CN105287261B - A kind of azalaic acid compound acne-removing cream containing rose oil and preparation method thereof - Google Patents
A kind of azalaic acid compound acne-removing cream containing rose oil and preparation method thereof Download PDFInfo
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- CN105287261B CN105287261B CN201510715946.0A CN201510715946A CN105287261B CN 105287261 B CN105287261 B CN 105287261B CN 201510715946 A CN201510715946 A CN 201510715946A CN 105287261 B CN105287261 B CN 105287261B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention relates to a kind of azalaic acid compound acne-removing cream containing rose oil and preparation method thereof, following steps are specifically included：The azalaic acid that percentage by weight is 10 20% is added in the deionized water of percentage by weight 40 65%, is heated to 80 85 DEG C, the chitosan and 5% propane diols for adding 1 1.5% mix, and it is standby that aqueous phase is made；The cetostearyl alcohol of percentage by weight 0.5 1% and cetearyl glucoside mixture, 1 2% stearine, 1.5 2% stearines of PEG 5,8 10% vegetable oil are mixed and be heated to 80 85 DEG C, fully melts, it is standby that oil phase is made；The aqueous phase and oil phase are mixed, are heated to 40 60 DEG C, the rose oil that percentage by weight is 0.3 0.5% is added, is stirred well to complete emulsification, is cooled to room temperature, be aged, obtain the azalaic acid compound acne-removing cream lotion containing rose oil.The preparation method is simple efficiently, short preparation period, natural pollution-free, and product property is stable, emulsifying effectiveness is good, and product anti-acne effect is good, and has whitening, light spot, crease-resistant, moisturizing and other effects simultaneously.
Description
Technical field
The present invention relates to a kind of anti-acne skin care item and preparation method thereof, in particular to a kind of azalea containing rose oil
Sour compound acne-removing cream and preparation method thereof.
Background technology
Being commonly called as of acne as whelk, also referred to as small pox, is mainly in teenager, is a kind of chronic inflammatory skin.
Product for resolving poxes in the market is often containing stimulating components such as alcohol, hormone and salicylic acids, nor pure natural
Plant extraction.Although some products have used this natural extract of azalaic acid, azalaic acid is under general condition
It can not be dissolved in water or oil.The improper azalaic acid that result in of preparation method can not be dispersed in skin care item well, it is dispelled
Acne effect is unstable, easily demulsification, can not be less readily available for absorption by the skin.
In view of drawbacks described above, creator of the present invention obtains the present invention finally by prolonged research and practice.
The content of the invention
To solve above-mentioned technological deficiency, the technical solution adopted by the present invention is, on the one hand provides one kind and contains rose oil
Azalaic acid compound acne-removing cream preparation method, comprise the following steps：
The preparation of aqueous phase：It is 40-65%'s that the azalaic acid that percentage by weight is 10-20% is added into percentage by weight
In deionized water, 80-85 DEG C is heated to, the chitosan and 5% propane diols for adding 1-1.5% mix, standby；
The preparation of oil phase：By percentage by weight be 0.5-1% cetostearyl alcohol and cetearyl glucoside mixture,
1-2% stearines, 1.5-2% PEG-5 stearines, 8-10% vegetable oil mix and are heated to 80-85 DEG C,
It is set fully to melt, it is standby；
The preparation of lotion：The aqueous phase and the oil phase are heated into 80-85 DEG C of mixing and emulsifying, after be cooled to 40-60 DEG C, add
Enter the rose oil that percentage by weight is 0.3-0.5%, be sufficiently stirred and be thoroughly mixed it, be cooled to room temperature, be aged, obtain
Azalaic acid compound acne-removing cream lotion containing rose oil.
Further, the heating-up temperature in the step a and step b is 80 DEG C.
Further, in the step c, the aqueous phase and the oil phase are heated to 80 DEG C of mixing and emulsifyings, after be cooled to
50 DEG C, the rose oil that percentage by weight is 0.3-0.5% is added, is sufficiently stirred and it is emulsified completely, be cooled to room temperature, it is old
Change, obtain lotion.
Further, in the step a, also need to add the Sodium Hyaluronate that percentage by weight is 0.1-0.5%, stir to institute
Sodium Hyaluronate is stated to be dissolved completely in the deionized water.
Further, in the step a, add the ceramide that percentage by weight is 0.5-2% and stir to being completely dissolved
In the deionized water.
Further, the vegetable oil includes percentage by weight for 3% evening primrose oil and 5-7% SIMMONDSIA CHINENSIS SEED OIL.
Further, also need to add the vitamin E that percentage by weight is 0.5-1.5% in the step c, fully mix.
Further, the MAP and 2- for the 1-1.5% that percentage by weight is are added in the step c
3% titanium dioxide, fully mix.
On the other hand azalaic acid compound acne-removing cream containing rose oil prepared by a kind of method as described above is provided.
Compared with the prior art the beneficial effects of the present invention are：Azalaic acid and rose oil are all natural plant extractions
Thing, the appropriate non-stimulated fanout free region of skin using to people, easily absorb, azalaic acid and rose oil are used simultaneously, rose
Oil can be remarkably reinforced the anti-acne effect of azalaic acid, and have the characteristics that wrinkle, light spot, pore refining, anti-aging, the anti-acne
Ointment preparation is simple, economical and efficient, short preparation period, natural pollution-free, and product property is stable, emulsifying effectiveness is good.
Embodiment
Embodiment 1
A kind of preparation method of the azalaic acid compound acne-removing cream containing rose oil, it is characterised in that comprise the following steps：
A) preparation of aqueous phase：Azalaic acid and 0.1-0.5% Sodium Hyaluronate that percentage by weight is 10-20% are added
Enter in the deionized water for being 40-65% to percentage by weight, be heated to 80-85 DEG C, add 1-1.5% chitosan, 5% the third
Glycol, 0.5-2% ceramide mix, standby；Azalaic acid has potent antibacterial sterilizing function, and has the smooth flesh of whitening
Skin, reduce the effect of pore, Sodium Hyaluronate has a skin care, moisturizing, it is crease-resistant, make the flexible effect of skin smooth, god
Through acid amides with skin anti-aging function is strengthened, skin is made to keep elasticity, it is smooth careful, reduce the effect of facial wrinkles are formed；
Under conditions of 80-85 DEG C, azalaic acid can not only be fully emulsified, and uniform dissolution in deionized water, improves azalaic acid
Permeability, stability, avoid the occurrence of demulsification, additionally it is possible to fully reacted with chitosan, generation dissolubility it is good
Chitosan azalea hydrochlorate, while propane diols further enhances the stability of azalaic acid, at such a temperature, additionally it is possible to ensure production
The abundant sterilizing of product.Solution temperature is less than 80 DEG C, and sterilizing is incomplete, and temperature is higher than 85 DEG C, is uprised for horsepower requirements, also easily
Destroy the stability of each composition.
B) preparation of oil phase：Cetostearyl alcohol and cetearyl glucoside that percentage by weight is 0.5-1% are mixed
Thing, 1-2% stearines, 1.5-2% PEG-5 stearines, 3% evening primrose oil, 5-7% SIMMONDSIA CHINENSIS SEED OIL
Mix and be heated to 80-85 DEG C, it is fully melted, it is standby；Evening primrose oil can reconcile emulsion, creams etc., SIMMONDSIA CHINENSIS SEED OIL tool
Have a high-temperature stability, and can osmotic absorption and softening skin cutin rapidly, allow skin to become soft flexible.
C) preparation of lotion：The aqueous phase and the oil phase are heated to 80-85 DEG C of mixing and emulsifying, after be cooled to 40-60
DEG C, addition percentage by weight is 0.3-0.5% rose oil, 0.5-1.5% vitamin E, 1-1.5% ascorbic acid phosphorus
The titanium dioxide of acid esters magnesium and 2-3%, it is sufficiently stirred and it is emulsified completely, be cooled to room temperature, is aged, obtains containing rose oil
Azalaic acid compound acne-removing cream lotion；Azalaic acid can not be maintained at the characteristic of uniform dissolution in aqueous phase at normal temperatures, in 80-
Cetostearyl alcohol and cetearyl glucoside mixture are added at 85 DEG C can ensure that azalaic acid forms stable and uniform and disperseed
Lotion；Stearine and PEG-5 stearines further ensure azalaic acid and can emulsified completely, are formed steady
Fixed lotion；MAP has reduction melanin, has the function that freckle removing and whitening, goes wrinkle, anti-aging, titanium dioxide
Titanium has white-skinned face function, has auxiliary and the effect consolidated for anti-acne.Rose oil be used alone can make skin smooth it is fine and smooth,
Smooth away wrinkles, light spot, azalaic acid, which is used alone, can directly suppress and kill skin surface and intrafollicular bacterium, eliminate cause of disease
Body, the generation and effect of inhibitory activity oxygen radical, be advantageous to anti-inflammatory, but rose oil and azalaic acid use simultaneously can make
Skin pore is penetrating, and penetration is strong, and rose oil can bring azalaic acid into skin depths, focus of going directly, eliminates germ, reaches
Anti-acne, whitening, the effect of light spot, effect is each used alone than its and is multiplied.
Embodiment 2
A kind of preparation method of the azalaic acid compound acne-removing skin makeup cream containing rose oil, comprises the following steps：
A) preparation of aqueous phase：10g azalaic acids are added in 65g deionized waters and are heated to 80 DEG C, add 1g shell
Glycan and with 5g propane diols, mix, it is standby；
B) preparation of oil phase：By 0.8g cetostearyl alcohols and cetearyl glucoside mixture, 1.5g glycerol stearates
Ester, 1.6gPEG-5 stearines, 8g SIMMONDSIA CHINENSIS SEED OILs are heated to 80 DEG C and make them fully melt oil phase is made, standby；
C) preparation of lotion：By aqueous phase and oil phase heating 80-85 degree mixing and emulsifyings, 50 DEG C of addition 0.3g roses are cooled to
Oil, stir and make its emulsification, room temperature is cooled to after emulsification, after being aged 24 hours, obtain the azalaic acid compound containing rose oil
Anti-acne skin makeup cream.
Embodiment 3
A kind of preparation method of the azalaic acid compound acne-removing skin makeup cream containing rose oil, comprises the following steps：
A) preparation of aqueous phase：10g azalaic acids and 0.1g Sodium Hyaluronates are added in 65g deionized waters and are heated to 80
DEG C, 5g propane diols, 1g chitosans, 0.5g2% ceramides are added, is mixed, it is standby；
B) preparation of oil phase：By 0.5g cetostearyl alcohols and cetearyl glucoside mixture, 1g stearines,
1.5gPEG-5 stearines, 3g evening primrose oil, the mixing of 5g SIMMONDSIA CHINENSIS SEED OILs, are heated to 80 DEG C and make it fully melt oil is made
It is mutually standby, it is standby；
C) preparation of lotion：Aqueous phase and oil phase are heated to 80 DEG C of mixing and emulsifyings, after be cooled to 40 DEG C of addition 0.3g roses
The vitamin E of caul-fat and 0.5g, stir and make its emulsification, room temperature is cooled to after emulsification, after being aged 24 hours, obtain containing rose
The azalaic acid compound acne-removing skin makeup cream of oil.
Embodiment 4
A kind of preparation method of the azalaic acid compound acne-removing skin makeup cream containing rose oil, comprises the following steps：
A) preparation of aqueous phase：20g azalaic acids and 0.5g Sodium Hyaluronates are added in 50g deionized waters and are heated to 85
DEG C, 5g propane diols, 1.5g chitosans, 1g2% ceramides are added, is mixed, it is standby；
B) preparation of oil phase：By 1g cetostearyl alcohols and cetearyl glucoside mixture, 2g stearines,
2gPEG-5 stearines, 3g evening primrose oil, the mixing of 7g SIMMONDSIA CHINENSIS SEED OILs, are heated to 85 DEG C and make them fully melt oil is made
It is mutually standby, it is standby；
C) preparation of lotion：Aqueous phase and oil phase are heated to 85 DEG C of mixing and emulsifyings, after be cooled to 60 DEG C of addition 0.5g roses
Caul-fat, stir and make its emulsification, room temperature is cooled to after emulsification, after being aged 24 hours, obtain the azalaic acid containing rose oil and answer
Square anti-acne skin makeup cream.
Embodiment 5
This embodiment 3 it is different simply 1g MAPs and 2g titanium dioxides are also added into step c
Titanium.
Embodiment 6
This embodiment 5 it is different simply 1.5g MAPs and 3g dioxies are also added into step c
Change titanium.
Embodiment 6
A kind of preparation method of the azalaic acid compound acne-removing skin makeup cream containing rose oil, comprises the following steps：
A) preparation of aqueous phase：18g azalaic acids and 0.1g Sodium Hyaluronates are soluble in water, are heated to 85 DEG C and add 5g third again
Glycol, 1.5g chitosans, 1g2% ceramides, stirring and dissolving are standby into aqueous phase；
B) preparation of oil phase：By 1g cetostearyl alcohols and cetearyl glucoside, 2g stearines, 2gPEG-5
Stearine, 3g evening primrose oil, the mixing of 6g SIMMONDSIA CHINENSIS SEED OILs, be heated to 80 DEG C it is fully melted that oil phase is made is standby；
C) preparation of lotion：Aqueous phase and oil phase are heated to 80-85 DEG C of mixing and emulsifying, are cooled to 50 DEG C of addition 0.5g roses
Caul-fat, 1g vitamin Es and preservative, stir and make its emulsification, room temperature is cooled to after emulsification, after being aged 24 hours, obtain 100g
The azalaic acid compound acne-removing skin makeup cream containing rose oil.
Use case：
It is as follows using the azalaic acid compound acne-removing skin makeup cream containing rose oil and the Contrast on effect case of commercially available Whelk-eliminating paste
Shown in table：
More than it was found from specific case, the azalaic acid compound acne-removing skin makeup cream anti-acne effect containing rose oil is obvious, day
It is so non-stimulated, the skin problem that whelk is brought can be effectively improved, while whitening, moisturizing, crease-resistant, light spot etc. can be played and made
With.
Presently preferred embodiments of the present invention is the foregoing is only, is merely illustrative for the purpose of the present invention, and it is non-limiting
's.Those skilled in the art understands, many changes can be carried out to it in the spirit and scope that the claims in the present invention are limited
And modification, or even it is equivalent, but fall within protection scope of the present invention.
Claims (9)
1. a kind of preparation method of the azalaic acid compound acne-removing cream containing rose oil, it is characterised in that comprise the following steps：
A) preparation of aqueous phase：It is going for 40-65% that the azalaic acid that percentage by weight is 10-20% is added into percentage by weight
In ionized water, 80-85 DEG C is heated to, the chitosan and 5% propane diols for adding 1-1.5% mix, standby；
B) preparation of oil phase：By the cetostearyl alcohol and cetearyl glucoside mixture, 1- that percentage by weight is 0.5-1%
2% stearine, 1.5-2% PEG-5 stearines, 8-10% vegetable oil mix and are heated to 80-85 DEG C, make
It fully melts, standby；
C) preparation of lotion：The aqueous phase and the oil phase are heated to 80-85 DEG C of mixing and emulsifying, after be cooled to 40-60 DEG C, add
Enter the rose oil that percentage by weight is 0.3-0.5%, be sufficiently stirred and it is emulsified completely, be cooled to room temperature, be aged, obtain
Compound lotion.
2. the preparation method of the azalaic acid compound acne-removing cream according to claim 1 containing rose oil, it is characterised in that
Heating-up temperature in the step a and step b is 80 DEG C.
3. the preparation method of the azalaic acid compound acne-removing cream according to claim 2 containing rose oil, it is characterised in that
In the step c, the aqueous phase and the oil phase are heated to 80 DEG C of mixing and emulsifyings, after be cooled to 50 DEG C, add weight hundred
Divide than the rose oil for 0.3-0.5%, be sufficiently stirred and it is emulsified completely, be cooled to room temperature, be aged, obtain lotion.
4. the preparation method of the azalaic acid compound acne-removing cream according to claim 3 containing rose oil, it is characterised in that
In the step a, also need to add the Sodium Hyaluronate that percentage by weight is 0.1-0.5%, stir complete to the Sodium Hyaluronate
Fully dissolved is in the deionized water.
5. the preparation method of the azalaic acid compound acne-removing cream according to claim 4 containing rose oil, it is characterised in that
In the step a, also need to add the ceramide that percentage by weight is 0.5-2%, stirring to be dissolved completely in it is described go from
In sub- water.
6. the preparation method of the azalaic acid compound acne-removing cream according to claim 3 containing rose oil, it is characterised in that
The vegetable oil includes the evening primrose oil that percentage by weight is 3% and 5-7% SIMMONDSIA CHINENSIS SEED OIL.
7. the preparation method of the azalaic acid compound acne-removing cream according to claim 6 containing rose oil, it is characterised in that
Also need to add the vitamin E that percentage by weight is 0.5-1.5% in the step c, fully mix.
8. the preparation method of the azalaic acid compound acne-removing cream according to claim 3 containing rose oil, it is characterised in that
Percentage by weight is added in the step c as 1-1.5% MAP and 2-3% titanium dioxide, fully
Mix.
A kind of 9. azalaic acid compound acne-removing containing rose oil prepared by preparation method as described in 1-8 any claims
Cream.
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2017019951A2 (en) * | 2015-07-30 | 2017-02-02 | Curology, Inc. | Compositions amd methods of treating acne and photoaging |
| CN111514162A (en) * | 2020-06-17 | 2020-08-11 | 禾大西普化学（四川）有限公司 | Azelaic acid/titanium dioxide hybrid composite material and preparation method thereof |
| CN112494416A (en) * | 2020-12-29 | 2021-03-16 | 贵州省植物园 | Skin care product using azalea extract and preparation method thereof |
| CN114601770A (en) * | 2022-04-24 | 2022-06-10 | 广州市白云莱茵化妆品厂 | Skin care product with acne removing and whitening effects |
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| EP0676198B1 (en) * | 1994-04-05 | 1998-10-07 | Agis Industries (1983) Ltd | Fungicidal compositions containing a combination of bifonazole and fluocinonide |
| CN1137911A (en) * | 1995-06-15 | 1996-12-18 | 鲁光 | Cuochuangjing face cream for curing acne |
| US5977277A (en) * | 1995-08-23 | 1999-11-02 | Mitsui Petrochemical Industries, Ltd | Acrylic ester, novel allyl ether, novel allyl carbonate, acrylic ester polymer, allyl ether polymer, allyl carbonate polymer and polymeric solid electrolyte |
| US6342486B1 (en) * | 1996-07-19 | 2002-01-29 | Mibelle Ag Cosmetics | Polymer glucan ether derivatives, their manufacturing as well as their use |
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