CN102178611B - High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof - Google Patents
High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof Download PDFInfo
- Publication number
- CN102178611B CN102178611B CN 201110101005 CN201110101005A CN102178611B CN 102178611 B CN102178611 B CN 102178611B CN 201110101005 CN201110101005 CN 201110101005 CN 201110101005 A CN201110101005 A CN 201110101005A CN 102178611 B CN102178611 B CN 102178611B
- Authority
- CN
- China
- Prior art keywords
- lustre
- soap base
- pearly
- composition
- fatty acids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Cosmetics (AREA)
Abstract
The invention relates to high-pearly-lustre high-foam soap base cleansing cream comprising the following constituents in percentage by weight: 32-36% of fatty acid, 14-22% of polyalcohol, 6.5-8% of potassium hydroxide, 1-4% of sodium L-lactic acid, 0.5-10% of anionic surface active agent, 0.2-4% of non-ionic surface active agent and the balance of deionized water. A preparation method of the soap base cleansing cream comprises the following steps of: A, adding the sodium L-lactic acid with a weight percentage of 1-4% into the ingredients of the soap base cleansing cream taking the fatty acid as the main material and placing into a reaction kettle; B, slowly heating to 70-78 DEG C under a normal pressure and stirring at a rotating speed of 300-500 revolutions per minute in the mean time; and C, keeping the temperature and stirring for 30-35 minutes, and then cooling to a normal temperature to obtain the high-pearly-lustre high-foam soap base cleansing cream. The high-pearly-lustre high-foam soap base cleansing cream provided by the invention has the characteristics of very fine foam and high-pearly lustre, meanwhile, the production technology is easy to control, and the gel state material is not generated.
Description
Technical field
The present invention relates to cosmetic composition, high foamy soap base facial cleaning cream of especially a kind of high pearly-lustre and preparation method thereof.
Background technology
In popular in the market clean the product, clean product of soap base class is more and more, and all there is sophisticated product in not only a lot of international major companies, and domestic a lot of daily use chemicals enterprise is also at clean product of soap base class of constantly releasing each conception of species.Clean product of soap base class has excellent washability, washes back skin sense along sliding bath sense and salubrious, receives liking of Chinese Consumer's especially.
Soap base class facial cleaning cream great majority for fatty acid and potassium hydroxide not exclusively neutralization form, wherein can add again some polyhydric alcohol be used for dispersion, stablize, moisture-keeping function.Behind the facial cleaning cream batching appropriate reaction that with the fatty acid is primary raw material, unneutralized fatty acid can provide some rich fat effect and pearlescent appearance.Excellent soap base facial cleaning cream should have good foam, also good pearly-lustre will be arranged simultaneously.If reach excellent foam, in general low carbon fatty acid content wants high, and degree of neutralization wants high; Good if desired pearly-lustre then needs a certain amount of higher aliphatic acid.But in actual production process, a large amount of gel state materials can occur, viscosity is very high, and these gel state materials often are attached on the stirring paddle and can't be uniformly dispersed, and operation is difficulty very.In order to overcome above-mentioned situation; Solve the problem that the gel state material disperses airplane crash; Needing to add big weight polyalcohol in the production process helps disperse; Generally need to drop into that polyhydric alcohol just can make the gel state material be uniformly dispersed more than 0.25 kilogram in per 1 kilogram of facial cleaning cream batching, the injected volume of polyhydric alcohol has reached more than 25%.Though a large amount of addings of polyhydric alcohol can solve the scattering problem in the production process, can cause the facial cleaning cream pearl effect poor, make that the soap base facial cleaning cream is difficult to have excellent foam and good pearly-lustre simultaneously.
Summary of the invention
The technical problem that the present invention will solve is, a kind of excellent foam that both had is provided, and has the high foamy soap base facial cleaning cream of high pearly-lustre of high pearly-lustre characteristic again; The present invention also provides the method for preparing of the high foamy soap base facial cleaning cream of a kind of high pearly-lustre, and this method has production technology to be controlled easily, can not produce the advantage of gel state material.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is: the high foamy soap base facial cleaning cream of a kind of high pearly-lustre, and it is characterized in that: by weight percentage, it comprises following component:
Among the present invention, fatty acid and potassium hydroxide generation saponification generate soap; Have good clean result, unreacted fatty acid can provide milky white product appearance to pearly-lustre, and polyhydric alcohol is used to disperse fatty acid soaps; Make production easy to operate, and provide low-temperature stability to reach the moistening effect to skin, the adding of D-lactic acid sodium can further improve the dispersibility of fatty acid soaps; Reduce the addition of polyhydric alcohol, make production more be prone to carry out, pearl effect is better.
As preferred version of the present invention, the percentage by weight of said D-lactic acid sodium is 1～3%.
Said fatty acid is a kind of in tetradecacarbon fatty acid, 16 carbon fatty acids, the stearic acid or their mixture.Certainly, the fatty acid among the present invention also can adopt 12 carbon fatty acids or 22 carbon fatty acids.
Said polyhydric alcohol is a kind of in glycerol, 1,3 butanediol or their mixture.Certainly, the polyhydric alcohol among the present invention also can adopt a kind of in propylene glycol, the PEG400 or their mixture.
Said anion surfactant is a cocos nucifera oil acyl glycine potassium, a kind of in the lauroyl collagen amino acid triethanolamine or their mixture.Anion surfactant also can adopt cocos nucifera oil acyl methyl taurine sodium.
Said non-ionic surface active agent is a kind of in glyceryl stearate, the cetearyl ether-30 or their mixture.Certainly, non-ionic surface active agent also can adopt a kind of in cetearyl ether-20, the hard ester acid esters of tristerin/PEG-100 or their mixture.
Also be added with percentage by weight in the high foamy soap base facial cleaning cream of said high pearly-lustre and be 0.01～0.3% hydroxypropyl emthylcellulose.Hydroxypropyl emthylcellulose can be used as dispersant, and material is uniformly dispersed.
Also be added with percentage by weight in the high foamy soap base facial cleaning cream of said high pearly-lustre and be 0.01%～0.3% methyl hydroxybenzoate and percentage by weight and be 0.01% the different plug azoles of methyl quinoline ketone.The different plug azoles of methyl hydroxybenzoate and methyl quinoline ketone can play antibacterial, antiseptical effect.
The present invention adopts D-lactic acid sodium to cooperate the dispersibility that improves soap base facial cleaning cream production material with polyhydric alcohol; Can reduce the consumption of polyhydric alcohol, reduce the production cost of soap base facial cleaning cream, in the process of producing, also can not produce the gel state material; Its production technology is simple, good operation.The present invention can possess excellent spumescence and good pearly-lustre characteristic simultaneously, has solved the technical barrier of always thirsting for solution in the prior art.
The method for preparing of the high foamy soap base facial cleaning cream of high pearly-lustre, take following steps:
A, in the soap base facial cleaning cream batching that with the fatty acid is primary raw material, to add percentage by weight be 1～4% D-lactic acid sodium, inserts in the agitated reactor then;
B, normal pressure slowly are heated to 70-78 ℃, and the rotating speed that changes with per minute 300-350 simultaneously stirs;
C, insulation 30-35 minute are cooled to room temperature then, get the high foamy soap base facial cleaning cream of high pearly-lustre.
This method is added 1～4% D-lactic acid sodium in the production process of preparation soap base facial cleaning cream, can strengthen the soap dispersibility of polyhydric alcohol, reduces the consumption of polyhydric alcohol; Can not produce the gel state material in the production process, material is uniformly dispersed, and makes production process control well, and is simple to operation, and products obtained therefrom had both had excellent foam simultaneously, had good pearly-lustre again.
A large amount of contrast experiments have been in the effect of invention artificial confirmation D-lactic acid sodium in the soap base facial cleaning cream, for example: will comprise 20% tetradecacarbon fatty acid, 6% 16 carbon fatty acid, 8% stearic material input agitated reactor; Be under 86% the situation at degree of neutralization, need to add 20% glycerol and 10% 1,3 butanols; Could guarantee to carry out smoothly in production process; Production process can not produce too much gel state material, though product has better foam, pearl effect is relatively poor.To comprise 20% tetradecacarbon fatty acid, 6% 16 carbon fatty acid, 8% stearic material drops into agitated reactor, adds 1.5% D-lactic acid sodium simultaneously, is under 86% the situation at degree of neutralization; Only need to add 1 of 16% glycerol and 2%; 3 butanediols just can guarantee not occur more difficult dispersive gel in the production process, and material is uniformly dispersed; And the product pearly-lustre is beautiful, has excellent foam simultaneously again.Above percentage ratio all is weight percentage.
In sum, the present invention has and uses polyhydric alcohol less, and cost is lower, and has the beneficial effect of excellent spumescence and good pearly-lustre characteristic simultaneously; It is simple that method of the present invention has technology, good operation, and material is uniformly dispersed, and can not produce the beneficial effect of gel state material.
The specific embodiment
The following example is used for exemplary the present invention, but the scope that does not limit the present invention in any way.
Embodiment 1:
The high foamy soap base facial cleaning cream of a kind of high pearly-lustre takes by weighing material as following weight percent:
Above-mentioned material is added agitated reactor, slowly be heated to 70 ℃ under the normal pressure, the rotating speed that changes with per minute 300 simultaneously stirs, and stirs, and is incubated 35 minutes; Be cooled to pearly-lustre then and separate out fully, promptly get the high foamy soap base facial cleaning cream finished product of high pearly-lustre.
Claims (5)
1. the high foamy soap base facial cleaning cream of one kind high pearly-lustre, it is characterized in that: by weight percentage, it comprises following component:
Said fatty acid is selected from tetradecacarbon fatty acid, 16 carbon fatty acids, stearic acid and composition thereof, or 12 carbon fatty acids, or 22 carbon fatty acids;
Said polyhydric alcohol is selected from glycerol, 1,3 butanediol and composition thereof, or a kind of in the propylene glycol, PEG400 or their mixture;
Said anion surfactant is selected from cocos nucifera oil acyl glycine potassium, lauroyl collagen amino acid triethanolamine and composition thereof, or cocos nucifera oil acyl methyl taurine sodium;
Said non-ionic surface active agent is selected from glyceryl stearate, cetearyl ether-30 and composition thereof, or a kind of in the cetearyl ether-20, tristerin/PEG-100 stearate or their mixture.
2. according to the high foamy soap base facial cleaning cream of the high pearly-lustre of claim 1, it is characterized in that: the percentage by weight of said D-lactic acid sodium is 1～3%.
3. the high foamy soap base facial cleaning cream of one kind high pearly-lustre, it is characterized in that: by weight percentage, it comprises following component:
Said fatty acid is selected from tetradecacarbon fatty acid, 16 carbon fatty acids, stearic acid and composition thereof, or 12 carbon fatty acids, or 22 carbon fatty acids;
Said polyhydric alcohol is selected from glycerol, 1,3 butanediol and composition thereof, or a kind of in the propylene glycol, PEG400 or their mixture;
Said anion surfactant is selected from cocos nucifera oil acyl glycine potassium, lauroyl collagen amino acid triethanolamine and composition thereof, or cocos nucifera oil acyl methyl taurine sodium;
Said non-ionic surface active agent is selected from glyceryl stearate, cetearyl ether-30 and composition thereof, or a kind of in the cetearyl ether-20, tristerin/PEG-100 stearate or their mixture.
4. the high foamy soap base facial cleaning cream of one kind high pearly-lustre, it is characterized in that: by weight percentage, it comprises following component:
Said fatty acid is selected from tetradecacarbon fatty acid, 16 carbon fatty acids, stearic acid and composition thereof, or 12 carbon fatty acids, or 22 carbon fatty acids;
Said polyhydric alcohol is selected from glycerol, 1,3 butanediol and composition thereof, or a kind of in the propylene glycol, PEG400 or their mixture;
Said anion surfactant is selected from cocos nucifera oil acyl glycine potassium, lauroyl collagen amino acid triethanolamine and composition thereof, or cocos nucifera oil acyl methyl taurine sodium;
Said non-ionic surface active agent is selected from glyceryl stearate, cetearyl ether-30 and composition thereof, or a kind of in the cetearyl ether-20, tristerin/PEG-100 stearate or their mixture.
5. the method for preparing of the high foamy soap base facial cleaning cream of each described high pearly-lustre of a claim 1-4 may further comprise the steps:
A, in the soap base facial cleaning cream batching that with the fatty acid is primary raw material, to add percentage by weight be 1～4% D-lactic acid sodium, inserts in the agitated reactor then;
B, normal pressure slowly are heated to 70 ℃-78 ℃, and the rotating speed that changes with per minute 300-500 simultaneously stirs;
C, insulated and stirred 30-35 minute, be cooled to room temperature then, the high foamy soap base facial cleaning cream of high pearly-lustre.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110101005 CN102178611B (en) | 2011-04-22 | 2011-04-22 | High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110101005 CN102178611B (en) | 2011-04-22 | 2011-04-22 | High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102178611A CN102178611A (en) | 2011-09-14 |
| CN102178611B true CN102178611B (en) | 2012-12-05 |
Family
ID=44565020
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110101005 Active CN102178611B (en) | 2011-04-22 | 2011-04-22 | High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102178611B (en) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103126911B (en) * | 2011-11-30 | 2015-09-09 | 南京华狮化工有限公司 | A kind of Soap-base facial cleanser compositions of gentleness and production technology thereof |
| CN103301051B (en) * | 2012-03-07 | 2015-01-21 | 南京华狮化工有限公司 | Transparent beauty treatment soap composition |
| CN103113997B (en) * | 2013-03-11 | 2014-10-29 | 河南正通化工有限公司 | Food-grade detergent and preparation method thereof |
| CN103142423B (en) * | 2013-04-01 | 2014-09-03 | 珀莱雅化妆品股份有限公司 | Soap-based cleansing cream not generating soap scum |
| CN103356400A (en) * | 2013-07-16 | 2013-10-23 | 浙江九九红玫瑰科技有限公司 | Soap-base facial cleanser and preparation method thereof |
| CN104257567B (en) * | 2014-10-22 | 2017-09-19 | 广东幸美化妆品股份有限公司 | A kind of oil-control face cleaning cream and preparation method thereof |
| CN104257527A (en) * | 2014-10-22 | 2015-01-07 | 广东幸美化妆品股份有限公司 | Moisturizing facial cleanser and preparation method thereof |
| CN105296195B (en) * | 2015-10-21 | 2018-01-19 | 广州立白企业集团有限公司 | A kind of liquid detergent composition of in-situ preparation pearling agent particle |
| CN106619224A (en) * | 2016-12-29 | 2017-05-10 | 广州市中通生化制品有限公司 | High-temperature stable soap-based cleansing foam and preparation method thereof |
| CN106619302A (en) * | 2016-12-29 | 2017-05-10 | 广州市中通生化制品有限公司 | Mild allergy-relieving cleansing milk and preparation method thereof |
| CN107260579B (en) * | 2017-08-08 | 2019-11-19 | 广州蜜妆生物科技有限公司 | A kind of mild face cleaning bubble and preparation method thereof |
| CN107616929A (en) * | 2017-10-18 | 2018-01-23 | 中山市莱香化妆品有限公司 | One kind removes oil type face cleaning cream and preparation method thereof |
| CN108403471B (en) * | 2018-03-29 | 2020-12-01 | 深圳市兰亭科技股份有限公司 | Pearlescent composition and preparation method and application thereof |
| CN108330006A (en) * | 2018-04-16 | 2018-07-27 | 苏州龙腾万里化工科技有限公司 | Multi-functional mild leather cleaning agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1996005233A1 (en) * | 1994-08-11 | 1996-02-22 | Shiseido Co., Ltd. | Low-molecular-weight acetylated hyaluronic acid, emollient, and processes for producing and purifying the acid |
| JP2003155225A (en) * | 2001-11-16 | 2003-05-27 | Pigeon Corp | Sheet for removing sunscreen for baby |
| CN101703454A (en) * | 2009-11-03 | 2010-05-12 | 广东名臣有限公司 | Washing-off type skin cleaning and nursing composite |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0987687A (en) * | 1995-09-26 | 1997-03-31 | Nendo Kagaku Kenkyusho:Kk | Fatty acid soap containing clay minerals |
-
2011
- 2011-04-22 CN CN 201110101005 patent/CN102178611B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1996005233A1 (en) * | 1994-08-11 | 1996-02-22 | Shiseido Co., Ltd. | Low-molecular-weight acetylated hyaluronic acid, emollient, and processes for producing and purifying the acid |
| JP2003155225A (en) * | 2001-11-16 | 2003-05-27 | Pigeon Corp | Sheet for removing sunscreen for baby |
| CN101703454A (en) * | 2009-11-03 | 2010-05-12 | 广东名臣有限公司 | Washing-off type skin cleaning and nursing composite |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102178611A (en) | 2011-09-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102178611B (en) | High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof | |
| CN105062731B (en) | One kind fermentation shea butter amino acid transparent soap | |
| CN102920616B (en) | Pearly-lustre type foamingly clean facial wash and preparation method thereof | |
| CN105907501A (en) | Transparent amino acid compound soap and preparation method thereof | |
| JPS63170498A (en) | Soap composition | |
| CN107157799A (en) | A kind of soap base mildy wash | |
| CN107245394A (en) | A kind of Multifunctional cold handmade soap containing the fiery sesame oil of deer oil and preparation method thereof | |
| CN106753921A (en) | Cold handmade soap processed and preparation method thereof | |
| CN110194998A (en) | Natural plants craft cold process soap and preparation method thereof | |
| CN103932896A (en) | Nano emulsion composition capable of being smeared to cream and preparation method thereof | |
| CN105616208A (en) | Aqueous whole oil-based color makeup composition and preparation method thereof | |
| CN107304391A (en) | A kind of blue or green bur essential oil soap and its make method by hand | |
| CN107304388A (en) | A kind of Diorite essential oil soap and its make method by hand | |
| CN101530384A (en) | Ostrich oil moisturizing and whitening cream and method for preparing same | |
| KR20140081965A (en) | Cream cosmetic composition comprising micro bubble | |
| EP3487976A1 (en) | Solid soap composition | |
| CN110339136B (en) | Charming composition and preparation method thereof | |
| CN106635482A (en) | Enzyme perfumed soap and preparation method thereof | |
| JP5835951B2 (en) | Cosmetics, method for producing the same, and oil / water phase separation inhibitor | |
| CN102973472B (en) | Skin-cleaning agent composition adopting gelatin as main material and preparation method thereof | |
| CN104771346A (en) | Lemongrass liquid soap and preparation method thereof | |
| CN104970999A (en) | Makeup remover cleansing gel and preparation method thereof | |
| CN101100632A (en) | Method for preparing synthetic soap | |
| CN103740518A (en) | Honey whitening and moisture-keeping facial soap | |
| CN104116648A (en) | Universal skin moisturizer |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: PROYA (HUZHOU) COSMETIC CO., LTD. Free format text: FORMER OWNER: HANGZHOU PROYA HOLDING CO., LTD. Effective date: 20120904 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 310012 HANGZHOU, ZHEJIANG PROVINCE TO: 313000 HUZHOU, ZHEJIANG PROVINCE |
|
| TA01 | Transfer of patent application right |
Effective date of registration: 20120904 Address after: 313000 No. 16, National Road, Huzhou Industrial Park, Zhejiang Province Applicant after: proya (Huzhou) Cosmetics Co., Ltd. Address before: 310012, room 1, building No. 1601, Europe and America Center, Xihu District World Trade Fair, Hangzhou, Zhejiang, Applicant before: Hangzhou PROYA Corporation |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: PROYA COSMETICS CO., LTD. Free format text: FORMER NAME: PROYA (HUZHOU) COSMETIC CO., LTD. |
|
| CP03 | Change of name, title or address |
Address after: Hangzhou City, Zhejiang province 310012 Xihu District World Trade Center Building 1, and Richland city (area D) room 1605 Patentee after: Proya Cosmetics Co., Ltd. Address before: 313000 No. 16, National Road, Huzhou Industrial Park, Zhejiang Province Patentee before: proya (Huzhou) Cosmetics Co., Ltd. |