CN107157799A - A kind of soap base mildy wash - Google Patents

A kind of soap base mildy wash Download PDF

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Publication number
CN107157799A
CN107157799A CN201710351930.5A CN201710351930A CN107157799A CN 107157799 A CN107157799 A CN 107157799A CN 201710351930 A CN201710351930 A CN 201710351930A CN 107157799 A CN107157799 A CN 107157799A
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CN
China
Prior art keywords
parts
soap base
mildy wash
base mildy
added
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710351930.5A
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Chinese (zh)
Inventor
蒋诚
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Shanghai Iraq Biotechnology Co Ltd
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Shanghai Iraq Biotechnology Co Ltd
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Application filed by Shanghai Iraq Biotechnology Co Ltd filed Critical Shanghai Iraq Biotechnology Co Ltd
Priority to CN201710351930.5A priority Critical patent/CN107157799A/en
Publication of CN107157799A publication Critical patent/CN107157799A/en
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70—Biological properties of the composition as a whole
    • A61K2800/72—Hypo-allergenic

Abstract

It is respectively the invention discloses a kind of parts by weight of soap base mildy wash including following components and each component：Deionized water：3000 ~ 4000 parts；Thickener：20 ~ 60 parts；EDTA disodiums：1 ~ 4 part；Organic solvent：1000 ~ 1500 parts；Allantoin：5 ~ 20 parts；Emulsifying agent：3000 ~ 3250 parts；Preservative：20 ~ 40 parts；PH adjusting agent：1200 ~ 1600 parts；Cocounut oil acyl isethionic acid ester sodium：20 ~ 400 parts；Essence：20 ~ 40 parts；The emulsifying agent is laurate, myristic acid, palmitic acid, stearic acid, ceteth 20, glycerine oleic acid, stearine.The present invention has formulation stable, reduces the excitant of soap base mildy wash, accomplishes clean without tight after washing, and improves and feels after washing.

Description

A kind of soap base mildy wash
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of soap base mildy wash.
Background technology
With expanding economy, the raising of living standards of the people, mildy wash has come into huge numbers of families mouthful, as consumption The necessity of person.Mildy wash best in quality should be provided simultaneously with cleaning, nutrition, the effect for protecting skin.At present in Chinese city Popular mildy wash system more than 90% is soap base mildy wash on field, but common soap base mildy wash can deposit cleaning capacity mistake By force, the shortcomings of washing difference between rear dry skin, unstable, product the batch of formula height.
The content of the invention
In order to overcome the deficiencies in the prior art, there is good cleaning energy it is an object of the invention to provide a kind of gentle stabilization The soap base mildy wash of power.
To reach above-mentioned purpose, the present invention is achieved by the following technical solutions.
A kind of soap base mildy wash, including following components and the parts by weight of each component are respectively：
Deionized water：3000~4000 parts；
Thickener：20~60 parts；
EDETATE SODIUM：1~4 part；
Organic solvent：1000~1500 parts；
Allantoin：5~20 parts；
Emulsifying agent：3000~3250 parts；
Preservative：20~40 parts；
PH adjusting agent：1200~1600 parts；
Cocounut oil acyl isethionic acid ester sodium：20~400 parts；
Essence：20~40 parts；
The emulsifying agent is laurate, myristic acid, palmitic acid, stearic acid, ceteth -20, glyceryl oleate, sweet Oleostearin acid esters, its weight ratio is 40~55：75~85：60~75：80~95：10~20：5~10:5~10.
Further the thickener is hydroxyethyl cellulose or xanthans.
Further the organic solvent is glycerine or 1,3- propane diols.
Further the preservative is methyl hydroxybenzoate, propylparaben, and its weight ratio is 1~2:1~2.
Further the pH adjusting agent is the KOH or NaOH solution that mass percent is 30%.
A kind of preparation method of soap base mildy wash is further additionally provided, is comprised the following steps：Precise each component It is standby；
(1) deionized water is added into aqueous phase pot, adds thickener, be warming up to 55~65 DEG C, obtain aqueous phase；
(2) emulsifying agent, preservative are added into oil phase pot, opens stirring, heating, be warming up to 80 DEG C -85 DEG C, obtain oil phase；
(3) vacuum emulsification pot is vacuumized, drawn water into vacuum emulsification pot, opened stirring, heating, be pumped into EDTA bis- Sodium, allantoin and organic solvent, are stirred until homogeneous, and are warming up to 80 DEG C -85 DEG C and are incubated 15~20 minutes；
(4) pH adjusting agent is pumped into vacuum emulsification pot, maintains the temperature at 80 DEG C -85 DEG C；
(5) vacuum emulsification pot is evacuated to -0.05mPa, oil phase is pumped into vacuum emulsification pot, oil phase exhausts follow-up Continuous homogeneous 5 minutes；10~15 minutes are incubated after the completion of homogeneous, is then cooled；
(6) when being cooled to 60 DEG C, cocounut oil acyl isethionic acid ester sodium is added, is kept for 60 DEG C stir 10~20 minutes, continues to drop Temperature；
(7) when being cooled to 45 DEG C, essence is added, continues to cool；
(8) when being cooled to 40 DEG C, discharging, filtering produce a kind of soap base mildy wash.
Further the rate of temperature fall is 1 DEG C/min.
Further in the step (6), the cocounut oil acyl isethionic acid ester sodium deionized water of 2 times of its weight dissolves in advance Feeding intake afterwards.
Beneficial effect：Compared with prior art, the advantage of the invention is that：
1) formulation stable, places three months under 48 degree of conditions of storage of high temperature and recovers room temperature, lotion is normal.Pasty consistence by Room temperature change denseness influence is little, and lotion is into bar, it is easy to smears and rinses；
2) formula is arranged in pairs or groups by rational material rate, reduces the excitant of soap base mildy wash；
3) the characteristics of formula remains clean after soap base mildy wash is washed, can be with because addition grease improves the sensation after washing It is clean without tight after accomplishing to wash, feel after effectively improving the washing of soap base mildy wash.
Embodiment
With reference to example, the present invention is described in further detail.
Embodiment 1
A kind of preparation method of soap base mildy wash, comprises the following steps：Precise each component is standby；
(1) 3450 parts cold of deionized water is added into aqueous phase pot, opens stirring, heating, be slowly sprinkled into hydroxyethyl cellulose 40 parts, it is warming up to 55~65 DEG C and stops heating, stirring obtains aqueous phase to material body homogeneous transparent；
(2) by 500 parts of laurate, 800 parts of myristic acid, 700 parts of palmitic acid, 900 parts of stearic acid, ceteth -20, 100 parts, 50 parts of glyceryl oleate, 100 parts of stearine, 20 parts of methyl hydroxybenzoate, the addition of 10 parts of propylparaben Oil phase pot, opens stirring, heating, is warming up to 80 DEG C -85 DEG C to complete melting, obtains oil phase；
(3) vacuum emulsification pot is vacuumized, drawn water into vacuum emulsification pot, opened stirring, heating, be pumped into EDETATE SODIUM 1200 parts of 2 parts, 10 parts of allantoin and glycerine, are stirred until homogeneous, and are warming up to 80 DEG C -85 DEG C and are incubated 15~20 minutes；
(4) 30% 1500 parts of KOH solution is pumped into vacuum emulsification pot, opens stirring, rotating speed 1300rpm, keeping body It is temperature at 80 DEG C -85 DEG C；
(5) vacuum emulsification pot is evacuated to -0.05mPa, speed of agitator rises to 3500rpm, and oil phase is pumped into vacuum Emulsify in pot, oil phase exhausts follow-up continuous insulated and stirred 15~20 minutes；Then cooled, stirred simultaneously with 1 DEG C/min of speed Mix speed and be reduced to 1000rpm；
(6) with deionized water 400 parts be swelled 200 parts of cocounut oil acyl isethionic acid ester sodium, when system is cooled to 60 DEG C, be pumped into The cocounut oil acyl isethionic acid ester sodium dissolved in advance, keep vacuum -0.05mPa, 60 DEG C stir 10~20 minutes, mixing speed 2000rpm, then proceedes to cooling；
(7) when being cooled to 45 DEG C, it is pumped into essence：Three 15 parts of flower FRAG86330196 essence, 10 parts of rose wood wood oil is kept Vacuum -0.05mPa, mixing speed 2000rpm, continue to cool；
(8) when being cooled to 40 DEG C, discharging, filtering produce a kind of soap base mildy wash.
Embodiment 2
It is identical with the preparation method of embodiment 1, except that the proportioning of each component：
3000 parts of ionized water, 20 parts of xanthans, 400 parts of laurate, 850 parts of myristic acid, 600 parts of palmitic acid, stearic acid 950 parts, ceteth -20,100 part, 50 parts of glyceryl oleate, 50 parts of stearine, 10 parts of methyl hydroxybenzoate, to hydroxyl 10 parts of propyl benzoate, 1 part of EDETATE SODIUM, 5 parts of allantoin, 1,3 1000 parts of propane diols, 1200 parts of 30% NaOH solution, coconut palm 20 parts of oleoyl isethionic acid ester sodium, essence：10 parts of Lavender, 10 parts of rose wood wood oil.
Embodiment 3
It is identical with the preparation method of embodiment 1, except that the proportioning of each component：
4000 parts of ionized water, 60 parts of hydroxyethyl cellulose, 550 parts of laurate, 750 parts of myristic acid, 750 parts of palmitic acid, 800 parts of stearic acid, ceteth -20,200 part, 100 parts of glyceryl oleate, 100 parts of stearine, methyl hydroxybenzoate 20 Part, 20 parts of propylparaben, 4 parts of EDETATE SODIUM, 20 parts of allantoin, 1500 parts of glycerine, 30% KOH solution 1600 Part, 400 parts of cocounut oil acyl isethionic acid ester sodium, essence：20 parts of sweet orange blossom oil, 20 parts of rose wood wood oil.
The soap base mildy wash of embodiment 1,2,3 is detected, foundation is detected：《Cosmetics health specification》(Ministry of Public Health, 2007), testing result see the table below：
Evaluation of result：According to《Cosmetics health specification》The requirement of (Ministry of Public Health, 2007), each index symbol of microorganism detection Close requirement, hygienic chemistry and detect that each index meets the requirements, toxicology detects nonirritant to eye microstimulation, to skin.
The present invention is illustrated according to above-described embodiment, it will be appreciated that above-described embodiment does not limit this in any form Invention, the technical scheme that all use equivalent substitution or equivalent transformation mode are obtained is within the scope of the present invention.

Claims (8)

1. a kind of soap base mildy wash, it is characterised in that the parts by weight including following components and each component are respectively：
Deionized water：3000 ~ 4000 parts；
Thickener：20 ~ 60 parts；
EDTA disodiums：1 ~ 4 part；
Organic solvent：1000 ~ 1500 parts；
Allantoin：5 ~ 20 parts；
Emulsifying agent：3000 ~ 3250 parts；
Preservative：20 ~ 40 parts；
PH adjusting agent：1200 ~ 1600 parts；
Cocounut oil acyl isethionic acid ester sodium：20 ~ 400 parts；
Essence：20 ~ 40 parts；
The emulsifying agent is that laurate, myristic acid, palmitic acid, stearic acid, ceteth -20, glyceryl oleate, glycerine are hard Resin acid ester, its weight ratio is 40 ~ 55：75~85：60~75：80~95：10~20：5~10:5~10.
2. a kind of soap base mildy wash according to claim 1, it is characterised in that the thickener be hydroxyethyl cellulose or Xanthans.
3. a kind of soap base mildy wash according to claim 1, it is characterised in that the organic solvent is glycerine or 1,3- third Glycol.
4. a kind of soap base mildy wash according to claim 1, it is characterised in that the preservative is methyl hydroxybenzoate, to hydroxyl Yl benzoic acid propyl ester, its weight ratio is 1 ~ 2:1~2.
5. a kind of soap base mildy wash according to claim 1, it is characterised in that the pH adjusting agent is that mass percent is 30% KOH or NaOH solution.
6. a kind of preparation method of soap base mildy wash according to any one of claim 1 ~ 5 claim, it is characterised in that Comprise the following steps：Precise each component is standby；
（1）Deionized water is added into aqueous phase pot, thickener is added, is warming up to 55 ~ 65 DEG C, obtains aqueous phase；
（2）Emulsifying agent, preservative are added into oil phase pot, stirring, heating is opened, is warming up to 80 DEG C -85 DEG C, obtains oil phase；
（3）Vacuum emulsification pot is vacuumized, drawn water into vacuum emulsification pot, stirring is opened, heats, suction EDTA disodiums, Allantoin and organic solvent, are stirred until homogeneous, and are warming up to 80 DEG C -85 DEG C and are incubated 15 ~ 20 minutes；
（4）PH adjusting agent is pumped into vacuum emulsification pot, 80 DEG C -85 DEG C are maintained the temperature at；
（5）Vacuum emulsification pot is evacuated to -0.05mPa, oil phase is pumped into vacuum emulsification pot, oil phase continues equal after exhausting Matter 5 minutes；10 ~ 15 minutes are incubated after the completion of homogeneous, is then cooled；
（6）When being cooled to 60 DEG C, cocounut oil acyl isethionic acid ester sodium is added, is kept for 60 DEG C stir 10 ~ 20 minutes, continues to cool；
（7）When being cooled to 45 DEG C, essence is added, continues to cool；
（8）When being cooled to 40 DEG C, discharging, filtering produce a kind of soap base mildy wash.
7. the preparation method of a kind of soap base mildy wash according to claim 6, it is characterised in that the rate of temperature fall is 1 DEG C/min.
8. a kind of preparation method of soap base mildy wash according to claim 6, it is characterised in that the step（6）In, coconut palm Oleoyl isethionic acid ester sodium with feeding intake again after the deionized water dissolving in advance of 2 times of its weight.
CN201710351930.5A 2017-05-18 2017-05-18 A kind of soap base mildy wash Pending CN107157799A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710351930.5A CN107157799A (en) 2017-05-18 2017-05-18 A kind of soap base mildy wash

Publications (1)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108294989A (en) * 2018-03-26 2018-07-20 广东名辰堂健康产业股份有限公司 A kind of anti-acne facial cleanser and its production method
CN109846759A (en) * 2019-04-19 2019-06-07 吉林省东鳌鹿业科技开发有限公司 A kind of deer oil facial cleanser and preparation method thereof
CN109966161A (en) * 2019-03-19 2019-07-05 曼秀雷敦(中国)药业有限公司 A kind of facial cleanser of floorboard with high oil content and preparation method thereof
CN109984960A (en) * 2019-05-07 2019-07-09 海南师范大学 A kind of beautiful essential oil facial cleanser of promise and preparation method thereof
CN110613675A (en) * 2019-10-28 2019-12-27 烟台华康海洋食品有限公司 Formula and preparation process of sea cucumber facial cleanser
CN114099382A (en) * 2021-11-22 2022-03-01 福建片仔癀化妆品有限公司 Soap-based facial cleanser and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102727391A (en) * 2012-07-06 2012-10-17 澳宝化妆品（惠州）有限公司 Mild moisturizing soap-based cleaning cream
CN104257527A (en) * 2014-10-22 2015-01-07 广东幸美化妆品股份有限公司 Moisturizing facial cleanser and preparation method thereof
CN105267085A (en) * 2015-09-29 2016-01-27 沈敬国 Skin-beautifying facial cleanser and preparation method thereof
CN105832572A (en) * 2016-04-07 2016-08-10 广州宏度精细化工有限公司 Amino acid facial cleanser and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102727391A (en) * 2012-07-06 2012-10-17 澳宝化妆品（惠州）有限公司 Mild moisturizing soap-based cleaning cream
CN104257527A (en) * 2014-10-22 2015-01-07 广东幸美化妆品股份有限公司 Moisturizing facial cleanser and preparation method thereof
CN105267085A (en) * 2015-09-29 2016-01-27 沈敬国 Skin-beautifying facial cleanser and preparation method thereof
CN105832572A (en) * 2016-04-07 2016-08-10 广州宏度精细化工有限公司 Amino acid facial cleanser and preparation method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108294989A (en) * 2018-03-26 2018-07-20 广东名辰堂健康产业股份有限公司 A kind of anti-acne facial cleanser and its production method
CN109966161A (en) * 2019-03-19 2019-07-05 曼秀雷敦(中国)药业有限公司 A kind of facial cleanser of floorboard with high oil content and preparation method thereof
CN109846759A (en) * 2019-04-19 2019-06-07 吉林省东鳌鹿业科技开发有限公司 A kind of deer oil facial cleanser and preparation method thereof
CN109984960A (en) * 2019-05-07 2019-07-09 海南师范大学 A kind of beautiful essential oil facial cleanser of promise and preparation method thereof
CN110613675A (en) * 2019-10-28 2019-12-27 烟台华康海洋食品有限公司 Formula and preparation process of sea cucumber facial cleanser
CN114099382A (en) * 2021-11-22 2022-03-01 福建片仔癀化妆品有限公司 Soap-based facial cleanser and preparation method thereof
CN114099382B (en) * 2021-11-22 2024-03-12 福建片仔癀化妆品有限公司 Soap-based facial cleanser and preparation method thereof

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Application publication date: 20170915