CN102370607B - Formula of bath cream with crystal salt and preparation method thereof - Google Patents
Formula of bath cream with crystal salt and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a formula of bath cream with crystal salt and a preparation method thereof. The bath cream comprises the following raw materials in percentage by mass: salt is not less than 15.0 percent and is not more than 45.0 percent, surfactant is not less than 12.0 percent and is not more than 25.0 percent, viscosity reductant is not less than 2.0 percent and is not more than 10.0 percent, humectant is not less than 1.0 percent and is not more than to 5.0 percent, nutrient additive is not less than or equal to 0.0 percent and is not more than 5.0 percent, complexing agent is not less than 0.1 percent and is not more than 2.0 percent, essence is not less than 0.2 percent and is not more than 1.0 percent, pH regulating agent is not less than or equal to 0.0 percent and is not more than 2.0 percent and the balance of pure water. Compared with the prior art, the formula of the bath cream with the crystal salt has the following advantages: the salt content of the bath cream can be randomly regulated within the range of 15 to 45 percent, and the effects of sterilizing, diminishing inflammation, relieving itching, promoting blood circulation, degreasing, removing keratin and the like in the salt can be fully exerted.
Description
Technical field
The invention belongs to the household chemicals technical field, particularly a kind of bath gel that contains microcrystal salt particles relates to the method for utilizing alcohol ether sulfosuccinate disodium to prepare this crystalline substance salt bath gel as viscosity reductant simultaneously.
Background technology
In recent years, salt (being NaCl) is day by day extensive in the application of cosmetic field, utilize salt sterilization, sterilization, antiinflammatory, antipruritic, invigorate blood circulation, the effect such as degrease, exfoliation, can make the cosmetics of everyday use of Various Functions by different proportion, these salt cosmeticses of everyday use, when making skin obtain cleaning-sterilizing, can also make it become smooth careful, can also play certain treatment and improvement effect to acne, common scytitis, Pruritus, hyperkeratosis etc., be the popular pollution-free family of new generation cosmetics of everyday use that has no side effect in the world in recent years.
But the stability influence that adds its prescription of salt pair at the cosmetics of everyday use prescription is larger, a small amount of salt (less than 5%), can in cosmetics of everyday use, play thickening power, the salt of excessive (surpassing 10%), the micellar structure that meeting deface activating agent forms in aqueous solution, make the interiors of products web frame destroyed, reduce the stable and mobile of product system, thereby cause saliferous emulsus daily chemical products system viscosity to descend, layering appearred within the shelf-life, analyse glue, bleed, the problems such as salt recrystallization, and be prone to the heat-resisting cold-resistant quality problem that can not reach the relevant national standard requirement, have a strong impact on the quality of product.
The saliferous cosmetics of everyday use is an extremely unsettled system, improve the stability of saliferous cosmetics of everyday use, this Unstable Systems was kept relative stability within the shelf-life, not affecting the use of product, generally is to add a certain amount of thickening agent with salt tolerance, suspension, thickening property, stability in the cosmetics of everyday use prescription.For example: " a kind of emulsified salt type skin-cleaning articles and preparation method thereof " (patent No.: ZL200410022594.2) utilize sodium carboxymethyl cellulose as thickening agent; " a kind of emulsified salt type Chinese herbal medicine emulsion used for washing and caring hair and preparation thereof " (patent No.: ZL200710065984.1) utilize Acrylates as thickening agent; " a kind of emulsified salt type cream for cleaning face and preparation method thereof " (patent No.: ZL200510010816.1) utilize salt tolerant to analyse a kind of as thickening agent in the cellulose.
At present, the saliferous cosmetics of everyday use is with major issue of common commercially available thickening agent ubiquity: in high saliferous (salt content surpasses 10% in the emulsus cosmetics of everyday use) cosmetics of everyday use, thickening agent unstable or inefficacy or suspension stability Wang ideal, can not make it to reach and keep desired viscosity, stability, suspension, thereby make product not good, the heat-resisting cold-resistant quality problems such as not up to standard of layering, bleed, flowability within the shelf-life, occur, its reason mainly is in numerous thickening agents, also fails to find to be fit to the single thickening agent that salt content surpasses 10% cosmetics of everyday use.Two or more thickening agent is composite, it is the main method that solves at present high saliferous cosmetics of everyday use thickening problem, " a kind of composite salt-resistant thickening agent, its preparation method and application thereof " (application number: 201010526491.5) disclose a kind ofly by HANSHENGJIAO, guar gum, the composite haloduric thickener of sodium alginate, can be applicable to salinity in 0～40% emulsus cosmetics of everyday use.Some high saliferous daily chemical products in order to solve the thickening problem, is selected to carry out QB/T 2744.2 " bath salt second portion: bathing salt " standard, in prescription, add an amount of single thickening agent after, product is made paste body shape.
Aspect the cosmetics of everyday use thickening, except using natural polymer as the thickening agent, many surfactants are exactly good thickening agent each other, such as anion surfactant fatty alcohol polyoxyethylene ether sulfate, zwitterionic surfactant betanin, non-ionic surface active agent alkylolamides and alkyl amine oxide etc., suit between them compositely just can form desirable cosmetics of everyday use formula system.
The inventor has carried out for many years research for emulsion form saliferous cosmetics of everyday use, obtaining breakthrough aspect the thickening of surfactant compound salt tolerant, and be applied to brilliant salt Chinese herbal medicine paste shampoo, also obtained the product patent (patent No.: ZL200910029316.2).Although hair washing has many similarities with clean skin series products with hair products on prescription, different instructions for uses has determined its diversity on prescription.In the R﹠D process of this formula for a product, for hair care, the hair care effect that increases product, the useful compositions such as silicone oil, pantothenylol, Chinese herbal medicine have been added, simultaneously also with reference to common shampoo prescription, selected cation guar gum and polyquaternary ammonium salt as hair conditioner, this two kinds of materials have also been brought into play the effect of thickening, stable, adjusting viscosity in formula for a product.In order to develop the brilliant salt formula of bath cream by the surfactant compound thickening, the wetting agent in this patent formulation, conditioner and Chinese herbal medicine composition are removed in test, the result is paste body shape by the product that surfactant compound and salt prescription form, and is mobile undesirable, need carry out viscosity reduction and regulate.
Present Chinese daily chemical articles industry, what be used for thinner has propylene glycol, glycerol, Polyethylene Glycol and a water-soluble silicon wet goods.Through testing: glycerol, Polyethylene Glycol and water-soluble silicon oil easily cause above-mentioned surfactant compound salt tolerant system bleed, layering, and heat-resisting resisting cold do not passed through yet, and satiny with rear skinfeel; Though propylene glycol can be regulated certain viscosity, can not reach commercially available salt-free like product state, (greater than 3%) caused product stability not good when addition was high, and foam also further reduces during use.
Alcohol ether sulfosuccinate disodium is the raw material commonly used of making shampoo, foam bath, bath gel, handwashing liquid, surgical operation cleaning and other cosmetics, washing daily chemical products etc., also can be used as emulsifying agent, dispersant, wetting agent, foaming agent etc.Its zest is low, and can significantly reduce the zest of other surfactants, and degreasing power is low, detergency is good, very easily flushing and without soapy feeling have good calcium soap to disperse and anti-performance of hard water, but alcohol ether sulfosuccinate disodium is difficult for thickening in all kinds of cosmetic formulations.Height bubble, good, the easy flushing of detergency of this product, subtract sliding effect, be difficult for all required for the present invention wanting of the characteristics such as thickening, particularly utilize itself and other surfactant compound, be mixed with that stable system, foam enrich, are easy to wash, skinfeel is comfortable, the brilliant salt bath gel of good fluidity, be all to have no open in prior art or the patent of having applied for.
Summary of the invention
The technical problem that solves:The present invention seeks to be difficult for for high saliferous cosmetics of everyday use viscosity the shortcoming of adjusting, a kind of brilliant salt formula of bath cream is provided, this crystalline substance salt bath gel is when keeping the basic functions such as daily bath gel washing, decontamination, by various mineral elements contained in the brilliant salt, also have sterilization, antiinflammatory, antipruritic, invigorate blood circulation, the effect such as degrease, exfoliation, product flowability and daily bath gel are without significant difference, and be easy to use.
Another object of the present invention provides a kind of method for preparing above-mentioned brilliant salt bath gel.
Technical scheme:Purpose of the present invention is achieved by the following technical programs.
A kind of brilliant salt bath gel, this bath gel is comprised of the raw material of following mass percent: 15.0%≤salt≤45.0%; 12.0%≤surfactant≤25.0%; 2.0%≤viscosity reductant≤10.0%; 1.0%≤wetting agent≤5.0%; 0.0＜nourishing additive agent≤5.0%; 0.1%≤chelating agent≤2.0%; 0.2%≤essence≤1.0%; 0.0＜pH adjusting agent≤2.0%; Remaining is pure water.
Described salt is well mine salt, sea salt or the lake salt that meets refined edible salt grade.
Described surfactant be anion and amphoteric ionic surfactant arbitrarily than mixture; wherein anion surfactant is a kind of in ammonium salt compound, sodium lauroyl glutamate, potassium alkyl phosphate or the fatty alcohol ether carboxylic acid sodium or any two kinds, and zwitterionic surfactant is a kind of in cocamido propyl betaine, empgen BB, dodecanamide propyl hydroxyl sulphur betanin or the imidazoline or any two kinds.
Described viscosity reductant is alcohol ether sulfosuccinate disodium.
Described wetting agent is cation pantothenylol, Jojoba oil or silicone oil.
Described nourishing additive agent is at least a in Flos Rosae Rugosae extracting solution, green tea extractive liquor, milk elite, polypeptide, the Hippocampus extracting solution.
Described chelating agent is EDTA.
Described pH adjusting agent is citric acid or sodium citrate salt.
The method for preparing above-mentioned brilliant salt bath gel, the method comprise the step of following order: in the agitator tank of homogeneous emulsifying machine, add pure water, chelating agent, and the intensification heating disinfection, and open and stir; Add respectively anion and zwitterionic surfactant, viscosity reductant, in vacuum be-the 0.07MPa state under stirring and dissolving; Under stirring, add salt; Under vacuum state, open the homogenizing function of mulser, the adjusting shearing force is 1500 ~ 2000rpm, homogenizing time 2 ~ 5 minutes, again under the vacuum stirring state, stir about 25 ~ 30 minutes; Material is cooled to 45 ~ 45 ℃, under stirring, adds wetting agent, nourishing additive agent, essence, pH adjusting agent; Above-mentioned gained material is evacuated to finished pot, after still aging about 24 hours, gets product.
Beneficial effect:
Compared with prior art, the present invention has following advantage: the bath gel salinity can any adjusting in 15% ~ 45% scope, can give full play to salt sterilization, antiinflammatory, antipruritic, invigorate blood circulation, the effect such as degrease, exfoliation.
The present invention does not use the natural polymer thickening agent, effectively solves the thickening problem of high salt formula of bath cream; Unique polynary prescription by alcohol ether sulfosuccinate disodium adjusting viscosity is composite, and the product foam enriches, is easy to flushing, comfortable, the good fluidity of skinfeel, heat-resisting cold-resistant, stable system; Do not use polyhydric alcohol in the prescription, overcome the quality problem such as the easy bleed of high salt bath gel, water oil content layer, salt recrystallization.
The flowability of product is close with common bath gel, the outward appearance of product and serviceability are all good, often use, when making skin obtain cleaning-sterilizing, can also blood circulation promoting, make it become smooth careful, can also play certain treatment and improvement effect to acne, common scytitis, Pruritus, hyperkeratosis, fat-reducing etc.
The specific embodiment
The present invention is further elaborated below in conjunction with embodiment, but be not limitation of the present invention, all any this areas of doing according to the disclosure of invention be equal to replacement, all belong to protection scope of the present invention.
Embodiment 1:
A kind of brilliant salt bath gel, the quality percentage composition of its each component is:
The well mine salt that meets refined edible salt grade: 45.0%;
Surfactant (sodium lauroyl glutamate and cocamido propyl betaine): 25.0%;
Alcohol ether sulfosuccinate disodium: 10.0%;
Jojoba oil: 5.0%;
Flos Rosae Rugosae extracting solution: 5.0%;
EDTA：2.0%；
Essence: 1.0%;
Citric acid: 2.0%;
Remaining is pure water.
Production technology:
In homogeneous emulsifying machine, in the agitator tank, add pure water, chelating agent, the intensification heating disinfection, and open common agitating function; Add respectively anion and zwitterionic surfactant, viscosity reductant, stirring and dissolving under vacuum state; Under common stirring, slowly add salt; Under vacuum state, open the homogenizing function of mulser, the adjusting shearing force is 1500 ~ 2000rpm, homogenizing time 2 ~ 5 minutes; Under the common stirring of vacuum, stir about 25 ~ 30 minutes; Material is cooled to 45 ~ 45 ℃, under common stirring, adds wetting agent, nourishing additive agent, essence, pH adjusting agent; Above-mentioned gained material is evacuated to finished pot, after still aging about 24 hours, gets product.(identical with the method for making of following examples)
Object of study: dermatitis patients, male 10 people wherein, women 5 people.
Using method: with the brilliant salt bath gel washing of the present invention affected part, during washing, bath gel after the affected part smoothens, is kept more than 5 minutes, after get suitable quantity of water, rub to foam abundant, clean with flushing with clean water again.Every day, each was used in conjunction for two weeks with once sooner or later.
Result of the test: cure rate 80%, obvious effective rate 90%, total effective rate 93%.
Object of study: skin Pruritus person, male 5 people wherein, women 5 people.
Using method: with Application Example 1.
Result of the test: cure rate 30%, obvious effective rate 60%, total effective rate 80%.
Embodiment 2
A kind of brilliant salt bath gel, the quality percentage composition of its each component is:
The sea salt that meets refined edible salt grade: 22.0%;
Surfactant (potassium alkyl phosphate and empgen BB): 12.0%
Alcohol ether sulfosuccinate disodium: 3.0%;
Cation pantothenylol: 1.0%;
Polypeptide: 5.0%;
EDTA：2.0%；
Essence: 1.0%;
Sodium citrate salt: 2.0%;
Remaining is pure water.
Object of study: dermatitis patients, male 10 people wherein, women 5 people.
Using method: with the brilliant salt bath gel washing of the present invention affected part, during washing, bath gel after the affected part smoothens, is kept more than 5 minutes, after get suitable quantity of water, rub to foam abundant, clean with flushing with clean water again.Every day, each was used in conjunction for two weeks with once sooner or later.
Result of the test: cure rate 60%, obvious effective rate 80%, total effective rate 85%.
Object of study: skin Pruritus person, male 5 people wherein, women 5 people.
Using method: with Application Example 1.
Result of the test: cure rate 28%, obvious effective rate 60%, total effective rate 78%.
Embodiment 3
A kind of brilliant salt bath gel, the quality percentage composition of its each component is:
The lake salt that meets refined edible salt grade: 25.0%;
Surfactant (fatty alcohol ether carboxylic acid sodium and dodecanamide propyl hydroxyl sulphur betanin): 13.0%
Alcohol ether sulfosuccinate disodium: 4.0%;
Silicone oil: 3.0%;
Green tea extractive liquor: 2.0%;
EDTA：0.8%；
Essence: 0.6%;
Citric acid: 2.0%;
Remaining is pure water.
Object of study: dermatitis patients, male 10 people wherein, women 5 people.
Using method: with the brilliant salt bath gel washing of the present invention affected part, during washing, bath gel after the affected part smoothens, is kept more than 5 minutes, after get suitable quantity of water, rub to foam abundant, clean with flushing with clean water again.Every day, each was used in conjunction for two weeks with once sooner or later.
Result of the test: cure rate 65%, obvious effective rate 82%, total effective rate 86%.
Object of study: skin Pruritus person, male 5 people wherein, women 5 people.
Using method: with Application Example 1.
Result of the test: cure rate 30%, obvious effective rate 60%, total effective rate 82%.
Embodiment 4
A kind of brilliant salt bath gel, the quality percentage composition of its each component is:
The well mine salt that meets refined edible salt grade: 35.0%;
Surfactant (ammonium salt compound and imidazoline): 15.0%
Alcohol ether sulfosuccinate disodium: 3.0%;
Cation pantothenylol: 1.0%;
Hippocampus extracting solution: 3.0%;
EDTA：1.0%；
Essence: 0.5%;
Sodium citrate salt: 1.0%;
Remaining is pure water.
Object of study: dermatitis patients, male 10 people wherein, women 5 people.
Using method: with the brilliant salt bath gel washing of the present invention affected part, during washing, bath gel after the affected part smoothens, is kept more than 5 minutes, after get suitable quantity of water, rub to foam abundant, clean with flushing with clean water again.Every day, each was used in conjunction for two weeks with once sooner or later.
Result of the test: cure rate 78%, obvious effective rate 88%, total effective rate 90%.
Object of study: skin Pruritus person, male 5 people wherein, women 5 people.
Using method: with Application Example 1.
Result of the test: cure rate 30%, obvious effective rate 65%, total effective rate 83%.
Embodiment 5
A kind of brilliant salt bath gel, the quality percentage composition of its each component is:
Well mine salt: 30.0%;
Surfactant (sodium lauroyl glutamate, potassium alkyl phosphate, cocamido propyl betaine and empgen BB): 16.0%;
Alcohol ether sulfosuccinate disodium: 4.0%;
Cation pantothenylol: 2.0%;
Flos Rosae Rugosae extracting solution: 3.0%;
EDTA：0.2%；
Essence: 0.4%;
Remaining is pure water.
Object of study: dermatitis patients, male 10 people wherein, women 5 people.
Using method: with the brilliant salt bath gel washing of the present invention affected part, during washing, bath gel after the affected part smoothens, is kept more than 5 minutes, after get suitable quantity of water, rub to foam abundant, clean with flushing with clean water again.Every day, each was used in conjunction for two weeks with once sooner or later.
Result of the test: cure rate 80%, obvious effective rate 85%, total effective rate 91%.
Object of study: skin Pruritus person, male 5 people wherein, women 5 people.
Using method: with Application Example 1.
Result of the test: cure rate 35%, obvious effective rate 65%, total effective rate 85%.
Claims (7)
1. a brilliant salt bath gel is characterized in that this bath gel is comprised of the raw material of following mass parts: 15.0%≤salt≤45.0%; 12.0%≤surfactant≤25.0%; 2.0%≤viscosity reductant≤10.0%; 1.0%≤wetting agent≤5.0%; 0.0＜nourishing additive agent≤5.0%; 0.1%≤chelating agent≤2.0%; 0.2%≤essence≤1.0%; 0.0＜pH adjusting agent≤2.0%; Remaining is pure water; Described surfactant be anion and amphoteric ionic surfactant arbitrarily than mixture, wherein anion surfactant is a kind of in ammonium salt compound, sodium lauroyl glutamate, potassium alkyl phosphate or the fatty alcohol ether carboxylic acid sodium or any two kinds, and zwitterionic surfactant is a kind of in cocamido propyl betaine, empgen BB, dodecanamide propyl hydroxyl sulphur betanin or the imidazoline or any two kinds; Described viscosity reductant is alcohol ether sulfosuccinate disodium.
2. brilliant salt bath gel according to claim 1 is characterized in that described salt is well mine salt, sea salt or the lake salt that meets refined edible salt grade.
3. brilliant salt bath gel according to claim 1 is characterized in that described wetting agent is cation pantothenylol, Jojoba oil or silicone oil.
4. brilliant salt bath gel according to claim 1 is characterized in that described nourishing additive agent is at least a in Flos Rosae Rugosae extracting solution, green tea extractive liquor, milk elite, polypeptide, the Hippocampus extracting solution.
5. brilliant salt bath gel according to claim 1 is characterized in that described chelating agent is EDTA.
6. brilliant salt bath gel according to claim 1 is characterized in that described pH adjusting agent is citric acid or sodium citrate salt.
7. the method for preparing the described brilliant salt bath gel of claim 1 is characterized in that the method comprises the step of following order:
(1) in the agitator tank of homogeneous emulsifying machine, add pure water, chelating agent, the intensification heating disinfection, and open and stir;
(2) add respectively anion and zwitterionic surfactant, viscosity reductant, in vacuum be-the 0.07MPa state under stirring and dissolving; Described viscosity reductant is alcohol ether sulfosuccinate disodium;
(3) under stirring, add salt;
(4) under vacuum state, open the homogenizing function of mulser, the adjusting shearing force is 1500 ~ 2000rpm, homogenizing time 2 ~ 5 minutes under the vacuum stirring state, stirred 25 ~ 30 minutes again;
(5) material is cooled to 45 ~ 45 ℃, under stirring, adds wetting agent, nourishing additive agent, essence, pH adjusting agent;
(6) above-mentioned gained material is evacuated to finished pot, after still aging 24 hours, gets product.
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| CN2011103395485A CN102370607B (en) | 2011-11-01 | 2011-11-01 | Formula of bath cream with crystal salt and preparation method thereof |
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| CN2011103395485A CN102370607B (en) | 2011-11-01 | 2011-11-01 | Formula of bath cream with crystal salt and preparation method thereof |
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| CN102370607B true CN102370607B (en) | 2013-01-23 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2538084C1 (en) * | 2013-07-25 | 2015-01-10 | Государственное бюджетное образовательное учреждение высшего профессионального образования "Уральская государственная медицинская академия Министерства здравоохранения и социального развития Российской Федерации" (ГБОУ ВПО УГМА Минздрава России) | Agent for treating and preventing atopic dermatitis |
| CN104800809B (en) * | 2015-05-06 | 2018-08-07 | 湖南盐业股份有限公司 | ginger juice foot bath salt and its processing method |
| CN104814894B (en) * | 2015-05-06 | 2017-11-24 | 湖南盐业股份有限公司 | Lavender foot bath salt and its processing method |
| CN104800127A (en) * | 2015-05-06 | 2015-07-29 | 湖南盐业股份有限公司 | Processing method of bathing salt as well as special device thereof, and application in processing foot bath salt |
| DE102015217507A1 (en) * | 2015-09-14 | 2017-03-16 | Henkel Ag & Co. Kgaa | Biosurfactants containing cosmetic cleansing agents with prebiotic activity |
| CN105748332A (en) * | 2016-04-15 | 2016-07-13 | 江苏省苏盐连锁有限公司南京分公司 | High-salinity bath gel |
| CN106418431A (en) * | 2016-09-30 | 2017-02-22 | 益盐堂（应城）健康盐制盐有限公司 | Compound low-sodium salt and preparation method and application thereof |
| CN109260117A (en) * | 2018-11-23 | 2019-01-25 | 谢锡金 | A kind of formula of bath cream with sterilizing function |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101011320A (en) * | 2007-01-17 | 2007-08-08 | 成都死海盐疗健康馆服务有限公司 | De-cutin shower salt |
| CN101152123A (en) * | 2007-09-03 | 2008-04-02 | 中盐东兴盐化股份有限公司 | Bath salt plaster for women and children |
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- 2011-11-01 CN CN2011103395485A patent/CN102370607B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101011320A (en) * | 2007-01-17 | 2007-08-08 | 成都死海盐疗健康馆服务有限公司 | De-cutin shower salt |
| CN101152123A (en) * | 2007-09-03 | 2008-04-02 | 中盐东兴盐化股份有限公司 | Bath salt plaster for women and children |
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Address after: 223200 No. 1 Jingshen Road, Chuzhou District, Huaian City, Jiangsu Province Patentee after: Jiangsu Salt Industry Research Institute Co., Ltd. Address before: 223200 No. 1 Jingshen Road, Chuzhou District, Huaian City, Jiangsu Province Patentee before: Jiangsu Salt Industry Research Institute |