CN105435280B - A kind of preparation method of high-efficiency plant deodorant - Google Patents
A kind of preparation method of high-efficiency plant deodorant Download PDFInfo
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- B01D—SEPARATION
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- B01D53/34—Chemical or biological purification of waste gases
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Abstract
The present invention relates to field of deodorization, more particularly to a kind of preparation method of high-efficiency plant deodorant, it includes extract solution A preparation, extract solution B preparation, feeding and blend step；It is an object of the invention to provide a kind of preparation method of high-efficiency plant deodorant, simplify the extraction process of plant deodorant, and then reduce production cost, substantially increase the content of effective active composition again simultaneously, the plant deodorant prepared can fundamentally remove stink by being reacted with foul smell molecule.
Description
Technical field
The present invention relates to field of deodorization, more particularly to a kind of preparation method of high-efficiency plant deodorant.
Background technology
China's domestic waste year output is about 1.4 hundred million tons, in addition to small part burning, compost or recycling, and 80%
Refuse landfill is transported to above carries out landfill disposal.In refuse landfill, organic domestic waste is decomposed by the microorganisms generation
A large amount of NH3、H2The foul gas such as S, great pollution, influence sanitationman and week are caused to the environment of refuse landfill and periphery
Side resident's is healthy, and the odor pollution that rubbish is produced is into a great society public hazards.So, effectively handle garbage loading embeading
The odor pollution that field rubbish is produced, reduces its broken ring to periphery ecological environment, and the protection people's is healthy, into rubbish
One important content of the rubbish comprehensive regulation.
The existing garbage deodorant of existing market mainly has chemical deodorizing agent, microbial deodorant and plant deodorant.Change
Learn deodorant cost higher, easily cause secondary pollution；Microbial deodorant is although with low cost, but is due to microorganism mixing hair
Ferment is difficult, and product is unstable, and has certain adaptability and growth cycle, so being difficult to reach deodorizing effect rapidly and efficiently；
Plant deodorant is a kind of oil extracted from natural tree, flowers and plants, juice or medicinal extract after microemulsified and water is mixed removes
Smelly dose, can be by biological degradable, nontoxic, non-secondary pollution.Based on chemical reaction and biophysics process during its mechanism of action
To eliminate stench, foul smell is transformed into odorless material, acid, alkalescence and neutral gas are functioned both on.
But existing plant deodorant is the oil or juice extracted from the plant with peat-reek mostly, and pass through
Add essence and pigment is blent and formed, stink is mainly diluted by the fragrance distributed in deodorant, so as to cover smelling for people
Feel, reach not smelly illusion, can not fundamentally deodorization；Existing product extraction process is complicated simultaneously, and production cost is high, effectively
Active component content is low, it is impossible to fundamentally remove foul smell, thus need badly a kind of production cost of research and development it is low, can by with foul smell point
Son reacts fundamentally deodorization, rather than the efficient quick plant deodorant for passing through encapsulation method deodorization simple preparation side
Method.
The content of the invention
It is an object of the invention to provide a kind of preparation method of high-efficiency plant deodorant, the extraction of plant deodorant is simplified
Technique, and then reduce production cost, while the content of effective active composition is substantially increased again, the plant deodorization prepared
Agent can fundamentally remove stink by being reacted with foul smell molecule.
In order to realize the above object the technical solution adopted by the present invention is：A kind of preparation method of high-efficiency plant deodorant,
It comprises the following steps：
1., extract solution A preparation, first weighs ginger, green onion, garlic, coriander, celery, and by their co-grindings, then with mixing
40-60 DEG C of the water immersion 22-26h of former 16-50 times of volume after crushing, then filtered, filter residue is repeated into immersion filtering 2
Secondary, the filtrate after the filtrate after filtering is filtered with Initial Soak mixes, and obtains extract solution A；
2., extract solution B preparation, first weighs capsicum, Chinese prickly ash, pepper, anise, rose, peppermint, jasmine, orange tangerine, shaddock
Son, lemon, bay, Chinese ilex, pine needle, aloe, camphor tree, and by their co-grindings, then with the raw material 16-50 after co-grinding
The 40-60% ethanol immersion 22-26h of times volume, then filtered, immersion filtering 2 times is repeated by filter residue, the filtrate after filtering with
Filtrate mixing after Initial Soak filtering, ethanol therein is reclaimed by way of distillation, extract solution B is obtained；
3., feeding, measures extract solution A, extract solution B, Flos Caryophylli extract, eucalyptus oil, yucca extract, camellia and extracts
Thing, ginkgo biloba p.e, Tea Polyphenols, surfactant and water；
4., mix, the raw material that 3. step has taken is mixed, high-efficiency plant deodorant is obtained.
It is preferred that, step is 1. in extract solution A preparation process, and ginger used, green onion, garlic, coriander, the mass ratio of celery are 1-
2：1-2：2-3：1-2：1-2.
It is preferred that, step is 1. in extract solution A preparation process, and ginger used, green onion, garlic, coriander, the mass ratio of celery are
1.5：1.5：2.5：1.5：1.5.
It is preferred that, step is 2. in extract solution B preparation process, capsicum used, Chinese prickly ash, pepper, anise, rose, peppermint,
Jasmine, orange tangerine, shaddock, lemon, bay, Chinese ilex, pine needle, aloe, the mass ratio of camphor tree are 1-3：1-3：1-3：1-3：1-3：2-
4：1-3：2-4：2-4：1-3：1-3：2-4：2-4：2-4：3-5.
It is preferred that, step is 2. in extract solution B preparation process, capsicum used, Chinese prickly ash, pepper, anise, rose, peppermint,
Jasmine, orange tangerine, shaddock, lemon, bay, Chinese ilex, pine needle, aloe, the mass ratio of camphor tree are 2：2：2：2：2：3：2：3：3：2：2：
3：3：3：4.
It is preferred that, 1. step in extract solution A preparation process, soaks the volume of the water used for the 35 of co-grinding raw material
Times, water temperature is 50 DEG C, and soak time is 24h.
It is preferred that, 2. step in extract solution B preparation process, soaks the volume of the ethanol used for co-grinding raw material body
Long-pending 35 times, concentration is 45%, and soak time is 24h.
It is preferred that, step 3. in measure the mass fraction of raw material and be：10 parts of extract solution A；10 parts of extract solution B；1 portion of cloves is carried
Take thing；1 part of eucalyptus oil；2 parts of yucca extracts；1 part of camellia flower extract；1 part of ginkgo biloba p.e；1 part of Tea Polyphenols；6 parts of tables
Face activating agent；65 parts of water.
It is preferred that, 3. step has measured mass fraction in material step, also be that 1 part of matrine and Dalmatian chrysanthemum are extracted
Thing.
Beneficial effects of the present invention are：
1st, preparation method of the invention, by the way of simple immersion, filtering and distillation, deodorization composition in plant is carried
Take out, extraction process is simple and easy to apply, greatly simplify the extraction process of existing plant deodorant.
2nd, preparation method of the invention carries out classification extraction to the plant for needing to extract, and takes full advantage of the thing of plant in itself
Rationality matter, further simplify extraction step, while also improving the efficiency of extraction.
3rd, the plant deodorant effective ingredient that preparation method of the invention is prepared all is extracted from natural plants, right
People and animals are without any side effects, without any secondary pollution, can fast deodorization, be a kind of pure natural environment protection deodorising product, and surface
Activating agent is a kind of generally acknowledged raw material of industry for food, cosmetics etc., nontoxic.
4th, the plant deodorant that preparation method of the invention is prepared has extremely strong weatherability and wide application sky
Between, will not be easily protected from environmental as microbial deodorant, whether in humid areas such as south, or it is dry in northwest etc.
Nonirrigated farmland area, its deodouring effect is substantially unaffected, and still has height in 50 DEG C of high temperature above or less than -10 DEG C cold environments
The deodorizing capability of effect；Plant deodorant application space is wider than microbial deodorant, can be used not only for rubbish, sewage, animal excreta
Just deodorization, moreover it can be used to public lavatory, indoor deodorization, has broad application prospects at the daily aspect of household.
5th, the plant deodorant that preparation method of the invention is prepared has the light fragrance of a flower and fruity, after sprinkling
One pure and fresh pleasant fragrance of thick air, so as to weaken the stink of foul smell, its aroma source changes in natural plant extracts
Existing market product is become and has mainly covered the present situation of foul smell by adding compound essence generation strong scent, be a kind of native annulus
Protect product.
6th, in the plant deodorant that preparation method of the invention is prepared containing cloves, aloe, yucca, camphor tree, garlic,
Camellia, ginkgo leaf, Tea Polyphenols, eucalyptus oil etc. can absorb decomposition sulfur dioxide, ammonia, hydrogen sulfide, benzene, formaldehyde, organic amine etc.
The plant extracts of foul smell molecule, reacts with foul smell molecule, is transformed into odorless material, can fundamentally go deodorization
Gas, environment purification, rather than cover stink by simple come deodorization changes that existing market product odor removal efficient is low to be showed
Shape, breaches industry technology bottleneck.
7th, it is also added into having in preparation method of the invention and suppresses harmful micro- life such as staphylococcus aureus, Escherichia coli
The matrine of thing and killing ability and the pyrethrum extract with fly eradication repelling effect, the plant deodorization prepared in guarantee
Have sterilization fly eradication ability while agent efficient deodorizing effect concurrently.
The deodorization mechanism for the plant deodorant that preparation method of the present invention is prepared is：On the one hand, have by addition and go
Eliminate the unusual smell molecule seasoning plant extracts and with purify air, produce fragrance fruit or flowers and plants plant extracts, pass through
Neutralize, adsorb stink, occur physical reactions with foul smell molecule, reach the purpose of deodorization.On the other hand, it can be absorbed and divided by addition
The plant extracts of the foul smell molecules such as sulfur dioxide, ammonia, hydrogen sulfide, benzene, formaldehyde, organic amine is solved, it is sent out with foul smell molecule
Raw reaction, odorless material is changed into by foul smell, so that foul smell is fundamentally removed, environment purification.Such as：Aloe can absorb decomposition
Formaldehyde；Cloves, garlic, camphor tree, yucca extract have extremely strong resistance and absorption capacity of decomposition to sulfur dioxide and ammonia, show
Write the concentration of reduction ammonia；Camellia can absorb Decomposition of benzene, cresols；Ginkgo leaf can absorb decomposing hydrogen sulfide；Tea Polyphenols energy
Enough absorb decomposes ammonia, organic amine etc..In addition, can have suppression staphylococcus aureus, Escherichia coli etc. harmful micro- by adding
The matrine of biological and killing ability and the pyrethrum extract with fly eradication repelling effect, are ensureing that plant deodorant is efficient
Have sterilization fly eradication ability while deodorizing effect concurrently.By independent research, industry technology bottleneck is breached, production has effectively been ensured
The quality of product, improves the deodorization effect of killing flies of product.
Embodiment
In order to facilitate the understanding of the purposes, features and advantages of the present invention, specific reality below to the present invention
The mode of applying elaborates.Many details are elaborated in the following description to fully understand the present invention.But this
Invention can be implemented with being much different from other modes described here, and those skilled in the art can be without prejudice to the present invention
Similar improvement is done in the case of intension, therefore the present invention is not limited to the specific embodiments disclosed below.
The following is specific embodiment
Embodiment 1
A kind of preparation method of high-efficiency plant deodorant, it comprises the following steps：
1., extract solution A preparation, first according to 1：2：2：2：1 mass ratio weighs ginger, green onion, garlic, coriander, celery, and by it
Co-grinding, then 22h is soaked with 60 DEG C of water of 16 times of volumes of raw material after co-grinding, then filtered, by filter residue
Immersion filtering 2 times is repeated, the filtrate after the filtrate after filtering is filtered with Initial Soak mixes, and obtains extract solution A；
2., extract solution B preparation, first according to 1：3：1：3：1：4：1：4：2：3：1：4：2：4：3 mass ratio weigh capsicum,
Chinese prickly ash, pepper, anise, rose, peppermint, jasmine, orange tangerine, shaddock, lemon, bay, Chinese ilex, pine needle, aloe, camphor tree, and will
Their co-grindings, then soak 26h with 40% ethanol of 50 times of volumes of raw material after co-grinding, then are filtered, by filter residue
Immersion filtering 2 times is repeated, the filtrate after the filtrate after filtering is filtered with Initial Soak mixes, and is reclaimed wherein by way of distillation
Ethanol, obtain extract solution B；
3., feeding, following raw materials are measured according to following mass fractions：10 parts of extract solution A；10 parts of extract solution B；1 portion of cloves
Extract；1 part of eucalyptus oil；2 parts of yucca extracts；1 part of camellia flower extract；1 part of ginkgo biloba p.e；1 part of Tea Polyphenols；6 parts
Surfactant；65 parts of water；1 part of matrine；1 part of pyrethrum extract；
4., mix, the raw material that 3. step has taken is mixed, high-efficiency plant deodorant is obtained.
Embodiment 2
A kind of preparation method of high-efficiency plant deodorant, it comprises the following steps：
1., extract solution A preparation, first according to 2：1：3：1：2 mass ratio weighs ginger, green onion, garlic, coriander, celery, and by it
Co-grinding, then 26h is soaked with 40 DEG C of water of 50 times of volumes of raw material after co-grinding, then filtered, by filter residue
Immersion filtering 2 times is repeated, the filtrate after the filtrate after filtering is filtered with Initial Soak mixes, and obtains extract solution A；
2., extract solution B preparation, first according to 3：1：3：1：3：2：3：2：3：1：3：2：4：2：5 mass ratio weigh capsicum,
Chinese prickly ash, pepper, anise, rose, peppermint, jasmine, orange tangerine, shaddock, lemon, bay, Chinese ilex, pine needle, aloe, camphor tree, and will
Their co-grindings, then soak 22h with 60% ethanol of 16 times of volumes of raw material after co-grinding, then are filtered, by filter residue
Immersion filtering 2 times is repeated, the filtrate after the filtrate after filtering is filtered with Initial Soak mixes, and is reclaimed wherein by way of distillation
Ethanol, obtain extract solution B；
3., feeding, following raw materials are measured according to following mass fractions：10 parts of extract solution A；10 parts of extract solution B；1 portion of cloves
Extract；1 part of eucalyptus oil；2 parts of yucca extracts；1 part of camellia flower extract；1 part of ginkgo biloba p.e；1 part of Tea Polyphenols；6 parts
Surfactant；65 parts of water；1 part of matrine；1 part of pyrethrum extract；
4., mix, the raw material that 3. step has taken is mixed, high-efficiency plant deodorant is obtained.
Embodiment 3
A kind of preparation method of high-efficiency plant deodorant, it comprises the following steps：
1., extract solution A preparation, first according to 1.5：1.5：2.5：1.5：1.5 mass ratio weigh ginger, green onion, garlic, coriander,
Celery, and by their co-grindings, 24h then is soaked with 50 DEG C of water of 35 times of volumes of raw material after co-grinding, then carry out
Filtering, immersion filtering 2 times is repeated by filter residue, and the filtrate after the filtrate after filtering is filtered with Initial Soak mixes, and obtains extract solution
A；
2., extract solution B preparation, first according to 2：2：2：2：2：3：2：3：3：2：2：3：3：3：4 mass ratio weigh capsicum,
Chinese prickly ash, pepper, anise, rose, peppermint, jasmine, orange tangerine, shaddock, lemon, bay, Chinese ilex, pine needle, aloe, camphor tree, and will
Their co-grindings, then soak 24h with 45% ethanol of 35 times of volumes of raw material after co-grinding, then are filtered, by filter residue
Immersion filtering 2 times is repeated, the filtrate after the filtrate after filtering is filtered with Initial Soak mixes, and is reclaimed wherein by way of distillation
Ethanol, obtain extract solution B；
3., feeding, following raw materials are measured according to following mass fractions：10 parts of extract solution A；10 parts of extract solution B；1 portion of cloves
Extract；1 part of eucalyptus oil；2 parts of yucca extracts；1 part of camellia flower extract；1 part of ginkgo biloba p.e；1 part of Tea Polyphenols；6 parts
Surfactant；65 parts of water；1 part of matrine；1 part of pyrethrum extract；
4., mix, the raw material that 3. step has taken is mixed, high-efficiency plant deodorant is obtained.
Checking：
The plant deodorant that the preparation method of embodiment 1, embodiment 2 and embodiment 3 is obtained is diluted with water 40-200 times,
Rubbish surface is sprayed on spraying apparatus, deodorizing effect is tested, while being one group of contrast experiment with existing plant deodorant, surveyed
Test result such as following table：
| Experimental group | Ammonia removal rate | Hydrogen sulfide removal rate | Odor concentration reduced rate |
| Embodiment 1 | 93% | 85% | 84% |
| Embodiment 2 | 94% | 87% | 86% |
| Embodiment 3 | 96% | 88% | 85% |
| Contrast groups | 82% | 62% | 60% |
Experiment can show that high-efficiency plant deodorant of the invention is relative to existing deodorant, its deodorization more than
Effect can be significantly improved.
The plant deodorant that the preparation method of the embodiment of the present invention 1, embodiment 2 and embodiment 3 is obtained simultaneously is used for public affairs
Toilet deodorization, can play sterilization effect of killing flies well altogether, for existing plant deodorant, be individual significant
It is progressive.
It should be noted that herein, term " comprising ", "comprising" or its any other variant are intended to non-row
His property is included, so that process, method, article or equipment including a series of key elements not only include those key elements, and
And also including other key elements being not expressly set out, or also include for this process, method, article or equipment institute inherently
Key element.
Specific case used herein is set forth to the principle and embodiment of the present invention, the explanation of above example
It is only intended to the method and its core concept for helping to understand the present invention.Described above is only the preferred embodiment of the present invention, should
When pointing out due to the finiteness of literal expression, and objectively there is unlimited concrete structure, for the common skill of the art
For art personnel, under the premise without departing from the principles of the invention, can also make it is some improve, retouching or change, can also be by
Above-mentioned technical characteristic is combined by rights；These improve retouching, change or combined, or the not improved structure by invention
Think and technical scheme directly applies to other occasions, be regarded as protection scope of the present invention.
Claims (9)
1. a kind of preparation method of high-efficiency plant deodorant, it is characterised in that it comprises the following steps：
1., extract solution A preparation, first weighs ginger, green onion, garlic, coriander, celery, and by their co-grindings, then use co-grinding
40-60 DEG C of the water immersion 22-26h of 16-50 times of volume of raw material afterwards, then filtered, filter residue is repeated into immersion filtering 2 times,
Filtrate after filtrate after filtering is filtered with Initial Soak mixes, and obtains extract solution A；
2., extract solution B preparation, first weighs capsicum, Chinese prickly ash, pepper, anise, rose, peppermint, jasmine, orange tangerine, shaddock, lemon
Lemon, bay, Chinese ilex, pine needle, aloe, camphor tree, and by their co-grindings, then with 16-50 times of body of raw material after co-grinding
Long-pending 40-60% ethanol immersion 22-26h, then filtered, immersion filtering 2 times is repeated by filter residue, the filtrate after filtering with it is first
Filtrate mixing after immersion filtering, ethanol therein is reclaimed by way of distillation, extract solution B is obtained；
3., feeding, measures extract solution A, extract solution B, Flos Caryophylli extract, eucalyptus oil, yucca extract, camellia flower extract, silver
Apricot leaf extract, Tea Polyphenols, surfactant and water；
4., mix, the raw material that 3. step has taken is mixed, high-efficiency plant deodorant is obtained.
2. a kind of preparation method of high-efficiency plant deodorant according to claim 1, it is characterised in that step 1. extract solution
In A preparation process, ginger used, green onion, garlic, coriander, the mass ratio of celery are 1-2：1-2：2-3：1-2：1-2.
3. a kind of preparation method of high-efficiency plant deodorant according to claim 2, it is characterised in that step 1. extract solution
In A preparation process, ginger used, green onion, garlic, coriander, the mass ratio of celery are 1.5：1.5：2.5：1.5：1.5.
4. a kind of preparation method of high-efficiency plant deodorant according to claim 1, it is characterised in that step 2. extract solution
In B preparation process, capsicum used, Chinese prickly ash, pepper, anise, rose, peppermint, jasmine, orange tangerine, shaddock, lemon, bay, winter
Green grass or young crops, pine needle, aloe, the mass ratio of camphor tree are 1-3：1-3：1-3：1-3：1-3：2-4：1-3：2-4：2-4：1-3：1-3：2-4：2-
4：2-4：3-5.
5. a kind of preparation method of high-efficiency plant deodorant according to claim 4, it is characterised in that step 2. extract solution
In B preparation process, capsicum used, Chinese prickly ash, pepper, anise, rose, peppermint, jasmine, orange tangerine, shaddock, lemon, bay, winter
Green grass or young crops, pine needle, aloe, the mass ratio of camphor tree are 2：2：2：2：2：3：2：3：3：2：2：3：3：3：4.
6. a kind of preparation method of high-efficiency plant deodorant according to claim 1, it is characterised in that step 1. extract solution
In A preparation process, the volume of the water used is soaked for 35 times of co-grinding raw material, water temperature is 50 DEG C, and soak time is
24h。
7. a kind of preparation method of high-efficiency plant deodorant according to claim 1, it is characterised in that step 2. extract solution
In B preparation process, the volume of the ethanol used is soaked for 35 times of co-grinding raw material volume, concentration is 45%, soak time
For 24h.
8. a kind of preparation method of high-efficiency plant deodorant according to claim 1, it is characterised in that step 3. in measure
The mass fraction of raw material is：10 parts of extract solution A；10 parts of extract solution B；1 part of Flos Caryophylli extract；1 part of eucalyptus oil；2 portions of yuccas are extracted
Thing；1 part of camellia flower extract；1 part of ginkgo biloba p.e；1 part of Tea Polyphenols；6 parts of surfactants；65 parts of water.
9. the preparation method of a kind of high-efficiency plant deodorant according to claim 8, it is characterised in that 3. feeding is walked step
In rapid, matrine and pyrethrum extract that mass fraction is 1 part have also been measured.
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| CN114377537A (en) * | 2022-01-14 | 2022-04-22 | 浙江工商大学 | Natural plant deodorant and preparation method and application thereof |
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