CN113057184A

CN113057184A - Composite plant liquid deodorant and preparation method thereof

Info

Publication number: CN113057184A
Application number: CN202110158938.6A
Authority: CN
Inventors: 叶平
Original assignee: Shanghai Juang Environmental Engineering Co ltd
Current assignee: Shanghai Juang Environmental Engineering Co ltd
Priority date: 2021-02-04
Filing date: 2021-02-04
Publication date: 2021-07-02

Abstract

The invention discloses a composite plant liquid deodorant and a preparation method thereof, wherein the deodorant comprises an extracting solution A, an extracting solution B, tea polyphenol, a yucca extract, a ginkgo leaf extract, a nano-silver solution, plant extracting elements, a surfactant and water; 12 parts of extracting solution A; 12 parts of an extracting solution B; 2 parts of clove extract; 1 part of tea polyphenol; 1 part of eucalyptus oil; 1 part of yucca extract; 1 part of ginkgo leaf extract; 1 part of nano silver solution: 1 part of plant extraction element (magnesium: 0.0047% sodium: 0.00035% zinc: 0.000065% potassium: 0.00068% iron: 0.00097% calcium: 0.0014% glycoside: 0.000865% saponin: 0.00097%); 8 parts of a surfactant; 60 parts of water. The composite plant liquid deodorant disclosed by the invention has the advantages that the antibacterial, disinfecting and deodorizing effects are greatly improved; the efficiency is improved by using classification extraction in the preparation process: the product is extracted from plant liquid, and has no side effect on human and animals; as an activator of enzyme, the plant extract can participate in enzymatic reaction, enhance the activity of plant extract and improve the purification efficiency.

Description

Composite plant liquid deodorant and preparation method thereof

Technical Field

The invention relates to a plant liquid deodorant and a preparation method thereof, in particular to a composite plant liquid deodorant and a preparation method thereof.

Background

In the field of domestic garbage treatment, China still starts to be in the beginning, and due to the imperfection of a garbage classification system and the limitation of the technical level, the garbage treatment in China still takes landfill as the main step. At present, the accumulated quantity of domestic garbage in cities in China exceeds 65 hundred million tons, the domestic garbage occupies about 35 hundred million square meters of land, among 660 cities in the country, 2/3 large and medium cities are surrounded by garbage, and 1/4 cities are forced to extend a way for solving the garbage crisis to the countryside, so that the secondary pollution of the garbage is caused, and the ecological environment of a city and countryside combined area is rapidly deteriorated. Therefore, the method effectively treats the odor pollution generated by the garbage in the garbage landfill, reduces the damage to the surrounding ecological environment, protects the health of people, and becomes an important content for the comprehensive treatment of the garbage.

The existing garbage deodorizers in the current market mainly comprise microbial deodorizers, chemical deodorizers and plant deodorizers. The microbial fermentation technology is difficult, and the product is unstable and is easily influenced by factors such as weather temperature and the like: chemical agents are harmful to human bodies and easily cause secondary pollution; most of the existing plant deodorizers are blended with essence, and the odor is diluted mainly through the fragrance emitted by the deodorizers, so that the smell of people is covered, the illusion of no odor is achieved, the plant deodorizers cannot be used for fundamentally deodorizing, and the plant deodorizers also have the antibacterial and disinfecting effects; therefore, it is necessary to develop a simple preparation method of a composite plant deodorant, which has low production cost and can radically deodorize through the reaction with odor molecules, rather than deodorize through a covering method.

Disclosure of Invention

The invention aims to overcome the defects of the prior art and provides a composite plant liquid deodorant and a preparation method thereof.

In order to solve the technical problems, the invention provides the following technical scheme:

the invention relates to a compound plant liquid deodorant, which comprises an extracting solution A, an extracting solution B, tea polyphenol, a yucca extract, a ginkgo leaf extract, a nano silver solution, plant extracting elements, a surfactant and water.

As a preferred technical scheme of the invention, the weight portions are as follows:

12 parts of an extracting solution A; 12 parts of an extracting solution B; 2 parts of clove extract; 1 part of tea polyphenol; 1 part of eucalyptus oil; 1 part of yucca extract; 1 part of ginkgo leaf extract; 1 part of nano silver solution: 1 part of plant extraction element (magnesium: 0.0047% sodium: 0.00035% zinc: 0.000065% potassium: 0.00068% iron: 0.00097% calcium: 0.0014% glycoside: 0.000865% saponin: 0.00097%); 8 parts of a surfactant; 60 parts of water.

The invention also provides a preparation method of the composite plant liquid deodorant, which is applied to the deodorant and comprises the following steps:

step S1: preparing an extracting solution A, namely weighing ginger, aloe, platycodon grandiflorum, wintergreen, laurel, mixing and crushing the ginger, the aloe, the platycodon grandiflorum, the wintergreen and the laurel, soaking the mixture in water which is 30-50 times of the volume of the mixture and is at 40-50 ℃ for 12-24 hours, filtering, repeatedly soaking and filtering filter residues for 2 times, and mixing the filtered filtrate with the primarily soaked and filtered filtrate to obtain the extracting solution A;

step S2: preparing an extracting solution B, namely weighing lemon, mint, pine needle, camphorwood, anise, grapefruit and pepper, mixing and crushing the lemon, the mint, the pine needle, the camphorwood, the anise, the grapefruit and the pepper, soaking the lemon, the peppermint, the pine needle, the camphorwood, the anise, the grapefruit and the pepper in 40-50% ethanol with the volume 30-50 times that of the mixed and crushed raw materials for 12-24h, filtering, repeatedly soaking and filtering filter residues for 2 times, mixing the filtered filtrate with the filtrate obtained after primary soaking and filtering, and recovering the ethanol in the filtrate by a distillation mode to;

step S3: taking materials, and measuring an extracting solution A, an extracting solution B, a clove extract, tea polyphenol, eucalyptus oil, a ginkgo leaf extract, a surfactant and water; step S3 is further added with nano silver solution, plant extract elements (magnesium: 0.0047% sodium: 0.00035% zinc: 0.000065% potassium: 0.00068% iron: 0.00097% calcium: 0.0014% glycoside: 0.000865% saponin: 0.00097%);

step S4: and (4) mixing, namely mixing the raw materials obtained in the step S3 together to obtain the compound plant deodorant.

Preferably, in the step S1, in the step of preparing the extract a, the mass ratio of the ginger, the aloe, the platycodon grandiflorum, the wintergreen, the ilex chinensis benth and the laurel is 1-3:1-3: 1-3: 1-3:1-4: 1-4:1-3.

Preferably, in the step S1, in the step of preparing the extracting solution a, the mass ratio of the ginger, the aloe, the platycodon grandiflorum, the wintergreen, the folium isatidis and the laurel is 1.5:1.5:1.5:2:2: 1.5.

Preferably, in the step S2, in the step of preparing the extracting solution B, the mass ratio of the lemon, the mint, the pine needle, the camphor wood, the aniseed, the grapefruit and the pepper is 1-2:1-4: 1-4:1-6: 1-6:1-6.

Preferably, in the step S2, in the step of preparing the extract B, the mass ratio of the lemon, the mint, the pine needle, the camphor wood, the aniseed, the grapefruit and the pepper is 1:2: 2:3: 3:3.

Preferably, in the step S1, in the preparation process of the extract a, the volume of water used for soaking is 50 times of that of the mixed and pulverized raw materials, the water temperature is 50 ℃, and the soaking time is 24 hours.

Preferably, in the step S2, in the preparation process of the extract B, the volume of ethanol used for soaking is 50 times of the volume of the mixed and pulverized raw materials, the concentration is 50%, and the soaking time is 24 hours.

Preferably, in the step S3, the raw materials are measured to be 12 parts by weight of the extract a; 12 parts of an extracting solution B; 2 parts of clove extract; 1 part of tea polyphenol; 1 part of eucalyptus oil; 1 part of yucca extract; 1 part of ginkgo leaf extract; 1 part of nano silver solution: 1 part of plant extraction element (magnesium: 0.0047% sodium: 0.00035% zinc: 0.000065% potassium: 0.00068% iron: 0.00097% calcium: 0.0014% glycoside: 0.000865% saponin: 0.00097%); 8 parts of a surfactant; 60 parts of water.

The invention has the following beneficial effects:

1. the obvious plants with the bacteriostatic function comprise ginger, platycodon grandiflorum, wintergreen, holly, green folium isatidis, lemon, mint, pine needle, anise, tea polyphenol and eucalyptus oil: lemon, mint, camphor wood, eucalyptus oil, ginkgo leaves, pepper and tea polyphenol have obvious bacteriostasis and deodorization effects: the nano-silver solution has obvious sterilization and disinfection functions, and the mixed use of the above solutions enables the composite plant liquid deodorant to have better antibacterial, disinfection and deodorization effects;

2. the product is prepared by soaking, filtering and distilling, and the process is simple: the efficiency is improved by using classification extraction in the preparation process: the product is extracted from plant liquid, has no side effect on human and animals, and has no secondary pollution;

3. the plant deodorant prepared by the preparation method has wider application space than a microbial deodorant, and has wide application prospect in aspects of garbage, sewage, plant and indoor deodorization;

4. the plant deodorant prepared by the preparation method has the deodorization mechanism that the plant extract capable of absorbing and decomposing odor molecules such as ammonia gas, hydrogen sulfide and the like is added to react with the odor molecules to convert the odor into odorless substances, so that the odor is fundamentally removed, and the environment is purified. For example, the camphor tree has extremely strong resistance and absorption and decomposition capacity to ammonia gas, and the concentration of the ammonia gas is obviously reduced; the ginkgo leaves can absorb and decompose hydrogen sulfide; the tea polyphenol can absorb and decompose ammonia, organic amine and the like;

5. the nano silver solution is added into the plant liquid deodorant prepared by the invention, the nano silver sterilization capability generates qualitative leap, few nano silver can generate strong sterilization effect, 650 kinds of bacteria can be killed within a few minutes, broad-spectrum sterilization is realized, no drug resistance exists, the healing of wounds, the growth of cells and the repair of damaged cells can be promoted, no toxic reaction exists, and no stimulation reaction is found on skin;

6. the plant extract elements are added into the plant liquid deodorant prepared by the invention, and magnesium and potassium are activators of a plurality of enzymes and used as activators of the enzymes to participate in enzymatic reaction, so that the activity of plant extract is enhanced, and the purification efficiency is improved: the zinc and the glycoside have the functions of antibiosis and sterilization: the saponin component can reduce the surface tension of the liquid to generate foam, so that the saponin component can be used as an emulsifier and has a bacteriostatic function;

7. the elements have extremely high chemical activity and excellent catalytic property, and have very good effects on deodorization and bacteriostasis.

Detailed Description

The following description of the preferred embodiments of the present invention is provided for the purpose of illustration and description, and is in no way intended to limit the invention.

The invention provides a composite plant liquid deodorant, which comprises an extracting solution A, an extracting solution B, tea polyphenol, a yucca extract, a ginkgo leaf extract, a nano silver solution, plant extracting elements, a surfactant and water.

The weight portions are as follows:

The invention also provides a preparation method of the composite plant liquid deodorant, which is applied to the deodorant and comprises the following steps: step S1: preparing an extracting solution A, namely weighing ginger, aloe, platycodon grandiflorum, wintergreen, laurel, mixing and crushing the ginger, the aloe, the platycodon grandiflorum, the wintergreen and the laurel, soaking the mixture in water which is 30-50 times of the volume of the mixture and is at 40-50 ℃ for 12-24 hours, filtering, repeatedly soaking and filtering filter residues for 2 times, and mixing the filtered filtrate with the primarily soaked and filtered filtrate to obtain the extracting solution A;

Example 1

Step S1, preparing an extracting solution A, mixing and crushing ginger, aloe, platycodon grandiflorum, wintergreen and laurel according to the mass ratio of 2:2:2:2:1:1:2, soaking the mixture in 40-DEG C water with 50 times of the volume of the mixture for 12 hours, filtering, repeatedly soaking and filtering filter residues for 2 times, and mixing the filtered filtrate with the primarily soaked and filtered filtrate to obtain the extracting solution A; step S2, preparing an extracting solution B, namely weighing lemon, mint, pine needle, camphorwood, anise, grapefruit and pepper in a mass ratio of 2:1: 1:2: 2:2, mixing and crushing the raw materials, soaking the raw materials for 12 hours in 40% ethanol with the volume 50 times that of the raw materials after mixing and crushing, filtering, repeatedly soaking and filtering filter residues for 2 times, mixing the filtered filtrate with the filtrate after primary soaking and filtering, and recovering ethanol in the filtrate in a distillation mode to obtain an extracting solution B; step S3, taking 12 parts by mass of raw materials of the extracting solution A; 12 parts of an extracting solution B; 2 parts of clove extract; 1 part of tea polyphenol; 1 part of eucalyptus oil; 1 part of yucca extract; 1 part of ginkgo leaf extract; 1 part of nano silver solution; 1 part of nano silver solution: 1 part of plant extraction elements (magnesium: 0.0047% sodium: 0.00035% zinc: 0.000065% potassium: 0.00068% iron: 0.00097% calcium: 0.0014% glycosides: 0.000865% saponin: 0.00097%): 8 parts of a surfactant; 60 parts of water. And step S3, mixing the raw materials obtained in the step S3 together to obtain the compound plant deodorant.

Example 2

Step S1, preparing an extracting solution A, mixing and crushing ginger, aloe, platycodon grandiflorum, wintergreen and laurel according to the mass ratio of 1:2:3:1.5:1:2:3, soaking the mixture for 18 hours in 45-DEG C water with the volume being 40 times of the original volume after mixing and crushing, filtering, repeatedly soaking and filtering filter residues for 2 times, and mixing the filtered filtrate with the primarily soaked and filtered filtrate to obtain the extracting solution A; step S2, preparing an extracting solution B, namely weighing lemon, mint, pine needle, camphorwood, anise, grapefruit and pepper in a mass ratio of 2:1: 3:2: 1:2, mixing and crushing the raw materials, soaking the raw materials for 18 hours in 45% ethanol with 40 times of volume of the mixed and crushed raw materials, filtering, repeatedly soaking and filtering filter residues for 2 times, mixing the filtered filtrate with the filtrate obtained after primary soaking and filtering, and recovering ethanol in the filtrate in a distillation mode to obtain an extracting solution B; step S3, taking 12 parts by mass of raw materials of the extracting solution A; 12 parts of an extracting solution B; 2 parts of clove extract; 1 part of tea polyphenol; 1 part of eucalyptus oil; 1 part of yucca extract; 1 part of ginkgo leaf extract; 8 parts of a surfactant; 1 part of nano silver solution; 1 part of nano silver solution: 1 part of plant extraction elements (magnesium: 0.0014% sodium: 0.00068% zinc: 0.000065% potassium: 0.00035% iron: 0.00097% calcium: 0.0047% glycosides: 0.000865% saponin: 0.00097%): 60 parts of water. And step S4, mixing the raw materials obtained in the step S3 together to obtain the compound plant deodorant.

Example 3

Step S1, preparing an extracting solution A, mixing and crushing ginger, aloe, platycodon grandiflorum, wintergreen and laurel according to the mass ratio of 3:2:1.5:4:2:2:3, soaking the mixture in 50-DEG C water with the volume being 30 times of the original volume of the mixture for 24 hours, filtering, repeatedly soaking and filtering filter residues for 2 times, and mixing the filtered filtrate with the primarily soaked and filtered filtrate to obtain the extracting solution A; step S2, preparing an extracting solution B, namely weighing lemon, mint, pine needle, camphorwood, anise, grapefruit and pepper in a mass ratio of 1:2: 4:3: 3:3, mixing and crushing the raw materials, soaking the raw materials for 24 hours in 50% ethanol with the volume 30 times that of the mixed and crushed raw materials, filtering, repeatedly soaking and filtering filter residues for 2 times, mixing the filtered filtrate with the filtrate obtained after primary soaking and filtering, and recovering ethanol in the filtrate in a distillation mode to obtain an extracting solution B; step S3, taking 12 parts by mass of raw materials of the extracting solution A; 12 parts of an extracting solution B; 2 parts of clove extract; 2 parts of tea polyphenol; 1 part of eucalyptus oil; 1 part of yucca extract; 1 part of ginkgo leaf extract; 8 parts of a surfactant; 1 part of nano silver solution; 1 part of nano silver solution: 1 part of plant extraction element (magnesium: 0.0047% sodium: 0.00035% zinc: 0.000065% potassium: 0.00068% iron: 0.00097% calcium: 0.0014% glycoside: 0.000865% saponin: 0.00097%); 60 parts of water. And step S4, mixing the raw materials obtained in the step S3 together to obtain the compound plant deodorant.

Verification process 1:

the plant deodorizers obtained by the preparation methods of example 1, example 2 and example 3 were diluted 50 and 100 times with water, sprayed on the surface of garbage by a spraying apparatus, and tested for deodorizing effects, and a set of comparative experiments were conducted using the existing plant deodorizers, and the test results are as follows:

1. diluting the deodorizer by 50 times

Group of	Hydrogen sulfide removal Rate%	Ammonia gas removal rate%
			Example 1	87.4	90.8
Example 2	89.3	93.7
			Example 3	93.5	97.1
Comparative example	80.2	85.3

2. Diluting deodorant 100 times

Group of	Hydrogen sulfide removal Rate%	Ammonia gas removal rate%
			Example 1	85.3	89.9
Example 2	85.6	90.1
			Example 3	89.6	90.7
Comparative example	72.4	76.0

Through the experiments, the composite plant deodorant has the advantage that the deodorization effect can be obviously improved compared with the existing deodorant.

And (3) verification process 2:

the plant deodorant obtained by the preparation methods of example 1, example 2 and example 3 was subjected to bacteriostatic performance test according to the test method of bacteriostatic effect in 2017 edition "disinfection specification" by using the existing plant deodorant as a set of comparative experiments, wherein the experimental strains are escherichia coli, staphylococcus aureus and candida albicans, the action time is 1min, and the test results are as follows:

group of	The antibacterial rate of escherichia coli is%	Staphylococcus aureus bacteriostasis rate%	Bacteriostasis rate of candida albicans%
				Example 1	99.97	99.98	98.28
Example 2	99.67	99.77	98.99
				Example 3	99.69	99.89	99.84
Comparative example	95.63	94.32	91.67

Through the experiments, the antibacterial effect of the composite plant deodorant disclosed by the invention can be obviously improved compared with that of the existing deodorant.

The invention has the following beneficial effects:

1. the obvious plants with the bacteriostatic function comprise ginger, platycodon grandiflorum, wintergreen, holly, green folium isatidis, lemon, mint, pine needle, anise, tea polyphenol and eucalyptus oil: lemon, mint, camphor wood, eucalyptus oil, ginkgo leaves, pepper and tea polyphenol have obvious bacteriostasis and deodorization effects: the nano silver solution has obvious sterilization and disinfection functions. The mixed use of the solutions enables the composite plant liquid deodorant to have higher antibacterial, disinfecting and deodorizing effects;

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. A compound plant liquid deodorant is characterized by comprising an extracting solution A, an extracting solution B, tea polyphenol, a yucca extract, a ginkgo leaf extract, a nano silver solution, plant extracting elements, a surfactant and water.

2. The compound plant liquid deodorant as claimed in claim 1, wherein the compound plant liquid deodorant comprises the following components in parts by weight:

3. A method for preparing a composite plant liquid deodorant, which is applied to the deodorant of any one of claims 1 to 2, characterized by comprising the steps of:

4. The method for preparing a composite plant liquid deodorant according to claim 3, wherein in the step S1, in the step of preparing the extracting solution A, the mass ratio of ginger, aloe, platycodon grandiflorum, wintergreen, ilex purpurea, and laurel is 1-3:1-3: 1-3: 1-3:1-4: 1-4:1-3.

5. The method for preparing the compound plant liquid deodorant as claimed in claim 3, wherein in the step S1, in the step of preparing the extracting solution A, the mass ratio of ginger, aloe, platycodon grandiflorum, wintergreen, ilex purpurea, and laurel is 1.5:1.5:1.5:1.5:2:2: 1.5.

6. The method for preparing the compound plant liquid deodorant according to claim 3, wherein in the step S2, in the step of preparing the extracting solution B, the mass ratio of the lemon, the mint, the pine needle, the camphor wood, the aniseed, the grapefruit and the pepper is 1-2:1-4: 1-4:1-6: 1-6:1-6.

7. The method for preparing the compound plant liquid deodorant as claimed in claim 3, wherein in the step S2, in the step of preparing the extracting solution B, the mass ratio of the lemon, the mint, the pine needle, the camphor wood, the aniseed, the grapefruit and the pepper is 1:2: 2:3: 3:3.

8. The method for preparing a composite plant liquid deodorant as claimed in claims 4-7, wherein in the step S1, the volume of water used for soaking in the preparation process of the extract A is 50 times of that of the mixed and crushed raw materials, the water temperature is 50 ℃, and the soaking time is 24 hours.

9. The method for preparing a composite plant liquid deodorant as claimed in claims 4-7, wherein in the step S2, ethanol is used for soaking in an amount 50 times the volume of the mixed pulverized material in the preparation process of the extract B, the concentration is 50%, and the soaking time is 24 h.

10. The method for preparing the compound plant liquid deodorant according to claim 1, wherein in the step S3, the raw materials are measured in parts by mass as 12 parts of an extracting solution A; 12 parts of an extracting solution B; 2 parts of clove extract; 1 part of tea polyphenol; 1 part of eucalyptus oil; 1 part of yucca extract; 1 part of ginkgo leaf extract; 1 part of nano silver solution: 1 part of plant extraction element (magnesium: 0.0047% sodium: 0.00035% zinc: 0.000065% potassium: 0.00068% iron: 0.00097% calcium: 0.0014% glycoside: 0.000865% saponin: 0.00097%); 8 parts of a surfactant; 60 parts of water.