CN106729862A - A kind of emulsifying purification of air gel and preparation method thereof - Google Patents
A kind of emulsifying purification of air gel and preparation method thereof Download PDFInfo
- Publication number
- CN106729862A CN106729862A CN201611126577.2A CN201611126577A CN106729862A CN 106729862 A CN106729862 A CN 106729862A CN 201611126577 A CN201611126577 A CN 201611126577A CN 106729862 A CN106729862 A CN 106729862A
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- Prior art keywords
- purification
- gel
- emulsifying
- air
- agent
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
Abstract
The present invention discloses a kind of emulsifying purification of air gel, and the purification of air gel includes plural gel agent, emulsifying agent and sustained release agent.Purification of air gel of the invention, can efficiently control the evaporation rate of volatility function ingredients, realize the long-acting linear release of volatility function ingredients.In addition, the invention also discloses the preparation method of the emulsifying purification of air gel, the preparation method equipment is simple, easily operation, obtained purification of air gel can effectively control the evaporation rate of deodorant, the pernicious gases such as the bad smell in air, formaldehyde, benzene in purify air are eliminated, and with good bactericidal action.
Description
Technical field
The present invention relates to a kind of air clearing product and preparation method thereof, especially it is a kind of for medium and small space with removing
Smelly, biocidal efficacies air clearing products, belong to daily-use chemical industry technical field.
Background technology
In recent years, the attention rate of Environmental Health is increasingly lifted with people with the improvement of people ' s living standards, people couple
The improvement growing interest of IAQ.In the ring of enclosed environment such as in-car, office, bedroom, parlor atmosphere draught-free
In border, the made interior trim such as paint, leather and fur products, resin, plastics, accessory all can more or less discharge formaldehyde, benzene and its
Homologue etc. is with unhappy smell and harmful gas.Air freshener, air purifying preparation become indispensable daily use chemicals
Product.
At present, the air freshener of in the market such as household volatilization liquid, automobile perfume seat, spraying with fresh air etc. is most
It act as covering smell, and the not up to purpose of purification of air by discharging flavor molecule, increased always volatilize in air on the contrary
The content of thing.
The content of the invention
A kind of properties of product stabilization, deodorant is provided it is an object of the invention to overcome above-mentioned the deficiencies in the prior art part
Performance is excellent and long-acting, it is convenient in the car, office, bedroom, the emulsifying air that uses in the environment of atmosphere draught-free such as parlor
Purification gel;Meanwhile, present invention also offers the preparation method of the emulsifying purification of air gel.
To achieve the above object, the technical scheme taken of the present invention is:A kind of emulsifying purification of air gel, the air
Purification gel includes plural gel agent, emulsifying agent and sustained release agent.The present invention is by gel powder by using plural gel agent
Compounding improves the physical and chemical performance of solid air freshening agent, and high-efficiency deodorant and perfume (or spice) are realized by adding emulsifying agent and sustained release agent
The continuous linear release of essence.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the plural gel agent is gellan gum
With at least one mixture in carragheen, polyethylene glycol, agar, gelatin, pectin, or agar and carragheen, polyethylene glycol,
At least one mixing at least one mixture in gelatin, pectin, or pectin and carragheen, polyethylene glycol, gelatin
At least one mixture in thing, or carragheen and polyethylene glycol, agar;
The emulsifying agent is at least one in stearate, Tween-80, peregal 0;
The sustained release agent is in sodium carboxymethylcellulose, hydroxypropyl cellulose, starch, dextrin, guar gum, xanthans
It is at least one.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the plural gel agent is in the sky
Weight/mass percentage composition in gas purification gel is 0.5~3%;Quality percentage of the emulsifying agent in the purification of air gel
Content is 0.5~7%;Weight/mass percentage composition of the sustained release agent in the purification of air gel is 0.01~1%.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the purification of air gel is also included
Composite enhancer, efficient deodorant, inorganic salts, water, essence and activator.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the composite enhancer increases for essence
The mixture of solvent and organic solvent;Wherein, the organic solvent is dipropylene glycol methyl ether, dipropylene glycol methyl ether acetate, gathers
At least one in ethylene glycol, MMB, solketal, DPG;
The efficient deodorant is stability chlorine dioxide, solid chlorine dioxide, potassium permanganate, carbamide peroxide, peroxide
Change at least one in calcium, Tea Polyphenols, amino acid, plant extracts, ferrate;
The inorganic salts are at least one in calcium chloride, sodium chloride, potassium chloride;
The activator is at least one in citric acid, tartaric acid, aluminium chloride, sodium dihydrogen phosphate, malic acid.
As the preferred embodiment of emulsifying purification of air gel of the present invention, each group in the purification of air gel
Point weight/mass percentage composition be:Plural gel agent 0.5~3%, emulsifying agent 0.5~7%, composite enhancer 0.01~8%, efficiently
It is deodorant 0.01~10%, sustained release agent 0.01~1%, inorganic salts 0.5~2.5%, essence 0.5-6%, activator 1~5%, remaining
It is water to measure.
Meanwhile, the present invention also provides a kind of preparation method of emulsifying purification of air gel as described above, methods described bag
Include following steps:
(1) by load weighted plural gel agent, emulsifying agent and sustained release agent, water input container, heating forms equal after boiling
Even solution;
(2) mixture of the mixture of load weighted high-efficiency deodorant and inorganic salts, composite enhancer and essence is put into
In solution obtained by step (1), after stirring, mixed solution is obtained;
(3) mixed solution obtained by step (2) is filled in container, condenses shaping, obtain final product purification of air gel precursors;
(4) activator is added in using the preceding purification of air gel precursors to obtained by step (3), is allowed to activate, obtained final product
Emulsifying purification of air gel of the present invention.
Emulsifying purification of air gel of the present invention is compounded to form plural gel agent by using various gel powders, makes product
Product can tolerate 100 DEG C of high temperature above, while less than -20 DEG C low temperature are can tolerate, while realizing the high-temperature stability of product and low
Temperature stability, and using cooperatively by emulsifying agent and sustained release agent, control releasing for essence and efficient deodorant to greatest extent
Put speed.The preparation method of emulsifying purification of air gel of the present invention is simple, low production cost, using side of the present invention
Emulsifying purification of air gel profile plasticity that method is prepared is strong, product physical and chemical performance stabilization, and deodoriging properties are excellent and long-acting, side
Just in the car, office, bedroom, use in the environment of atmosphere draught-free such as parlor.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter
Measure the component of percentage composition:Plural gel agent:Agar 2.5%, polyethylene glycol 0.5%;Emulsifying agent:Tween-80 1.5%, tristearin
Sour sodium 5.5%;Composite enhancer:Essence solubilizer 1%, dipropylene glycol methyl ether acetate 2%, polyethylene glycol 1%;Efficient smelly eliminating
Agent:Solid chlorine dioxide 3%;Sustained release agent:Sodium alginate 0.3%;Inorganic salts:Potassium chloride 0.5%;Essence 2%;Activator:Phosphorus
Acid dihydride sodium 3%;Balance of water.
Efficient deodorant in emulsifying purification of air gel of the present invention uses solid chlorine dioxide, and chlorine dioxide is with strong
Oxidisability, evaporateing into air can be with harmful substances such as oxidation of formaldehyde, benzene, and with bactericidal action.
The emulsifying purification of air gel of the present embodiment is prepared from using following methods:
(1) by load weighted plural gel agent, emulsifying agent and sustained release agent, water input container, heating forms equal after boiling
Even solution;
(2) mixture of the mixture of load weighted high-efficiency deodorant and inorganic salts, composite enhancer and essence is put into
In solution obtained by step (1), after stirring, mixed solution is obtained;
(3) mixed solution obtained by step (2) is filled in container, condenses shaping, obtain final product purification of air gel precursors;
(4) activator is added in using the preceding purification of air gel precursors to obtained by step (3), is allowed to activate, obtained final product
Emulsifying purification of air gel of the invention.
Embodiment 2
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter
Measure the component of percentage composition:Plural gel agent:Carragheen 1%, polyethylene glycol 1%;Emulsifying agent:Potassium stearate 4%;Complex intensifying
Agent:Essence solubilizer 1%, solketal 1.5%;Efficient deodorant:Plant extracts 1%;Sustained release agent:Carboxymethylcellulose calcium
Sodium 0.5%;Inorganic salts:Potassium chloride 2%;Essence 5%;Balance of water.
Efficient deodorant in emulsifying purification of air gel of the present invention uses plant extracts, also contains in plant extracts
There are substantial amounts of flavone compound, polyphenol compound, protein hydrolytic amino acid etc., to the formaldehyde in room air, toluene, benzene
There is good catharsis Deng toxic gas.
The emulsifying purification of air gel of the present embodiment is prepared from using the method such as embodiment 1.
Embodiment 3
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter
Measure the component of percentage composition:Plural gel agent:Gellan gum 0.1%, carragheen 0.2%, polyethylene glycol 0.2%;Emulsifying agent:Tell
Temperature -80 0.5%;Composite enhancer:Essence solubilizer 0.005%, dipropylene glycol methyl ether 0.005%;Efficient deodorant:Gao Meng
Sour potassium 0.005%, carbamide peroxide 0.005%;Sustained release agent:Sodium carboxymethylcellulose 0.005%, hydroxy propyl cellulose 0.005%;
Inorganic salts:Potassium chloride 1.5%, sodium chloride 1%;Essence 0.5%;Activator:Citric acid 0.5%, tartaric acid 0.5%;It is balance of
Water.
The emulsifying purification of air gel of the present embodiment is prepared from using the method such as embodiment 1.
Embodiment 4
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter
Measure the component of percentage composition:Plural gel agent:Agar 1.5%, carragheen 1%;Emulsifying agent:Peregal 0 6.5%;Complex intensifying
Agent:Essence solubilizer 4%, solketal 2%, DPG 2%;Efficient deodorant:Potassium permanganate 10%;Sustained release agent:Form sediment
Powder 0.5%, dextrin 0.5%;Inorganic salts:Calcium chloride 1.5%;Essence 6%;Activator:Malic acid 5%;Balance of water.
The emulsifying purification of air gel of the present embodiment is prepared from using the method such as embodiment 1.
The com-parison and analysis experiment of the product stability of embodiment 5 and performance
The emulsifying purification of air gel for determining various embodiments of the present invention purifies the product stability of gel with commercial air
And performance, and be compared, as a result as shown in table 1:
Each embodiment of table 1 purifies the product stability and performance analytical table of gel with commercial air
Measure project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Commercial samples 1 | Commercial samples 2 |
- 20 DEG C of low-temperature stabilities | Not water outlet | Not water outlet | Not water outlet | Not water outlet | Not water outlet | Water outlet |
60 DEG C of high-temperature stabilities | Not water outlet | Not water outlet | Not water outlet | Not water outlet | Dissolving | A small amount of water |
Lotion intensity (MPa) | 110 | 110 | 108 | 109 | 105 | 90 |
Squeeze out regimen condition | It is less | It is less | It is less | It is less | It is less | It is more |
Residual quantity (%) | 8.51 | 8.50 | 8.48 | 8.52 | 9.67 | 1.91 |
Lotion acid resistance | It is acidproof | It is acidproof | It is acidproof | It is acidproof | Meet acid dissolving | It is acidproof |
Use number of days | 40 | 40 | 40 | 40 | 35 | 20 |
From the test result in table 1, compared with commercially available prod, the emulsifying purification of air of embodiment of the present invention 1-4
The lotion combination property of gel preferably, combines the advantage of two class commercially available prod, and has use time more long, shows its product
Stable performance, deodoriging properties are excellent and long-acting, it is seen then that emulsifying purification of air gel within the scope of the present invention is respectively provided with
Good deodorizing effect and stability.
It is last to should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope is protected, although being explained in detail to the present invention with reference to preferred embodiment, one of ordinary skill in the art should
Understand, technical scheme can be modified or equivalent, without deviating from the essence of technical solution of the present invention
And scope.
Claims (10)
1. a kind of emulsifying purification of air gel, it is characterised in that the purification of air gel includes plural gel agent, emulsifying agent
And sustained release agent.
2. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the plural gel agent be gellan gum with
At least one mixture in carragheen, polyethylene glycol, agar, gelatin, pectin, or it is agar and carragheen, polyethylene glycol, bright
At least one mixture at least one mixture in glue, pectin, or pectin and carragheen, polyethylene glycol, gelatin,
Or at least one mixture in carragheen and polyethylene glycol, agar.
3. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the emulsifying agent is stearate, tells
At least one in temperature -80, peregal 0.
4. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the sustained release agent is carboxymethylcellulose calcium
At least one in sodium, hydroxypropyl cellulose, starch, dextrin, guar gum, xanthans.
5. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the plural gel agent is in the air
Weight/mass percentage composition in purification gel is 0.5~3%;Quality percentage of the emulsifying agent in the purification of air gel contains
Measure is 0.5~7%;Weight/mass percentage composition of the sustained release agent in the purification of air gel is 0.01~1%.
6. the emulsifying purification of air gel as described in claim any one of 1-5, it is characterised in that the purification of air gel
Also include composite enhancer, efficient deodorant, inorganic salts, water, essence and activator.
7. emulsifying purification of air gel as claimed in claim 6, it is characterised in that the composite enhancer is essence solubilising
Agent and the mixture of organic solvent;Wherein, the organic solvent is dipropylene glycol methyl ether, dipropylene glycol methyl ether acetate, poly- second
At least one in glycol, MMB, solketal, DPG;
The efficient deodorant be stability chlorine dioxide, solid chlorine dioxide, potassium permanganate, carbamide peroxide, calper calcium peroxide,
At least one in Tea Polyphenols, amino acid, plant extracts, ferrate;
The inorganic salts are at least one in calcium chloride, sodium chloride, potassium chloride;
The activator is at least one in citric acid, tartaric acid, aluminium chloride, sodium dihydrogen phosphate, malic acid.
8. emulsifying purification of air gel as claimed in claim 6, it is characterised in that each component in the purification of air gel
Weight/mass percentage composition be:Plural gel agent 0.5~3%, emulsifying agent 0.5~7%, composite enhancer 0.01~8%, efficiently disappear
Smelly dose 0.01~10%, sustained release agent 0.01~1%, inorganic salts 0.5~2.5%, essence 0.5-6%, activator 1~5%, surplus
It is water.
9. the emulsifying purification of air gel as described in claim 6 or 8, it is characterised in that each in the purification of air gel
The weight/mass percentage composition of component is:Plural gel agent 2~3%, emulsifying agent 4~7%, composite enhancer 2.5~8%, efficiently disappear
Smelly dose 1~10%, sustained release agent 0.3~1%, inorganic salts 1.5~2.5%, essence 2~6%, activator 1~5%, balance of water.
10. the preparation method of the emulsifying purification of air gel as described in claim any one of 6-9, it is characterised in that described
Method is comprised the following steps:
(1) by load weighted plural gel agent, emulsifying agent and sustained release agent, water input container, heating forms uniform molten after boiling
Liquid;
(2) mixture of the mixture of load weighted high-efficiency deodorant and inorganic salts, composite enhancer and essence is put into step
(1) in the solution obtained by, after stirring, mixed solution is obtained;
(3) mixed solution obtained by step (2) is filled in container, condenses shaping, obtain final product purification of air gel precursors;
(4) activator is added in using the preceding purification of air gel precursors to obtained by step (3), is allowed to activate, obtain final product this hair
The bright emulsifying purification of air gel.
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Cited By (15)
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CN107970478A (en) * | 2017-11-11 | 2018-05-01 | 丁玉琴 | A kind of solid air freshening agent |
CN108042969A (en) * | 2017-12-01 | 2018-05-18 | 杭州凯博特环保科技开发有限公司 | Long-acting type formaldehyde scavenger |
CN108465121A (en) * | 2018-06-30 | 2018-08-31 | 上海澳克林新材料科技有限公司 | A kind of plant essence extracting solution eliminating smell agent and preparation method thereof |
CN108993144A (en) * | 2018-07-11 | 2018-12-14 | 黄锦山 | A kind of efficient automobile purification agent for treating waste gas and preparation method thereof |
CN109169730A (en) * | 2018-07-11 | 2019-01-11 | 佛山实瑞先导材料研究院(普通合伙) | A kind of gel type air freshener and preparation method thereof |
CN109331208A (en) * | 2018-11-02 | 2019-02-15 | 江门市和馨香精技术有限公司 | A kind of air cleaning gel and preparation method thereof with cream texture |
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CN110252098A (en) * | 2018-03-12 | 2019-09-20 | 山东奥古生物科技有限公司 | A kind of air cleaning cream and preparation method thereof |
CN110292845A (en) * | 2018-03-23 | 2019-10-01 | 江苏兰谷环保科技股份有限公司 | A kind of enhancing micella air purifying preparation and its preparation, application method and application |
CN110585467A (en) * | 2019-09-25 | 2019-12-20 | 深圳市绿安居科技有限公司 | Air purification gel composition and preparation method thereof |
CN111672316A (en) * | 2020-05-20 | 2020-09-18 | 南京风清扬健康科技有限公司 | Composite material for removing formaldehyde for vehicle and preparation process |
CN113082270A (en) * | 2021-04-15 | 2021-07-09 | 何明磊 | Fragrance-expanding and peculiar smell-removing aromatherapy oil and preparation method thereof |
CN113396901A (en) * | 2021-06-25 | 2021-09-17 | 新乡市康大消毒剂有限公司 | Gel for slowly releasing chlorine dioxide and preparation method thereof |
TWI760121B (en) * | 2021-02-26 | 2022-04-01 | 艾爾金股份有限公司 | Slow-release chlorine dioxide gel and preparation method thereof |
CN114599405A (en) * | 2019-11-05 | 2022-06-07 | 雷克特和科尔曼(海外)家用卫生有限公司 | Composition comprising a metal oxide and a metal oxide |
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CN110292845A (en) * | 2018-03-23 | 2019-10-01 | 江苏兰谷环保科技股份有限公司 | A kind of enhancing micella air purifying preparation and its preparation, application method and application |
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CN109169730A (en) * | 2018-07-11 | 2019-01-11 | 佛山实瑞先导材料研究院(普通合伙) | A kind of gel type air freshener and preparation method thereof |
CN108993144A (en) * | 2018-07-11 | 2018-12-14 | 黄锦山 | A kind of efficient automobile purification agent for treating waste gas and preparation method thereof |
CN109331208A (en) * | 2018-11-02 | 2019-02-15 | 江门市和馨香精技术有限公司 | A kind of air cleaning gel and preparation method thereof with cream texture |
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CN110585467A (en) * | 2019-09-25 | 2019-12-20 | 深圳市绿安居科技有限公司 | Air purification gel composition and preparation method thereof |
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TWI760121B (en) * | 2021-02-26 | 2022-04-01 | 艾爾金股份有限公司 | Slow-release chlorine dioxide gel and preparation method thereof |
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