CN109054881A - A kind of distilled pyroligneous acid for deodorant and preparation method thereof and deodorant and its application method with the distilled pyroligneous acid - Google Patents

A kind of distilled pyroligneous acid for deodorant and preparation method thereof and deodorant and its application method with the distilled pyroligneous acid Download PDF

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Publication number
CN109054881A
CN109054881A CN201810893756.1A CN201810893756A CN109054881A CN 109054881 A CN109054881 A CN 109054881A CN 201810893756 A CN201810893756 A CN 201810893756A CN 109054881 A CN109054881 A CN 109054881A
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China
Prior art keywords
deodorant
pyroligneous acid
distilled
distilled pyroligneous
preparation
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CN201810893756.1A
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Chinese (zh)
Inventor
黄志新
石兆维
陈超
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Tangshan New Yarno Biotechnology Co Ltd
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Tangshan New Yarno Biotechnology Co Ltd
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Priority to CN201810893756.1A priority Critical patent/CN109054881A/en
Publication of CN109054881A publication Critical patent/CN109054881A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10CWORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
    • C10C5/00Production of pyroligneous acid distillation of wood, dry distillation of organic waste
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N61/00Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q15/00Anti-perspirants or body deodorants
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10CWORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
    • C10C1/00Working-up tar
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10CWORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
    • C10C1/00Working-up tar
    • C10C1/04Working-up tar by distillation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Animal Behavior & Ethology (AREA)
  • Public Health (AREA)
  • Wood Science & Technology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Biotechnology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The present invention relates to a kind of distilled pyroligneous acid for deodorant and preparation method thereof and deodorant and its application method with the distilled pyroligneous acid, with horse-tail, leaflet eucalyptus and lichee wood etc. for primary raw material, according to a certain ratio, after destructive distillation, standing for a long time, the purification link such as take log vinegar liquid, then distilled, filtered obtain distilled pyroligneous acid.Using single flash wood vinegar as primary raw material, a certain proportion of surfactant and alcohol are equipped with up to deodorant.Deodorant of the invention has the characteristics that nontoxic, efficient sterilizing, obvious to containing area air purification effect.

Description

A kind of distilled pyroligneous acid for deodorant and preparation method thereof and there is the distillation The deodorant and its application method of wood vinegar
Technical field
The present invention relates to the technical fields of the preparation of plant waste branch dry distillation liquid, purification and application, and in particular to Yi Zhongyong In distilled pyroligneous acid of deodorant and preparation method thereof and deodorant and its application method with the distilled pyroligneous acid.
Background technique
Important one is exactly that Solid Waste Treatment and Resources utilizes in environmental protection, the resource utilization of pollutant It is the trend of the following environmental protection industry development.Branch of the raw materials used in the present invention horse-tail, leaflet eucalyptus, lichee wood etc. etc. is China's heat The common crop in band area, locality generally collect these as fuel, directly light, and generate bulk gas pollutant, are The important sources of local woods environmental pollution concerning farmers.These branch leaves without collection etc. then self rot, release various VOCs is toxic, pernicious gas.A new generation's charing cogeneration facility, can directly using grow in soil stalk, trees, bamboo, The agriculturals such as fruit tree, shell, countryside wastes, in environmentally friendly manner, efficiently, environmental protection, continuously to these plant wastes into Row charing, becomes carbonization product, eventually passes back to soil.It and is raw material through new one using the branch of horse-tail, leaflet eucalyptus, lichee wood etc. During generation charing cogeneration facility processing carbonization product, the plant destructive distillation liquid product collected is sent out through many experiments Now there is stronger taste removal deodorizing sterilizing effect.
Wood vinegar is with the acidic liquid of acetic acid pH value 3 or so as main component, extremely with the ingredient and color of vinegar It is similar.Manufacturing process is briefly exactly obtained from the flue gas natural cooling liquefaction emerged during producing charcoal.Wood Vinegar liquid typically contains the substances such as organic acid, phenols, ketone, contains K, Ca, Mg, Zn, Ge simultaneously, and the minerals such as Mn, Fe have Also contain Aneurine and B2.But the wood vinegar ingredient and effect that different timber obtain are very different.Wood vinegar is generally in height Have the function of stronger sterilization, antibacterial under concentration, there is antibacterial effect at low concentrations.Can be used for purifying household kitchen, The peculiar smell of lavatory, the stink of the generations such as Pet fur, excreta, residence cultivate factory, livestock and poultry fish market, rubbish factory, sewage treatment Factory and industrial peculiar smell place etc. are deodorized only by react with toxic and harmful gas such as nitrogen, sulphur compound and VOCs in stink Change effect.
Summary of the invention
The invention is intended to provide a kind of distilled pyroligneous acid for deodorant and preparation method thereof and have distillation wood The deodorant and its application method of vinegar liquid, to solve the deficiencies in the prior art, the technical problem to be solved in the present invention is logical Following technical scheme is crossed to realize.
A kind of preparation method of the distilled pyroligneous acid for deodorant, comprising the following steps:
S1, horse-tail, leaflet eucalyptus, lichee wood are mixed to progress destructive distillation in proportion, stood, obtaining log vinegar liquid;
S2, the part for removing log vinegar liquid surface layer and bottom 10%;
S3, the remainder of log vinegar liquid is distilled, is filtered, obtaining distilled pyroligneous acid.
Preferably, the ratio in the S1 is 8:1:1.
Preferably, the time stood in the S1 is 6 months.
The present invention also provides a kind of distilled pyroligneous acid for deodorant, the distilled pyroligneous acid is used such as preceding any institute The preparation method stated is made.
Preferably, the distilled pyroligneous acid 1.5-2.5% containing organic acid, phenols 3.5-4.5%, ironic citrate 1-1.5%.
The present invention also provides a kind of deodorant, ingredient and ratio be it is preceding it is any as described in distilled pyroligneous acid 50%, surface Activating agent 2.5%, 95% alcohol 2.5%.
The present invention also provides a kind of application methods of deodorant, by sprinkling after 10-100 times of foregoing deodorization dilution agent It uses.
Deodorant of the invention has the characteristics that nontoxic, efficient sterilizing, obvious to containing area air purification effect. For the present invention using plant dry distillation liquid as main component, application method is easy, and dilution is splashed by spraying, to confined space type stench field Institute, such as various livestock and poultry colony houses, the organic, toxic of sewage treatment station, pernicious gas have good deodorization and sterilization effect.This hair Bright deodorant also has to harmful microbe antibacterial action, acts on the expeling of mosquito etc..Sprinkling can once maintain air Pure and fresh 3-5 days.Summer is alternatively arranged as the smells such as bad smell of perspiration with perfume elimination, and makes one to feel nice and cool.
Specific embodiment
The design feature that the present invention is further explained combined with specific embodiments below.
A kind of embodiment 1: preparation method of the distilled pyroligneous acid for deodorant, comprising the following steps:
S1, horse-tail, leaflet eucalyptus, lichee wood are mixed to progress destructive distillation in proportion, stood, obtaining log vinegar liquid;
S2, the part for removing log vinegar liquid surface layer and bottom 10%;
S3, the remainder of log vinegar liquid is distilled, is filtered, obtaining distilled pyroligneous acid.
Embodiment 2: on the basis of embodiment 1, the ratio in the S1 is 8:1:1, and the time stood in the S1 is 6 A month.
Embodiment 3: it is made and is steamed using the preparation method of the distilled pyroligneous acid for deodorant as described in embodiment 1 or 2 Evaporate wood vinegar.
Embodiment 4: on the basis of embodiment 3, the distilled pyroligneous acid 1.5-2.5% containing organic acid, phenols 3.5- 4.5%, ironic citrate 1-1.5%.
Embodiment 5: a kind of deodorant, ingredient and ratio are the distilled pyroligneous acid 50% as described in embodiment 3 or 4, surface Activating agent 2.5%, 95% alcohol 2.5%.
Embodiment 6: a kind of application method of deodorant, by spray after 10-100 times of deodorization dilution agent as described in Example 5 Spill use.
It is raw material through a new generation's charing cogeneration facility processing charing using the branch of horse-tail, leaflet eucalyptus, lichee wood etc. During product, the plant destructive distillation liquid product collected is found to have stronger taste removal deodorizing sterilizing through many experiments and imitates Fruit.
Example 1, certain exhibit halls taste removal.The exhibit halls ground is false lawn, and about 160 square meter of area is spraying with 20 times of liquid, Each about 1 liter of dosage, spray time about 5 minutes.The false peculiar plastics alkene in lawn burns the foul gas taste generated and disappears after having sprayed, Lasts 5-7 days.
Example 2, certain suburb pig farm.The pig farm is located at certain suburb village west, and live pig livestock on hand 500, pig house distributes stench. Spraying, about 1 liter of every house dosage with 20 times of liquid, stench disappearance, continuous administration January can't smell the foul smell that leaks in pig house substantially.
Embodiment described above only expresses one embodiment of the present invention, and but it cannot be understood as to this The limitation of invention scope.It should be pointed out that for those of ordinary skill in the art, in the premise for not departing from present inventive concept Under, various modifications and improvements can be made.These are all within the scope of protection of the present invention.

Claims (7)

1. a kind of preparation method of the distilled pyroligneous acid for deodorant, it is characterised in that: the following steps are included:
S1, horse-tail, leaflet eucalyptus, lichee wood are mixed to progress destructive distillation in proportion, stood, obtaining log vinegar liquid;
S2, the part for removing log vinegar liquid surface layer and bottom 10%;
S3, the remainder of log vinegar liquid is distilled, is filtered, obtaining distilled pyroligneous acid.
2. preparation method according to claim 1, it is characterised in that: the ratio in the S1 is 8:1:1.
3. preparation method according to claim 1, it is characterised in that: the time stood in the S1 is 6 months.
4. a kind of distilled pyroligneous acid for deodorant, it is characterised in that: the distilled pyroligneous acid uses such as claim 1- 3 any preparation methods are made.
5. distilled pyroligneous acid according to claim 4, it is characterised in that: the distilled pyroligneous acid 1.5- containing organic acid 2.5%, phenols 3.5-4.5%, ironic citrate 1-1.5%.
6. a kind of deodorant, it is characterised in that: its ingredient and ratio are distilled pyroligneous acid 50% as described in claim 4 or 5, Surfactant 2.5%, 95% alcohol 2.5%.
7. a kind of application method of deodorant, it is characterised in that: after 10-100 times of deodorization dilution agent as claimed in claim 6 Sprinkling uses.
CN201810893756.1A 2018-08-08 2018-08-08 A kind of distilled pyroligneous acid for deodorant and preparation method thereof and deodorant and its application method with the distilled pyroligneous acid Pending CN109054881A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110339693A (en) * 2019-07-16 2019-10-18 河南碳索新材料科技有限公司 A kind of plant type air deodorization agent of farm and preparation method thereof
CN110354183A (en) * 2019-07-26 2019-10-22 唐山市新雅诺生物科技有限公司 Nantural non-toxic mosquito repellent product and preparation method thereof
CN110358566A (en) * 2019-08-23 2019-10-22 山东省分析测试中心 A kind of preparation method and application of peony seeds shell wood vinegar and its carrier
CN111742936A (en) * 2020-07-14 2020-10-09 唐山进海新材料有限公司 Antibacterial liquid containing wood vinegar composition and preparation method thereof
CN112155018A (en) * 2020-10-20 2021-01-01 唐山市新雅诺生物科技有限公司 Plant source health disinfectant and preparation method thereof
CN112957899A (en) * 2021-03-08 2021-06-15 北京环卫集团环卫服务有限公司 Deodorant and preparation method and application thereof

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Publication number Priority date Publication date Assignee Title
FR2163366A1 (en) * 1971-12-16 1973-07-27 Achard Max Deodorant compsn - based on glycerin and chlorohydrol
KR20010087805A (en) * 2001-06-07 2001-09-26 정남수 Refining apparatus and method for sap
CN105586064A (en) * 2016-01-13 2016-05-18 河北天善生物技术有限公司 Method for preparing refined wood vinegar from crop straw
CN106511188A (en) * 2017-01-06 2017-03-22 陕西中医药大学 Hand-washing mousse containing wild jujube core and shell wood vinegar and preparation method and application of hand-washing mousse
CN108187475A (en) * 2018-01-15 2018-06-22 长沙海之源环保科技有限公司 A kind of deodorant compositions and its application

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2163366A1 (en) * 1971-12-16 1973-07-27 Achard Max Deodorant compsn - based on glycerin and chlorohydrol
KR20010087805A (en) * 2001-06-07 2001-09-26 정남수 Refining apparatus and method for sap
CN105586064A (en) * 2016-01-13 2016-05-18 河北天善生物技术有限公司 Method for preparing refined wood vinegar from crop straw
CN106511188A (en) * 2017-01-06 2017-03-22 陕西中医药大学 Hand-washing mousse containing wild jujube core and shell wood vinegar and preparation method and application of hand-washing mousse
CN108187475A (en) * 2018-01-15 2018-06-22 长沙海之源环保科技有限公司 A kind of deodorant compositions and its application

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110339693A (en) * 2019-07-16 2019-10-18 河南碳索新材料科技有限公司 A kind of plant type air deodorization agent of farm and preparation method thereof
CN110354183A (en) * 2019-07-26 2019-10-22 唐山市新雅诺生物科技有限公司 Nantural non-toxic mosquito repellent product and preparation method thereof
CN110358566A (en) * 2019-08-23 2019-10-22 山东省分析测试中心 A kind of preparation method and application of peony seeds shell wood vinegar and its carrier
CN111742936A (en) * 2020-07-14 2020-10-09 唐山进海新材料有限公司 Antibacterial liquid containing wood vinegar composition and preparation method thereof
CN112155018A (en) * 2020-10-20 2021-01-01 唐山市新雅诺生物科技有限公司 Plant source health disinfectant and preparation method thereof
CN112957899A (en) * 2021-03-08 2021-06-15 北京环卫集团环卫服务有限公司 Deodorant and preparation method and application thereof

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