino acid crystal soap (DHC) of comparative example 5:
| Raw material | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Cocoyl glutamic acid | 35 | 0 | 0 | 0 |
| Lauroyl glutamate | 0 | 35 | 0 | 0 |
| Myristoyl glutamic acid | 0 | 0 | 35 | 0 |
| Lauroyl glycine | 0 | 0 | 0 | 35 |
| Ethyl alcohol | 11 | 11 | 11 | 11 |
| Glycerine | 10 | 10 | 10 | 10 |
| Triethanolamine | 27 | 27 | 27 | 27 |
| Water | To 100 | To 100 | To 100 | To 100 |
Embodiment 1-7
| Raw material | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| Cocoyl glutamic acid | 23 | 20 | 0 | 11.7 | 12.5 | 13 |
| Lauroyl glutamate | 12 | 0 | 25 | 11.7 | 12.5 | 12 |
| Myristoyl glutamic acid | 0 | 15 | 10 | 11.7 | 10 | 6 |
| Lauroyl glycine | 0 | 0 | 0 | 0 | 0 | 4 |
| Ethyl alcohol | 11 | 11 | 11 | 11 | 11 | 11 |
| Glycerine | 10 | 10 | 10 | 10 | 10 | 10 |
| Triethanolamine | 27 | 27 | 27 | 27 | 27 | 27 |
| Water | To 100 | To 100 | To 100 | To 100 | To 100 | To 100 |
N- acylamino acid, ethyl alcohol, glycerine, water 70~75 DEG C will be stirred and heated to as material according to the above ratio, and kept
Constant temperature is completely dissolved material；55~65 DEG C are heated to using triethanolamine as second material, constant temperature, for use；Second material is slowly added to
It into material, is slowly stirred, 70~75 DEG C of constant temperature are saponified 15~20 minutes, obtain soap lye；Obtained soap lye is sprayed into a small amount of second
Alcohol defoaming, is then injected into silica gel mould, demoulds after cooled and solidified, and packaging is made to obtain the clean of solid amino acid after finishing
Face product.
Test case 1: foam test
1, test apparatus: Roche foam meter
2, testing procedure
(1) device is built, distilled water is added in super water-bath, opens super water-bath, constant temperature is in 40 positive and negative 0.5.Claim
900ml distilled water is added in the anhydrous magnesium sulfate and anhydrous calcium chloride solution measured 2.5g sample to be tested, respectively take 50ml.Use water-bath
41.5 °C are heated to, with distilled water flushing scale inside pipe wall, then scale inside pipe wall is rinsed with prepare liquid and must rinse well.
(2) graded tube piston is closed, injects about 50ml test solution with other minim pipette, stands 1min, regulating piston,
Make liquid level just at 50ml scale.
(3) minim pipette is filled 200ml test solution, minim pipette is arranged on prior ready pipe support and and scale
The section of pipe makes solution flow to the center of graded tube at vertical configuration, and the outlet of minim pipette should be placed on and 700mm graduation mark water
On horizontal line.
(4) piston for opening minim pipette, flows down solution.When the solution stream in minim pipette is complete, stopwatch is started immediately, and
Foam height is measured, 5min is then passed through, 10min, 15min re-record height, and foam value indicates it with foam height.
The above test 3 times is repeated, tube wall must be cleaned before test in order to avoid influencing data every time.Take being averaged for test
Value makees final result.
3, test specimen: the solid amino acid cleansing product of embodiment 1-7 and comparative example 1-5
1 foaming properties of table
| Just fall foam height (mm) | Foam height (mm) after 15 minutes | |
| Comparative example 1 | 140 | 137 |
| Comparative example 2 | 82 | 61.3 |
| Comparative example 3 | 123.3 | 36.3 |
| Comparative example 4 | 39.7 | 23 |
| Comparative example 5 | 80 | 60 |
| Embodiment 1 | 148.3 | 146.3 |
| Embodiment 2 | 149.7 | 145.3 |
| Embodiment 3 | 102.3 | 93 |
| Embodiment 4 | 161.7 | 158.7 |
| Embodiment 5 | 172.7 | 170.3 |
| Embodiment 6 | 143.3 | 140 |
As seen from the above table, only the foaming power of 1 product of comparative example and foam stability are best, the embodiment 1-6's by compounding
The abundant exquisiteness of foam, and stability is good.
Test case 2: dissolubility test
1, it test method: takes 5g product to be placed in a beaker in the normal-temperature water that 20g is added, observes the dissolved state of product.It is less susceptible to
It is dissolved in water meter and shows that the hardness of product is higher, it is more durable, it is easily worked transport.
2, test specimen: the solid amino acid cleansing product of embodiment 1-6 and comparative example 1-5.
2 solubility property of table
| It is completely dissolved the required time | |
| Comparative example 1 | 2 hours |
| Comparative example 2 | 2 hours 40 points |
| Comparative example 3 | 1 hour 40 points |
| Comparative example 4 | 4 hours 24 points |
| Comparative example 5 | 1 hour 40 points |
| Embodiment 1 | 3 hours 25 points |
| Embodiment 2 | 4 hours 38 points |
| Embodiment 3 | 3 hours 28 points |
| Embodiment 4 | 3 hours 26 points |
| Embodiment 5 | 3 hours 30 points |
| Embodiment 6 | 3 hours 19 points |
The completely required time longest of dissolution, illustrates that the hardness of product is higher, is less susceptible to dissolve needed for comparative example 4, other
The dissolution time of comparative example is shorter, and especially commercially available comparative example 5, hardness is not high, and product in use process is caused not to be durable.Compounding
Product embodiments 1-6 afterwards, the time being completely dissolved extend, and the hardness after illustrating amino acid compounding all increases.
Test case 3: transparency test
1, test method: solid amino acid cleansing product is cut into a thickness of flat and smooth thin in ± 0 .15mm of 6 .5, two sides
Piece measures the numerical value of the black backing time reflectivity of sample bottom liner in the fixed cylinder that not light influences on leucometer
(R0) and sample bottom liner blank interior numerical value (R in light reflectivity when serving as a contrast∞), and according to formula T (%)=(1-R0/R∞)×
100% calculates the transparency of product.
2, test specimen: the solid amino acid cleansing product of embodiment 1-6 and comparative example 1-5.
3 transparency of table
| Transparency | |
| Comparative example 1 | 89 |
| Comparative example 2 | 85 |
| Comparative example 3 | 15 |
| Comparative example 4 | 10 |
| Comparative example 5 | 88 |
| Embodiment 1 | 91 |
| Embodiment 2 | 89 |
| Embodiment 3 | 90 |
| Embodiment 4 | 87 |
| Embodiment 5 | 84 |
| Embodiment 6 | 85 |
As can be seen from the above table, the transparency of the solid amino acid cleansing product obtained after amino acid compounding is all good.
In conclusion it will be seen that solid amino acid cleansing product (the comparative example 1- that single amino acid is prepared
4) in the more or less all existing defects of foaming characteristic, foam stability, hardness and transparency comprehensive performance, such as comparative example 1, blistering
Power, foam stability and transparency are all very excellent, but hardness is very poor, and comparative example 4 has splendid hardness, but opaque, and steep
Foam amount is less.Even commercial product (comparative example 5), hardness be also it is very poor, be not durable very much in use.The present invention
By the compounding between amino acid, so that the comprehensive performance of solid amino acid cleansing product is optimal.
Test case 4:PH test
1, hydrogen phthalate first (PH=4) and mixed phosphate (PH=6.86) mark test method: are prepared with 250ml volumetric flask
It is fixed.With calibration liquid rinse beaker, it is then charged into appropriate calibration liquid.It measures solution temperature and PH meter temperature is calibrated according to solution temperature,
With the solution of calibration calibration PH meter, solution is changed every time all rinsed probe with wash bottle and then dried calibration with paper and finish.
2, test specimen: the solid amino acid cleansing product of embodiment 1-6 and comparative example 1-5.2g sample is weighed, is added
Distilled water is configured to solution to 20ml.
4 pH value of table
| PH value | |
| Comparative example 1 | 6.53 |
| Comparative example 2 | 6.39 |
| Comparative example 3 | 6.58 |
| Comparative example 4 | 7.32 |
| Comparative example 5 | 6.70 |
| Embodiment 1 | 6.38 |
| Embodiment 2 | 6.50 |
| Embodiment 3 | 6.98 |
| Embodiment 4 | 6.33 |
| Embodiment 5 | 6.34 |
| Embodiment 6 | 6.73 |
As can be seen from the above table, the solid amino acid cleansing product obtained after amino acid compounding is faintly acid, mild non-stimulated.
Claims (10)
1. a kind of face cleaning product of solid amino acid, raw material includes following component:
N~acylamino acid: 30~38%；
Triethanolamine: 18~28%；
Ethyl alcohol: 5~13%；
Polyalcohol: 5~15%；
Surplus is water；
N~the acylamino acid is that cocoyl glutamic acid and lauroyl glutamate mix, its ratio be 1.5:1~
2:1。
2. a kind of face cleaning product of solid amino acid, raw material includes following component:
N~acylamino acid: 30~38%；
Triethanolamine: 18~28%；
Ethyl alcohol: 5~13%；
Polyalcohol: 5~15%；
Surplus is water；N~the acylamino acid is that cocoyl glutamic acid and myristoyl glutamic acid mix, ratio
Example is 4:3~1:1.
3. a kind of face cleaning product of solid amino acid, raw material includes following component:
N~acylamino acid: 30~38%；
Triethanolamine: 18~28%；
Ethyl alcohol: 5~13%；
Polyalcohol: 5~15%；
Surplus is water；N~the acylamino acid is that lauroyl glutamate and myristoyl glutamic acid mix, ratio
Example is 5:2~5:3.
4. a kind of face cleaning product of solid amino acid, raw material includes following component:
N~acylamino acid: 30~38%；
Triethanolamine: 18~28%；
Ethyl alcohol: 5~13%；
Polyalcohol: 5~15%；
Surplus is water；
N~the acylamino acid be cocoyl glutamic acid, lauroyl glutamate and myristoyl glutamic acid mixing and
At its ratio be 1:1:1~5:5:4.
5. a kind of face cleaning product of solid amino acid, raw material includes following component:
N~acylamino acid: 30~38%；
Triethanolamine: 18~28%；
Ethyl alcohol: 5~13%；
Polyalcohol: 5~15%；
Surplus is water；N~the acylamino acid is cocoyl glutamic acid, lauroyl glutamate, myristoyl paddy ammonia
Acid, lauroyl glycine ratio are 2:2:1:1~6:5:3:2.
6. the face cleaning product of solid amino acid according to claims 1 to 5, which is characterized in that the polyalcohol is second two
At least one of alcohol, propylene glycol, dipropylene glycol, butanediol, glycerine, pentaerythrite, xylitol, sorbierite.
7. the face cleaning product of solid amino acid according to claims 1 to 5, which is characterized in that the solid amino acid
Face cleaning product further includes the plant extracts of 1~5 parts by weight；The plant extracts is green-tea extract, chamomile extraction
Object, Herba Saussureae Involueratae extract, aloe extract, purslane extract, mulberry root bark extract, ginseng extract, Herba Lysimachiae foenumgraeci extract,
At least one of gadol extract, Astragalus Root P.E, marine algae extract.
8. the face cleaning product of solid amino acid according to claims 1 to 5, which is characterized in that the solid amino acid
Face cleaning product further includes the urea of 1~5 parts by weight, trehalose, glycine betaine, EDTA-2Na, at least one in Etidronic Acid
Kind.
9. the face cleaning product of solid amino acid according to claims 1 to 5, which is characterized in that the solid amino acid
Face cleaning product, further includes the skin conditioning agent of 1~5 parts by weight, and the skin conditioning agent is shea butter, olive fruit oil, Bai Chi
At least one of flower seed oil, wheat-germ oil.
10. the preparation method of the face cleaning product of solid amino acid according to claims 1 to 5, which is characterized in that including with
Lower step:
(1) materials such as N- acylamino acid, water, ethyl alcohol, polyalcohol are mixed and is used as material, be stirred and heated to 70~75 DEG C, and
Constant temperature is kept, material is completely dissolved；
(2) 55~65 DEG C are heated to using triethanolamine as second material, constant temperature, for use；
(3) second material is slowly added into material, is slowly stirred, 70~75 DEG C of constant temperature are saponified 15~20 minutes, obtain soap lye；
(4) soap lye for obtaining step (3) sprays a small amount of ethyl alcohol and defoams, and is then injected into silica gel mould, demoulds after cooled and solidified,
Packaging is made to obtain the face cleaning product of solid amino acid after finishing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910494964.9A CN110251428A (en) | 2019-06-10 | 2019-06-10 | A kind of solid amino acid cleansing product and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910494964.9A CN110251428A (en) | 2019-06-10 | 2019-06-10 | A kind of solid amino acid cleansing product and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110251428A true CN110251428A (en) | 2019-09-20 |
Family
ID=67917226
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910494964.9A Pending CN110251428A (en) | 2019-06-10 | 2019-06-10 | A kind of solid amino acid cleansing product and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110251428A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111925872A (en) * | 2020-09-16 | 2020-11-13 | 广州美果生物科技有限公司 | Amino acid Q bomb handmade soap and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105062731A (en) * | 2015-08-20 | 2015-11-18 | 广州栋方生物科技股份有限公司 | Fermented-shea-butter amino acid transparent soap |
| CN105419991A (en) * | 2015-11-09 | 2016-03-23 | 重庆琥珀茶油有限公司 | Face-cleansing skin-moisturizing tea oil soap |
| CN105907501A (en) * | 2016-04-29 | 2016-08-31 | 佛山市芊茹化妆品有限公司 | Transparent amino acid compound soap and preparation method thereof |
| CN107435000A (en) * | 2017-08-04 | 2017-12-05 | 广州集芳丹生物科技有限公司 | A kind of pure amino acid facial soap and preparation method thereof |
| CN109370785A (en) * | 2018-09-30 | 2019-02-22 | 江门职业技术学院 | A kind of amino acid soap and preparation method thereof containing dried orange peel extracts |
-
2019
- 2019-06-10 CN CN201910494964.9A patent/CN110251428A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105062731A (en) * | 2015-08-20 | 2015-11-18 | 广州栋方生物科技股份有限公司 | Fermented-shea-butter amino acid transparent soap |
| CN105419991A (en) * | 2015-11-09 | 2016-03-23 | 重庆琥珀茶油有限公司 | Face-cleansing skin-moisturizing tea oil soap |
| CN105907501A (en) * | 2016-04-29 | 2016-08-31 | 佛山市芊茹化妆品有限公司 | Transparent amino acid compound soap and preparation method thereof |
| CN107435000A (en) * | 2017-08-04 | 2017-12-05 | 广州集芳丹生物科技有限公司 | A kind of pure amino acid facial soap and preparation method thereof |
| CN109370785A (en) * | 2018-09-30 | 2019-02-22 | 江门职业技术学院 | A kind of amino acid soap and preparation method thereof containing dried orange peel extracts |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111925872A (en) * | 2020-09-16 | 2020-11-13 | 广州美果生物科技有限公司 | Amino acid Q bomb handmade soap and preparation method thereof |
| CN111925872B (en) * | 2020-09-16 | 2021-11-12 | 广州美果生物科技有限公司 | Amino acid Q bomb handmade soap and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105062731B (en) | One kind fermentation shea butter amino acid transparent soap | |
| CN109401869B (en) | Liquid skin cleaning composition and preparation method and application thereof | |
| CN106010831B (en) | A kind of handmade soap and preparation method thereof | |
| CN106109275B (en) | A kind of foaming bath oil and preparation method thereof rich in vegetable oil | |
| CN105853271A (en) | Personnel cleaning composition containing Tuwei rose flower extract | |
| CN103690394A (en) | Anionic surfactant-free bubble bath agent | |
| CN109628242B (en) | Mild and stable soap-based facial cleanser and preparation method thereof | |
| CN107384597A (en) | A kind of amino acid soap and preparation method thereof | |
| CN109288725A (en) | A kind of transparent amino acid pattern is without silicone oil shampoo | |
| CN107648073A (en) | A kind of gentle oil-containing makeup removing foam | |
| CN110251428A (en) | A kind of solid amino acid cleansing product and preparation method thereof | |
| CN114452235B (en) | Avocado oil cleansing bubbles and preparation method thereof | |
| CN106366207B (en) | A kind of faenum graecum water-soluble polysaccharide hand cleanser and preparation method thereof | |
| RU2762972C1 (en) | Solid cleansing compositions and methods for their preparation | |
| CN110772437A (en) | Wash-free cleaning composition capable of rapidly absorbing oil, preparation method and application thereof in hair wet tissue | |
| CN107982110A (en) | One kind is without silicone oil shampoo | |
| CN108836938A (en) | A kind of environment-friendly composite foam hoof bath foam and preparation method thereof | |
| CN111437219B (en) | Weakly acidic body wash and preparation method thereof | |
| CN113876604B (en) | Amino acid facial cleanser with high paste forming temperature and preparation method thereof | |
| CN110384634A (en) | A kind of man's shower cream and preparation method thereof of more foam easy cleanings | |
| CN112516007B (en) | Cleaning composition | |
| CN108743444A (en) | Camellia breast shower frost and preparation method thereof | |
| CN108670893B (en) | Amino acid cleansing cream composition and preparation method thereof | |
| CN113476329A (en) | Plant sterol (ester) grease applied to shampoo or shower gel | |
| CN110946785A (en) | Mild cleansing cream |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |