CN107648061A - A kind of shampoo with anti-dandruff nourishing pearly-lustre and preparation method thereof - Google Patents
A kind of shampoo with anti-dandruff nourishing pearly-lustre and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
A kind of percentage by weight of the shampoo with anti-dandruff nourishing pearly-lustre, which forms, is：N fatty acyl group L glycinates 10 25%; alcohol ether glucoside 5 15%; AEO 2 5%; Cocoamidopropyl betaine 1 5%, AEO carboxylic acid sodium 1 3%, the alcohol 0.5 1.5% of C16 18; saualane 0.3 3%; amino acid/11 1.5%, cation opsonizing agent 0.05 0.8%, deionized water surplus.The present invention has without silicone oil, and non-stimulated having is anti-dandruff, nourishes, the advantages of pearly-lustre.
Description
Technical field
The invention belongs to a kind of shampoo, and in particular to a kind of shampoo and its preparation side with anti-dandruff nourishing pearly-lustre
Method.
Background technology
Turn into the fashion trend of current hair washing hydrosphere without silicone oil shampoo.And many no silicone oil shampoos of in the market are single
Pure removes silicone oil, causes the conditioning performance of shampoo and reduces, is the degeneration of technology.It is really by gentle without silicone oil shampoo
Surfactant, special grease and effectively nursing scalp composition etc. shampoo without silicone oil technology by obtaining, its core effect
It is nursing scalp.Without silicone oil wash shield product should moderate performance, easily cleaned after use, the effect for making hair smooth, which is equal to, to be contained
Silicone oil product, it is most important that also there is the function of nursing scalp.
N- fatty acid acylamino acids system surfactant has low irritant, hypotoxicity, mildness, strong antibiotic property and gone
Dirty ability, in addition abundant and fine and smooth foaminess and excellent compatibility turn into the new lover of daily use chemicals industry, are no silicone oil hair washings
The first choice of gentle surfactant in water, but because of the problems such as hardly possible thickens, hair conditioning is not strong in application process, and extensively should not
With.
The factor that primarily forms of dandruff is sebum, fungi and private medical service.From cause, in the market is most to go
Bits product with the addition of the anti-dandruff agent for suppressing fungi in shampoo.These anti-dandruff agents have certain excitant and toxicity, are not inconsistent
Be fated the theory of modern safe green.From sebum angle, it can turn into anti-dandruff from the Sage Extract shampoo of natural no stimulation
An antipruritic big Research Thinking.
Saualane can strengthen maintenance epidermis, Sage Extract；Affinity is strong, can melt with the sebum film of mankind itself as one
Body, one layer of natural barrier is formed in skin surface；The peroxidating of skin lipid can be suppressed, can effectively infiltrate through skin, and promote
Enter the propagation of skin base cell；Skin pore can be opened, promote blood microcirculation, promote the metabolism of cell, helped
Repair damaged cell；Mycostatic growth can be pressed down.The advantages of saualane, meets nursing scalp and nourishes the theory being combined with anti-dandruff,
It is one of optimal candidate for substituting traditional silicone oil.But current saualane is particularly true in cream or mildy wash.
A kind of amino acid that number of patent application is 201610536892.6 is without silicone oil shampoo, and that application discloses a kind of ammonia
Base acid includes amino acid surfactant without silicone oil shampoo；The amino acid surfactant is main active ingredient；It is described
Amino acid also contains water, NMF, conditioner and preservative without silicone oil shampoo.The work of other class surfaces is added in embodiment
Property agent and water-soluble grease composition.The defects of this kind is formulated is：1. anti-dandruff component is not directed in the documents formula, it is anti-dandruff
Effect is little；2. the grease added in the documents Example formulations is water-soluble grease, water-soluble grease is in cleaning process
In can be rinsed out with current, be not easy to be attached on the hair tip and scalp, nurse scalp efficacy unobvious；3. the documents are implemented
It is both needed to add pearling agent and thickener in example formula, it is impossible to be really achieved green, moderate performance purpose.
Number of patent application be 201610586803.9 it is a kind of containing the shampoo of amino acid surfactant and its preparation side
Method, with amino acid surfactant it is main surfactant in the invention shampoo, is had one's hair wash in amino acid surfactant
One or more kinds of small molecular alcohols are added in the preparation technology of water, add dissolving of the lipid amino acid in surfactant
Property, but viscosity modifier has still been used in embodiment, illustrate that the problem of amino is acid-thickened does not solve at all.
The content of the invention
It is an object of the invention to provide one kind without silicone oil, the non-stimulated shampoo and its system with anti-dandruff nourishing pearly-lustre
Preparation Method.
Using N- fatty acid acylamino acids system's surfactant and alcohol ether glucoside as primary surfactant in shampoo of the present invention,
With the gentle surfactant compatibility such as alcohol ether carboxylate, Cocoamidopropyl betaine, acid-base modifier is done with amino acid, in addition
The saualane of nursing effect is moistened with Sage Extract, makes product gently non-stimulated, there is good cleaning force, cardability, go
Bits ability and viscosity, and there is pearl effect.
The purpose of the present invention is realized by the following method：
A kind of shampoo with anti-dandruff nourishing pearly-lustre, it is characterised in that the mass percent of shampoo, which forms, is：
N- fatty acyl group-L- glycinates in foregoing invention are the compounds for having below formula：
Wherein：R be carbon number 8-18 saturations or unsaturation, straight or branched aliphatic acid alkyl；M is K or Na.N‐
The preferred N- lauroyls-L- Sodium Glycinates of fatty acyl group-L- glycinates, N- lauroyl-L- glycine potassium, N- cocounut oil acyls
Base-L- Sodium Glycinates or N- cocoyl-L- glycine potassium.
Alcohol ether glucoside in foregoing invention is the compound for having below formula：
Wherein：R is the alkyl that carbon number is 8-18, m 1.2-1.8, n 1-3.The preferred C of alcohol ether glucoside12-14Alcohol ether sugar
Glycosides (m=1.2, n=2) or C16-18Alcohol ether glucoside (n=3, m=1.8).
AEO in foregoing invention is the compound for having below formula：
R-(OCH2CH2)nOH
Wherein R is carbon number 8-18 alkyl, n 3-9.The preferred C of AEO12-14Fatty alcohol polyoxy
Vinethene (n=9), C16-18AEO (n=7) selects C12-14AEO (n=5)
AEO carboxylic acid sodium in foregoing invention is the compound for having below formula：
R-(OCH2CH2)nOCH2COONa
Wherein R is carbon number 8-18 alkyl, n 3-9.The preferred C of AEO carboxylic acid sodium12-14Fat
Alcohol APEO carboxylic acid sodium (n=9), or C16-18AEO carboxylic acid sodium (n=7)
Amino acid in foregoing invention refers to the one or more in glycine, glutamic acid, methyl amimoacetic acid, lysine.
Cation opsonizing agent in foregoing invention refers to hydroxypropyl guar gum trimethyl ammonium chloride, Polyquaternium-10, SC-
60th, one kind in JR-400.
The PH of shampoo is 6.5-7.0 in foregoing invention
The viscosity of shampoo is 2500-4000cP in foregoing invention
The preparation method of shampoo of the present invention, comprises the following steps：
(1) formed by shampoo, by saualane, C16-18Alcohol, alcohol ether glucoside and AEO Hybrid Heating arrive
50-80 DEG C, preferably 60-70 DEG C, heat while stirring, and obtain A phases；
(2) formed by shampoo, by N- fatty acyl group-L- glycinates, Cocoamidopropyl betaine, fatty alcohol polyoxy
Vinethene carboxylic acid sodium, amino acid and deionized water Hybrid Heating preferably 60-70 DEG C, heat while stirring to 50-80 DEG C, obtain B
Phase；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add cation opsonizing agent, mixing is equal
It is even, obtain product.
It is of the invention compared with existing invention, have the following advantages that：
1. selecting with the close saualane of human skin to substitute traditional silicone oil, it can assign no silicon shampoo brand-new taste
Profit, nursing scalp, Sage Extract and anti-dandruff effect；
2. the N- fatty acyl group-L- glycinates and alcohol ether glucoside compounding from natural no stimulation are used as main Surfactant,
Make the shampoo that there is the advantages of excitant is low, foam is fine and smooth, while make that hair is smooth, plentiful spends after washing；
3. it is to help table from AEO, Cocoamidopropyl betaine and fat alcohol APEO carboxylic acid sodium
Face activating agent, is compounded with primary surfactant by a certain percentage, and the shampoo viscosity prepared is preferable, solves amino acid
The problem of being shampoo thickening；
4. from amino acid as acid-base modifier, with other compositions compatibility in the formula, the shampoo tool prepared
There is special pearl effect.
Embodiment
Embodiment 1：Each weight of material percentage is as follows：
The preparation method of shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol, C12-14Alcohol ether glucoside (m=1.2, n=2), C12-14Fatty alcohol
APEO (n=9) Hybrid Heating heats while stirring to 60 DEG C, obtains A phases；
(2) formed by shampoo, by N- lauroyl-L- Sodium Glycinates, Cocoamidopropyl betaine, C16-18Fatty alcohol
APEO carboxylic acid sodium (n=7), glutamic acid, glycine and deionized water Hybrid Heating heat while stirring, obtained to 60 DEG C
Obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add JR400, be well mixed, obtain
Product.
Embodiment 2：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol, C16-18Alcohol ether glucoside (n=3, m=1.8) and C12-14Fat
Alcohol APEO (n=5) Hybrid Heating heats while stirring to 65 DEG C, obtains A phases；
(2) formed by shampoo, by N- lauroyl-L- glycine potassium, Cocoamidopropyl betaine, C12-14Fatty alcohol
APEO carboxylic acid sodium (n=9), glycine, glutamic acid and deionized water Hybrid Heating heat while stirring, obtained to 65 DEG C
Obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add Polyquaternium-10, mixing is equal
It is even, obtain product.
Embodiment 3：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol, C12-14Alcohol ether glucoside (m=1.2, n=2) and C12-14Fat
Alcohol APEO (n=5) Hybrid Heating heats while stirring to 50 DEG C, obtains A phases；
(2) formed by shampoo, by N- cocoyl-L- glycine potassium, Cocoamidopropyl betaine, C16-18Fatty alcohol
APEO carboxylic acid sodium (n=7), methyl amimoacetic acid and deionized water Hybrid Heating heat while stirring to 80 DEG C, obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add hydroxypropyl guar gum trimethyl
Ammonium chloride, it is well mixed, obtains product.
Embodiment 4：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol, C12-14Alcohol ether glucoside (m=1.2, n=2) and C16-18Fat
Alcohol APEO (n=7) Hybrid Heating heats while stirring to 80 DEG C, obtains A phases；
(2) formed by shampoo, by N- cocoyl-L- Sodium Glycinates, Cocoamidopropyl betaine, C16-18Fatty alcohol
APEO carboxylic acid sodium (n=7), lysine and deionized water Hybrid Heating heat while stirring to 80 DEG C, obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add SC-60, be well mixed, obtain
Product.
Embodiment 5：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol, C12-14Alcohol ether glucoside (m=1.2, n=2) and C12-14Fat
Alcohol APEO (n=5) Hybrid Heating heats while stirring to 70 DEG C, obtains A phases；
(2) formed by shampoo, by N- cocoyl-L- glycine potassium, Cocoamidopropyl betaine, C12-14Fatty alcohol
APEO carboxylic acid sodium (n=9), methyl amimoacetic acid, glutamic acid and deionized water Hybrid Heating heat while stirring, obtained to 70 DEG C
Obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add cation opsonizing agent, mixing is equal
It is even, obtain product.
Comparative example 1：Each weight of material percentage is as follows：
The preparation method of shampoo is as follows：
(1) formed by shampoo, by C16-18Alcohol, C12-14Alcohol ether glucoside (m=1.2, n=2), C12-14Fatty alcohol polyoxy second
Alkene ether (n=9) Hybrid Heating heats while stirring to 60 DEG C, obtains A phases；
(2) formed by shampoo, by N- lauroyl-L- Sodium Glycinates, Cocoamidopropyl betaine, C16-18Fatty alcohol
APEO carboxylic acid sodium (n=7), glutamic acid, glycine and deionized water Hybrid Heating heat while stirring, obtained to 60 DEG C
Obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add JR400, be well mixed, obtain
Product.
Compared with Example 1, comparative example 1 does not add saualane, and the anti-dandruff property of prepared product and smoothness are undesirable.
Comparative example 2：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol, C12-14Alcohol ether glucoside (m=1.2, n=2) and C16-18Fat
Alcohol APEO (n=7) Hybrid Heating heats while stirring to 80 DEG C, obtains A phases；
(2) formed by shampoo, by N- cocoyl-L- Sodium Glycinates, Cocoamidopropyl betaine, C16-18Fatty alcohol
APEO carboxylic acid sodium (n=7), citric acid and deionized water Hybrid Heating heat while stirring to 80 DEG C, obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add SC-60, be well mixed, obtain
Product.
Compared with Example 2, the PH conditioning agents used in comparative example 2 are citric acid, and the product of preparation is without pearl effect.
Comparative example 3：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol and C12-14 AEOs (n=5) mixing add
Heat heats while stirring to 50 DEG C, obtains A phases；
(2) formed by shampoo, by N- cocoyl-L- glycine potassium, Cocoamidopropyl betaine, C16-18 fat
Alcohol APEO carboxylic acid sodium (n=7), methyl amimoacetic acid and deionized water Hybrid Heating heat while stirring to 80 DEG C, obtain B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add hydroxypropyl guar gum trimethyl
Ammonium chloride, it is well mixed, obtains product.
Compared with Example 3, comparative example 3 does not add AEO, and the product year prepared is undesirable.
Comparative example 4：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
(1) formed by shampoo, by saualane, C16-18Alcohol and C12-14 alcohol ether glucosides (m=1.2, n=2) Hybrid Heating
To 50 DEG C, heat while stirring, obtain A phases；
(2) form by shampoo, by N- cocoyl-L- glycine potassium, Cocoamidopropyl betaine, methyl amimoacetic acid and go
Ionized water Hybrid Heating heats while stirring to 80 DEG C, obtains B phases；
(3) B is added in A phases, and be stirred continuously, be cooled to less than 40 DEG C, add hydroxypropyl guar gum trimethyl
Ammonium chloride, it is well mixed, obtains product.
Compared with Example 4, comparative example 4 does not add AEO and AEO carboxylic acid sodium,
The product viscosity prepared is undesirable.
Comparative example 5：Each weight of material percentage is as follows：
The preparation method of above-mentioned shampoo is as follows：
Formed by shampoo, by saualane, C16-18 alcohol, C16-18 alcohol ether glucosides (n=3, m=1.8), C12-14 fat
Alcohol APEO (n=5), N- lauroyl-L- glycine potassium, Cocoamidopropyl betaine, C12-14 fatty alcohol polyoxies
Vinethene carboxylic acid sodium (n=9), glycine, glutamic acid and deionized water Hybrid Heating heat while stirring to 70 DEG C, to be cooled
To less than 40 DEG C, JR400 is added, is well mixed, obtains product.
Compared with Example 5, the preparation method of comparative example 5 is different, the product layering prepared, unstable.To embodiment
Tested with comparative example：
1st, irritant experiment method：The experiments of 4 health white of selection are respectively cut experiment rabbit back both sides dorsal body setae with rabbit
Remove, shave as far as possible totally, unhairing scope control is in 3cm × 3cm, application area 2.5cm × 2.5cm.Tested material about 5g is taken, with chicken
Egg white is mixed well in right amount, is uniformly applied on left side depilation skin, right side applies egg as control.Smear 1 time, keep daily
4h, continuously smear 14d.Since 2d, first cropping, check plot and test block are equally handled before each coating.Animal subject
4h after coating, to warm 0.9% sodium chloride solution cleaning check plot and test block, stand experimental rabbit person's bath 1h. and visually observe pair
According to the skin change in area and test block.Calculate each daily top of animal.Pass through skin wound repair strength grading table
Evaluation response result, the results are shown in Table 1.
2nd, anti-dandruff property and dry hair smoothness evaluation method：By the hair washing described in the embodiment 3,5 and comparative example 1 of preparation
Water, the volunteer for being respectively issued to 100 ages 18-40 year test use.Wherein 50 males of volunteer, 50 women, will
For hope person using hair washing in the same manner during hair washing water sample, every kind of shampoo is continuous with two weeks respectively, according to oneself
Sensation scores shampoo, and scoring is worst using 5 points of systems, 1 point, and 3 points moderate, and 5 points are best, and score more high effect is more
It is good.Various using effects evaluate average mark knot.
3rd, viscosity measurement：With reference to GB/T 5561-2012, experimental result is shown in Table 1.
4th, pH value assay method：With reference to GB/T 6368-2008, experimental result is shown in Table 1.
The result of the test such as following table of embodiment 1,2,3,4 and 5 and comparative example 1,2,3,4 and 5 gained shampoos
| Experiment numbers | Outward appearance | PH value | Viscosity | Anti-dandruff property | Dry hair smoothness | Excitant |
| Embodiment 1 | Milky, there is pearly-lustre | 6.7 | 3500 | 4.6 | 4.0 | It is nonirritant |
| Embodiment 2 | Milky, there is pearly-lustre | 6.5 | 3000 | 4.7 | 4.1 | It is nonirritant |
| Embodiment 3 | Milky, there is pearly-lustre | 6.6 | 3800 | 4.5 | 4.2 | It is nonirritant |
| Embodiment 4 | Milky, there is pearly-lustre | 7.0 | 2600 | 4.4 | 4.5 | It is nonirritant |
| Embodiment 5 | Milky, there is pearly-lustre | 6.8 | 4000 | 4.4 | 4.4 | It is nonirritant |
| Comparative example 1 | Milky, there is pearly-lustre | 6.6 | 3000 | 3.6 | 3.0 | It is nonirritant |
| Comparative example 2 | Milky, no pearly-lustre | ‐‐‐‐ | ‐‐‐‐ | ‐‐‐‐ | ‐‐‐‐ | ‐‐‐‐ |
| Comparative example 3 | Milky, there is pearly-lustre | 6.9 | 1200 | ‐‐‐‐ | ‐‐‐‐ | It is nonirritant |
| Comparative example 4 | Milky, there is pearly-lustre | 6.5 | 1500 | ‐‐‐‐ | ‐‐‐‐ | It is nonirritant |
| Comparative example 5 | Layering | ‐‐‐‐ | ‐‐‐‐ | ‐‐‐‐ | ‐‐‐‐ | ‐‐‐‐ |
As can be seen from Table 1, the product of preparation is nonirritant, and comparative example 1 does not add saualane, and the product of preparation is smooth
Degree and anti-dandruff property are bad；Comparative example 2 replaces amino acid to adjust pH value with citric acid, and the product of preparation is without pearl effect；Comparative example 3
Addition alcohol ether glucoside and alcohol ether, sodium alcohol ether carboxylate, the product viscosity prepared are undesirable with not having respectively in comparative example 4；Contrast
The preparation method of example 5 is different from the preparation method of embodiment, by the other compositions in addition to cation opsonizing agent together, prepares
Product it is unstable, lamination is serious.Embodiment 1-5, within the scope of the present invention, obtained product are gently non-stimulated,
With good cleaning force, cardability, chip-removing capacity and viscosity, and there is pearl effect, good market prospect.
Claims (13)
1. a kind of shampoo with anti-dandruff nourishing pearly-lustre, it is characterised in that percentage by weight composition is as follows：
2. a kind of shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 1, it is characterised in that N- fatty acyl groups-L- is sweet
Propylhomoserin salt is the compound for having below formula：
Wherein：R be carbon number 8-18 saturations or unsaturation, straight or branched aliphatic acid alkyl；M is K or Na.
3. a kind of shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 2, it is characterised in that N- fatty acyl groups-L- is sweet
Propylhomoserin salt is N- lauroyl-L- Sodium Glycinates, N- lauroyl-L- glycine potassium, N- cocoyl-L- Sodium Glycinates or N-
Cocoyl-L- glycine potassium.
4. a kind of shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 1, it is characterised in that alcohol ether glucoside is that have
The compound of below formula：
Wherein：R is the alkyl that carbon number is 8-18, m 1.2-1.8, n 1-3.
A kind of 5. shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 4, it is characterised in that alcohol ether glucoside C12-14
Alcohol ether glucoside or C16-18Alcohol ether glucoside.
A kind of 6. shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 1, it is characterised in that aliphatic alcohol polyethenoxy
Ether is the compound for having below formula：
R-(OCH2CH2)nOH
Wherein R is carbon number 8-18 alkyl, n 3-9.
A kind of 7. shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 6, it is characterised in that aliphatic alcohol polyethenoxy
Ether AEO is C12-14AEO, C16-18AEO selects C12-14Fatty alcohol
APEO.
A kind of 8. shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 1, it is characterised in that aliphatic alcohol polyethenoxy
Ether carboxylic acid sodium is the compound for having below formula：
R-(OCH2CH2)nOCH2COONa
Wherein R is carbon number 8-18 alkyl, n 3-9.
A kind of 9. shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 8, it is characterised in that aliphatic alcohol polyethenoxy
Ether carboxylic acid sodium is C12-14AEO carboxylic acid sodium or C16-18AEO carboxylic acid sodium.
10. a kind of shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 1, it is characterised in that amino acid is sweet ammonia
One or more in acid, glutamic acid, methyl amimoacetic acid, lysine.
11. a kind of shampoo with anti-dandruff nourishing pearly-lustre as claimed in claim 1, it is characterised in that cation opsonizing agent is
One kind in hydroxypropyl guar gum trimethyl ammonium chloride, Polyquaternium-10, SC-60, JR-400.
A kind of 12. shampoo with anti-dandruff nourishing pearly-lustre as described in claim any one of 1-11, it is characterised in that hair washing
The PH of water is 6.5-7.0, viscosity 2500-4000cP.
13. a kind of preparation method of shampoo with anti-dandruff nourishing pearly-lustre as described in claim any one of 1-12, it is special
Sign is to comprise the following steps：
(1) formed by shampoo, by saualane, C16-18Alcohol, alcohol ether glucoside and AEO Hybrid Heating are to 50-80
DEG C, preferably 60-70 DEG C, heat while stirring, obtain A phases；
(2) formed by shampoo, by N- fatty acyl group-L- glycinates, Cocoamidopropyl betaine, aliphatic alcohol polyethenoxy
Ether carboxylic acid sodium, amino acid and deionized water Hybrid Heating preferably 60-70 DEG C, heat while stirring to 50-80 DEG C, obtain B phases；
(3) B is added in A phases, and is stirred continuously, be cooled to less than 40 DEG C, add cation opsonizing agent, be well mixed,
Obtain product.
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| CN201710961497.7A CN107648061B (en) | 2017-10-17 | 2017-10-17 | Shampoo with dandruff removing, nourishing and pearly luster and preparation method thereof |
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| CN201710961497.7A CN107648061B (en) | 2017-10-17 | 2017-10-17 | Shampoo with dandruff removing, nourishing and pearly luster and preparation method thereof |
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| CN107648061A true CN107648061A (en) | 2018-02-02 |
| CN107648061B CN107648061B (en) | 2020-09-22 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114767557A (en) * | 2022-04-27 | 2022-07-22 | 广州天玺生物科技有限公司 | Milk cap shampoo and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1651129A (en) * | 2004-11-30 | 2005-08-10 | 中国日用化学工业研究院 | Surface active agent alcohol ether glucoside and its preparation method |
| CN103271834A (en) * | 2013-06-18 | 2013-09-04 | 中国日用化学工业研究院 | Non-irritant pollution-free moisturizing pearly lustre bath foam and preparation method thereof |
| CN105560102A (en) * | 2015-12-25 | 2016-05-11 | 名臣健康用品股份有限公司 | Natural health-care hair-washing and hair-caring composition |
-
2017
- 2017-10-17 CN CN201710961497.7A patent/CN107648061B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1651129A (en) * | 2004-11-30 | 2005-08-10 | 中国日用化学工业研究院 | Surface active agent alcohol ether glucoside and its preparation method |
| CN103271834A (en) * | 2013-06-18 | 2013-09-04 | 中国日用化学工业研究院 | Non-irritant pollution-free moisturizing pearly lustre bath foam and preparation method thereof |
| CN105560102A (en) * | 2015-12-25 | 2016-05-11 | 名臣健康用品股份有限公司 | Natural health-care hair-washing and hair-caring composition |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114767557A (en) * | 2022-04-27 | 2022-07-22 | 广州天玺生物科技有限公司 | Milk cap shampoo and preparation method thereof |
| CN114767557B (en) * | 2022-04-27 | 2023-11-24 | 广州天玺生物科技有限公司 | Milk cap shampoo and preparation method thereof |
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| CN107648061B (en) | 2020-09-22 |
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