CN106726873A - Amino acid clean water and preparation method thereof - Google Patents

Amino acid clean water and preparation method thereof Download PDF

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Publication number
CN106726873A
CN106726873A CN201611039110.4A CN201611039110A CN106726873A CN 106726873 A CN106726873 A CN 106726873A CN 201611039110 A CN201611039110 A CN 201611039110A CN 106726873 A CN106726873 A CN 106726873A
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amino acid
clean water
skin
weight
nmf
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秦燕燕
罗萍
马娟娟
宋坤
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Xi'an Bo He Medical Technology Co Ltd
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Xi'an Bo He Medical Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/524Preservatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
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  • Birds (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention belongs to the technical field of skin care face cleaning; specifically related to a kind of amino acid clean water and preparation method thereof; amino acid clean water is All Pure Nature amino acid type surfactant; without soap base; mean ph value with skin is consistent; while clean water understands various dirts; the weak acid environment of skin can be safeguarded; and diaphragm is formed in skin surface, skin affinity is outstanding, does not stimulate skin; skin protection function can rapidly be recovered after clean skin; make skin profit, acid-base balance, the purpose of skin health is safeguarded so as to reach, suitable any skin quality simultaneously can long-term use;The preparation method of amino acid clean water, can prepare above-mentioned amino acid clean water, and method is simple to operation, it is easy to industrialize, with good application value.

Description

Amino acid clean water and preparation method thereof
Technical field
The invention belongs to the technical field of skin care face cleaning, and in particular to a kind of amino acid clean water and preparation method thereof.
Background technology
Used as daily cleaning cosmetic product, the performance quality of face cleaning product has very big influence to skin.Skin it is good and , there be close contact bad the reason for the acid-base value of skin and cosmetics.Human body surface is due to retaining urea, uric acid, salt Point, the acidic materials such as lactic acid, amino acid, free fatty, therefore skin surface is usually faintly acid, the east application on human skin of health PH value should be between 4.5~6.5.Skin can only make skin be in absorption nutrition in its normal pH value range, Optimum state, and with the optimal state such as elasticity, gloss, moisture, and the ability for resisting extraneous erosion.
Additionally, the use to skin care item has been not limited to skin makeup, skin care industry at present, some are also extended to dermopathic auxiliary Help therapy field.For as a example by the impaired related skin disease of skin barrier, this is dept. of dermatology's clinically most common class Skin disease, such as:The skins such as sensitive, berloque dermatitis, steroid dependent dermatitis, acne, chloasma, atopic dermatitis Disease, has a strong impact on the physical and mental health of patient.
But the face cleaning product of prior art is mostly that pH value is generally more than 9.5 based on soap base class.This kind of face cleaning is produced Product, feel very clean with very strong cleaning effect, after use, and skin can also seem after even having used a period of time It is bright.However, skin now and it is non-real improve, but exfoliating excessively and hurts the illusion produced by skin.This kind of product Cleaning effect is fine on product surface, but substantially damages skin silently, and because its pH value is higher, therefore long-term use is unavoidable Can injured skin.The patient being especially damaged to skin barrier, sb.'s illness took a turn for the worse to aggravate it.Therefore, improving face cleaning product comprehensively Performance, while with face cleaning functions such as the facial dust of removal, greases, also with the effect for safeguarding skin health, is not only The skin care method and development trend of face cleaning product science, while being also the growing demand of consumers in general.
In order to solve the above problems, the invention provides a kind of amino acid clean water and preparation method thereof, the amino acid Clean water, while various dirts are gently removed, safeguards the weak acid environment of skin, and forms diaphragm in skin surface, The purpose of skin health is safeguarded so as to reach, the preparation method of amino acid clean water can prepare above-mentioned cleaning of good performance Water.
The content of the invention
It is an advantage of the invention to provide a kind of amino acid clean water, it is native amino acid type surface that it is contained Activating agent, the amino acid faintly acid clean water without soap base;
It is still another object of the present invention to provide a kind of amino acid clean water, it is gently removing various dirts Meanwhile, the weak acid environment of skin is safeguarded, and diaphragm is formed in skin surface, reach the purpose for safeguarding skin health;
It is still another object of the present invention to provide a kind of preparation method of amino acid clean water, it passes through to add entirely Natural amino acid type surfactant so that the amino acid clean water of preparation has good skin care purpose.
In order to solve the above problems, the invention provides a kind of amino acid clean water, including following percentage by weight original Material:
Amino acid surfactant 10%~40%, NMF 3%~20%, Purslane extract 0.5%~5%, lemon Lemon acid 0.02%~0.3%, preservative 0.3%~2%, balance of purified water.
Preferably, the amino acid clean water includes the raw material of following percentage by weight:
Amino acid surfactant 15%~32%, NMF 3%~18%, Purslane extract 1%~4%, lemon Acid 0.02%~0.2%, preservative 0.3%~2%, balance of purified water.
Preferably, the amino acid clean water includes the raw material of following percentage by weight:
Amino acid surfactant 25%, NMF 8%, Purslane extract 2%, citric acid 0.05%, preservative 0.6%, balance of purified water.
Preferably, the amino acid surfactant be fatty acyl group glutamate, fat acidyl glycine salt class, One or more of fatty acyl group alanine salt.
Preferably, the amino acid surfactant is sodium lauroyl glutamate, cocoyl Sodium Glycinate, cocounut oil One or more of acyl glutamic acid disodium.
Preferably, the NMF is one or more of polyalcohol, amino acid humectant, NMF NMF.
Preferably, the NMF is glycerine, trimethylglycine lactone, one kind of PCA sodium or several Kind.
A kind of preparation method of amino acid clean water, comprises the following steps:
1) according to percentage by weight, by 10%~40% amino acid surfactant, 3%~20% NMF, 0.5%~5% Purslane extract, in 0.02%~0.3% citric acid addition purified water, stirring is allowed to disperse, and is formed Dispersion soln;
2) above-mentioned dispersion soln is heated to 80~85 DEG C, 30~60min of stirring and dissolving, until solution is transparent clarification Shape, stands to remove blibbing;
3) solution for removing blibbing is cooled to 43~50 DEG C, adds the anti-corrosion that percetage by weight is 0.3%~2% Agent, continues to stir 30~45min, stands 12~24h, obtains final product watery amino acid clean water.
Preferably, in step 1) in, the percetage by weight of amino acid surfactant is 15%~32%, NMF Percetage by weight is 3%~18%, and the percetage by weight of Purslane extract is 1%~4%, and the percetage by weight of citric acid is 0.02%~0.2%.
Preferably, in step 1) in, the percetage by weight of amino acid surfactant is 25%, the weight hundred of NMF Fraction is 8%, and the percetage by weight of Purslane extract is 2%, and the percetage by weight of citric acid is 0.05%;Step 3) in The percetage by weight of preservative is 0.6%.
Beneficial effects of the present invention:
1st, the amino acid clean water that the present invention is provided, it uses All Pure Nature amino acid type surfactant to be made, and percent Hundred are free of soap base, and its skin composition gently can effectively remove various dirts, and form diaphragm in skin surface, so as to realize Safeguard the purpose of skin health.
2nd, the present invention provide amino acid clean water, its product in itself be in faintly acid, pH stable between 5.5~6.5, Average pH value with skin is completely the same, and skin affinity is outstanding, does not stimulate skin, without tight feeling, can be extensive rapidly after clean skin Multiple skin protection function, makes skin profit, acid-base balance, and suitable any skin quality simultaneously can long-term use.
3rd, the amino acid clean water that the present invention is provided, the skin of its various skin quality of cleaning is especially suitable for sensitive, changes The barrier damaged skin such as cosmetic dermatitis, steroid dependent dermatitis, acne, chloasma, atopic dermatitis.
4th, the amino acid clean water that the present invention is provided, it is different from other cleaning products of market, general face cleaning cream and makeup removing It is too strong to there is degreasing power in water, washes rear dry disadvantage.It is gentle non-stimulated, it is moist not tight after cleaning.
5th, the amino acid clean water that the present invention is provided, its is fully transparent, and in low temperature, (4 DEG C or so) are arrived (48 DEG C) holdings of high temperature Fabulous stability and transparency, without layering or flocculation.
6th, the preparation method of the amino acid clean water that the present invention is provided, it can use the amino acid surface of All Pure Nature activity Agent, prepares the amino acid clean water of skin care of good performance.
Specific embodiment
With reference to specific embodiment, the present invention is described in further detail, to make those skilled in the art's reference Specification word can be implemented according to this.
It should be appreciated that it is used herein such as " have ", "comprising" and " including " term is not precluded from one or many Individual other presence or addition.
Embodiment 1
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 20%, NMF 11%, Purslane extract 2%, citric acid 0.05%, preservative 0.6%, purify water surplus;
Wherein, amino acid surfactant is sodium lauroyl glutamate, and NMF is including percentage by weight is 6% three Methylglycine lactone, 3% glycerine, 2% PCA sodium.
Embodiment 2
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 25%, NMF 8%, Purslane extract 2%, citric acid 0.05%, preservative 0.6%, purify water surplus;
Wherein, amino acid surfactant is sodium lauroyl glutamate, and NMF is including percentage by weight is 2% three Methylglycine lactone, 5% glycerine, 1% PCA sodium.
Embodiment 3
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 20%, NMF 9%, Purslane extract 2%, citric acid 0.05%, preservative 0.6%, purify water surplus;
Wherein, amino acid surfactant be weight percentage be 10% cocoyl Sodium Glycinate and 10% cocounut oil Acyl glutamic acid disodium, NMF be weight percentage for 2% trimethylglycine lactone, 5% glycerine, 2% L- pyrroles Pyrrolidone carboxylic acid's sodium.
Embodiment 4
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 10%, NMF 20%, Purslane extract 0.5%, citric acid 0.02%, preservative 0.3%, purify water surplus;
Wherein, amino acid surfactant is sodium lauroyl glutamate, and NMF is including percentage by weight is 4% three Methylglycine lactone, 13% glycerine, 3% PCA sodium.
Embodiment 5
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 40%, NMF 3%, Purslane extract 1%, citric acid 0.2%, preservative 0.9%, purify water surplus;
Wherein, amino acid surfactant is sodium lauroyl glutamate, and NMF is including percentage by weight is 1% three Methylglycine lactone, 1% glycerine, 1% PCA sodium.
Embodiment 6
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 15%, NMF 18%, Purslane extract 3%, citric acid 0.3%, preservative 1.5%, purify water surplus;
Wherein, amino acid surfactant is sodium lauroyl glutamate, and NMF is including percentage by weight is 5% three Methylglycine lactone, 9% glycerine, 4% PCA sodium.
Embodiment 7
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 32%, NMF 15%, Purslane extract 4%, citric acid 0.15%, preservative 2%, purify water surplus;
Wherein, amino acid surfactant is sodium lauroyl glutamate, and NMF is including percentage by weight is 4% three Methylglycine lactone, 8% glycerine, 3% PCA sodium.
Embodiment 8
A kind of amino acid clean water, including following percentage by weight raw material:
Amino acid surfactant 25%, NMF 5%, Purslane extract 5%, citric acid 0.1%, preservative 0.6%, purify water surplus;
Wherein, amino acid surfactant is sodium lauroyl glutamate, and NMF is including percentage by weight is 1% three Methylglycine lactone, 3% glycerine, 1% PCA sodium.
The essence that percentage by weight is 0.3%~0.8% can also be added in embodiment 1 to embodiment 8.
Embodiment 9
One kind prepares embodiment 1, the preparation method of the amino acid clean water in embodiment 3 to embodiment 8, including following step Suddenly:
According to percentage by weight, by 10%~40% amino acid surfactant, 3%~20% NMF, 0.5% ~5% purslane, in 0.02%~0.3% citric acid addition purified water, stirring is allowed to disperse, and forms dispersion soln;
Above-mentioned dispersion soln is heated to 80 DEG C, stirring and dissolving 30min, until solution is transparent clarification shape, stands to remove Remove blibbing;
The solution for removing blibbing is cooled to 43 DEG C, the preservative that percetage by weight is 0.3%~2% is added, after Continuous stirring 45min, stands 12h, obtains final product watery amino acid clean water.
Embodiment 10
One kind prepares embodiment 1, the preparation method of the amino acid clean water in embodiment 3 to embodiment 8, including following step Suddenly:
According to percentage by weight, by 15%~32% amino acid surfactant, 3%~18% NMF, 1%~ 4% purslane, in 0.02%~0.2% citric acid addition purified water, stirring is allowed to disperse, and forms dispersion soln;
Above-mentioned dispersion soln is heated to 85 DEG C, stirring and dissolving 60min, until solution is transparent clarification shape, stands to remove Remove blibbing;
The solution for removing blibbing is cooled to 50 DEG C, the preservative that percetage by weight is 0.3%~2% is added, after 30~45min of continuous stirring, stands 24h, obtains final product watery amino acid clean water.
Embodiment 11
A kind of preparation method of the amino acid clean water for preparing embodiment 2, comprises the following steps:
According to percentage by weight, by 25% amino acid surfactant, 8% NMF, 2% purslane is extracted Liquid, in 0.05% citric acid addition purified water, stirring is allowed to disperse, and forms dispersion soln;
Above-mentioned dispersion soln is heated to 83 DEG C, stirring and dissolving 45min, until solution is transparent clarification shape, stands to remove Remove blibbing;
The solution for removing blibbing is cooled to 46 DEG C, the preservative that percetage by weight is 0.6% is added, continues to stir 30~45min, stands 24h, obtains final product watery amino acid clean water.
Selection above-described embodiment 1 to the amino acid clean water of embodiment 8 carries out skin care test;
First, embodiment 1 to the pH value of the amino acid clean water of embodiment 8 is shown in Table 1:
Table 1
PH value
Embodiment 1 5.9
Embodiment 2 5.6
Embodiment 3 5.6
Embodiment 4 5.7
Embodiment 5 5.5
Embodiment 6 5.6
Embodiment 7 5.8
Embodiment 8 6.0
Skin on face is normally in faintly acid, pH5.5 or so, if using the soap of strong basicity or other are similar Face cleaning product, except excitant by force in addition to, can also change the acid or alkali environment of skin surface, the metabolism for skin has quite Negative effect, and the product cleaning capacity of strong basicity is too strong, and the sebum film on cuticula is washed, also easily by skin Grease between cell and cell is washed, and here it is cause one of key factor of dry skin, cleans excessive harm, It is probably more than unclean, often excessively it is accountable with cleaning as the problems such as pachylosis, thick pore, dark sore, allergy.
And, the present invention provide a kind of amino acid clean water itself be in faintly acid, pH stable 5.5~6.5 it Between, the average pH value with skin is completely the same, and skin affinity is outstanding, does not stimulate skin, without tight feeling, can be rapid after clean skin Recover skin protection function, make skin profit, acid-base balance, suitable any skin quality simultaneously can long-term use.
Secondly, the amino acid clean water to embodiment 1 to embodiment 8 carries out skin moisture content test
50 25-30 Sui women triers of test, first record the keratoderma moisture for using preceding subject, afterwards Start respectively trier face continuously painting embodiment 1 to embodiment 8 amino acid clean water, smearing position be face 10 ×10mm2The skin of area, 10 × 10mm at is selected in the face of same trier again2The skin of area, any skin care is not smeared Product, it is sooner or later each daily once, continuous to smear 2 months, the keratoderma moisture tested in application area afterwards is and on probation Before compare, probability keratoderma moisture takes eight groups of data for wherein trying out embodiment 1 to embodiment 8, and data are shown in Table 2:
Table 2
Result shows, moisture content of skin than not using preceding increasing,
Clean water of the invention is made of All Pure Nature amino acid type surfactant, 100% be free of soap base, its skin into Dividing gently can effectively remove various dirts, and form diaphragm in skin surface, so as to realize safeguarding the purpose of skin health.
And, this product can clean the skin of various skin quality, be especially suitable for sensitive, berloque dermatitis, hormone dependant The barrier damaged skins such as property dermatitis, acne, chloasma, atopic dermatitis;This product is different from other cleaning products of market, general clean It is too strong to there is degreasing power in face cream and makeup remover, washes rear dry disadvantage.It is gentle non-stimulated, it is moist not tight after cleaning.
And, the preparation method of the amino acid clean water that the present invention is provided, the amino acid clean water prepared is fully transparent, In low temperature, (4 DEG C or so) are arrived (48 DEG C) holdings of high temperature fabulous stability and transparency, without layering or flocculation phenomenon.
Although embodiment of the present invention is disclosed as above, it is not restricted to listed in specification and implementation method With, various suitable the field of the invention can be applied to entirely, for those skilled in the art, it is easily achieved Other modification, therefore under the universal limited without departing substantially from claim and equivalency range, the present invention is not limited to spy Fixed details.

Claims (10)

1. a kind of amino acid clean water, it is characterised in that the raw material including following percentage by weight:
Amino acid surfactant 10%~40%, NMF 3%~20%, Purslane extract 0.5%~5%, citric acid 0.02%~0.3%, preservative 0.3%~2%, balance of purified water.
2. amino acid clean water as claimed in claim 1, it is characterised in that the amino acid clean water includes following weight hundred Divide the raw material of ratio:
Amino acid surfactant 15%~32%, NMF 3%~18%, Purslane extract 1%~4%, citric acid 0.02%~0.2%, preservative 0.3%~2%, balance of purified water.
3. amino acid clean water as claimed in claim 2, it is characterised in that the amino acid clean water includes following weight hundred Divide the raw material of ratio:
Amino acid surfactant 25%, NMF 8%, Purslane extract 2%, citric acid 0.05%, preservative 0.6%, Balance of purified water.
4. the amino acid clean water as described in any one in claims 1 to 3, it is characterised in that the amino acid surface is lived Property agent for fatty acyl group glutamate, fat acidyl glycine salt class, fatty acyl group alanine salt one or more.
5. amino acid clean water as claimed in claim 4, it is characterised in that the amino acid surfactant is lauroyl One or more of sodium glutamate, cocoyl Sodium Glycinate, cocoyl disodium glutamate.
6. the amino acid clean water as described in any one in claims 1 to 3, it is characterised in that the NMF is polynary One or more of alcohol, amino acid humectant, NMF NMF.
7. amino acid clean water as claimed in claim 6, it is characterised in that the NMF is glycerine, trimethylglycine One or more of lactone, PCA sodium.
8. a kind of preparation method of amino acid clean water, it is characterised in that comprise the following steps:
1) according to percentage by weight, by 10%~40% amino acid surfactant, 3%~20% NMF, 0.5%~ 5% Purslane extract, in 0.02%~0.3% citric acid addition purified water, stirring is allowed to disperse, and forms dispersion molten Liquid;
2) above-mentioned dispersion soln is heated to 80~85 DEG C, 30~60min of stirring and dissolving, until solution is transparent clarification shape, it is quiet Put to remove blibbing;
3) solution for removing blibbing is cooled to 43~50 DEG C, adds the preservative that percetage by weight is 0.3%~2%, Continue to stir 30~45min, stand 12~24h, obtain final product watery amino acid clean water.
9. the preparation method of amino acid clean water as claimed in claim 8, it is characterised in that in step 1) in, amino acid table The percetage by weight of face activating agent is 15%~32%, and the percetage by weight of NMF is 3%~18%, Purslane extract Percetage by weight is 1%~4%, and the percetage by weight of citric acid is 0.02%~0.2%.
10. the preparation method of amino acid clean water as claimed in claim 9, it is characterised in that in step 1) in, amino acid table The percetage by weight of face activating agent is 25%, and the percetage by weight of NMF is 8%, and the percetage by weight of Purslane extract is 2%, the percetage by weight of citric acid is 0.05%;Step 3) in preservative percetage by weight be 0.6%.
CN201611039110.4A 2016-11-21 2016-11-21 Amino acid clean water and preparation method thereof Pending CN106726873A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107260562A (en) * 2017-06-20 2017-10-20 彭再辉 Amino acid mildy wash and preparation method thereof

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Application publication date: 20170531