CN105832572A - Amino acid facial cleanser and preparation method thereof - Google Patents

Abstract

The invention relates to an amino acid facial cleanser and a preparation method thereof. The amino acid facial cleanser consists of the following components: sodium cocoyl glutamate, a mixture of potassium cocoyl glycinate, hydroxystearic acid and tocopherol, 1,3-butanediol, PEG400 (polyethylene glycol 400), sorbitol, methyl sodium lauroyl taurine, lauryl hydroxysultaine, potassium hydroxide, polyquaternium cationic surfactants, an emulsifier, a dispersant, sodium chloride, essence, a preservative and de-ionized water. The amino acid facial cleanser prepared by the invention is mild and non-irritant, good in skin-friendly and moisturizing properties, rich and thick in foam, good in skin cleanliness after being washed and good in stability, and the paste (the facial cleanser) appears to be pearly, delicate, soft and smooth and the paste has an optimum paste forming temperature.

Description

Aminoacid cleansing milk and preparation method thereof

Technical field

The present invention relates to cosmetic field, particularly relate to a kind of aminoacid cleansing milk and preparation method thereof.

Background technology

What traditional cleansing milk was focused on is all high-efficiency cleaning, pore cleanser, deoils, and but have ignored product itself Stimulation to skin, it is in order to improve cleaning force and ability of deoiling, and adds the surfactant that alkalescence is extremely strong, Foaming agent, the composition such as soap base, and the skin of human body is weakly acidic, uses Diazolidinyl Urea for a long time. More seriously, the sebum film of skin also can be destroyed.Once lose sebum film, outside skin is highly susceptible to Boundary injures.And aminoacid cleansing milk is the cleansing milk that in all cleansing milk, pro-skin is gentle.Gentle pro-skin is low Stimulating, sensitive skin can use.

Although amino acid cleansing cream has a lot of advantage, but still suffers from many not enough at present at technical elements, Such as: the problems, especially single amino acid class table such as difficult thickening, knot cream point low, mastic thick, poor stability There is the problem that foam is abundant not, cleaning force is inadequate, do not wash clean in the cleansing milk prepared of living.

The most basic effect of facial cleaning cream is to clean skin of face, and it is big that general amino acid cleansing cream is suitable for crowd Mostly being dryness, sensitive skin, because foam is the abundantest, for loose bulla, easily disappear, cleaning dynamics is not Enough.And when skin universal oil, the mixed type partially of people in summer, it is unnecessary that cleaning force can cause skin to have not Fat residue, blocks pore, and impact uses sense, simultaneously as skin clean does not thoroughly produce small pox The black first order issue of acne.For face cleaning product, abundant fine and smooth foam not only can affect product Cleaning capacity, also can affect the use sense of consumer simultaneously.

Amino acid cleansing cream system difficulty thickening, is embodied in the mastic being difficult to that mastic is made molding strip, at present Most amino-acids system mainly uses thickening method, two kinds of methods of crystallization process to prepare mastic.Crystallization process, adds Substantial amounts of powder of amino acids, causes mastic knot cream harder, and mastic is coarse, makes troubles to production fill, with Time due to mastic too hard, be difficult to extrude flexible pipe, also affect the use sense of consumer.Thickening method is used to prepare , often there is the phenomenon of low temperature fruit jelly conglomeration in mastic, and under cryogenic conditions, mastic chance water is not easy to melt, shadow Sound bubble, thus affects the use sense of consumer.

The more difficult control of stability of aminoacid mastic, there are room temperature shelf and tests out in general amino acid cleansing breast The problem that water is thinning, under cryogenic conditions, mastic is hardening, fruit jelly, the problem of conglomeration, and heat-resisting rear mastic divides Layer, return thick problem.

The height of amino acid cleansing cream knot cream point affects production efficiency, ties cream point low (less than 38 DEG C), cooling Time is long, and especially in summer, the temperature of recirculated cooling water is between 30-40 DEG C, and material body to be made is cooled to Less than 38 DEG C, the time of cooling is longer, maybe needs to consume the more energy by cooling water refrigeration, causes producing Efficiency reduces.

Summary of the invention

Based on this, it is necessary to for the problems referred to above, it is provided that a kind of aminoacid cleansing milk and preparation method thereof.

Concrete technical scheme is as follows:

A kind of aminoacid cleansing milk, by percentage to the quality, it includes following components:

The solid content of described methyl lauroyl sodium taurocholate is 50～60%.

In the present invention, sorbitol used is the sorbitol solution of 69～71wt%, Pyrusussuriensis in producing for cosmetic industry The conventional form of alcohol, as long as the amount of contained sorbitol is consistent with the present invention, it is also possible to other concentration or form Sorbitol substitutes.

Methyl lauroyl sodium taurocholate used in the present invention (50～60% solid content) is during cosmetic industry produces The common type of methyl lauroyl sodium taurocholate, if the amount of contained methyl lauroyl sodium taurocholate and the present invention Unanimously, it is also possible to the methyl lauroyl sodium taurocholate of other purity substitutes.

Wherein in some embodiments, by percentage to the quality, described aminoacid cleansing milk includes following components:

Wherein in some embodiments, by percentage to the quality, described aminoacid cleansing milk includes following group Point:

Wherein in some embodiments, described cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixing of tocopherol The mass percent proportioning of thing is: cocos nucifera oil acyl glycine potassium 70～80%, hydroxy stearic acid 20～30%, fertility Phenol 0.5～1.0%, above-mentioned summation is 100%.

Wherein in some embodiments, described polyquaternary ammonium salt cationoid surfactant is polyquaternary ammonium salt-7, gathers Quaternary ammonium salt-43 and the mixture of water, its mass percent proportioning is: polyquaternary ammonium salt-7 3～5%, polyquaternary ammonium salt -43 5～7%, surplus be water.

Wherein in some embodiments, described emulsifying agent is the mixed of PEG-100 stearate and glyceryl stearate Compound, its mass percent proportioning is: PEG-100 stearate 40～60%, glyceryl stearate 40～60%.

Wherein in some embodiments, described dispersant be PEG/PPG-25/30 polymer and The mixture of PEG/PPG-10/30 polymer, its mass percent proportioning is: PEG/PPG-25/30 polymer 90～95%, PEG/PPG-10/30 polymer 5～10%.

Wherein in some embodiments, also include following components by percentage to the quality: essence 0.1～0.2% And preservative 0.1～0.2%.More preferably preservative 0.1～0.15%.Further it is preferably essence 0.18～0.2% and preservative 0.1～0.12%.

The present invention also provides for the preparation method of above-mentioned aminoacid cleansing milk, comprises the following steps:

Step A: sterilization；

Step B: weigh described cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3-fourth Glycol, PEG400, sorbitol, emulsifying agent, dispersant are in main cooker, and heating for dissolving also stirs；

Step C: weigh described potassium hydroxide and appropriate amount of deionized water, stirring and dissolving, be slowly added to while stirring Main cooker, insulated and stirred；

Step D: weigh described sodium cocoyl glutamate, methyl lauroyl sodium taurocholate, lauryl weight ratio Glycine betaine, is first slowly sprinkled into main cooker by described sodium cocoyl glutamate, and agitating heating is dissolved, after insulation froth breaking, Sequentially add clout, stirring and dissolving, stir after begin to cool down；

Step E: weigh described sodium chloride appropriate amount of deionized water heating for dissolving and add main cooker the most afterwards, then by institute State polyquaternary ammonium salt cationoid surfactant to dilute with remaining deionized water, add main cooker, stir；

Step F: weigh described essence, preservative, be sequentially added into main cooker, after stirring, mastic is treated in stirring Rear fine and smooth discharging.

Wherein in some embodiments, described preparation method comprises the following steps:

Step A: sterilization: take the medical alcohol that volumetric concentration is 75% and carry out vessel sterilization；

Step B: weigh described cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3-fourth Glycol, PEG400, sorbitol, emulsifying agent, dispersant, in main cooker, are heated to 70～85 DEG C and dissolve and stir Mix uniformly；

Step C: weigh described potassium hydroxide and appropriate amount of deionized water, stirring and dissolving after being heated to 70～85 DEG C, It is slowly added to main cooker, insulated and stirred 5～20min while stirring；

Step D: weigh described sodium cocoyl glutamate, methyl lauroyl sodium taurocholate, lauryl hydroxyl sulphur Base glycine betaine, is first slowly sprinkled into main cooker by described sodium cocoyl glutamate, and agitating heating is dissolved, and is incubated froth breaking After, sequentially add clout, stirring and dissolving, stir after begin to cool down；

Step E: when main cooker is cooled to 50～65 DEG C, weighs described sodium chloride, heat by appropriate amount of deionized water Add main cooker after dissolving completely to 50～65 DEG C, more described polyquaternary ammonium salt cationoid surfactant is remained Deionized water dilution, add main cooker, stir；

Step F: weigh described essence, preservative, is sequentially added into when main cooker is cooled to 40～45 DEG C, stirring After Jun Yun, stir discharging after mastic is fine and smooth uniformly.

The present invention compares the advantage of prior art and has the beneficial effect that

The present inventor team, by substantial amounts of research, breaches the technological difficulties of aminoacid cleansing milk, Based on crystallization process, it is aided with neutralisation and thickening method, prepares stable amino acid cleansing milk；The present invention is by ammonia Base acids table is lived and has been carried out reasonably compounding forming certain micellar concentration with other gentle surfactant, and adds Addition polymerization quaternaries cation reaches foam enhancing and the effect of steady bubble, promotes foam total amount and quality so that product There is abundant fine and smooth soft and smooth foam, improve the aminoacid cleansing milk cleaning force to skin, reach good Wash rear skin cleanliness factor.The most reasonably surfactant and the collocation of polyhydric alcohol proportioning, improve aminoacid cream The knot cream point of body, improves the fine and smooth degree of mastic outward appearance, prepares pearl in the case of without pearling agent The fine and smooth mastic of light.

Aminoacid cleansing milk prepared by the present invention is a aminoacid cleansing milk integrating many merits, Except gentleness is non-stimulated, pro-skin moisture retention is good, and the most prominent feature is to have abundant dense foam, washes Rear skin cleanliness factor is good, and heat-resisting, cold-resistant, shelf are tested highly stable, mastic outward appearance exquisiteness molding, nothing Grain sense, pearly-lustre exquisiteness is soft and smooth, and has optimal knot cream temperature, knot cream point control between 38～45 DEG C, It is convenient to produce.

Detailed description of the invention

The present invention is further illustrated below in conjunction with embodiment.

Raw materials used in embodiment it is commercially available common raw material, wherein:

Sodium cocoyl glutamate, trade name: HONDU SCG-95, have purchased from Shanghai grand degree fine chemistry industry Limit company；

Cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, mass percent proportioning is: cocos nucifera oil Acyl glycine potassium 70～80%, hydroxy stearic acid 20～30%, tocopherol 0.5～1.0%, above-mentioned summation is 100%, Trade name: HONDU SCA-75, purchased from Shanghai Hong Du Fine Chemical Co., Ltd；

Methyl lauroyl sodium taurocholate, trade name: HONDU LT-40, content is 50～60%, purchased from upper Hai Hongdu Fine Chemical Co., Ltd；

Polyquaternary ammonium salt cationoid surfactant (mixture of polyquaternary ammonium salt-7, polyquaternary ammonium salt-43 and water), Mass percent proportioning is: polyquaternary ammonium salt-7 3～5%, polyquaternary ammonium salt-43 5～7%, surplus are water, trade name For: Supcare 620, purchased from Shanghai Hong Du Fine Chemical Co., Ltd；

Emulsifying agent: PEG-100 stearate and the mixture of glyceryl stearate, mass percent proportioning is: PEG-100 stearate 40-60%, glyceryl stearate 40-60%, trade name: HONDU A-165, Purchased from Shanghai Hong Du Fine Chemical Co., Ltd；

Dispersant: PEG/PPG-25/30COPOLYMER's and PEG/PPG-10/30COPOLYMER is mixed Compound, mass percent proportioning is: PEG/PPG-25/30 COPOLYMER 90～95%, PEG/PPG-10/30COPOLYMER 5～10%, trade name: SAPPCHEM PC25, purchased from Shanghai Hong Du Fine Chemical Co., Ltd；

Sorbitol, mass percent concentration is the sorbitol solution of 69～71wt%, purchased from Luo Gaite；

Lauryl hydroxyl sulfo betaine is purchased from flower king；

Potassium hydroxide is purchased from excellent profit moral.

Embodiment and comparative example

A kind of aminoacid cleansing milk, by percentage to the quality, its component comprised asks for an interview table 1 below:

Table 1 embodiment 1～3 and the formula table of comparative example 1～4

Note: "-" represent without

Its preparation method is:

Step A: sterilization: take the medical alcohol that volumetric concentration is 75% and carry out vessel sterilization；

Step B: weigh cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3 butylene glycol, PEG400, sorbitol, emulsifying agent, dispersant, in main cooker, are heated to 70～85 DEG C and dissolve and stir；

Step C: weigh potassium hydroxide and appropriate amount of deionized water, stirring and dissolving after being heated to 70～85 DEG C, limit Stirring limit is slowly added to main cooker, insulated and stirred 5～20min；

Step D: weigh sodium cocoyl glutamate, methyl lauroyl sodium taurocholate, lauryl weight ratio sweet Dish alkali, is first slowly sprinkled into main cooker by sodium cocoyl glutamate, and agitating heating is dissolved, and after insulation froth breaking, then depends on Secondary addition clout, stirring and dissolving, stir after begin to cool down；

Step E: when main cooker is cooled to 50～65 DEG C, weighs sodium chloride, be heated to by appropriate amount of deionized water 50～65 DEG C dissolve completely after add main cooker, then by polyquaternary ammonium salt cationoid surfactant with remaining go from The dilution of sub-water adds main cooker after stirring evenly, and stirs；

Step F: weighed essence, preservative, is sequentially added into when main cooker is cooled to 40～45 DEG C, and stirring is all After even, the discharging after mastic is fine and smooth uniformly of middle stirring at low speed.

To embodiment 1～3 and comparative example 1～4 gained sample carry out evaluation on probation, be mainly reflected in use process In to foam, cleanliness factor, the evaluation of moisture feeling.

Method particularly includes: sample is issued to 20 testers and contrasts use.When tester uses sample Use same procedure is carried out, and each sample respectively uses two weeks, tester according to oneself feel comment Point.Ten point system is taked in scoring, and 1 point worst, and 10 points best.

The concrete clean method of tester is: every day uses sooner or later, first uses clear water to drench skin of face, The product using the present invention adds suitable quantity of water in the palm of the hand in right amount, after rubbing foaming, is applied to face and circumference of eyes, And gently rub skin of face about one minute；Then rinse well with clear water, morning and evening every day repeat the above steps, After each sample uses two weeks, product is marked, the results are shown in Table 2.

Table 2 embodiment 1～3 and comparative example 1～4 try out evaluation table

Test event	Lather quickness	Foaming abundancy degree	Wash rear cleanliness factor	Degree is moistened after washing
					Embodiment 1	9.0	9.5	9.2	9.5
Embodiment 2	8.8	8.9	9.2	9.0
					Embodiment 3	8.5	8.5	8.2	8.8
Comparative example 1	8.3	8.4	8.0	8.5
					Comparative example 2	7.8	8.0	7.8	8.3
Comparative example 3	8.3	8.3	9.0	8.5
					Comparative example 4	7.5	7.5	7.8	7.8

Test result indicate that, with the addition of cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, first Base lauroyl sodium taurocholate, the aminoacid cleansing milk of embodiment gained of lauryl hydroxyl sulfo betaine, its In use lather quickness, foaming abundancy degree, wash rear cleanliness factor, wash after moisten degree have lifting, all Better than comparative example.

Cleansing milk mastic to the preparation of embodiment 1～3 comparative example 1～4 carries out the test of foaming power.Method of testing With reference to Ross-Miles method, the mensuration of GBT 13173.6-2000 detergent foaming power.

Test condition is: 0.25% deionized water solution, experimental temperature 40 ± 0.5 DEG C, tests 5 minutes and reads foam Highly.Average test data such as table 3:

Table 3 foaming power test result

Test event	Average foam height (mm)
		Embodiment 1	75
Embodiment 2	68
		Embodiment 3	65
Comparative example 1	45
		Comparative example 2	40
Comparative example 3	42
		Comparative example 4	30

Test result indicate that, the facial milk cleanser foaming power of embodiment is more preferable than the foaming power of the facial milk cleanser of comparative example.Join Side adds cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, methyl lauroyl taurine The foaming power of facial milk cleanser can be made after sodium, lauryl hydroxyl sulfo betaine, polyquaternary ammonium salt-7 and polyquaternary ammonium salt-43 More preferably.

To the embodiment of the present invention 1～3 and comparative example 1～4 wash rear cleanliness factor and investigate, select 20 test person Member, use equal amount (0.1 gram) BB frost/eyeliner on each tester's the back of the hand with smearing out identical faces Long-pending (2*3cm)/draw the lines that thickness length is identical, weigh test sample (embodiment and comparative example sample respectively Product) 0.2g, spread upon at the back of the hand figure, after a small amount of water-wet the back of the hand, softly clean 30s, rush with clear water Totally, clean effect is observed.

Evaluation criterion:

Cleanliness factor is the best: BB frost/eyeliner is rinsed well completely, does not sees the marking.

Cleanliness factor is general: BB frost/eyeliner is rinsed well the most completely, still has the inconspicuous marking.

Cleanliness factor is poor: BB frost/eyeliner is rinsed well the most completely, still has the obvious marking of residual.

Experimental result is shown in Table 4:

Rear cleanliness factor test result washed by table 4

Test event	Cleanliness factor the best (%)	Cleanliness factor is general (%)	Cleanliness factor poor (%)
				Embodiment 1	95%	5%	0
Embodiment 2	90%	10%	0
				Embodiment 3	80%	20%	0
Comparative example 1	45%	35%	20%
				Comparative example 2	10%	45%	40%
Comparative example 3	70%	20%	10%
				Comparative example 4	10%	50%	40%

Experimental result: the cleanliness factor after facial milk cleanser prepared by the formula in scope of embodiments is washed is preferable.Explanation is joined Side adds cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, methyl lauroyl taurine Sodium, lauryl hydroxyl sulfo betaine have remarkable result to the lifting of formula cleannes.

To embodiment 1～3 and the knot cream point of comparative example 1～4 contrast, ask for an interview table 5:

Cream temperature comparisons's result tied by table 5

Test result indicate that, the knot cream temperature of embodiment gained aminoacid cleansing milk is wanted than the knot cream temperature of comparative example Height, in formula add cocos nucifera oil acyl glycine potassium & hydroxy stearic acid & tocopherol, methyl lauroyl sodium taurocholate, The lifting of gained cleansing milk knot cream point is had significantly by the proportioning of lauryl hydroxyl sulfo betaine and polyhydric alcohol Effect.

To embodiment 1～3 and the outward appearance of comparative example 1～4, smear and stability contrast, ask for an interview table 6,7:

Table 6 outward appearance, smear result

Test event	Outward appearance, smear evaluation after preparation discharging 24 hours
		Embodiment 1	Outward appearance is fine and smooth, present soft and smooth pearly-lustre, be easily spread, smear is good
Embodiment 2	Outward appearance is fine and smooth, soft, present soft and smooth pearly-lustre, easily sprawl, smear good
		Embodiment 3	Outward appearance is fine and smooth, soft, present soft and smooth pearly-lustre, easily sprawl, smear good
Comparative example 1	Outward appearance powdery, have fine grained, the most firmly, the most easy to apply
		Comparative example 2	Outward appearance is coarse, the most easy to apply
Comparative example 3	Dilute soft, coarse, the not molding of outward appearance
		Comparative example 4	Outward appearance is coarse, hard, without pearly-lustre, be not easy to smear

Test result indicate that, the mastic of the aminoacid cleansing milk prepared by embodiment, outward appearance exquisiteness is soft, easily Sprawl, smear good, use sense more preferably.

Table 7 stability test result

Test result indicate that, the stability of the aminoacid cleansing milk of embodiment gained is better than comparative example.

Each technical characteristic of embodiment described above can combine arbitrarily, for making description succinct, the most right The all possible combination of each technical characteristic in above-described embodiment is all described, but, if these skills There is not contradiction in the combination of art feature, is all considered to be the scope that this specification is recorded.

Embodiment described above only have expressed the several embodiments of the present invention, and it describes more concrete and detailed, But can not therefore be construed as limiting the scope of the patent.It should be pointed out that, for this area For those of ordinary skill, without departing from the inventive concept of the premise, it is also possible to make some deformation and change Entering, these broadly fall into protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be with appended power Profit requires to be as the criterion.

Claims (10)

1. an aminoacid cleansing milk, it is characterised in that by percentage to the quality, it includes following components:

The solid content of described methyl lauroyl sodium taurocholate is 50～60%.

Aminoacid cleansing milk the most according to claim 1, it is characterised in that by percentage to the quality, its Including following components:

Aminoacid cleansing milk the most according to claim 2, it is characterised in that by percentage to the quality, its Including following components:

4. according to the aminoacid cleansing milk described in any one of claims 1 to 3, it is characterised in that described cocos nucifera oil Acyl glycine potassium, hydroxy stearic acid, the mass percent proportioning of mixture of tocopherol be: the sweet ammonia of cocos nucifera oil acyl Acid potassium 70～80%, hydroxy stearic acid 20～30%, tocopherol 0.5～1.0%, above-mentioned summation is 100%.

5. according to the aminoacid cleansing milk described in any one of claims 1 to 3, it is characterised in that described poly-season Ammonium salt cationoid surfactant is the mixture of polyquaternary ammonium salt-7, polyquaternary ammonium salt-43 and water, its quality hundred Proportion by subtraction proportioning is: polyquaternary ammonium salt-7 3～5%, polyquaternary ammonium salt-43 5～7%, surplus are water.

6. according to the aminoacid cleansing milk described in any one of claims 1 to 3, it is characterised in that described emulsifying Agent is the mixture of PEG-100 stearate and glyceryl stearate, and its mass percent proportioning is: PEG-100 Stearate 40～60%, glyceryl stearate 40～60%.

7. according to the aminoacid cleansing milk described in any one of claims 1 to 3, it is characterised in that described dispersion Agent is PEG/PPG-25/30 polymer and the mixture of PEG/PPG-10/30 polymer, and its mass percent is joined Ratio is: PEG/PPG-25/30 polymer 90～95%, PEG/PPG-10/30 polymer 5～10%.

8. according to the aminoacid cleansing milk described in any one of claims 1 to 3, it is characterised in that also include with The following components of mass percent: essence 0.1～0.2% and preservative 0.1～0.2%.

9. the preparation method of the aminoacid cleansing milk described in a claim 8, it is characterised in that include with Lower step:

Step A: sterilization；

Step B: weigh described cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3-fourth Glycol, PEG400, sorbitol, emulsifying agent, dispersant are in main cooker, and heating for dissolving also stirs；

Step C: weigh described potassium hydroxide and appropriate amount of deionized water, stirring and dissolving, be slowly added to while stirring Main cooker, insulated and stirred；

Step D: weigh described sodium cocoyl glutamate, methyl lauroyl sodium taurocholate, lauryl weight ratio Glycine betaine, is first slowly sprinkled into main cooker by described sodium cocoyl glutamate, and agitating heating is dissolved, after insulation froth breaking, Sequentially add clout, stirring and dissolving, stir after begin to cool down；

Step E: weigh described sodium chloride appropriate amount of deionized water heating for dissolving and add main cooker the most afterwards, then by institute State polyquaternary ammonium salt cationoid surfactant to dilute with remaining deionized water, add main cooker, stir；

Step F: weigh described essence, preservative, be sequentially added into main cooker, after stirring, mastic is treated in stirring Rear fine and smooth discharging.

The preparation method of aminoacid cleansing milk the most according to claim 9, it is characterised in that include Following steps:

Step A: sterilization: take the medical alcohol that volumetric concentration is 75% and carry out vessel sterilization；

Step B: weigh described cocos nucifera oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3-fourth Glycol, PEG400, sorbitol, emulsifying agent, dispersant, in main cooker, are heated to 70～85 DEG C and dissolve and stir Mix uniformly；

Step C: weigh described potassium hydroxide and appropriate amount of deionized water, stirring and dissolving after being heated to 70～85 DEG C, It is slowly added to main cooker, insulated and stirred 5～20min while stirring；

Step D: weigh described sodium cocoyl glutamate, methyl lauroyl sodium taurocholate, lauryl hydroxyl sulphur Base glycine betaine, is first slowly sprinkled into main cooker by described sodium cocoyl glutamate, and agitating heating is dissolved, and is incubated froth breaking After, sequentially add clout, stirring and dissolving, stir after begin to cool down；

Step E: when main cooker is cooled to 50～65 DEG C, weighs described sodium chloride, heat by appropriate amount of deionized water Add main cooker after dissolving completely to 50～65 DEG C, more described polyquaternary ammonium salt cationoid surfactant is remained Deionized water dilution, add main cooker, stir；

Step F: weigh described essence, preservative, is sequentially added into when main cooker is cooled to 40～45 DEG C, stirring After Jun Yun, stir discharging after mastic is fine and smooth uniformly.