CN107260562A - Amino acid mildy wash and preparation method thereof - Google Patents
Amino acid mildy wash and preparation method thereof Download PDFInfo
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- CN107260562A CN107260562A CN201710467382.2A CN201710467382A CN107260562A CN 107260562 A CN107260562 A CN 107260562A CN 201710467382 A CN201710467382 A CN 201710467382A CN 107260562 A CN107260562 A CN 107260562A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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Abstract
The invention discloses a kind of amino acid mildy wash and preparation method thereof, the amino acid mildy wash is mainly made up of sodium lauroyl glutamate, glycerine, polyethylene glycol 8, myristic acid, stearic acid, stearic acid diethylene glycol dilaurate, cocoyl glutamic acid, NMF 50, SF 1 and deionized water.Product safety of the present invention is stable, and foaming abundancy is fine and smooth, is worked well after washing, skin has moist feeling, smooth feeling, no tight feeling.
Description
【Technical field】
The present invention relates to amino acid mildy wash and preparation method thereof, belong to cosmetic technical field.
【Background technology】
Amino acid is the common name of the class organic compound containing amino and carboxyl.It is to constitute biological body protein and same
The relevant most basic material of vital movement, is the base unit for constituting protein molecule in vivo, with biological life
Activity has close relationship.It has special physiological function in antibody, is indispensable nutritional ingredient in organism
One of.What natural amino acid had now been found that has kind more than 300, and the amino acid of wherein needed by human body there are about 22 kinds, divides nonessential
Amino acid and essential amino acid (human body itself can not be synthesized).It is another to have acid, alkalescence, neutral, heterocycle classification, it is according to its chemistry
Qualitative classification.Amino acid is the base unit for constituting protein, is widely used in food, medicine, additive and cosmetic industry.
As biotechnology industry is increasingly becoming one of the major industry in the 21 century whole world, the demand of amino acid is increasing,
Varietal change is more and more faster, and technological innovation is more and more newer.
Amino acid mildy wash is the gentle mildy wash of most pro-skin in all mildy wash.The characteristics of its is maximum is exactly high-efficiency cleaning
While, gentle pro-skin, low stimulation, child and sensitive skin can be used.What traditional mildy wash was focused on is all high-efficient cleaning
Clean, pore cleanser, deoil, but have ignored stimulation of the product to skin in itself.Traditional mildy wash is in order to improve cleaning force and deoil
Ability, adds the compositions such as alkalescence extremely strong surfactant, foaming agent, soap base, and the skin of human body is weakly acidic, length
Time use can stimulate skin.More seriously, the sebum film of skin can be also destroyed.Once losing sebum film, skin holds very much
It is vulnerable to external injury.What amino acid mildy wash was used is then weakly acidic amino acid surfactant, pH value and human body flesh
Skin is approached, and it is the base substance for constituting protein to add amino acid, so gentle pro-skin, being not only adapted to the MM of small pox skin makes
With such as:Microbubble water is even more the cleaning products that sensitive skin few in number can also be safe to use.Real pure amino acid class
That of mildy wash, particularly ivory paste, toothpaste-like that, be usually with amino acid series table live in, it is most gentle and
And be that active quantities must be prepared in 95% powdery sodium glutamate raw material.It, which is formulated consumption, will typically reach more than 20 points,
Paste can just be made, this system has a simple method to debate not, some lotions are squeezed and come out, general to 45 degree of heating with
On, if lotion is changed into complete clear.More transparent clarification, illustrates that body material sodium glutamate is purer, active quantities are got over
Height, the sensation after this branch product is washed can be more beautiful.General real amino acid cleansing cream, after meeting is more than 40 degree, there is softening
Phenomenon, but it does not influence the use quality of product.Because amino acid table is lived, its person's character is determined.Good amino acids is washed one's face production
Product, it should be more stable with watery or gelatinous quality, composition is also more excellent, and foam volume will not be especially more,
There are some powdered amino acid face wash products, in general, relatively can be almost for cleaning strength and excitant；Separately
Outside, there are some brands also to add some ferment compositions in the product to improve clean effect, comparatively just compare high-quality
A bit.
Although amino acid cleansing cream has many advantages, but but still suffers from many deficiencies in technical elements at present, for example：It is difficult
Thicken, tie the problems such as cream point is low, lotion is thick, stability is poor, the mildy wash that especially prepared by the work of single amino acid class table, which exists, to be steeped
Foam not enough enriches, cleaning force not enough, the problem of do not wash clean.The most basic effect of face cleaning cream is clean surface portion skin, typically
Amino acid cleansing cream to be applicable crowd be dryness, sensitive mostly, because foam not enough enriches, be loose bulla, easily disappear,
Cleaning dynamics is inadequate.And when the skin of summer people universal oil, mixed type partially, cleaning force not enough can cause skin to have unnecessary oil
Fat is remained, and blocks pore, influences use feeling, while as skin cleaning does not thoroughly produce small pox acne blackhead etc. and asked
Topic.For face cleaning product, the cleaning capacity of product can not only be influenceed by enriching fine and smooth foam, while can also influence to disappear
The use feeling of the person of expense.The hardly possible thickening of amino acid cleansing cream system, is embodied in the lotion for being difficult to that lotion is made to shaping strip, big at present
Partial amino-acid system mainly prepares lotion using two methods of thickening method, crystallisation.Crystallisation, adds substantial amounts of amino acid powder
End, causes that lotion knot cream is harder, and lotion is coarse, to produce it is filling make troubles, simultaneously because lotion is too hard, be difficult extrusion soft
Pipe, also influences the use feeling of consumer.The lotion prepared using thickening method, often occurs the phenomenon of low temperature jelly conglomeration, low
Lotion meets water and is not easy to melt under the conditions of temperature, influence foaming, so as to influence the use feeling of consumer.The stability of amino acid lotion
There is lotion under the problem of test water outlet of room temperature shelf is thinning, cryogenic conditions and be hardened in more difficult control, general amino acid cleansing breast,
The problem of jelly, conglomeration, and the layering of heat-resisting rear lotion, the problem of return thick.The height influence life of amino acid cleansing cream knot cream point
Produce efficiency, knot cream point is low (less than 38 DEG C), and the time of cooling is long, especially in summer, the temperature of recirculated cooling water 30-40 DEG C it
Between, therefore material body is cooled to less than 38 DEG C, the time of cooling is longer, or cooling water refrigeration is needed to consume more energy
Source, causes production efficiency to reduce.
【The content of the invention】
The invention aims to the defect for overcoming prior art, there is provided a kind of safety and stability, fizzy amino
Sour mildy wash.
It is another object of the present invention in order to provide the preparation method of the amino acid mildy wash.
Amino acid mildy wash, it is characterised in that be made up of following weight percent composition：
A phases：
B phases：
Cocoyl glutamic acid 5-25%
NMF-50 1-5%
C phases：
SF-1 1-5%
Deionized water 2-10%
D phases：
Preservative 0.08-0.12%
Essence 0.01-0.1%
Wherein the summation of A phase, B phase, C phase and D phases is 100%.
Amino acid mildy wash as described above, it is characterised in that：By following weight than component constitute：
A phases：
B phases：
Cocoyl glutamic acid 10%
NMF-50 3%
C phases：
SF-1 2%
Deionized water 5%
D phases：
Preservative 0.1%
Essence 0.03%.
Sodium lauroyl glutamate, cocoyl glutamic acid are all the coco-nut oil fatty acid lifes by Pidolidone and plant derivation
Production is formed.Neutralize into after salt, there is foam exquisiteness, low irritant, hypotoxicity, good biodegradability.To people
Body skin compatibility is good, is a gentle moist type surfactant base, and being particularly suitable for children, pregnant woman and sensitive skin person makes
With.A kind of single amino acid table of addition, which is lived, has addition limitation, and too high levels have crystal precipitation, and very few foam is not rich enough
It is rich.The present invention is used using sodium lauroyl glutamate with the collocation of cocoyl glutamic acid, obtains possessing the foam for enriching exquisiteness, excellent
The amino acid mildy wash of good feel.
Sodium lauroyl glutamate foamability is better than SLS (lauryl sodium sulfate)；From natural resources, it is easy to biological
Degraded；It is low to skin and eye irritation using safety, no allergic reaction；Solution is in faintly acid, similar to skin；It is skin
Lotion as mild as a dove, it makes skin have soft and moist sensation, thus it is possible to vary the thixotropy of lotion so that originally relative
Solid lotion becomes soft, lotion easy drawout when washing by rubbing with the hands.Although sodium lauroyl glutamate foaming abundancy, as single
One surfactant, exists and easily separates out crystal, and feel is coarse, washes the not good defect of rear feel, addition is no more than 30%.
And cocoyl glutamic acid has good compatibility with skin, mildness, neutrality all shows good dissolubility.Similar soap base
The abundant foam of surfactant smooth, with smooth feel, easily rinses well, is worked well after washing, skin tool
There is a moist feeling, smooth feeling, not tight feeling.Although it is fine and smooth that cocoyl glutamic acid foam is used alone, not enough enrich, do ammonification
There is the problem of test water outlet of room temperature shelf is thinning in base acid mildy wash.
Cocoyl glutamic acid is compounded with sodium lauroyl glutamate, improves its foam quality, and improving foam feel improves skin
Sense.Lotion under the problem of water outlet is thinning, cryogenic conditions is avoided to be hardened simultaneously, the problems such as jelly, conglomeration.
The introducing of card ripple (SF-1) in the present invention, forms web frame, it is to avoid particle is separated out, while SF-1 can also cause lotion
There is viscoplasticity, it is to avoid lotion is coarse.It is additionally added in the present invention and helps table work (myristic acid, PEG-8) to make under its cryogenic conditions
Lotion is met water and easily melted, and improves frothing capacity, foam feel.Stearic acid diethylene glycol dilaurate can cause as main thickener
Lotion knot cream temperature stabilization, it is to avoid the problem of thinning under normal temperature.Adjusted in the amount 5-15% of glycerine, glycerine make it that lotion low temperature is steady
It is qualitative more preferable.
The present invention, which can be suitably added, assigns fat agent, and it is clear that some water miscible greases etc. (myristic acid, stearic acid) can increase its
The ability of clean oil-control.
The preparation method of amino acid mildy wash of the present invention, it is characterised in that comprise the following steps：
A, by A heat phases to 90 DEG C, stirring and dissolving completely, cooling；
B, when being cooled to 60 DEG C, add B phases and stir：
C, C, D phase are added when being cooled to 45 DEG C stir, discharging.
The pH value of product produced by the present invention is 5.5~7.5.
The present invention is for existing amino acid cleaning products, with advantages below：
Product safety of the present invention is stable, and foaming abundancy is fine and smooth, is worked well after washing, skin has moist feeling, smooth feeling, nothing
Tight feeling.
【Embodiment】
With reference to specific embodiment, the invention will be further described：
Table 1：Embodiment 1-3 each group distribution ratio, is represented with weight percentage.
Embodiment 1-3 and comparative example 1-2 preparation method are as follows：
A, by A heat phases to 90 DEG C, stirring and dissolving is complete；
B, when being cooled to 60 DEG C, add B phases and stir：
C, C, D phase are added when being cooled to 45 DEG C stir, discharging.
1-3 of the embodiment of the present invention and comparative example 1-2 testing performance index result is as follows：
1. outward appearance：White lotion
2.pH values：5.5-7.5
3. heat-resistant stability investigates (48 DEG C × 24h)：It is qualified
4. cold-resistant study on the stability (- 15 DEG C × 24h)：It is qualified.
The experiment of Performance Evaluation of the embodiment of the present invention is as follows：
First, skin irritation test：
2.5~3kg healthy rabbits 50 are selected, every rabbit back is symmetrical to select shaving 2.5cm at 202, it is right with itself
Carried out according to test method(s), 50 rabbits are divided into five groups of 1-5, every group applies one embodiment product, correspondence embodiment 1-3 and contrast respectively
Example 1-2, applies 0.5g products of the present invention every time or bare substrate, twice daily, left side or right side is administered at random, observe and record
The reacting phenomenon of skin after 24h, 72h.
As a result show：Rubefaction, hair are had no after product 24h, 72h for applying 1-3 of the embodiment of the present invention and comparative example 1-2
The local excitations such as rash, water lump are reacted.
2nd, efficacy validation：
50 volunteers are selected, are divided into the product obtained by 5 test control groups, every group of 10 people, the use embodiment 1 of group 1,
Product of the group 2 obtained by embodiment 2, the like comparative example 2, product acts on face, sooner or later each time daily, continuously makes
With one month, effect recording was in table 2.
Effect is described：
Effect is obvious：Moisturizing cleaning capacity is excellent, and skin-tightening is flexible；
There is improvement：Moisturizing cleaning capacity is general.
Effect is poor：Moisturizing cleaning capacity is poor, and skin is tight.
Embodiment 1-3 and comparative example 1-2 both effectiveness result of the test is as shown in table 2.
Table 2：
| Group | Effect is obvious | There is improvement | Effect is poor | Allergic reaction |
| 1 | 20 | 6 | 4 | Nothing |
| 2 | 23 | 5 | 2 | Nothing |
| 3 | 18 | 7 | 3 | Nothing |
| 4 | 3 | 18 | 9 | Nothing |
| 5 | 5 | 15 | 10 | Nothing |
Experimental result：Substantially it can be seen that the product effect that each component of the present invention is compounded is substantially better than pair from staining effect
Ratio 1 and 2.
Claims (4)
1. amino acid mildy wash, it is characterised in that be made up of following weight percent composition：A phases：
B phases：
Cocoyl glutamic acid 5-25%
NMF-50 1-5%
C phases：
SF-1 1-5%
Deionized water 2-10%
D phases：
Preservative 0.08-0.12%
Essence 0.01-0.1%
Wherein the summation of A phase, B phase, C phase and D phases is 100%.
2. amino acid mildy wash according to claim 1, it is characterised in that：By following weight than component constitute：
A phases：
B phases：
Cocoyl glutamic acid 10%
NMF-50 3%
C phases：
SF-1 2%
Deionized water 5%
D phases：
Preservative 0.1%
Essence 0.03%.
3. the preparation method of the amino acid mildy wash described in claim 1 or 2, it is characterised in that comprise the following steps：
A, by A heat phases to 90 DEG C, stirring and dissolving completely, cooling；
B, when being cooled to 60 DEG C, add B phases and stir：
C, C, D phase are added when being cooled to 45 DEG C stir, discharging.
4. the preparation method of amino acid mildy wash according to claim 3, it is characterised in that the pH value of products obtained therefrom is 5.5
~7.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710467382.2A CN107260562A (en) | 2017-06-20 | 2017-06-20 | Amino acid mildy wash and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710467382.2A CN107260562A (en) | 2017-06-20 | 2017-06-20 | Amino acid mildy wash and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107260562A true CN107260562A (en) | 2017-10-20 |
Family
ID=60067884
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201710467382.2A Pending CN107260562A (en) | 2017-06-20 | 2017-06-20 | Amino acid mildy wash and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114948775A (en) * | 2022-07-11 | 2022-08-30 | 广州市韵柯莱化妆品科技有限公司 | Amino acid oil-control facial cleanser and preparation method thereof |
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|---|---|---|---|---|
| DE19838034A1 (en) * | 1998-08-21 | 2000-02-24 | Beiersdorf Ag | Use of N-acyl amino acid surfactants to inhibit adsorption of lauryl ether sulfate on human skin during washing, especially in cosmetic or dermatological cleansing compositions |
| JP2004143072A (en) * | 2002-10-23 | 2004-05-20 | Kose Corp | Cleaner composition |
| US20060154847A1 (en) * | 2002-12-19 | 2006-07-13 | Schmid Karl H | Soft detergent mixtures |
| CN102048653A (en) * | 2011-01-06 | 2011-05-11 | 广州壹凡化工有限公司 | Amino acid type weak acid facial cleanser and preparation method thereof |
| CN102327198A (en) * | 2010-10-28 | 2012-01-25 | 深圳市金因生物技术有限公司 | Amino acid cleansing cream and preparation method thereof |
| CN105832572A (en) * | 2016-04-07 | 2016-08-10 | 广州宏度精细化工有限公司 | Amino acid facial cleanser and preparation method thereof |
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| CN106214523A (en) * | 2016-08-31 | 2016-12-14 | 苏州菲博特环保科技有限公司 | Amino acid cleansing mousse and preparation method thereof |
| CN106491381A (en) * | 2016-12-06 | 2017-03-15 | 诺斯贝尔化妆品股份有限公司 | A kind of gentle pure amino acid facial cleaning cream of crystal type |
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2017
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19838034A1 (en) * | 1998-08-21 | 2000-02-24 | Beiersdorf Ag | Use of N-acyl amino acid surfactants to inhibit adsorption of lauryl ether sulfate on human skin during washing, especially in cosmetic or dermatological cleansing compositions |
| JP2004143072A (en) * | 2002-10-23 | 2004-05-20 | Kose Corp | Cleaner composition |
| US20060154847A1 (en) * | 2002-12-19 | 2006-07-13 | Schmid Karl H | Soft detergent mixtures |
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| CN106214523A (en) * | 2016-08-31 | 2016-12-14 | 苏州菲博特环保科技有限公司 | Amino acid cleansing mousse and preparation method thereof |
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| CN106491381A (en) * | 2016-12-06 | 2017-03-15 | 诺斯贝尔化妆品股份有限公司 | A kind of gentle pure amino acid facial cleaning cream of crystal type |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114948775A (en) * | 2022-07-11 | 2022-08-30 | 广州市韵柯莱化妆品科技有限公司 | Amino acid oil-control facial cleanser and preparation method thereof |
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Application publication date: 20171020 |
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