CN107412012A - A kind of microemulsified makeup removing gel and preparation method thereof - Google Patents

A kind of microemulsified makeup removing gel and preparation method thereof Download PDF

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Publication number
CN107412012A
CN107412012A CN201710069242.XA CN201710069242A CN107412012A CN 107412012 A CN107412012 A CN 107412012A CN 201710069242 A CN201710069242 A CN 201710069242A CN 107412012 A CN107412012 A CN 107412012A
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CN
China
Prior art keywords
microemulsified
glycerine
gel
makeup removing
stir
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710069242.XA
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Chinese (zh)
Inventor
李继承
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Ante Cosmetics Ltd By Share Ltd
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Suzhou Ante Cosmetics Ltd By Share Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Ante Cosmetics Ltd By Share Ltd filed Critical Suzhou Ante Cosmetics Ltd By Share Ltd
Priority to CN201710069242.XA priority Critical patent/CN107412012A/en
Publication of CN107412012A publication Critical patent/CN107412012A/en
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A61K8/068—Microemulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
    • A61K8/8182—Copolymers of vinyl-pyrrolidones. Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/14—Preparations for removing make-up
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Emergency Medicine (AREA)
  • Dispersion Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of microemulsified makeup removing gel and preparation method thereof, microemulsified makeup removing gel is included with component：Caprylic/capric triglyceride, glycerine triethyl group capronate, micro-emulsifier and skin detergents, olive oil, tocopherol acetate, acrylamide dimethyltaurine ammonium/VP copolymers, Sodium Hyaluronate, preservative, the diglycerol ethers of PPG 9, glycerine, butanediol, Sensiva SC50, pungent glycol, essence, deionized water surplus；The microemulsified makeup removing gel of the present invention, its makeup removing effect is good, thorough noresidue of removing ornaments and formal dress, easy to use, and has moisturizing and nourishing skin effect；Its preparation method is easily achieved, can be with scale volume production.

Description

A kind of microemulsified makeup removing gel and preparation method thereof
Technical field
The present invention relates to cosmetic field, specifically a kind of microemulsified makeup removing gel and preparation method thereof.
Background technology
The existing makeup removal products of in the market mainly have following several types：Makeup remover, make-up remover, makeup remover and makeup removing breast；Unload Adornment oil and make-up remover are typically made up of substantial amounts of mineral oil, vegetable oil, wax class, Synthetic Oil and a small amount of cleansing, right The lubricant component of color make-up has preferable dissolving power, but use is excessively greasy, and face cleaning product is also needed to after makeup removing and does emphasis cleaning；Unload Adornment water is mainly equipped with partial skin cleansing and lipid solubilization composition using water as solvent, and it dissolves to high oil content color make-up cleans Ability is very limited to be generally required to consume a longer time；Makeup removing breast has grease to the molten of color make-up between makeup remover and makeup remover Solution can make general light make-up makeup removing become easy plus the part cleaning action of emulsifying agent, but because makeup removing breast is using emulsification Agent is by obtained by grease emulsifying, and its grain diameter of grease is disperseed larger, and limited to the lipid solubilization in color make-up, emulsifying agent used is to cleaning Taking-up ability is also very limited, often more greasy feeling.
Due to above mentioned problem be present, a kind of makeup removal products for having skin-care effect concurrently than more comprehensive excellent effect are now needed To meet the consumption demand increasingly increased
The content of the invention
For above-mentioned technical problem, the purpose of the present invention is：Propose a kind of microemulsified makeup removing gel and its system Preparation Method.
What the technical solution of the present invention was realized in：A kind of microemulsified makeup removing gel, comprising below by quality point The raw material components that number calculates：Caprylic/capric triglyceride 22.0%~28.0%, glycerine triethyl group capronate 14.0%~ 19.0%th, micro-emulsifier and skin detergents 10.0%-20.0%, olive oil 6.0%-8.0%, tocopherol acetate 0.1% ~0.5%, acrylamide dimethyltaurine ammonium/VP copolymers 0.1%~0.3%, Sodium Hyaluronate 0.02%~0.05%, Preservative 0.6%~0.8%, PPG-9 diglycerols ether 1.0%~4.0%, glycerine 12.0%~18.0%, butanediol 5.0%~ 9.0%th, Sensiva SC50 0.10%~0.20%, pungent glycol 0.10%~0.3%, essence 0.05%~0.10%, go from Sub- water surplus.
Preferably, described microemulsified and skin detergents be respectively 10.0%~15.0% octyl dodecanol polyethers -25 and 0%~5.0% Natrulon H-10 laurate.
Preferably, described preservative includes Phenoxyethanol 0.50%~0.65% and methyl p-hydroxybenzoate 0.10% ~0.15%.
Above-mentioned microemulsified makeup removing gel its preparation method comprises the following steps：
(1) micro-emulsifier and skin detergents are added into caprylic/capric triglyceride, glycerine triethyl group capronate Hybrid Heating 70 ~75 DEG C, stirring and dissolving, then olive oil, tocopherol acetate are added into stirring；
(2) acrylamide dimethyltaurine ammonium/VP copolymers, Sodium Hyaluronate are sprinkled into deionized water stir at a slow speed Mix, speed of agitator is 500~800rpm, persistently stir 30 minutes to be completely dispersed uniformly；
(3) it is then successively that PPG-9 is double by 70 DEG C or so the dissolvings of methyl p-hydroxybenzoate and Phenoxyethanol Hybrid Heating Glycerin ether, glycerine, butanediol, Sensiva SC50, pungent glycol input, are stirred 15 minutes with 300~600rpm rotating speeds；
(4) compound made from step (3) is poured at a slow speed in the obtained material of step (2) while stirring, heating 70~75 DEG C, stir；
(5) keep step (1) and step (4) made from temperature of charge be 70~75 DEG C, by material made from step (1) with 500~800rpm rotating speed is persistently stirred, and material made from step (4) is poured slowly into material made from above-mentioned steps (1), Lasting to stir and be cooled to 50 DEG C at a slow speed, addition essence persistently stirs 15 minutes.
Due to the utilization of above-mentioned technical proposal, the present invention has following advantages compared with prior art：
The microemulsified makeup removing gel of the present invention, its makeup removing effect is good, thorough noresidue of removing ornaments and formal dress, easy to use, and with guarantor Warm nourishes rough skin effect；Its preparation method is easily achieved, can be with scale volume production.
Embodiment
The present invention is further illustrated with reference to embodiment.
A kind of microemulsified makeup removing gel of the present invention, includes the following raw material components calculated as mass fraction：Octanoic acid/ Triglyceride DDD 22.0%~28.0%, glycerine three (thylhexoic acid) ester 14.0%~19.0%, microemulsified ＆ skin detergentses 10.0%~20.0%, olive (OLEA EUROPAEA) fruit oil 6.0%~8.0%, tocopherol acetate 0.1%~ 0.5%th, acrylamide dimethyltaurine ammonium/VP copolymers 0.1%-0.3%, Sodium Hyaluronate 0.02%~0.05%, anti- Rotten agent 0.6%~0.8%, PPG-9 diglycerols ether 1.0%~4.0%, glycerine 12.0%~18.0%, butanediol 5.0%~ 9.0%th, Sensiva SC50 0.10%-0.20%, pungent glycol 0.10%-0.3%, essence 0.05%~0.10%, deionization Water surplus.
Wherein, the octyl dodecanol polyethers -25 and 0% of described microemulsified ＆ skin detergentses preferably 10.0%~15.0%~ 5.0% Natrulon H-10 laurate；Described preservative includes Phenoxyethanol 0.50%~0.65% and P-hydroxybenzoic acid Methyl esters 0.10%~0.15%.
Embodiment 1-5 constituent content is as shown in the table：
Wherein, each component unit is percentage, and each raw material summation of formula in each embodiment is 100%, constituent content It is to add the component for 0.
Above-described embodiment 1-5 microemulsified makeup removing gel is prepared as follows：
(1) microemulsified ＆ skin detergentses are added into caprylic/capric triglyceride, (thylhexoic acid) ester of glycerine three Hybrid Heating 70 ~75 DEG C, stirring and dissolving, then olive (OLEA EUROPAEA) fruit oil, tocopherol acetate are added into stirring；
(2) acrylamide dimethyltaurine ammonium/VP copolymers, Sodium Hyaluronate are sprinkled into deionized water stir at a slow speed Mix, speed of agitator is 500~800rpm, persistently stir 30 minutes to be completely dispersed uniformly；
(3) it is then successively that PPG-9 is double by 70 DEG C or so the dissolvings of methyl p-hydroxybenzoate and Phenoxyethanol Hybrid Heating Glycerin ether, glycerine, butanediol, Sensiva SC50, pungent glycol input, are stirred 15 minutes with 300~600rpm rotating speeds；
(4) compound made from step (3) is poured at a slow speed in the obtained material of step (2) while stirring, heating 70~75 DEG C, stir；
(5) keep step (1) and step (4) made from temperature of charge be 70-75 DEG C, by material made from step (1) with 500~800rpm rotating speed is persistently stirred, and material made from step (4) is poured slowly into material made from above-mentioned steps (1), Lasting to stir and be cooled to 50 DEG C at a slow speed, addition essence persistently stirs 15 minutes.
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow person skilled in the art Scholar can understand present disclosure and be carried out, and it is not intended to limit the scope of the present invention, all according to the present invention The equivalent change or modification that Spirit Essence is made, it should all cover within the scope of the present invention.

Claims (4)

  1. The gel 1. a kind of microemulsified is removed ornaments and formal dress, it is characterised in that include the following raw material components calculated as mass fraction：Octanoic acid/the last of the ten Heavenly stems Acid glycerol three ester 22.0%~28.0%, glycerine triethyl group capronate 14.0%~19.0%, micro-emulsifier and skin detergents 10.0%~ 20.0%th, olive oil 6.0%~8.0%, tocopherol acetate 0.1%~0.5%, acrylamide dimethyltaurine ammonium/VP are common Polymers 0.1%~0.3%, Sodium Hyaluronate 0.02%~0.05%, preservative 0.6%~0.8%, PPG-9 diglycerols ether 1.0%~ 4.0%th, glycerine 12.0%~18.0%, butanediol 5.0%~9.0%, Sensiva SC50 0.10%~0.20%, pungent glycol 0.10%~ 0.3%th, essence 0.05%~0.10%, deionized water surplus.
  2. The gel 2. microemulsified according to claim 1 is removed ornaments and formal dress, it is characterised in that：Described microemulsified and skin detergents be respectively The Natrulon H-10 laurate of 10.0%~15.0% octyl dodecanol polyethers -25 and 0%~5.0%.
  3. The gel 3. microemulsified according to claim 1 is removed ornaments and formal dress, it is characterised in that：Described preservative includes Phenoxyethanol 0.50%~0.65% and methyl p-hydroxybenzoate 0.10%~0.15%.
  4. 4. a kind of preparation method of microemulsified makeup removing gel as claimed in claim 1, it is characterised in that comprise the following steps：
    （1）Micro-emulsifier and skin detergents are added into caprylic/capric triglyceride, glycerine triethyl group capronate Hybrid Heating 70~75 DEG C, stirring and dissolving, then olive oil, tocopherol acetate are added into stirring；
    （2）Acrylamide dimethyltaurine ammonium/VP copolymers, Sodium Hyaluronate are sprinkled into deionized water stir at a slow speed, is stirred Mix rotating speed is 500~800rpm, persistently stir 30 minutes to be completely dispersed uniformly；
    （3）70 DEG C or so of methyl p-hydroxybenzoate and Phenoxyethanol Hybrid Heating are dissolved, then successively by PPG-9 diglycerols Ether, glycerine, butanediol, Sensiva SC50, pungent glycol input, are stirred 15 minutes with 300~600rpm rotating speeds；
    （4）While stirring by step（3）Obtained compound pours at a slow speed step（2）In obtained material, 70~75 DEG C are heated, is stirred Mix uniformly；
    （5）Keep step（1）And step（4）Obtained temperature of charge is 70~75 DEG C, by step（1）Obtained material is with 500 ~800rpm rotating speed persistently stirs, by step（4）Obtained material is poured slowly into above-mentioned steps（1）In obtained material, hold Continue and stir and be cooled at a slow speed 50 DEG C, add essence and persistently stir 15 minutes.
CN201710069242.XA 2017-02-09 2017-02-09 A kind of microemulsified makeup removing gel and preparation method thereof Pending CN107412012A (en)

Priority Applications (1)

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CN201710069242.XA CN107412012A (en) 2017-02-09 2017-02-09 A kind of microemulsified makeup removing gel and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201710069242.XA CN107412012A (en) 2017-02-09 2017-02-09 A kind of microemulsified makeup removing gel and preparation method thereof

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109662909A (en) * 2019-01-28 2019-04-23 广州尊伊化妆品有限公司 Cleansing oil gel essence with self-emulsifying skin moistening effect and preparation method thereof
CN110755283A (en) * 2019-11-05 2020-02-07 广州欧卡娜化妆品有限公司 Nano micro-emulsified makeup removing lotion and preparation method thereof
CN115645310A (en) * 2022-10-10 2023-01-31 上海臻臣化妆品有限公司 Cleansing gel and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1849109A (en) * 2003-09-10 2006-10-18 宝洁公司 Skin care composition
CN104367516A (en) * 2014-11-24 2015-02-25 广州神采化妆品有限公司 Mild eye and lip cleansing gel and preparation method thereof
CN106333898A (en) * 2016-10-08 2017-01-18 广州丹奇日用化工厂有限公司 Multi-moisturizing double-layer makeup remover and preparation method thereof
CN106726770A (en) * 2016-12-28 2017-05-31 广州环亚化妆品科技有限公司 A kind of makeup removing micelle composition and preparation method thereof and the application in makeup remover

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1849109A (en) * 2003-09-10 2006-10-18 宝洁公司 Skin care composition
CN100435779C (en) * 2003-09-10 2008-11-26 宝洁公司 Skin care composition
CN104367516A (en) * 2014-11-24 2015-02-25 广州神采化妆品有限公司 Mild eye and lip cleansing gel and preparation method thereof
CN106333898A (en) * 2016-10-08 2017-01-18 广州丹奇日用化工厂有限公司 Multi-moisturizing double-layer makeup remover and preparation method thereof
CN106726770A (en) * 2016-12-28 2017-05-31 广州环亚化妆品科技有限公司 A kind of makeup removing micelle composition and preparation method thereof and the application in makeup remover

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裘炳毅等: "《现代化妆品科学与技术》", 31 March 2016, 中国轻工业出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109662909A (en) * 2019-01-28 2019-04-23 广州尊伊化妆品有限公司 Cleansing oil gel essence with self-emulsifying skin moistening effect and preparation method thereof
CN110755283A (en) * 2019-11-05 2020-02-07 广州欧卡娜化妆品有限公司 Nano micro-emulsified makeup removing lotion and preparation method thereof
CN115645310A (en) * 2022-10-10 2023-01-31 上海臻臣化妆品有限公司 Cleansing gel and preparation method thereof

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