CN105907501A - Transparent amino acid compound soap and preparation method thereof - Google Patents
Transparent amino acid compound soap and preparation method thereof Download PDFInfo
- Publication number
- CN105907501A CN105907501A CN201610277759.3A CN201610277759A CN105907501A CN 105907501 A CN105907501 A CN 105907501A CN 201610277759 A CN201610277759 A CN 201610277759A CN 105907501 A CN105907501 A CN 105907501A
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- China
- Prior art keywords
- acid
- aminoacid
- transparent soap
- composite transparent
- glutamic acid
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/04—Carboxylic acids or salts thereof
- C11D1/10—Amino carboxylic acids; Imino carboxylic acids; Fatty acid condensates thereof
Abstract
The invention discloses a transparent amino acid compound soap, comprising the following components by weight percent: 30-40% of long-chain acyl glutamic acid, 5-15% of polyhydric alcohols, 20-30% of triethanolamine, 1-10% of fatty acid, 0.2-2% of sodium hydroxide, with the balance being water. Components of the transparent amino acid compound soap are combined within a very certain range; due to the significant synergism, the prepared transparent compound soap has a moderate hardness, a relatively strong foaming ability and cleaning power; and the soap is faintly acid.
Description
Technical field
The invention belongs to household chemicals field, more particularly to a kind of aminoacid composite transparent soap and preparation method thereof.
Background technology
Aminoacid transparent soap is a kind of hands with amino acid type surfactant as primary surfactant risen in recent years
Work soap, has high, the good skin-friendly of faintly acid, transparency and safety, the feature weak to skin irritation, is increasingly consumed
Person is accepted.But, the production technology of current aminoacid transparent soap is the most ripe, and main cause is amino acid pattern surface activity
Foaming power and the cleaning force of agent are weak, cause soap body to be difficult to meet the demand of consumer's deep layer cleaning;Additionally there are amino acid pattern
The problem that the become soap body of surfactant is the softest, is easily caused deformation of products, in-convenience in use.
Chinese patent application CN201410470096.8 discloses the transparent solid of a kind of amino acid surfactant substrate
Soap, its composition includes each component of following weight portion: amino acid surfactant 55-75 part, pure water 3-13 part, Oleum Ricini gathers
Oxygen vinyl Ether (15-40EO) 3-10 part, glycerol 3-8 part, glucose 3-10 part, ethanol 2-8 part, PH poising agent 0.1-3 part, perfume (or spice)
Essence 0.2-0.5 part.This invention have employed castor oil polyoxyethylene ether (15-40EO) as auxiliary surfactant to promote soap
The cleaning force of body, but this cosurfactant is the solubilizing agent of a kind of high hlb, and foaming power own is weak, plays soap body
Bubble power castering action is little.
Summary of the invention
Based on this, it is an object of the invention to provide a kind of weakly acidic aminoacid composite transparent soap, have hardness moderate,
Foaming power and the stronger feature of cleaning force.
The concrete technical scheme solving above-mentioned technical problem is as follows:
A kind of aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Fatty acyl glutamic acid 30-40%
Polyhydric alcohol 5-15%
Triethanolamine 20-30%
Fatty acid 1-10%
Sodium hydroxide 0.2-2%
Water surplus.
Preferably, can also add sapindoside in aminoacid composite transparent soap of the present invention, its addition is
0.1-2wt%.Sapindoside is a kind of natural nonionic surfactant extracted in plant Fructus Sapindi Mukouossi fruit, has
Foaming abundancy, feel exquisiteness, strong detergency, the effect such as antibacterial.Sapindoside joins and can play increasing in aminoacid transparent soap
Bubble, surely bubble, lifting wash the effect of sense.
In a preferred embodiment of the invention, described fatty acyl glutamic acid be lauroyl glutamate, cocos nucifera oil acyl glutamic acid,
Myristoyl glutamate, one or more mixing of stearoyl-glutamic acid.
It is further preferred that the mixture that described fatty acyl glutamic acid is lauroyl glutamate and stearoyl-glutamic acid, institute
Stating the weight of lauroyl glutamate and stearoyl-glutamic acid in mixture is (1-5): (1-5).
In a preferred embodiment of the invention, described polyhydric alcohol be glycerol, propylene glycol, butanediol, pentanediol, oneself two
Alcohol, sorbitol, erithritol, ethanol, PEG-8, Polyethylene Glycol-32, dipropylene glycol, diglycerol, glycerin polyether-26, poly-sweet
Oil-10, one or more mixing of polyglycereol-8.
It is further preferred that the mixture that described polyhydric alcohol is erithritol and sorbitol, in described mixture erithritol and
The weight of sorbitol is (1-5): (1-5).The compound of erithritol and sorbitol on the one hand can saturating with improving product
Lightness, on the other hand can increase the hardness of product.
In a preferred embodiment of the invention, described fatty acid is octanoic acid, capric acid, lauric acid, myristic acid, Petiolus Trachycarpi
Acid, stearic acid, oleic acid, linoleic acid, linolenic acid, erucic acid, arachidic acid, behenic acid, lignin acid, cerinic acid, montanic acid, Apis cerana Fabricius acid
One or more mixing.
It is further preferred that the mixture that described fatty acid is lauric acid, myristic acid and erucic acid, the moon in described mixture
The weight of cinnamic acid, myristic acid and erucic acid is (1-5): (1-5): (1-5).
The aminoacid transparent soap of the present invention can be prepared by conventional production technology, following preparation method, its bag
Include following steps: fatty acyl glutamic acid, polyhydric alcohol are sequentially added into agitated kettle by (1), heat up and are heated to 80-85 DEG C, and constant temperature stirs
To being completely dissolved;(2) triethanolamine and water are mixed, be heated to 70-75 DEG C, be then slowly added into agitated kettle, constant temperature stirring 30-
40 minutes;(3) fatty acid is added agitated kettle, stirring and dissolving;(4) sodium hydroxide is dissolved in water, then is slowly added into stirring
Pot, insulated and stirred 30-50 minute;(5) temperature is down to 50-60 DEG C, then in turn through froth breaking, injection molding, cooling, the demoulding, wind
Dry, packaging obtains aminoacid composite transparent soap.
The feature of this technique is have employed secondary saponification method, first by fatty acyl glutamic acid and triethanolamine saponification, with
Rear fatty acid and sodium hydroxide secondary saponification.Have an advantage in that and prepare fatty acyl glutamic acid three ethanol by controlled saponification
Amine salt and fatty acid sodium salt.The mildness of fatty acyl glutamic acid triethanolamine salt and transparency fatty acyl sodium glutamate are high, fat
The foaming power of fat acid sodium-salt and cleaning force are stronger than fatty acid triethanol amine salt.Therefore the aminoacid prepared by secondary soap method is combined
Transparent soap is more better than a common saponification method in terms of transparency and foaming power, cleaning force.
Relative to prior art, technical scheme has the advantages that 1, the present invention uses fatty acyl paddy
Propylhomoserin and triethanolamine saponification prepare fatty acyl glutamic acid triethanolamine salt, fatty acid and sodium hydroxide saponification reaction and prepare
Fatty acid sodium salt, two kinds of prepared surfactants have good complementary action, and fatty acyl glutamic acid triethanolamine salt is permissible
Reducing the zest of fatty acid sodium salt, fatty acid sodium salt can promote the foaming power of system, cleaning force and soap body hardness, each component
Raw material combines with the ratio in the range of determining very much, due to its significant potentiation, prepared composite transparent soap hardness
Moderate, foaming power and cleaning force are relatively strong, and in faintly acid.2, the technique that the present invention uses is simple, simple equipments, it is simple to extensive
Produce.
Detailed description of the invention
For a more detailed description to the present invention below in conjunction with detailed description of the invention, but embodiments of the present invention are not limited to
This, for the technological parameter indicated the most especially or condition, can refer to routine techniques and carry out.
Embodiment 1
A kind of aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Lauroyl glutamate 40%
Glycerol 5%
Propylene glycol 5%
Ethanol 5%
Triethanolamine 30%
Stearic acid 10%
Sodium hydroxide 2%
Water surplus.
Production technology, comprises the following steps: lauroyl glutamate, glycerol, propylene glycol, ethanol are sequentially added into stirring by (1)
Pot, heats up and is heated to 80-85 DEG C, and constant temperature stirs to being completely dissolved;(2) triethanolamine and water are mixed, are heated to 70-75 DEG C,
Being slowly added into agitated kettle, constant temperature stirs 30-40 minute;(3) stearic acid is added agitated kettle, stirring and dissolving;(4) by sodium hydroxide
It is dissolved in water, then is slowly added into agitated kettle, insulated and stirred 30-50 minute;(5) temperature is down to 50-60 DEG C, the most successively warp
Cross froth breaking, injection molding, cooling, the demoulding, air-dried, packaging acquisition aminoacid composite transparent soap.
Embodiment 2
A kind of aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Cocos nucifera oil acyl glutamic acid 30%
Glycerol 2%
PEG-8 2%
Ethanol 1%
Triethanolamine 20%
Lauric acid 1%
Sodium hydroxide 0.2%
Sapindoside 1%
Water surplus.
Production technology, comprises the following steps: cocos nucifera oil acyl glutamic acid, glycerol, PEG-8, ethanol are sequentially added into by (1)
Agitated kettle, heats up and is heated to 80-85 DEG C, and constant temperature stirs to being completely dissolved;(2) triethanolamine and water are mixed, be heated to 70-75
DEG C, it being slowly added into agitated kettle, constant temperature stirs 30-40 minute;(3) lauric acid is added agitated kettle, stirring and dissolving;(4) by hydrogen-oxygen
Change sodium to be dissolved in water, then be slowly added into agitated kettle, insulated and stirred 30-50 minute;(5) sapindoside is dissolved in water,
Add agitated kettle, stir;(6) temperature is down to 50-60 DEG C, then in turn through froth breaking, injection molding, cooling, the demoulding, air-dry,
Packaging obtains aminoacid composite transparent soap.
Embodiment 3
A kind of aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Lauroyl glutamate 20%
Myristoyl glutamate 15%
Natrulon H-10 5%
Propylene glycol 3%
Ethanol 2%
Triethanolamine 25%
Myristic acid 3%
Arachidic acid 2%
Sodium hydroxide 0.5%
Sapindoside 2%
Water surplus.
Production technology is similar to embodiment 2, does not repeats them here.
Embodiment 4
A kind of aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Lauroyl glutamate 30%
Stearoyl-glutamic acid 6%
Sorbitol 10%
Erithritol 2%
Triethanolamine 26%
Lauric acid 0.5%
Myristic acid 2.5%
Erucic acid 0.5%
Sodium hydroxide 0.5%
Sapindoside 0.1%
Water surplus.
Production technology is similar to embodiment 2, does not repeats them here.
Embodiment 5
A kind of aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Lauroyl glutamate 6%
Stearoyl-glutamic acid 30%
Sorbitol 2%
Erithritol 10%
Triethanolamine 26%
Lauric acid 2.5%
Myristic acid 0.5%
Erucic acid 2.5%
Sodium hydroxide 0.5%
Sapindoside 0.5%
Water surplus.
Production technology is similar to embodiment 2, does not repeats them here.
Embodiment 6
A kind of aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Lauroyl glutamate 18%
Stearoyl-glutamic acid 18%
Sorbitol 6%
Erithritol 6%
Triethanolamine 26%
Lauric acid 1.5%
Myristic acid 1.5%
Erucic acid 1.5%
Sodium hydroxide 0.5%
Sapindoside 1.2%
Water surplus.
Production technology is similar to embodiment 2, does not repeats them here.
Embodiment 7
Aminoacid composite transparent soap obtained by embodiment 1-6 is carried out hardness test and cleaning test, and comparative example 1-is set
3, wherein comparative example 3 is commercially available aminoacid transparent soap, and concrete test is as follows:
Comparative example 1
A kind of aminoacid transparent soap, it is mainly made up of the component of following weight percentage ratio:
Lauroyl glutamate 36%
Sorbitol 6%
Ethanol 6%
Triethanolamine 25%
Water surplus.
Production technology is similar to embodiment 1, does not repeats them here.
Comparative example 2
A kind of aminoacid transparent soap, it is mainly made up of the component of following weight percentage ratio:
Lauroyl glutamate 36%
Sorbitol 6%
Ethanol 6%
Stearic acid 5%
Triethanolamine 25%
Water surplus.
Production technology is similar to embodiment 1, does not repeats them here.
Foaming power and cleaning force method of testing are as follows: test object: each experimental group is 10 volunteers, age 15-55
In year, skin quality is healthy, it is possible to by Normalization rule product, and cooperating personnel complete appraisal on request, has certain statement
Ability, the impression after energy actual response use;Using method: take 1g product be placed in get blisters net in, get blisters after adding fraction of water, see
Examine its foaming power, then with hands, foam be coated in massage 15 times of looping the most gently, allow foam throughout whole face, then with moistening
Towel defoam, with the hands hold cold water and raise the portion of washing one's face, clean up, experience its clean-up performance.Concrete test result is shown in
Table 1.
Table 1 test result record
As seen from Table 1, the PH of the aminoacid composite transparent soap prepared by embodiment 1-6 is respectively less than 7, in faintly acid;Embodiment 1-6
Understanding with the hardness balance of comparative example 1-3, the aminoacid composite transparent soap hardness prepared by the present invention gets a promotion;Embodiment 1-
3 understand with the hardness balance of embodiment 4-6, comparative example 1, and the compounding of sorbitol and erithritol can increase the hard of product further
Degree;Embodiment 1-6 understands with foaming power and the cleaning force contrast of comparative example 1-3, the aminoacid composite transparent prepared by the present invention
The cleaning force of soap and foaming power are more preferably;Embodiment 1-3 understands with embodiment 4-6, the foaming power of comparative example 2 and cleaning force contrast,
Foaming power and the cleaning force of the amino acid complex transparent soap of the mixture containing lauric acid, myristic acid and erucic acid obtain into one
Step promotes;Embodiment 1 and the foaming power of embodiment 2 and cleaning force contrast understand, and the aminoacid containing sapindoside is compound thoroughly
The foaming power of bright soap and cleaning force are more preferably.
The above, be only presently preferred embodiments of the present invention, and the present invention not does any pro forma restriction, therefore
All contents without departing from technical solution of the present invention, any simply repair made for any of the above embodiments according to the technical spirit of the present invention
Change, equivalent variations and modification, all still fall within the range of technical solution of the present invention.
Claims (9)
1. an aminoacid composite transparent soap, it is mainly made up of the component of following weight percentage ratio:
Fatty acyl glutamic acid 30-40%
Polyhydric alcohol 5-15%
Triethanolamine 20-30%
Fatty acid 1-10%
Sodium hydroxide 0.2-2%
Water surplus.
Aminoacid composite transparent soap the most according to claim 1, it is characterised in that described aminoacid composite transparent soap is also
Can add sapindoside, the addition of described sapindoside is 0.1-2wt%.
Aminoacid composite transparent soap the most according to claim 1, it is characterised in that described fatty acyl glutamic acid is lauroyl
Glutamic acid, cocos nucifera oil acyl glutamic acid, myristoyl glutamate, one or more mixing of stearoyl-glutamic acid.
Aminoacid composite transparent soap the most according to claim 3, it is characterised in that described fatty acyl glutamic acid is lauroyl
Glutamic acid and the mixture of stearoyl-glutamic acid, in described mixture, the weight portion of lauroyl glutamate and stearoyl-glutamic acid is joined
Than being (1-5): (1-5).
Aminoacid composite transparent soap the most according to claim 1, it is characterised in that described polyhydric alcohol be glycerol, propylene glycol,
Butanediol, pentanediol, hexanediol, sorbitol, erithritol, ethanol, PEG-8, Polyethylene Glycol-32, dipropylene glycol, double sweet
Oil, one or more mixing of glycerin polyether-26, Natrulon H-10, polyglycereol-8.
Aminoacid composite transparent soap the most according to claim 5, it is characterised in that described polyhydric alcohol is erithritol and Pyrusussuriensis
The mixture of alcohol, in described mixture, the weight of erithritol and sorbitol is (1-5): (1-5).
Aminoacid composite transparent soap the most according to claim 1, it is characterised in that described fatty acid is octanoic acid, capric acid, the moon
The acid of cinnamic acid, myristic acid, Palmic acid, stearic acid, oleic acid, linoleic acid, linolenic acid, erucic acid, arachidic acid, behenic acid, lignin, wax
Acid, montanic acid, one or more mixing of Apis cerana Fabricius acid.
Aminoacid composite transparent soap the most according to claim 7, it is characterised in that described fatty acid is lauric acid, lima bean
Cool acid and the mixture of erucic acid, in described mixture, the weight of lauric acid, myristic acid and erucic acid is (1-5): (1-
5): (1-5).
9. the method for the aminoacid composite transparent soap that a kind is prepared described in any one of claim 1-8, it is characterised in that include as
Lower step: fatty acyl glutamic acid, polyhydric alcohol are sequentially added into agitated kettle by (1), heat up and are heated to 80-85 DEG C, constant temperature stirring is to complete
CL;(2) triethanolamine and water being mixed, be heated to 70-75 DEG C, be then slowly added into agitated kettle, constant temperature stirring 30-40 divides
Clock;(3) fatty acid is added agitated kettle, stirring and dissolving;(4) sodium hydroxide is dissolved in water, then is slowly added into agitated kettle, protect
Temperature stirring 30-50 minute;(5) temperature is down to 50-60 DEG C, then in turn through froth breaking, injection molding, cooling, the demoulding, air-dried, packaging
Obtain aminoacid composite transparent soap.
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CN201610277759.3A CN105907501A (en) | 2016-04-29 | 2016-04-29 | Transparent amino acid compound soap and preparation method thereof |
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Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106398905A (en) * | 2016-09-06 | 2017-02-15 | 佛山市芊茹化妆品有限公司 | Application of hydroxyl substituent of 2-amino-2-methyl propane in amino acid transparent soap |
CN106929231A (en) * | 2017-03-08 | 2017-07-07 | 蔡颖欣 | A kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay and preparation method thereof |
CN107115209A (en) * | 2017-05-18 | 2017-09-01 | 广州同隽医药科技有限公司 | A kind of solid-state amino acid surfactant composition |
CN107435000A (en) * | 2017-08-04 | 2017-12-05 | 广州集芳丹生物科技有限公司 | A kind of pure amino acid facial soap and preparation method thereof |
CN107653125A (en) * | 2017-08-31 | 2018-02-02 | 广西小燕蛇业有限公司 | A kind of amino acid handmade soap and preparation method thereof |
CN107746761A (en) * | 2017-11-27 | 2018-03-02 | 上海清轩生物科技有限公司 | A kind of amino acid composite transparent soap containing camellia seed oil and preparation method thereof |
CN108823013A (en) * | 2018-08-28 | 2018-11-16 | 湖南青茶萃化妆品有限公司 | amino acid camellia handmade soap and preparation method thereof |
CN109652239A (en) * | 2018-11-27 | 2019-04-19 | 安徽省玉兔日用化学品有限公司 | A kind of amino acid perfumed soap and its processing technology containing Rhizoma Polygonati extract |
CN110251428A (en) * | 2019-06-10 | 2019-09-20 | 江门职业技术学院 | A kind of solid amino acid cleansing product and preparation method thereof |
CN110835587A (en) * | 2019-11-20 | 2020-02-25 | 茗汲(浙江)生物科技有限公司 | White tea antibacterial handmade soap and preparation method thereof |
CN112940882A (en) * | 2019-12-11 | 2021-06-11 | 广东柏亚化妆品有限公司 | Transparent composite soap and preparation method thereof |
EP4138770A4 (en) * | 2020-04-23 | 2024-01-03 | Henkel Ag & Co Kgaa | Transparent shampoo bar and method for preparing the same |
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Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106398905A (en) * | 2016-09-06 | 2017-02-15 | 佛山市芊茹化妆品有限公司 | Application of hydroxyl substituent of 2-amino-2-methyl propane in amino acid transparent soap |
CN106929231A (en) * | 2017-03-08 | 2017-07-07 | 蔡颖欣 | A kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay and preparation method thereof |
CN107115209A (en) * | 2017-05-18 | 2017-09-01 | 广州同隽医药科技有限公司 | A kind of solid-state amino acid surfactant composition |
CN107435000A (en) * | 2017-08-04 | 2017-12-05 | 广州集芳丹生物科技有限公司 | A kind of pure amino acid facial soap and preparation method thereof |
CN107653125A (en) * | 2017-08-31 | 2018-02-02 | 广西小燕蛇业有限公司 | A kind of amino acid handmade soap and preparation method thereof |
CN107746761A (en) * | 2017-11-27 | 2018-03-02 | 上海清轩生物科技有限公司 | A kind of amino acid composite transparent soap containing camellia seed oil and preparation method thereof |
CN108823013A (en) * | 2018-08-28 | 2018-11-16 | 湖南青茶萃化妆品有限公司 | amino acid camellia handmade soap and preparation method thereof |
CN109652239A (en) * | 2018-11-27 | 2019-04-19 | 安徽省玉兔日用化学品有限公司 | A kind of amino acid perfumed soap and its processing technology containing Rhizoma Polygonati extract |
CN110251428A (en) * | 2019-06-10 | 2019-09-20 | 江门职业技术学院 | A kind of solid amino acid cleansing product and preparation method thereof |
CN110835587A (en) * | 2019-11-20 | 2020-02-25 | 茗汲(浙江)生物科技有限公司 | White tea antibacterial handmade soap and preparation method thereof |
CN112940882A (en) * | 2019-12-11 | 2021-06-11 | 广东柏亚化妆品有限公司 | Transparent composite soap and preparation method thereof |
EP4138770A4 (en) * | 2020-04-23 | 2024-01-03 | Henkel Ag & Co Kgaa | Transparent shampoo bar and method for preparing the same |
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