CN107754584A - A kind of spray liniment for indoor harmful substance of degrading and preparation method thereof - Google Patents
A kind of spray liniment for indoor harmful substance of degrading and preparation method thereof Download PDFInfo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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- A01N59/16—Heavy metals; Compounds thereof
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- B01D—SEPARATION
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- B01D53/007—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by irradiation
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- B01D53/06—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with moving adsorbents, e.g. rotating beds
- B01D53/10—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with moving adsorbents, e.g. rotating beds with dispersed adsorbents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
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- B01D2253/102—Carbon
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- B01D2253/11—Clays
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- B01D2255/00—Catalysts
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- B01D2255/20707—Titanium
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- B01D2255/80—Type of catalytic reaction
- B01D2255/802—Photocatalytic
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Abstract
The invention discloses a kind of spray liniment for indoor harmful substance of degrading and preparation method thereof, and in particular to environmentally friendly finishing field, with weight, including following component：10~15 parts of photocatalyst, 5~10 parts of chitosan, 5~10 parts of nano transition metal powder, 10~15 parts of adsorbent, 20~30 parts of acetic acid, 5~7 parts of sodium acid carbonate, 10~20 parts of mountain locust tree ethanol extract, 5~10 parts of pink blossom China tree ethanol extract, 10~15 parts of chrysanthemum ethanol extract, 80~100 parts of deionized water.It is short, cheap and easy to use that scheme provided by the invention has the advantages that resolving harmful gas takes.
Description
Technical field
The present invention relates to environmentally friendly finishing field, specially a kind of spray liniment and its preparation for indoor harmful substance of degrading
Method.
Background technology
Indoor decoration pollution refers to that oxygen, formaldehyde, benzene, ammonia and volatility that harmful health is mixed into room air are organic
The phenomenon of the gases such as thing.It is well known that being fitted up to indoor particulate matter, a variety of environmental problems can be brought, such as：Use
Building materials containing poisonous and harmful substances can have an impact to IAQ；Various dust can be produced in fitment process, are discarded
Thing and noise pollution, these can all seriously affect the life of people.The source of indoor decoration pollution is a lot, wherein having suitable one
Partially due to caused by material used in fitment process is improper, including the volatile organic matter gas such as formaldehyde, benzene, dimethylbenzene
Body.But the pernicious gas volatilized in finishing material then can cause one as removed not in time to the health for the personnel of moving in
Fixed harm.
Therefore, after the completion of new house finishing, resident family can not register one's residence at once.User typically uses room ventilation to exclude to fill
Repair the pernicious gas brought.However, by the way of ventilation, not only time-consuming, efficiency is low, and can only discharge in indoor building materials
Pernicious gas through discharging, except useless not thorough.
In order to more thoroughly remove the pernicious gas such as formaldehyde caused by interior decoration, also occur some on the market and carry
For the service company for the treatment of air indoor.Although its improvement service provided can administer the pernicious gas of interior, but
Price is universal costly.Therefore develop it is a both saved money, again take shorter air pollution treatment product be urgently to be resolved hurrily
The problem of.
The content of the invention
It is an object of the invention to solve the problems, such as conventional process indoor harmful gas, time-consuming, it is high to expend, there is provided one
The spray liniment of kind for indoor harmful substance of degrading and preparation method thereof, scheme provided by the invention has resolving harmful gas consumption
When it is short, cheap and easy to use the advantages that.
To achieve the above object, the present invention provides following technical scheme：
A kind of spray liniment for indoor harmful substance of degrading, with weight, including following component：Photocatalyst
10~15 parts, 5~10 parts of chitosan, 5~10 parts of nano transition metal powder, 10~15 parts of adsorbent, 20~30 parts of acetic acid, carbonic acid
5~7 parts of hydrogen sodium, 10~20 parts of mountain locust tree ethanol extract, 5~10 parts of pink blossom China tree ethanol extract, chrysanthemum ethanol extract
10~15 parts, 80~100 parts of deionized water.
Wherein, the pernicious gas in photocatalyst decomposable asymmetric choice net air, nano transition metal powder can kill the bacterium in air, shell
Glycan can play a part of carrier so that photocatalyst and nano transition metal powder have the function that sustained release is sterilized.Also, photocatalyst
Sterilization can both be lifted except useless effect by being mixed with nano transition metal powder, and the light wave that can also widen photocatalyst absorbs model
Enclose, make it in visible light environment, equally with strong resolving harmful gas and sterilizing function.
Meanwhile adsorbent is further comprises in the component of spray liniment, for adsorbing the peculiar smell in air so that indoor environment is more
Add health.
Preferably, the one kind of the photocatalyst in nano titanium oxide, nano zine oxide, nano zirconium dioxide,
Or their mixture.
Preferably, the one kind of the nano transition metal powder in nano-silver powder, copper nanoparticle, or theirs are mixed
Compound.
Preferably, the one kind of the adsorbent in activated carbon, diatomite and bentonite, or their mixing
Thing.
Preferably, the system of the mountain locust tree ethanol extract, pink blossom China tree ethanol extract and chrysanthemum ethanol extract
Preparation Method comprises the following steps respectively：
(1) preparation of mountain locust tree ethanol extract
(1.1) after taking mountain Pagoda Flower to dry, grinding, mountain Pagoda Flower powder is obtained；
(1.2) it is in mass ratio 1 in the Pagoda Flower powder of mountain:4 add the ethanol solution that volume fraction is 60~80%,
Ultrasound 60~80min of extraction, filtering, takes filtrate；
(1.3) filtrate is rotated to doing, and obtains described mountain locust tree ethanol extract；
(2) preparation method of pink blossom China tree ethanol extract is identical with step (1)；
(3) preparation method of chrysanthemum ethanol extract is identical with step (1).
Preferably, with weight, including following component：7~10 parts of titanium dioxide, nano zine oxide 1~3
Part, 2~5 parts of nano zirconium dioxide, 5~10 parts of chitosan, 2~6 parts of nano-silver powder, 3~5 parts of copper nanoparticle, activated carbon 3~5
Part, 3~5 parts of diatomite, 3~5 parts of bentonite, 20~30 parts of acetic acid, 5~7 parts of sodium acid carbonate, mountain locust tree ethanol extract 10~
20 parts, 5~10 parts of pink blossom China tree ethanol extract, 10~15 parts of chrysanthemum ethanol extract, 80~100 parts of deionized water.
The present invention also provides the preparation method of above-mentioned spray liniment, and the preparation method comprises the following steps：
S01, by it is default proportioning weigh titanium dioxide, nano zine oxide, nano zirconium dioxide, chitosan, nano-silver powder and
Copper nanoparticle, it is well mixed, oil bath heating is to 100~120 DEG C and is stirred continuously, and obtains mixed-powder A；
S02, by default proportioning activated carbon, diatomite and bentonite are weighed, and after being heated to 80~90 DEG C, be cooled to room
Temperature, obtain mixed powder B；
S03, mixed-powder A is well mixed with mixed powder B, adds acetic acid, sodium acid carbonate and deionized water, filter out miscellaneous
After matter, solution for later use is taken；
S04, mountain locust tree ethanol extract, pink blossom China tree ethanol extract and the extraction of chrysanthemum ethanol are added in the solution
Thing, the spray liniment for indoor harmful substance of degrading is produced after dissolving.
More specifically, in step S01, oil bath temperature is 110 DEG C.
More specifically, in step S02, heating-up temperature is 87 DEG C.
More specifically, after step S04, in addition to step S05, the step S05 specific as follows：By spray liniment with
Ethanol is 1 in mass ratio:1 blends use.
Beneficial effects of the present invention are：
In scheme provided by the invention, the pernicious gas in photocatalyst decomposable asymmetric choice net air, nano transition metal powder can kill
The bacterium gone out in air, chitosan can play a part of carrier so that there is sustained release to sterilize for photocatalyst and nano transition metal powder
Function.Also, photocatalyst and nano transition metal powder, which mix, can both lift sterilization except useless effect, can also widen light
The light wave absorption region of catalyst, makes it in visible light environment, equally with strong resolving harmful gas and sterilizing function.
Meanwhile adsorbent is further comprises in the component of spray liniment, for adsorbing the peculiar smell in air so that indoor environment is more
Add health.
Embodiment
Embodiment 1
A kind of spray liniment for indoor harmful substance of degrading, with weight, the spray liniment includes such as the following group
Point：7 parts of titanium dioxide, 1 part of nano zine oxide, 2 parts of nano zirconium dioxide, 5 parts of chitosan, 2 parts of nano-silver powder, copper nanoparticle 3
Part, 3 parts of activated carbon, 3 parts of diatomite, 3 parts of bentonite, 20 parts of acetic acid, 5 parts of sodium acid carbonate, 10 parts of mountain locust tree ethanol extract, powder
5 parts of flower China tree ethanol extract, 10 parts of chrysanthemum ethanol extract, 100 parts of deionized water.
Embodiment 2
A kind of spray liniment for indoor harmful substance of degrading, with weight, the spray liniment includes such as the following group
Point：8 parts of titanium dioxide, 2 parts of nano zine oxide, 3 parts of nano zirconium dioxide, 7 parts of chitosan, 2 parts of nano-silver powder, copper nanoparticle 3
Part, 5 parts of activated carbon, 4 parts of diatomite, 5 parts of bentonite, 25 parts of acetic acid, 7 parts of sodium acid carbonate, 13 parts of mountain locust tree ethanol extract, powder
7 parts of flower China tree ethanol extract, 12 parts of chrysanthemum ethanol extract, 100 parts of deionized water.
Embodiment 3
A kind of spray liniment for indoor harmful substance of degrading, with weight, the spray liniment includes such as the following group
Point：8 parts of titanium dioxide, 2 parts of nano zine oxide, 3 parts of nano zirconium dioxide, 7 parts of chitosan, 4 parts of nano-silver powder, copper nanoparticle 4
Part, 4 parts of activated carbon, 4 parts of diatomite, 4 parts of bentonite, 25 parts of acetic acid, 6 parts of sodium acid carbonate, 15 parts of mountain locust tree ethanol extract, powder
7 parts of flower China tree ethanol extract, 13 parts of chrysanthemum ethanol extract, 100 parts of deionized water.
Embodiment 4
A kind of spray liniment for indoor harmful substance of degrading, with weight, the spray liniment includes such as the following group
Point：10 parts of titanium dioxide, 3 parts of nano zine oxide, 5 parts of nano zirconium dioxide, 10 parts of chitosan, 6 parts of nano-silver powder, copper nanoparticle
5 parts, 5 parts of activated carbon, 5 parts of diatomite, 5 parts of bentonite, 30 parts of acetic acid, 7 parts of sodium acid carbonate, 20 parts of mountain locust tree ethanol extract,
10 parts of pink blossom China tree ethanol extract, 15 parts of chrysanthemum ethanol extract, 100 parts of deionized water.
Comparative example 1
A kind of spray liniment for indoor harmful substance of degrading, with weight, the spray liniment includes such as the following group
Point：4 parts of copper nanoparticle, 4 parts of activated carbon, 4 parts of diatomite, 4 parts of bentonite, 25 parts of acetic acid, 6 parts of sodium acid carbonate, mountain locust tree ethanol
15 parts of extract, 7 parts of pink blossom China tree ethanol extract, 13 parts of chrysanthemum ethanol extract, 100 parts of deionized water.
Comparative example 2
A kind of spray liniment for indoor harmful substance of degrading, with weight, the spray liniment includes such as the following group
Point：7 parts of chitosan, 4 parts of nano-silver powder, 4 parts of copper nanoparticle, 4 parts of activated carbon, 4 parts of diatomite, 4 parts of bentonite, 25 parts of acetic acid,
6 parts of sodium acid carbonate, 15 parts of mountain locust tree ethanol extract, 7 parts of pink blossom China tree ethanol extract, 13 parts of chrysanthemum ethanol extract, go
100 parts of ionized water.
Comparative example 3
A kind of spray liniment for indoor harmful substance of degrading, with weight, the spray liniment includes such as the following group
Point：8 parts of titanium dioxide, 2 parts of nano zine oxide, 3 parts of nano zirconium dioxide, 7 parts of chitosan, 4 parts of activated carbon, 4 parts of diatomite are swollen
4 parts of profit soil, 25 parts of acetic acid, 6 parts of sodium acid carbonate, 15 parts of mountain locust tree ethanol extract, 7 parts of pink blossom China tree ethanol extract, chrysanthemum
13 parts of ethanol extract, 100 parts of deionized water.
Test case 1
Decoration company holds consultation with cell, chooses the 24 set houses of just having fitted up completion of the same cell with building building, random to divide
For 8 groups, numbering is A~H.Made of the component that A~D groups house is provided from embodiment 1~4 respectively at spray liniment
Reason, insecticide-applying way is spray painting；Made of the component that E~G groups house is provided from comparative example 1~3 respectively at spray liniment
Reason, H groups house spray painting with dosage distilled water as contrast, 2 times a day, each spray painting 1min.After 20 days, measure and count room
Interior pernicious gas content such as table 1 below：
The room air situation statistical form of table 1
To sum up state：From the experiment effect of A~D groups and H groups, spray liniment provided by the invention has degraded indoor harmful
The effect of gas, and the best results of C groups；Meanwhile by A~D and the results showed that titanium dioxide of E groups, it is nano oxidized
Zinc, nano zirconium dioxide, chitosan, nano-silver powder, the addition of copper nanoparticle cause possessed by spray liniment provided by the invention
Degrade indoor harmful gas it is better；From A~D groups and F~G group experimental results, titanium dioxide, nano zine oxide,
Removing when useless effect is more than both any exclusive uses is removed when nano zirconium dioxide is applied in combination with nano-silver powder, copper nanoparticle
Useless effect, there is the function of Synergistic, so that the effect of spray liniment provided by the invention degraded indoor harmful gas is more
It is good.
Claims (10)
1. a kind of spray liniment for indoor harmful substance of degrading, it is characterised in that with weight, including such as the following group
Point：10~15 parts of photocatalyst, 5~10 parts of chitosan, 5~10 parts of nano transition metal powder, 10~15 parts of adsorbent, acetic acid 20~
30 parts, 5~7 parts of sodium acid carbonate, 10~20 parts of mountain locust tree ethanol extract, 5~10 parts of pink blossom China tree ethanol extract, chrysanthemum second
10~15 parts of alcohol extracting thing, 80~100 parts of deionized water.
2. a kind of spray liniment for indoor harmful substance of degrading according to claim 1, it is characterised in that the light touches
The one kind of matchmaker in nano titanium oxide, nano zine oxide, nano zirconium dioxide, or their mixture.
A kind of 3. spray liniment for indoor harmful substance of degrading according to claim 1, it is characterised in that the nanometer
The one kind of transition metal powder in nano-silver powder, copper nanoparticle, or their mixture.
A kind of 4. spray liniment for indoor harmful substance of degrading according to claim 1, it is characterised in that the absorption
The one kind of agent in activated carbon, diatomite and bentonite, or their mixture.
A kind of 5. spray liniment for indoor harmful substance of degrading according to claim 1, it is characterised in that the mountain thorn
The preparation method of Chinese scholartree ethanol extract, pink blossom China tree ethanol extract and chrysanthemum ethanol extract comprises the following steps respectively：
(1) preparation of mountain locust tree ethanol extract
(1.1) after taking mountain Pagoda Flower to dry, grinding, mountain Pagoda Flower powder is obtained；
(1.2) it is in mass ratio 1 in the Pagoda Flower powder of mountain:4 add the ethanol solution that volume fraction is 60~80%, ultrasound
60~80min is extracted, filtering, takes filtrate；
(1.3) filtrate is rotated to doing, and obtains described mountain locust tree ethanol extract；
(2) preparation method of pink blossom China tree ethanol extract is identical with step (1)；
(3) preparation method of chrysanthemum ethanol extract is identical with step (1).
6. according to a kind of any described spray liniment for indoor harmful substance of degrading of Claims 1 to 4, it is characterised in that
With weight, including following component：7~10 parts of titanium dioxide, 1~3 part of nano zine oxide, nano zirconium dioxide 2
~5 parts, 5~10 parts of chitosan, 2~6 parts of nano-silver powder, 3~5 parts of copper nanoparticle, 3~5 parts of activated carbon, 3~5 parts of diatomite,
3~5 parts of bentonite, 20~30 parts of acetic acid, 5~7 parts of sodium acid carbonate, 10~20 parts of mountain locust tree ethanol extract, pink blossom China tree second
5~10 parts of alcohol extracting thing, 10~15 parts of chrysanthemum ethanol extract, 80~100 parts of deionized water.
7. a kind of preparation method of spray liniment as claimed in claim 6, it is characterised in that including following preparation process：
S01, by it is default proportioning weigh titanium dioxide, nano zine oxide, nano zirconium dioxide, chitosan, nano-silver powder and nanometer
Copper powder, it is well mixed, oil bath heating is to 100~120 DEG C and is stirred continuously, and obtains mixed-powder A；
S02, by default proportioning activated carbon, diatomite and bentonite are weighed, and after being heated to 80~90 DEG C, be cooled to room temperature, obtain
To mixed powder B；
S03, mixed-powder A is well mixed with mixed powder B, adds acetic acid, sodium acid carbonate and deionized water, filter out impurity
Afterwards, solution for later use is taken；
S04, mountain locust tree ethanol extract, pink blossom China tree ethanol extract and chrysanthemum ethanol extract are added in the solution,
The spray liniment for indoor harmful substance of degrading is produced after dissolving.
8. preparation method according to claim 7, it is characterised in that in step S01, oil bath temperature is 110 DEG C.
9. preparation method according to claim 7, it is characterised in that in step S02, heating-up temperature is 87 DEG C.
10. preparation method according to claim 7, it is characterised in that after step S04, in addition to step S05, institute
It is specific as follows to state step S05：It is 1 in mass ratio by spray liniment and ethanol:1 blends use.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109603532A (en) * | 2019-01-10 | 2019-04-12 | 上海滢晶环保科技有限公司 | A kind of composite spraying agent and preparation method thereof of decomposing formaldehyde benzene homologues TVOC |
| CN110124495A (en) * | 2019-05-21 | 2019-08-16 | 河南园田环保科技有限公司 | A kind of New deodouring deodorant and preparation method and application method |
| CN110433448A (en) * | 2019-08-20 | 2019-11-12 | 舍用环境科技(宁波)有限公司 | A kind of strong penetration type formaldehyde scavenger and preparation method thereof |
| CN111001285A (en) * | 2019-12-28 | 2020-04-14 | 康丽莱(山东)环境科技有限公司 | Formaldehyde decomposition deodorant |
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| CN106256377A (en) * | 2015-06-17 | 2016-12-28 | 冒玉兰 | A kind of Epipremnum aureum (Linde et Andre) (Bunting.) air freshener and preparation method thereof |
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