CN106729862A - A kind of emulsifying purification of air gel and preparation method thereof - Google Patents

A kind of emulsifying purification of air gel and preparation method thereof Download PDF

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Publication number
CN106729862A
CN106729862A CN201611126577.2A CN201611126577A CN106729862A CN 106729862 A CN106729862 A CN 106729862A CN 201611126577 A CN201611126577 A CN 201611126577A CN 106729862 A CN106729862 A CN 106729862A
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CN
China
Prior art keywords
purification
gel
emulsifying
air
agent
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Pending
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CN201611126577.2A
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Chinese (zh)
Inventor
梁绮明
张六平
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JIANGMEN HEXIN ESSENCE TECHNOLOGY Co Ltd
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JIANGMEN HEXIN ESSENCE TECHNOLOGY Co Ltd
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Priority to CN201611126577.2A priority Critical patent/CN106729862A/en
Publication of CN106729862A publication Critical patent/CN106729862A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/012Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material

Abstract

The present invention discloses a kind of emulsifying purification of air gel, and the purification of air gel includes plural gel agent, emulsifying agent and sustained release agent.Purification of air gel of the invention, can efficiently control the evaporation rate of volatility function ingredients, realize the long-acting linear release of volatility function ingredients.In addition, the invention also discloses the preparation method of the emulsifying purification of air gel, the preparation method equipment is simple, easily operation, obtained purification of air gel can effectively control the evaporation rate of deodorant, the pernicious gases such as the bad smell in air, formaldehyde, benzene in purify air are eliminated, and with good bactericidal action.

Description

A kind of emulsifying purification of air gel and preparation method thereof
Technical field
The present invention relates to a kind of air clearing product and preparation method thereof, especially it is a kind of for medium and small space with removing Smelly, biocidal efficacies air clearing products, belong to daily-use chemical industry technical field.
Background technology
In recent years, the attention rate of Environmental Health is increasingly lifted with people with the improvement of people ' s living standards, people couple The improvement growing interest of IAQ.In the ring of enclosed environment such as in-car, office, bedroom, parlor atmosphere draught-free In border, the made interior trim such as paint, leather and fur products, resin, plastics, accessory all can more or less discharge formaldehyde, benzene and its Homologue etc. is with unhappy smell and harmful gas.Air freshener, air purifying preparation become indispensable daily use chemicals Product.
At present, the air freshener of in the market such as household volatilization liquid, automobile perfume seat, spraying with fresh air etc. is most It act as covering smell, and the not up to purpose of purification of air by discharging flavor molecule, increased always volatilize in air on the contrary The content of thing.
The content of the invention
A kind of properties of product stabilization, deodorant is provided it is an object of the invention to overcome above-mentioned the deficiencies in the prior art part Performance is excellent and long-acting, it is convenient in the car, office, bedroom, the emulsifying air that uses in the environment of atmosphere draught-free such as parlor Purification gel;Meanwhile, present invention also offers the preparation method of the emulsifying purification of air gel.
To achieve the above object, the technical scheme taken of the present invention is:A kind of emulsifying purification of air gel, the air Purification gel includes plural gel agent, emulsifying agent and sustained release agent.The present invention is by gel powder by using plural gel agent Compounding improves the physical and chemical performance of solid air freshening agent, and high-efficiency deodorant and perfume (or spice) are realized by adding emulsifying agent and sustained release agent The continuous linear release of essence.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the plural gel agent is gellan gum With at least one mixture in carragheen, polyethylene glycol, agar, gelatin, pectin, or agar and carragheen, polyethylene glycol, At least one mixing at least one mixture in gelatin, pectin, or pectin and carragheen, polyethylene glycol, gelatin At least one mixture in thing, or carragheen and polyethylene glycol, agar;
The emulsifying agent is at least one in stearate, Tween-80, peregal 0;
The sustained release agent is in sodium carboxymethylcellulose, hydroxypropyl cellulose, starch, dextrin, guar gum, xanthans It is at least one.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the plural gel agent is in the sky Weight/mass percentage composition in gas purification gel is 0.5~3%;Quality percentage of the emulsifying agent in the purification of air gel Content is 0.5~7%;Weight/mass percentage composition of the sustained release agent in the purification of air gel is 0.01~1%.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the purification of air gel is also included Composite enhancer, efficient deodorant, inorganic salts, water, essence and activator.
Used as the preferred embodiment of emulsifying purification of air gel of the present invention, the composite enhancer increases for essence The mixture of solvent and organic solvent;Wherein, the organic solvent is dipropylene glycol methyl ether, dipropylene glycol methyl ether acetate, gathers At least one in ethylene glycol, MMB, solketal, DPG;
The efficient deodorant is stability chlorine dioxide, solid chlorine dioxide, potassium permanganate, carbamide peroxide, peroxide Change at least one in calcium, Tea Polyphenols, amino acid, plant extracts, ferrate;
The inorganic salts are at least one in calcium chloride, sodium chloride, potassium chloride;
The activator is at least one in citric acid, tartaric acid, aluminium chloride, sodium dihydrogen phosphate, malic acid.
As the preferred embodiment of emulsifying purification of air gel of the present invention, each group in the purification of air gel Point weight/mass percentage composition be:Plural gel agent 0.5~3%, emulsifying agent 0.5~7%, composite enhancer 0.01~8%, efficiently It is deodorant 0.01~10%, sustained release agent 0.01~1%, inorganic salts 0.5~2.5%, essence 0.5-6%, activator 1~5%, remaining It is water to measure.
Meanwhile, the present invention also provides a kind of preparation method of emulsifying purification of air gel as described above, methods described bag Include following steps:
(1) by load weighted plural gel agent, emulsifying agent and sustained release agent, water input container, heating forms equal after boiling Even solution;
(2) mixture of the mixture of load weighted high-efficiency deodorant and inorganic salts, composite enhancer and essence is put into In solution obtained by step (1), after stirring, mixed solution is obtained;
(3) mixed solution obtained by step (2) is filled in container, condenses shaping, obtain final product purification of air gel precursors;
(4) activator is added in using the preceding purification of air gel precursors to obtained by step (3), is allowed to activate, obtained final product Emulsifying purification of air gel of the present invention.
Emulsifying purification of air gel of the present invention is compounded to form plural gel agent by using various gel powders, makes product Product can tolerate 100 DEG C of high temperature above, while less than -20 DEG C low temperature are can tolerate, while realizing the high-temperature stability of product and low Temperature stability, and using cooperatively by emulsifying agent and sustained release agent, control releasing for essence and efficient deodorant to greatest extent Put speed.The preparation method of emulsifying purification of air gel of the present invention is simple, low production cost, using side of the present invention Emulsifying purification of air gel profile plasticity that method is prepared is strong, product physical and chemical performance stabilization, and deodoriging properties are excellent and long-acting, side Just in the car, office, bedroom, use in the environment of atmosphere draught-free such as parlor.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention It is described further.
Embodiment 1
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter Measure the component of percentage composition:Plural gel agent:Agar 2.5%, polyethylene glycol 0.5%;Emulsifying agent:Tween-80 1.5%, tristearin Sour sodium 5.5%;Composite enhancer:Essence solubilizer 1%, dipropylene glycol methyl ether acetate 2%, polyethylene glycol 1%;Efficient smelly eliminating Agent:Solid chlorine dioxide 3%;Sustained release agent:Sodium alginate 0.3%;Inorganic salts:Potassium chloride 0.5%;Essence 2%;Activator:Phosphorus Acid dihydride sodium 3%;Balance of water.
Efficient deodorant in emulsifying purification of air gel of the present invention uses solid chlorine dioxide, and chlorine dioxide is with strong Oxidisability, evaporateing into air can be with harmful substances such as oxidation of formaldehyde, benzene, and with bactericidal action.
The emulsifying purification of air gel of the present embodiment is prepared from using following methods:
(1) by load weighted plural gel agent, emulsifying agent and sustained release agent, water input container, heating forms equal after boiling Even solution;
(2) mixture of the mixture of load weighted high-efficiency deodorant and inorganic salts, composite enhancer and essence is put into In solution obtained by step (1), after stirring, mixed solution is obtained;
(3) mixed solution obtained by step (2) is filled in container, condenses shaping, obtain final product purification of air gel precursors;
(4) activator is added in using the preceding purification of air gel precursors to obtained by step (3), is allowed to activate, obtained final product Emulsifying purification of air gel of the invention.
Embodiment 2
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter Measure the component of percentage composition:Plural gel agent:Carragheen 1%, polyethylene glycol 1%;Emulsifying agent:Potassium stearate 4%;Complex intensifying Agent:Essence solubilizer 1%, solketal 1.5%;Efficient deodorant:Plant extracts 1%;Sustained release agent:Carboxymethylcellulose calcium Sodium 0.5%;Inorganic salts:Potassium chloride 2%;Essence 5%;Balance of water.
Efficient deodorant in emulsifying purification of air gel of the present invention uses plant extracts, also contains in plant extracts There are substantial amounts of flavone compound, polyphenol compound, protein hydrolytic amino acid etc., to the formaldehyde in room air, toluene, benzene There is good catharsis Deng toxic gas.
The emulsifying purification of air gel of the present embodiment is prepared from using the method such as embodiment 1.
Embodiment 3
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter Measure the component of percentage composition:Plural gel agent:Gellan gum 0.1%, carragheen 0.2%, polyethylene glycol 0.2%;Emulsifying agent:Tell Temperature -80 0.5%;Composite enhancer:Essence solubilizer 0.005%, dipropylene glycol methyl ether 0.005%;Efficient deodorant:Gao Meng Sour potassium 0.005%, carbamide peroxide 0.005%;Sustained release agent:Sodium carboxymethylcellulose 0.005%, hydroxy propyl cellulose 0.005%; Inorganic salts:Potassium chloride 1.5%, sodium chloride 1%;Essence 0.5%;Activator:Citric acid 0.5%, tartaric acid 0.5%;It is balance of Water.
The emulsifying purification of air gel of the present embodiment is prepared from using the method such as embodiment 1.
Embodiment 4
A kind of embodiment of emulsifying purification of air gel of the present invention, the purification of air gel of the present embodiment contains following matter Measure the component of percentage composition:Plural gel agent:Agar 1.5%, carragheen 1%;Emulsifying agent:Peregal 0 6.5%;Complex intensifying Agent:Essence solubilizer 4%, solketal 2%, DPG 2%;Efficient deodorant:Potassium permanganate 10%;Sustained release agent:Form sediment Powder 0.5%, dextrin 0.5%;Inorganic salts:Calcium chloride 1.5%;Essence 6%;Activator:Malic acid 5%;Balance of water.
The emulsifying purification of air gel of the present embodiment is prepared from using the method such as embodiment 1.
The com-parison and analysis experiment of the product stability of embodiment 5 and performance
The emulsifying purification of air gel for determining various embodiments of the present invention purifies the product stability of gel with commercial air And performance, and be compared, as a result as shown in table 1:
Each embodiment of table 1 purifies the product stability and performance analytical table of gel with commercial air
Measure project Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Commercial samples 1 Commercial samples 2
- 20 DEG C of low-temperature stabilities Not water outlet Not water outlet Not water outlet Not water outlet Not water outlet Water outlet
60 DEG C of high-temperature stabilities Not water outlet Not water outlet Not water outlet Not water outlet Dissolving A small amount of water
Lotion intensity (MPa) 110 110 108 109 105 90
Squeeze out regimen condition It is less It is less It is less It is less It is less It is more
Residual quantity (%) 8.51 8.50 8.48 8.52 9.67 1.91
Lotion acid resistance It is acidproof It is acidproof It is acidproof It is acidproof Meet acid dissolving It is acidproof
Use number of days 40 40 40 40 35 20
From the test result in table 1, compared with commercially available prod, the emulsifying purification of air of embodiment of the present invention 1-4 The lotion combination property of gel preferably, combines the advantage of two class commercially available prod, and has use time more long, shows its product Stable performance, deodoriging properties are excellent and long-acting, it is seen then that emulsifying purification of air gel within the scope of the present invention is respectively provided with Good deodorizing effect and stability.
It is last to should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected The limitation of scope is protected, although being explained in detail to the present invention with reference to preferred embodiment, one of ordinary skill in the art should Understand, technical scheme can be modified or equivalent, without deviating from the essence of technical solution of the present invention And scope.

Claims (10)

1. a kind of emulsifying purification of air gel, it is characterised in that the purification of air gel includes plural gel agent, emulsifying agent And sustained release agent.
2. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the plural gel agent be gellan gum with At least one mixture in carragheen, polyethylene glycol, agar, gelatin, pectin, or it is agar and carragheen, polyethylene glycol, bright At least one mixture at least one mixture in glue, pectin, or pectin and carragheen, polyethylene glycol, gelatin, Or at least one mixture in carragheen and polyethylene glycol, agar.
3. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the emulsifying agent is stearate, tells At least one in temperature -80, peregal 0.
4. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the sustained release agent is carboxymethylcellulose calcium At least one in sodium, hydroxypropyl cellulose, starch, dextrin, guar gum, xanthans.
5. emulsifying purification of air gel as claimed in claim 1, it is characterised in that the plural gel agent is in the air Weight/mass percentage composition in purification gel is 0.5~3%;Quality percentage of the emulsifying agent in the purification of air gel contains Measure is 0.5~7%;Weight/mass percentage composition of the sustained release agent in the purification of air gel is 0.01~1%.
6. the emulsifying purification of air gel as described in claim any one of 1-5, it is characterised in that the purification of air gel Also include composite enhancer, efficient deodorant, inorganic salts, water, essence and activator.
7. emulsifying purification of air gel as claimed in claim 6, it is characterised in that the composite enhancer is essence solubilising Agent and the mixture of organic solvent;Wherein, the organic solvent is dipropylene glycol methyl ether, dipropylene glycol methyl ether acetate, poly- second At least one in glycol, MMB, solketal, DPG;
The efficient deodorant be stability chlorine dioxide, solid chlorine dioxide, potassium permanganate, carbamide peroxide, calper calcium peroxide, At least one in Tea Polyphenols, amino acid, plant extracts, ferrate;
The inorganic salts are at least one in calcium chloride, sodium chloride, potassium chloride;
The activator is at least one in citric acid, tartaric acid, aluminium chloride, sodium dihydrogen phosphate, malic acid.
8. emulsifying purification of air gel as claimed in claim 6, it is characterised in that each component in the purification of air gel Weight/mass percentage composition be:Plural gel agent 0.5~3%, emulsifying agent 0.5~7%, composite enhancer 0.01~8%, efficiently disappear Smelly dose 0.01~10%, sustained release agent 0.01~1%, inorganic salts 0.5~2.5%, essence 0.5-6%, activator 1~5%, surplus It is water.
9. the emulsifying purification of air gel as described in claim 6 or 8, it is characterised in that each in the purification of air gel The weight/mass percentage composition of component is:Plural gel agent 2~3%, emulsifying agent 4~7%, composite enhancer 2.5~8%, efficiently disappear Smelly dose 1~10%, sustained release agent 0.3~1%, inorganic salts 1.5~2.5%, essence 2~6%, activator 1~5%, balance of water.
10. the preparation method of the emulsifying purification of air gel as described in claim any one of 6-9, it is characterised in that described Method is comprised the following steps:
(1) by load weighted plural gel agent, emulsifying agent and sustained release agent, water input container, heating forms uniform molten after boiling Liquid;
(2) mixture of the mixture of load weighted high-efficiency deodorant and inorganic salts, composite enhancer and essence is put into step (1) in the solution obtained by, after stirring, mixed solution is obtained;
(3) mixed solution obtained by step (2) is filled in container, condenses shaping, obtain final product purification of air gel precursors;
(4) activator is added in using the preceding purification of air gel precursors to obtained by step (3), is allowed to activate, obtain final product this hair The bright emulsifying purification of air gel.
CN201611126577.2A 2016-12-09 2016-12-09 A kind of emulsifying purification of air gel and preparation method thereof Pending CN106729862A (en)

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Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107970478A (en) * 2017-11-11 2018-05-01 丁玉琴 A kind of solid air freshening agent
CN108042969A (en) * 2017-12-01 2018-05-18 杭州凯博特环保科技开发有限公司 Long-acting type formaldehyde scavenger
CN108465121A (en) * 2018-06-30 2018-08-31 上海澳克林新材料科技有限公司 A kind of plant essence extracting solution eliminating smell agent and preparation method thereof
CN108993144A (en) * 2018-07-11 2018-12-14 黄锦山 A kind of efficient automobile purification agent for treating waste gas and preparation method thereof
CN109169730A (en) * 2018-07-11 2019-01-11 佛山实瑞先导材料研究院(普通合伙) A kind of gel type air freshener and preparation method thereof
CN109331208A (en) * 2018-11-02 2019-02-15 江门市和馨香精技术有限公司 A kind of air cleaning gel and preparation method thereof with cream texture
CN109550385A (en) * 2018-11-30 2019-04-02 广东美沃布朗科技有限公司 A kind of new function filtrate and preparation method thereof of oxygenation and releasable negative oxygen ion
CN110252098A (en) * 2018-03-12 2019-09-20 山东奥古生物科技有限公司 A kind of air cleaning cream and preparation method thereof
CN110292845A (en) * 2018-03-23 2019-10-01 江苏兰谷环保科技股份有限公司 A kind of enhancing micella air purifying preparation and its preparation, application method and application
CN110585467A (en) * 2019-09-25 2019-12-20 深圳市绿安居科技有限公司 Air purification gel composition and preparation method thereof
CN111672316A (en) * 2020-05-20 2020-09-18 南京风清扬健康科技有限公司 Composite material for removing formaldehyde for vehicle and preparation process
CN113082270A (en) * 2021-04-15 2021-07-09 何明磊 Fragrance-expanding and peculiar smell-removing aromatherapy oil and preparation method thereof
CN113396901A (en) * 2021-06-25 2021-09-17 新乡市康大消毒剂有限公司 Gel for slowly releasing chlorine dioxide and preparation method thereof
TWI760121B (en) * 2021-02-26 2022-04-01 艾爾金股份有限公司 Slow-release chlorine dioxide gel and preparation method thereof
CN114599405A (en) * 2019-11-05 2022-06-07 雷克特和科尔曼(海外)家用卫生有限公司 Composition comprising a metal oxide and a metal oxide

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107970478A (en) * 2017-11-11 2018-05-01 丁玉琴 A kind of solid air freshening agent
CN108042969A (en) * 2017-12-01 2018-05-18 杭州凯博特环保科技开发有限公司 Long-acting type formaldehyde scavenger
CN110252098A (en) * 2018-03-12 2019-09-20 山东奥古生物科技有限公司 A kind of air cleaning cream and preparation method thereof
CN110292845B (en) * 2018-03-23 2021-09-24 江苏兰谷环保科技股份有限公司 Air purifying agent for enhancing micelle property and preparation, use method and application thereof
CN110292845A (en) * 2018-03-23 2019-10-01 江苏兰谷环保科技股份有限公司 A kind of enhancing micella air purifying preparation and its preparation, application method and application
CN108465121A (en) * 2018-06-30 2018-08-31 上海澳克林新材料科技有限公司 A kind of plant essence extracting solution eliminating smell agent and preparation method thereof
CN109169730A (en) * 2018-07-11 2019-01-11 佛山实瑞先导材料研究院(普通合伙) A kind of gel type air freshener and preparation method thereof
CN108993144A (en) * 2018-07-11 2018-12-14 黄锦山 A kind of efficient automobile purification agent for treating waste gas and preparation method thereof
CN109331208A (en) * 2018-11-02 2019-02-15 江门市和馨香精技术有限公司 A kind of air cleaning gel and preparation method thereof with cream texture
CN109550385A (en) * 2018-11-30 2019-04-02 广东美沃布朗科技有限公司 A kind of new function filtrate and preparation method thereof of oxygenation and releasable negative oxygen ion
CN110585467A (en) * 2019-09-25 2019-12-20 深圳市绿安居科技有限公司 Air purification gel composition and preparation method thereof
CN114599405A (en) * 2019-11-05 2022-06-07 雷克特和科尔曼(海外)家用卫生有限公司 Composition comprising a metal oxide and a metal oxide
CN111672316A (en) * 2020-05-20 2020-09-18 南京风清扬健康科技有限公司 Composite material for removing formaldehyde for vehicle and preparation process
TWI760121B (en) * 2021-02-26 2022-04-01 艾爾金股份有限公司 Slow-release chlorine dioxide gel and preparation method thereof
CN113082270A (en) * 2021-04-15 2021-07-09 何明磊 Fragrance-expanding and peculiar smell-removing aromatherapy oil and preparation method thereof
CN113396901A (en) * 2021-06-25 2021-09-17 新乡市康大消毒剂有限公司 Gel for slowly releasing chlorine dioxide and preparation method thereof

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Application publication date: 20170531

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