CN106074256A - A kind of solid spray makeup removing gel and preparation method and application - Google Patents
A kind of solid spray makeup removing gel and preparation method and application Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/34—Alcohols
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- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
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Abstract
The invention discloses a kind of solid spray makeup removing gel and preparation method and application.Described solid spray makeup removing gel is prepared from by following material component by percentage to the quality: filler: 35 65, gentle surfactant: 6 30, hydrophilic tax fat agent: 2 10, PH regulator: 0.05 0.6, natural detergent: 28, gum deposit agent: 0.1 1.0, polyhydric alcohol wetting agent: 3 15, colloid sclerosing agent: 0.5 3, anti-allergic agent: 0.1 0.5, essence: 0.05 0.3, solubilizing agent: 0.2 0.8, preservative: 0.1 0.8.The solid spray makeup removing gel novel appearance that the present invention prepares, in golden transparent shape solid, solid intensity is high, makeup removing performance is good, formulation stable, it is easy to spraying, it is injected on skin and can form one layer of thin film uniform, that silk is sliding, salubrious, supplement current makeup removal products category dosage form well.
Description
Technical field
The present invention relates to a kind of cleaning products, be specially a kind of solid spray makeup removing gel and preparation method thereof and answer
With.
Background technology
Nowadays social life makes to apply some make up, especially use the people of color make-up product to get more and more, along with people couple
The demand of color make-up product persistence and the environmental effect gone from bad to worse, common face cleaning makeup removal products is not enough to thoroughly clean skin
On dirt.But if makeup removing is not thorough, the cosmetics of residual will cause a series of skin problem, so skin clean
Makeup removal products is brisk in the market can the phase.Makeup removing series products mainly has makeup remover, makeup remover and makeup removing breast in the market.Makeup remover,
Makeup remover exists in liquid form, and the bad system of suspension dynamics of formula is not easy stable, is easily generated floccule or precipitation.If with
Solid-state or emulsus (makeup removing breast) form exist, it is possible to resolve the problems referred to above, but this series products need to use through spread form, easily causes clear
Clean uneven.If the shortcoming in terms of having makeup removal products can simultaneously solve two above, it will have more preferable usability.
Patent documentation CN 102836089 B and CN 104146880 A reports a kind of sprayable spray skin-care solid
Body glue, product keeps solid forms, is atomized by pump head during use, be injected on skin can be formed one layer uniformly, silk sliding, clearly
Refreshing thin film, this technology is now mainly used in the moisturizing nursing of skin.
Summary of the invention
In order to solve technical problem present in prior art, it is an object of the invention to provide a kind of all-transparent makeup removing solid
Spray body gel, novel appearance, occupation mode is novel, is difficult to reveal, and makeup removing ability is strong, and gentleness does not stimulates, and easily rinses, and unloads after washing
Non-greasy, can supplement current makeup removal products category dosage form well.
Another object of the present invention is to provide the preparation method of above-mentioned solid spray makeup removing gel.
The technical solution adopted in the present invention is as follows.
A kind of solid spray makeup removing gel, is prepared from by following material component by percentage to the quality:
Filler: 35-65,
Gentle surfactant: 6-30,
Hydrophilic composes fat agent: 2-10,
PH regulator: 0.05-0.6,
Natural detergent: 2-8,
Gum deposit agent: 0.1-1.0,
Polyhydric alcohol wetting agent: 3-15,
Colloid sclerosing agent: 0.5-3,
Anti-allergic agent: 0.1-0.5,
Essence: 0.05-0.3,
Solubilizing agent: 0.2-0.8,
Preservative: 0.1-0.8.
Present invention also offers the preparation method of described spraying makeup removing gel, comprise the steps:
(1) with polyhydric alcohol wetting agent moistening gum deposit agent, add PH regulator after pulp, add filler, be heated with stirring to 85
± 2 DEG C, adding anti-allergic agent and dissolve, under heat-retaining condition, 300 ~ 400r/min stirs 5-10 minute；
(2) temperature 85 ± 2 DEG C, colloid sclerosing agent is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 70 ± 2
℃；
(3) gentle surfactant and hydrophilic tax fat agent, natural detergent, stirring and dissolving are added；
(4) by essence, solubilizing agent mixing, add when 58 ± 2 DEG C, stir；
When (5) 56 ± 2 DEG C, preservative is added, stir；
(6) keeping material 50 ± 2 DEG C of temperature of body, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation, then at once
After standing completion of cure.
Preferably, described filler is deionized water.
Preferably, described gentle surfactant includes alkyl polyglucoside, cocoyl both sexes sodium acetate, sodium lauroyl sarcosine
With the one in amino acid surfactant, more preferably alkyl polyglucoside.
Preferably, described hydrophilic compose fat agent include PEG-7 sodium cocoglyceryl ester, PEG-7 caprylic/capric triglyceride,
PEG-9 Yue Guisuanzhi &PPG-26 butylol polyether-26& butanediol (useful commercial name CS26).
Preferably, described PH regulator includes citric acid, sodium citrate.
Preferably, described natural detergent is Fructus Sapindi Mukouossi extracting solution.
Preferably, described gum deposit agent includes the one in low-acyl gellan gum and HANSHENGJIAO, and the lowest acyl group knot is cold
Glue.
Preferably, described polyhydric alcohol wetting agent includes more than one in propylene glycol, glycerol, butanediol and sorbitol, more
It is preferably propylene glycol.
Preferably, described colloid sclerosing agent is calcium chloride solution, and calcium chloride solution refers to the aqueous solution of calcium chloride, in solution
The concentration of calcium chloride is 0.4-0.6 mol/L.
Preferably, described anti-allergic agent include allantoin, hamamelis extract, glycyrrhizic acid dipotassium, water-soluble bisabolol and
More than one in Herba portulacae extract, more preferably allantoin.
Preferably, described essence is that cosmetic field commonly uses raw material, including the one in the fragrance of a flower and fruital.
Preferably, described solubilizing agent is that cosmetic field commonly uses raw material, including tween 20 and polyoxyethylene hydrogenated Oleum Ricini
In one, more preferably tween 20.
Preferably, described preservative is the raw material that cosmetic field is conventional, including imidazolidinyl urea, methylisothiozoline
The compound of one or more in ketone, phenoxyethanol, chlorphenesin and methyl parahydroxybenzoate.
Described solid spray makeup removing gel is used for removing ornaments and formal dress, face cleaning, cleaning skin product scope.
Compared with prior art, the beneficial effects of the present invention is:
(1) providing a kind of all-transparent solid makeup removing spray gel, novel appearance, occupation mode is novel, is difficult to reveal, and spraying is all
Even, makeup removing ability is strong, and gentleness does not stimulates, and easily rinses, and unloads and washes rear non-greasy, and effective moisturizing supplements current makeup removal products well
Category dosage form.
(2) preparation method of this solid spray makeup removing gel is simple, and equipment requirements is low, low cost, it is easy to manipulation.
Detailed description of the invention
The present invention is expanded on further below in conjunction with specific embodiment.Should be understood that these embodiments are merely to illustrate the present invention
Rather than limit the range of application of the present invention.In following example, the various raw materials used in the present invention all can pass through business
Channel is buied.
Embodiment 1
Weigh following component (percentage by weight) according to quantity:
Deionization: 60.0；Alkyl polyglucoside: 18.0；CS26:5.0；Citric acid, sodium citrate: 0.2；Fructus Sapindi Mukouossi extracting solution: 4.0；
Low-acyl gellan gum: 0.5；Propylene glycol: 9.0；Calcium chloride solution (0.4mol/L): 2.0；Allantoin: 0.3；Essence: 0.1；Tell
Temperature-20: 0.5；Preservative: 0.4.
Preparation process is as follows:
(1) with propylene glycol moistening low-acyl gellan gum, add citric acid, sodium citrate regulation PH after pulp, add deionization
Water, is heated with stirring to 83 DEG C, adds allantoin and dissolves, and under heat-retaining condition, 300r/min stirs 5 minutes；
(2) temperature 83 DEG C, calcium chloride solution is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 72 DEG C；
(3) alkyl polyglucoside and CS26, Fructus Sapindi Mukouossi extracting solution, stirring and dissolving are added；
(4) by essence, tween 20 mixing, add in above material when 58 DEG C, stir；
When (5) 58 DEG C, preservative is added, stir.
(6) keeping with the above 52 DEG C of temperature of material, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation at once,
Then after standing 2 hours completion of cures.
Obtain the solid spray makeup removing gel of the present embodiment for without mobility solid product, product can be made by pump head extruding
Atomization, is evenly distributed on skin surface.Through stability test (-15 DEG C ,-4 DEG C, room temperature, 40 DEG C, 50 DEG C, natural lighting, fluorescence
Light irradiation) index such as the abnormal smells from the patient of record product, outward appearance, viscosity, pH change weekly, after one month, product is the most muddy, indices
All meet the requirement of " cosmetics health specification ".
Embodiment 2
Weigh following component (percentage by weight) according to quantity:
Deionized water: 58.0；Alkyl polyglucoside: 23.0；CS26:6.0；Citric acid, sodium citrate: 0.4；Fructus Sapindi Mukouossi extracting solution:
6.0；Low-acyl gellan gum: 0.7；Propylene glycol: 3.0；Calcium chloride solution (0.5mol/L): 2.0；Allantoin: 0.3；Essence: 0.2；
Tween 20: 0.2；Preservative: 0.2.
Preparation process is as follows:
(1) with propylene glycol moistening low-acyl gellan gum, add citric acid, sodium citrate regulation PH after pulp, add deionization
Water, is heated with stirring to 85 DEG C, adds allantoin and dissolves, and under heat-retaining condition, 300r/min stirs 10 minutes；
(2) temperature 85 DEG C, calcium chloride solution is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 70 DEG C；
(3) alkyl polyglucoside and CS26, Fructus Sapindi Mukouossi extracting solution, stirring and dissolving are added；
(4) by essence, tween 20 mixing, add in above material when 54 DEG C, stir；
When (5) 54 DEG C, preservative is added, stir；
(6) keeping with the above 50 DEG C of temperature of material, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation, then at once
After standing 2 hours completion of cures.
Obtain the solid spray makeup removing gel of the present embodiment for without mobility solid product, product can be made by pump head extruding
Atomization, is evenly distributed on skin surface.Through stability test (-15 DEG C ,-4 DEG C, room temperature, 40 DEG C, 50 DEG C, natural lighting, fluorescence
Light irradiation) index such as the abnormal smells from the patient of record product, outward appearance, viscosity, pH change weekly, after one month, product is the most muddy, indices
All meet the requirement of " cosmetics health specification ".
Embodiment 3
Weigh following component (percentage by weight) according to quantity:
Deionized water: 65.0；Alkyl polyglucoside: 10.0；CS26:4.0；Citric acid, sodium citrate: 0.2；Fructus Sapindi Mukouossi extracting solution:
3.0；Low-acyl gellan gum: 0.6；Propylene glycol: 14.0；Calcium chloride solution (0.5mol/L): 2.0；Allantoin: 0.2；Essence:
0.1；Tween 20: 0.4；Preservative: 0.5.
Preparation process is as follows:
(1) with propylene glycol moistening low-acyl gellan gum, add citric acid, sodium citrate regulation PH after pulp, add deionization
Water, is heated with stirring to 87 DEG C, adds allantoin and dissolves, and under heat-retaining condition, 400r/min stirs 10 minutes；
(2) temperature 87 DEG C, calcium chloride solution is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 70 DEG C；
(3) alkyl polyglucoside and CS26, Fructus Sapindi Mukouossi extracting solution, stirring and dissolving are added；
(4) by essence, tween 20 mixing, add in above material when 56 DEG C, stir；
When (5) 56 DEG C, preservative is added, stir；
(6) keeping with the above 50 DEG C of temperature of material, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation, then at once
After standing 2 hours completion of cures.
Obtain the solid spray makeup removing gel of the present embodiment for without mobility solid product, product can be made by pump head extruding
Atomization, is evenly distributed on skin surface.Through stability test (-15 DEG C ,-4 DEG C, room temperature, 40 DEG C, 50 DEG C, natural lighting, fluorescence
Light irradiation) index such as the abnormal smells from the patient of record product, outward appearance, viscosity, pH change weekly, after one month, product is the most muddy, indices
All meet the requirement of " cosmetics health specification ".
Embodiment 4
Weigh following component (percentage by weight) according to quantity:
Deionized water: 63.0；Alkyl polyglucoside: 12.0；CS26:8.0；Citric acid, sodium citrate: 0.25；Fructus Sapindi Mukouossi extracting solution:
2.0；Low-acyl gellan gum: 0.4；Propylene glycol: 12.0；Calcium chloride solution (0.6mol/L): 0.5；Allantoin: 0.5；Essence:
0.05；Tween 20: 0.7；Preservative: 0.6.
Preparation process is as follows:
(1) with propylene glycol moistening low-acyl gellan gum, add citric acid, sodium citrate regulation PH after pulp, add deionization
Water, is heated with stirring to 85 DEG C, adds allantoin and dissolves, and under heat-retaining condition, 400r/min stirs 8 minutes；
(2) temperature 85 DEG C, calcium chloride solution is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 68 DEG C；
(3) alkyl polyglucoside and CS26, Fructus Sapindi Mukouossi extracting solution, stirring and dissolving are added；
(4) by essence, tween 20 mixing, add in above material when 58 DEG C, stir；
When (5) 58 DEG C, preservative is added, stir；
(6) keeping with the above 48 DEG C of temperature of material, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation, then at once
After standing 2 hours completion of cures.
Obtain the solid spray makeup removing gel of the present embodiment for without mobility solid product, product can be made by pump head extruding
Atomization, is evenly distributed on skin surface.Through stability test (-15 DEG C ,-4 DEG C, room temperature, 40 DEG C, 50 DEG C, natural lighting, fluorescence
Light irradiation) index such as the abnormal smells from the patient of record product, outward appearance, viscosity, pH change weekly, after one month, product is the most muddy, indices
All meet the requirement of " cosmetics health specification ".
Embodiment 5
Weigh following component (percentage by weight) according to quantity:
Deionized water: 35.0；Alkyl polyglucoside: 27.0；CS26:10.0；Citric acid, sodium citrate: 0.6；Fructus Sapindi Mukouossi extracting solution:
8.0；Low-acyl gellan gum: 0.1；Propylene glycol: 15.0；Calcium chloride solution (0.6mol/L): 3.0；Allantoin: 0.3；Essence:
0.3；Tween 20: 0.6；Preservative: 0.1.
Preparation process is as follows:
(1) with propylene glycol moistening low-acyl gellan gum, add citric acid, sodium citrate regulation PH after pulp, add deionization
Water, is heated with stirring to 85 DEG C, adds allantoin and dissolves, and under heat-retaining condition, 350r/min stirs 8 minutes；
(2) temperature 85 DEG C, calcium chloride solution is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 68 DEG C；
(3) alkyl polyglucoside and CS26, Fructus Sapindi Mukouossi extracting solution, stirring and dissolving are added；
(4) by essence, tween 20 mixing, add in above material when 58 DEG C, stir；
When (5) 58 DEG C, preservative is added, stir；
(6) keeping with the above 48 DEG C of temperature of material, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation, then at once
After standing 2 hours completion of cures.
Obtain the solid spray makeup removing gel of the present embodiment for without mobility solid product, product can be made by pump head extruding
Atomization, is evenly distributed on skin surface.Through stability test (-15 DEG C ,-4 DEG C, room temperature, 40 DEG C, 50 DEG C, natural lighting, fluorescence
Light irradiation) index such as the abnormal smells from the patient of record product, outward appearance, viscosity, pH change weekly, after one month, product is the most muddy, indices
All meet the requirement of " cosmetics health specification ".
Embodiment 6
Weigh following component (percentage by weight) according to quantity:
Deionized water: 65.0；Alkyl polyglucoside: 6.0；CS26:2.0；Citric acid, sodium citrate: 0.05；Fructus Sapindi Mukouossi extracting solution:
8.0；Low-acyl gellan gum: 1.0；Propylene glycol: 15.0；Calcium chloride solution (0.6mol/L): 1.0；Allantoin: 0.1；Essence:
0.25；Tween 20: 0.8；Preservative: 0.8.
Preparation process is as follows:
(1) with propylene glycol moistening low-acyl gellan gum, add citric acid, sodium citrate regulation PH after pulp, add deionization
Water, is heated with stirring to 85 DEG C, adds allantoin and dissolves, and under heat-retaining condition, 400r/min stirs 8 minutes；
(2) temperature 85 DEG C, calcium chloride solution is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 68 DEG C；
(3) alkyl polyglucoside and CS26, Fructus Sapindi Mukouossi extracting solution, stirring and dissolving are added；
(4) by essence, tween 20 mixing, add in above material when 58 DEG C, stir；
When (5) 58 DEG C, preservative is added, stir；
(6) keeping with the above 48 DEG C of temperature of material, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation, then at once
After standing 2 hours completion of cures.
Obtain the solid spray makeup removing gel of the present embodiment for without mobility solid product, product can be made by pump head extruding
Atomization, is evenly distributed on skin surface.Through stability test (-15 DEG C ,-4 DEG C, room temperature, 40 DEG C, 50 DEG C, natural lighting, fluorescence
Light irradiation) index such as the abnormal smells from the patient of record product, outward appearance, viscosity, pH change weekly, after one month, product is the most muddy, indices
All meet the requirement of " cosmetics health specification ".
The makeup removing performance evaluation of product
Carried out using the evaluation test of sense by 20 professional group members.Use the solid spray makeup removing gel products prepared
Remove ornaments and formal dress, and the Performance comparision newborn with certain makeup remover on market and makeup removing, product beta test one month, following 6 projects are entered
Row is evaluated: 1) makeup removing ability；2) lubricity；3) zest；4) rear greasy feeling is used；5) coating homogeneity；6) rear moisturizing is used
Property.
In following evaluation, professional group member is evaluated with four grades, and marks.Then commented by it
Point summation carries out the evaluation of five grades of following " ◎ ◎ "～"×", and " ◎ ◎ " and " ◎ " are qualified.But, even " ◎
◎ " or " ◎ ", if there being the group member of more than 1 to make 0 point of situation about evaluating, then it is defective.
5 grade evaluations based on scoring summation:
◎ ◎: 50≤scoring summation≤60 point, can thoroughly removal dressing easily, clean convenient, noresidue and without tight, glutinous greasy
And the untoward reaction such as stimulation；
◎: 40≤scoring summation≤50 point, can removal dressing easily, it is easy to cleaning, noresidue, the most non-stimulated；
Zero: 30≤scoring summation≤40 point, can clean removal dressing, it is simple to cleans, slightly remain, glutinous greasy and stimulation etc. instead
Should；
△: 20≤scoring summation≤30 point, cleaning capacity is general, has a more residual, and with after have tight, stick greasy and stimulation etc.
Untoward reaction；
×: scoring summation≤20 point, cleaning capacity is poor, have a more residual, and with rear tight, to stick greasy and stimulation etc. bad instead
Should be serious.
Evaluation criterion (is marked):
1) makeup removing ability:
3: makeup removing effect is the best；
2: remove ornaments and formal dress effective；
1: makeup removing effect is not so good；
0: remove ornaments and formal dress hardly.
2) lubricity
3: there is lubricity very much；
2: there is lubricity；
1: less there is lubricity；
0: almost without lubricity.
3) zest (occur skin itch, red pimple, twinge, the symptom such as decortication)
3: do not stimulate；
2: do not stimulate；
1: have a little stimulation；
0: stimulate very much.
4) rear greasy feeling is used
3: non-greasy completely；
2: basic non-greasy；
1: have the most greasy；
0: the most greasy.
5) coating homogeneity
3: even spread completely；
2: substantially uniform coating；
1: have the most uneven；
0: the most uneven.
6) rear moisture retention is used
For measuring the moisture retention of each product after carrying out removing ornaments and formal dress with cleansing product, cleaning with water again, carry out keratodermatitis moisture content
Test: weigh the change of water content of stratum corneum by the change of keratodermatitis capacitance before and after measurement use product, thus
Evaluating the moisture-keeping efficacy of makeup removal products, this kind of method carries out quantification to the moisture of keratodermatitis, it is possible to delicately
The change of reaction skin moisture content.
Experimental technique: bend side at candidate left and right forearm and mark 3 × 3cm2The square Experimental Area of size, makees with left arm
For the test zone of moisturizer, the corresponding symmetrical region of right arm is blank, then with Corneometer CM825 (moisture content
Test probe) detect the moisture at each test position, it is repeated 5 times and draws stationary value.Moisture content is calculated: moisture content with following formula
=(test value-blank value)/blank value × 100%.
Above evaluation result is shown in table 1 and table 2.
Table 1: evaluation result
As shown in table 1, the makeup removal products of the embodiment 1 ~ 4 that the present invention relates to is lubricity when a kind of ability of makeup removing height, cleaning
Do not stimulate after excellent, cleaning, non-greasy being further able to gives the makeup removal products of moisturizing after cleaning.Additionally, for embodiment
The cleansing product of 1 ~ 4, does not has any group member to make the evaluation of 0 point at arbitrary assessment item.
Table 2: water-retaining property test result
| Evaluate | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Certain makeup remover on market | Certain makeup removing breast on market |
| Makeup removing ability | ◎ | ◎◎ | ◎ | ◎◎ | ◎ | ◎ | ◎◎ | ◎◎ |
| Lubricity | ◎ | ◎ | ◎◎ | ◎ | ◎ | ◎ | ◎◎ | ◎ |
| Zest | ◎◎ | ◎ | ◎ | ◎◎ | ◎ | ◎◎ | ◎ | ◎ |
| Use rear greasy feeling | ◎ | ◎◎ | ◎ | ◎◎ | ◎◎ | ◎◎ | ○ | ◎◎ |
| Coating homogeneity | ◎◎ | ◎◎ | ◎◎ | ◎◎ | ◎◎ | ◎ | ○ | ○ |
Being known by table 2, good water-retaining property of the present invention, higher than commercial samples.Wherein, embodiment 3 replenishing water and preserving moisture is preferable.
Gained solid spray of the present invention makeup removing gel, novel appearance, occupation mode is novel, is difficult to reveal, and coating uniformly, is unloaded
Adornment ability is strong, and gentleness does not stimulates, and easily rinses, and unloads and washes rear non-greasy.
Existing makeup remover for contrast can be existing like product or mainly have following component (weight hundred
Proportion by subtraction):
Olive oil: 4.0, decolour macadamia nut oil: 4.0, Polyethylene Glycol: 10.0, DC 345:4.0, sorbester p37: 7.0, palm acid ethyl
Own ester: 62, soil temperature-20:9.
Existing makeup removing breast for contrast can be existing like product or mainly have following component (weight hundred
Proportion by subtraction):
Polydimethylsiloxane: 12, isomery hexadecane: 8, propylene glycol: 6, methyl hydroxybenzoate: 0.3, sodium chloride: 1.0, EDTA-2Na:
0.1, butanediol: 8.0, glycerol: 10.0, deionized water: surplus.
It is only more than several concrete preferred embodiment of the present invention, it should be understood that these embodiments are merely to illustrate the present invention
Rather than restriction the scope of the present invention, after having read the present invention, the those skilled in the art's various equivalences to the present invention
The amendment of form all falls within claims of the present invention and is limited, and protection scope of the present invention should be with the claims in the present invention
Accurate.
Claims (10)
1. a solid spray makeup removing gel, it is characterised in that be prepared from by following material component by percentage to the quality:
Filler: 35-65,
Gentle surfactant: 6-30,
Hydrophilic composes fat agent: 2-10,
PH regulator: 0.05-0.6,
Natural detergent: 2-8,
Gum deposit agent: 0.1-1.0,
Polyhydric alcohol wetting agent: 3-15,
Colloid sclerosing agent: 0.5-3,
Anti-allergic agent: 0.1-0.5,
Essence: 0.05-0.3,
Solubilizing agent: 0.2-0.8,
Preservative: 0.1-0.8.
A kind of solid spray makeup removing gel the most according to claim 1, it is characterised in that described filler is deionization
Water；Described gentle surfactant includes alkyl polyglucoside, cocoyl both sexes sodium acetate, sodium lauroyl sarcosine or amino acid surface
One in activating agent.
A kind of solid spray makeup removing gel the most according to claim 1, it is characterised in that described hydrophilic is composed fat agent and included
PEG-7 sodium cocoglyceryl ester, PEG-7 caprylic/capric triglyceride, PEG-9 Yue Guisuanzhi &PPG-26 butylol polyether-26& fourth two
Alcohol.
A kind of solid spray makeup removing gel the most according to claim 1, it is characterised in that described PH regulator includes Fructus Citri Limoniae
One in acid, sodium citrate；Described natural detergent is Fructus Sapindi Mukouossi extracting solution；Described gum deposit agent include low-acyl gellan gum and
One in HANSHENGJIAO.
A kind of solid spray makeup removing gel the most according to claim 1, it is characterised in that described polyhydric alcohol wetting agent includes
More than one in propylene glycol, glycerol, butanediol and sorbitol.
A kind of solid spray makeup removing gel the most according to claim 1, it is characterised in that described colloid sclerosing agent is chlorination
Calcium solution, calcium chloride solution is the aqueous solution of calcium chloride, and the concentration of Chlorine in Solution calcium is 0.4-0.6 mol/L.
A kind of solid spray makeup removing gel the most according to claim 1, it is characterised in that described anti-allergic agent includes allantois
More than one in element, hamamelis extract, glycyrrhizic acid dipotassium, water-soluble bisabolol and Herba portulacae extract；Described essence is
Cosmetic field commonly uses raw material, including the one in the fragrance of a flower and fruital.
A kind of solid spray makeup removing gel the most according to claim 1, it is characterised in that described solubilizing agent is cosmetics necks
Raw material is commonly used in territory, including the one in tween 20 and polyoxyethylene hydrogenated Oleum Ricini；Described preservative is that cosmetic field is commonly used
Raw material, including in imidazolidinyl urea, Methylisothiazolinone, phenoxyethanol, chlorphenesin and methyl parahydroxybenzoate
The compound of one or more.
9. prepare described in claims 1 a kind of solid spray makeup removing gel method, it is characterised in that include walking as follows
Rapid:
(1) with polyhydric alcohol wetting agent moistening gum deposit agent, add PH regulator after pulp, add filler, be heated with stirring to 85
± 2 DEG C, adding anti-allergic agent and dissolve, under heat-retaining condition, 300 ~ 400r/min stirs 5-10 minute；
(2) temperature 85 ± 2 DEG C, colloid sclerosing agent is joined in (1), stirring and dissolving 2 minutes, rear slow cooling to 70 ± 2 DEG C；
(3) gentle surfactant and hydrophilic tax fat agent, natural detergent, stirring and dissolving are added；
(4) by essence, solubilizing agent mixing, add when 58 ± 2 DEG C, stir；
When (5) 56 ± 2 DEG C, preservative is added, stir；
(6) keeping material 50 ± 2 DEG C of temperature of body, be filled into transparent PET bottle, rotation spraying pump head completes fractional pack operation, then at once
After standing completion of cure.
10. the application in preparation makeup removing, face cleaning, cleaning skin product of the solid spray makeup removing gel described in claim 1.
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|---|---|---|---|
| CN201610502445.9A CN106074256A (en) | 2016-06-30 | 2016-06-30 | A kind of solid spray makeup removing gel and preparation method and application |
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| CN111616990A (en) * | 2020-07-14 | 2020-09-04 | 广州美兮生物科技有限公司 | Solid spray, preparation method thereof and cosmetic |
| CN112274466A (en) * | 2020-10-28 | 2021-01-29 | 花安堂生物科技集团有限公司 | Smoothie spray and preparation method thereof |
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Application publication date: 20161109 |