CN103271834A - Non-irritant pollution-free moisturizing pearly lustre bath foam and preparation method thereof - Google Patents
Non-irritant pollution-free moisturizing pearly lustre bath foam and preparation method thereof Download PDFInfo
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- CN103271834A CN103271834A CN2013102406119A CN201310240611A CN103271834A CN 103271834 A CN103271834 A CN 103271834A CN 2013102406119 A CN2013102406119 A CN 2013102406119A CN 201310240611 A CN201310240611 A CN 201310240611A CN 103271834 A CN103271834 A CN 103271834A
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Abstract
Non-irritant pollution-free moisturizing pearly lustre bath foam is prepared from the following ingredients in mass percent: 3-7% glucoside, 4-10% of alcohol etherglucoside alkyl citrate, 3-6% of coconut oil fatty acid monoethanolamine, 0.1-0.3% of cationic surface active agent, 2-4% of glycerinum, 0.2-0.4% of thickening agent, 0.2-0.5% of other additives, and the balance of deionized water. The non-irritant pollution-free moisturizing pearly lustre bath foam has the advantages of being non-irritant, pollution-free, mild, safe and moisturizing and having the pearl effect.
Description
Technical field
The invention belongs to a kind of bath foam and preparation method thereof, be specifically related to pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin and preparation method thereof.
Background technology
Bath foam is compared with fancy soap, and because its pH and human body skin approach, character milder, foam are abundanter, and become consumer for the first-selected product of whole body skin cleaning.Along with improving constantly of living standard, consumer also improves gradually for the requirement of bath foam.Not only require to have lower zest, higher moisture retention and better bioaffinity, also pay attention to the outward appearance of product simultaneously.At present, the surfactant that traditional bath foam prescription such as CN102949319A and CN102988203A are commonly used is sulfonate and sulfuric acid product, these surfactants stimulate bigger, need in final products, add stain or pearling agent as patent CN102178615A, CN100444826C and CN102342899A for improving the bath foam outward appearance, pollute.
Summary of the invention
The objective of the invention is to overcome the deficiency of existing prescription, provide a kind of nonirritant, pearly-lustre bath foam of free of contamination Glycerin and preparation method thereof.
The present invention selects for use natural, non-stimulated glucosides and alcohol ether glucoside citrate as main active matter, make this bath foam have gentleness, safety and moist effect of preserving moisture, the present invention simultaneously makes glucosides and fatty acid distribution of coconut oil monoethanolamine compatibility earlier in preparation process, make this bath foam have pearl effect need not to add under the condition of pearling agent.
Purpose of the present invention realizes by following technology:
Pearly-lustre bath foam of the present invention is characterized in that it being that composition by following mass percent constitutes:
Glucosides 3-7%,
Alcohol ether glucoside citrate 4-10%,
Fatty acid distribution of coconut oil monoethanolamine 3-6%,
Cationic surfactant 0.1%-0.3%,
Glycerol 2-4%,
Thickening agent 0.2-0.4%,
Other auxiliary agent 0.2-0.5%,
The deionized water surplus.
Glucosides in the foregoing invention is the chemical compound with following general formula:
Wherein: R is that carbon number is the alkyl of 12-14, and m is 1.2-1.8, and n is 0-3, and when n＞0, this glucosides is alcohol ether glucoside; When n=0, this glucosides is alkyl polyglucoside.
Cationic surfactant in the foregoing invention is cetyl trimethyl ammonium bromide or poly hexamethylene biguanide.
Thickening agent in the foregoing invention is xanthan gum, sodium carboxymethyl cellulose, sodium alginate, carrageenan or pectin.
Other auxiliary agents in the foregoing invention are: antiseptic and essence.In antiseptic such as sodium benzoate or the Kazon one or both; Essence can be universal product, does not limit kind.
The preparation method of bath foam of the present invention is as follows:
(1) presses raw material and form, glucosides and fatty acid distribution of coconut oil monoethanolamine are added the 30-40% of required deionized water gross weight, be heated with stirring to 60-80
oC treats to dissolve fully the back cooling, places 8-10 h, obtains to have the surfactant stock solution of pearl effect;
(2) form the 30-40% that thickening agent is joined required deionized water gross weight by raw material, stirring obtains thickening agent stock solution;
(3) successively surfactant stock solution, alcohol ether glucoside citrate, cationic surfactant, glycerol, thickening agent stock solution and other auxiliary agents of step (1) gained are added in the remaining deionized water by the raw material composition, regulate pH to 6-8 with acid or alkali, can obtain the pearly-lustre bath foam of Glycerin.
Described acid such as citric acid; Described alkali is sodium hydroxide or potassium hydroxide.
The present invention compared with prior art has following advantage:
1. select for use natural, non-stimulated glucosides and alcohol ether glucoside citrate as main active matter, make this bath foam have gentleness, safety and moist effect of preserving moisture;
2. in preparation process, make glucosides and fatty acid distribution of coconut oil monoethanolamine compatibility earlier, make this bath foam have pearl effect;
3. select carboxymethyl cellulose derivative and the safe thickening agent that derives from natural product for use, the mildness of this prescription and safety are protected.
The specific embodiment
Embodiment 1
A kind of pearly-lustre bath foam of non-stimulated, pollution-free Glycerin, its component by mass percent:
C12-14 alkyl polyglucoside 3%,
Alcohol ether glucoside citrate 10%,
Fatty acid distribution of coconut oil monoethanolamine 5%,
Cetyl trimethyl ammonium bromide 0.1%,
Glycerol 2%,
Xanthan gum 0.2%,
Sodium benzoate 0.1%,
Essence 0.1%
The deionized water surplus.
Preparation process is:
1. according to the above ratio alkyl polyglucoside and fatty acid distribution of coconut oil monoethanolamine are joined 30% of required deionized water gross weight, be heated with stirring to 70
oC treats to dissolve fully the back cooling, places 8 h, obtains the surfactant stock solution A with pearl effect.
2. according to the above ratio xanthan gum is joined 30% of required deionized water gross weight, stirring obtains thickening agent stock solution B.
3. successively stock solution A, alcohol ether glucoside citrate, cetyl trimethyl ammonium bromide, glycerol, stock solution B, sodium benzoate and essence are added remaining deionized water for stirring by material rate, with Fructus Citri Limoniae acid for adjusting pH to 6.5, can obtain the pearly-lustre bath foam of Glycerin.
Embodiment 2
A kind of pearly-lustre bath foam of non-stimulated, pollution-free Glycerin, its component by mass percent:
C12-14 alcohol ether glucoside 5%,
Alcohol ether glucoside citrate 8%,
Fatty acid distribution of coconut oil monoethanolamine 4%,
Poly hexamethylene biguanide 0.15%,
Glycerol 4%,
Sodium alginate 0.2%,
Kazon 0.2%,
Essence 0.2%
The deionized water surplus.
Preparation process is:
1. by above-mentioned ratio alcohol ether glucoside and fatty acid distribution of coconut oil monoethanolamine are joined 40% of required deionized water gross weight, be heated with stirring to 80
oC treats to dissolve fully the back cooling, places 9 h, obtains the surfactant stock solution A with pearl effect.
2. by above-mentioned ratio xanthan gum is joined 30% of required deionized water gross weight, stirring obtains thickening agent stock solution B.
3 add remaining deionized water for stirring with A liquid, alcohol ether glucoside citrate, poly hexamethylene biguanide, glycerol, B liquid, Kazon and essence successively by raw material ratio, with Fructus Citri Limoniae acid for adjusting pH to 7, can obtain the pearly-lustre bath foam of Glycerin.
Embodiment 3
A kind of pearly-lustre bath foam of non-stimulated, pollution-free Glycerin, its component by mass percent:
C12-14 alcohol ether glucoside 6%,
Alcohol ether glucoside citrate 6%,
Fatty acid distribution of coconut oil monoethanolamine 6%,
Poly hexamethylene biguanide 0.3%,
Glycerol 4%,
Sodium carboxymethyl cellulose 0.3%,
Sodium benzoate 0.2%,
Essence 0.1%
The deionized water surplus.
Preparation process is:
1. by above-mentioned ratio alcohol ether glucoside and fatty acid distribution of coconut oil monoethanolamine are joined 35% of required deionized water gross weight, be heated with stirring to 75
oC treats that surfactant dissolves the back cooling fully, places 10 h, obtains the surfactant stock solution A with pearl effect.
2. by above-mentioned ratio xanthan gum is joined 40% of required deionized water gross weight, stirring obtains thickening agent stock solution B.
3. successively A liquid, alcohol ether glucoside citrate, poly hexamethylene biguanide, glycerol, B liquid, sodium benzoate and essence are added remaining deionized water for stirring by raw material ratio, regulate pH to 7.5 with NaOH, can obtain the pearly-lustre bath foam of Glycerin.
Embodiment 4
A kind of pearly-lustre bath foam of non-stimulated, pollution-free Glycerin, its component by mass percent:
C12-14 alkyl polyglucoside 7%,
Alcohol ether glucoside citrate 4%,
Fatty acid distribution of coconut oil monoethanolamine 3%,
Cetyl trimethyl ammonium bromide 0.1%,
Glycerol 3%,
Pectin 0.4%,
Kazon 0.2%,
Essence 0.3%
The deionized water surplus.
Preparation process is:
1. by above-mentioned ratio alkyl polyglucoside and fatty acid distribution of coconut oil monoethanolamine are joined 30% of required deionized water gross weight, be heated with stirring to 80
oC treats that surfactant dissolves the back cooling fully, places 9.5 h, obtains the surfactant stock solution A with pearl effect.
2. by above-mentioned ratio xanthan gum is joined 30% of required deionized water gross weight, stirring obtains thickening agent stock solution B.
3 add remaining deionized water for stirring with A liquid, alcohol ether glucoside citrate, cetyl trimethyl ammonium bromide, glycerol, B liquid, Kazon and essence successively by raw material ratio, regulate pH to 8 with KOH, can obtain the pearly-lustre bath foam of Glycerin.
Claims (9)
1. the pearly-lustre bath foam of non-stimulated, a pollution-free Glycerin is characterized in that it being that composition by following mass percent constitutes:
Glucosides 3-7%,
Alcohol ether glucoside citrate 4-10%,
Fatty acid distribution of coconut oil monoethanolamine 3-6%,
Cationic surfactant 0.1%-0.3%,
Glycerol 2-4%,
Thickening agent 0.2-0.4%,
Other auxiliary agent 0.2-0.5%,
The deionized water surplus.
2. the pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin as claimed in claim 1 is characterized in that described glucosides is the chemical compound with following general formula:
Wherein: R is that carbon number is the alkyl of 12-14, and m is 1.2-1.8, and n is 0-3, and when n＞0, this glucosides is alcohol ether glucoside; When n=0, this glucosides is alkyl polyglucoside.
3. the pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin as claimed in claim 1 is characterized in that described cationic surfactant is cetyl trimethyl ammonium bromide or poly hexamethylene biguanide.
4. the pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin as claimed in claim 1 is characterized in that described thickening agent is xanthan gum, sodium carboxymethyl cellulose, sodium alginate, carrageenan or pectin.
5. the pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin as claimed in claim 1 is characterized in that described other auxiliary agents are antiseptic and essence.
6. the pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin as claimed in claim 5 is characterized in that described antiseptic is one or both in sodium benzoate or the Kazon.
7. as the preparation method of the pearly-lustre bath foam of each described a kind of non-stimulated, pollution-free Glycerin of claim 1-6, it is characterized in that comprising the steps:
(1) presses raw material and form, glucosides and fatty acid distribution of coconut oil monoethanolamine are added the 30-40% of required deionized water gross weight, be heated with stirring to 60-80
oC treats to dissolve fully the back cooling, places 8-10 h, obtains to have the surfactant stock solution of pearl effect;
(2) form the 30-40% that thickening agent is joined required deionized water gross weight by raw material, stirring obtains thickening agent stock solution;
(3) successively surfactant stock solution, alcohol ether glucoside citrate, cationic surfactant, glycerol, thickening agent stock solution and other auxiliary agents of step (1) gained are added in the remaining deionized water by the raw material composition, regulate pH to 6-8 with acid or alkali, can obtain the pearly-lustre bath foam of Glycerin.
8. the preparation method of the pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin as claimed in claim 7 is characterized in that described acid is citric acid.
9. the preparation method of the pearly-lustre bath foam of a kind of non-stimulated, pollution-free Glycerin as claimed in claim 7 is characterized in that described alkali is sodium hydroxide or potassium hydroxide.
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| CN201310240611.9A CN103271834B (en) | 2013-06-18 | 2013-06-18 | Non-irritant pollution-free moisturizing pearly lustre bath foam and preparation method thereof |
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| CN201310240611.9A CN103271834B (en) | 2013-06-18 | 2013-06-18 | Non-irritant pollution-free moisturizing pearly lustre bath foam and preparation method thereof |
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| CN103271834B CN103271834B (en) | 2015-06-10 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104194968A (en) * | 2014-09-19 | 2014-12-10 | 江苏万淇生物科技有限公司 | Washing product containing AEG (Alkyl Ethoxy Polyglycosides) for hand washing dishes |
| CN104323925A (en) * | 2014-09-29 | 2015-02-04 | 江苏万淇生物科技有限公司 | Bath lotion being green, environmental-protective and gentle and containing glucoside derivative |
| CN105342939A (en) * | 2015-12-15 | 2016-02-24 | 山东消博士消毒科技股份有限公司 | Disinfectant bath wash capable of reducing operative incision infection and preparation technology of disinfectant bath wash |
| CN106176291A (en) * | 2015-05-06 | 2016-12-07 | 金红叶纸业集团有限公司 | Hand-mouth baby wet tissue compositional liquor and wet tissue |
| CN107648061A (en) * | 2017-10-17 | 2018-02-02 | 中国日用化学工业研究院 | A kind of shampoo with anti-dandruff nourishing pearly-lustre and preparation method thereof |
| CN108578272A (en) * | 2018-04-19 | 2018-09-28 | 山东顺皓聚氨酯保温材料有限公司 | A kind of polyhexamethylene guanide/biguanide hydrochloride shower cream and preparation method thereof |
| CN115386356A (en) * | 2022-09-14 | 2022-11-25 | 广汉市福客科技有限公司 | Blocking remover for oil-gas well and preparation method thereof |
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| US20040266891A1 (en) * | 1999-04-14 | 2004-12-30 | Mcintyre Group, Ltd. | Alkanolamide surfactant emulsions and process therefor |
| CN102631295A (en) * | 2012-03-30 | 2012-08-15 | 中国日用化学工业研究院 | Multifunctional foam liquid soap containing glucoside and derivatives of glucoside, and preparation method thereof |
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| US20040266891A1 (en) * | 1999-04-14 | 2004-12-30 | Mcintyre Group, Ltd. | Alkanolamide surfactant emulsions and process therefor |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104194968A (en) * | 2014-09-19 | 2014-12-10 | 江苏万淇生物科技有限公司 | Washing product containing AEG (Alkyl Ethoxy Polyglycosides) for hand washing dishes |
| CN104323925A (en) * | 2014-09-29 | 2015-02-04 | 江苏万淇生物科技有限公司 | Bath lotion being green, environmental-protective and gentle and containing glucoside derivative |
| CN106176291A (en) * | 2015-05-06 | 2016-12-07 | 金红叶纸业集团有限公司 | Hand-mouth baby wet tissue compositional liquor and wet tissue |
| CN105342939A (en) * | 2015-12-15 | 2016-02-24 | 山东消博士消毒科技股份有限公司 | Disinfectant bath wash capable of reducing operative incision infection and preparation technology of disinfectant bath wash |
| CN107648061A (en) * | 2017-10-17 | 2018-02-02 | 中国日用化学工业研究院 | A kind of shampoo with anti-dandruff nourishing pearly-lustre and preparation method thereof |
| CN107648061B (en) * | 2017-10-17 | 2020-09-22 | 中国日用化学工业研究院 | Shampoo with dandruff removing, nourishing and pearly luster and preparation method thereof |
| CN108578272A (en) * | 2018-04-19 | 2018-09-28 | 山东顺皓聚氨酯保温材料有限公司 | A kind of polyhexamethylene guanide/biguanide hydrochloride shower cream and preparation method thereof |
| CN115386356A (en) * | 2022-09-14 | 2022-11-25 | 广汉市福客科技有限公司 | Blocking remover for oil-gas well and preparation method thereof |
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| CN103271834B (en) | 2015-06-10 |
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