CN105832572B - Amino acid facial cleanser and preparation method thereof - Google Patents
Amino acid facial cleanser and preparation method thereof Download PDFInfo
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- CN105832572B CN105832572B CN201610213333.1A CN201610213333A CN105832572B CN 105832572 B CN105832572 B CN 105832572B CN 201610213333 A CN201610213333 A CN 201610213333A CN 105832572 B CN105832572 B CN 105832572B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8182—Copolymers of vinyl-pyrrolidones. Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Abstract
The present invention relates to a kind of amino acid facial cleanser and preparation method thereof, the amino acid facial cleanser includes following components:Sodium cocoyl glutamate, cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3 butanediols, PEG400, sorbierite, methyl bay sodium acyl taurine, lauryl hydroxyl sulfo betaine, potassium hydroxide, polyquaternium cationoid surfactant, emulsifier, dispersant, sodium chloride, essence, preservative, deionized water.Amino acid facial cleanser prepared by the present invention is mildly non-stimulated, and pro-skin moisture retention is good, has abundant dense foam, washes that rear skin cleanliness factor is good, and stability is good, and lotion appearance pearly-lustre exquisiteness is soft and smooth, and has best knot cream temperature.
Description
Technical field
The present invention relates to cosmetic fields, more particularly to a kind of amino acid facial cleanser and preparation method thereof.
Background technology
What traditional facial cleanser was focused on is all high-efficiency cleaning, pore cleanser, deoils, and but has ignored product itself to skin
Stimulation adds the extremely strong surfactant of alkalinity to improve cleaning force and ability of deoiling, foaming agent, the ingredients such as soap base,
And the skin of human body is weakly acidic, use for a long time can stimulate skin.More seriously, the sebum film of skin can also be broken
It is bad.Once losing sebum film, skin is highly susceptible to external injury.And amino acid facial cleanser is most pro-skin temperature in all facial cleansers
The facial cleanser of sum.Mild pro-skin, low stimulation, sensitive skin can use.
Although amino acid cleansing cream has many advantages, but in technical aspect, but there are still many deficiencies at present, such as：It is difficult
The problems such as cream point is low, lotion is thick, stability is poor is tied in thickening, and the facial cleanser that especially prepared by the work of single amino acid class table has bubble
Foam is not abundant enough, cleaning force not enough, the problem of not washing clean.
The most basic effect of face cleaning cream is that clean surface portion skin, general amino acid cleansing cream target user are dry mostly
Property, sensitive because foam is not abundant enough be loose bulla, easily disappear, cleaning dynamics is inadequate.And when the skin of summer people
Generally oil, mixed type, cleaning force can not enough cause skin to have extra fat residue to skin partially, block pore, influence use feeling, together
When as skin cleaning the problems such as being not thorough and generating small pox acne blackhead.For face cleaning product, enrich thin
Greasy foam can not only influence the cleaning capacity of product, while can also influence the use feeling of consumer.
Amino acid cleansing cream system difficulty thickens, and is embodied in the lotion for being difficult to that lotion is made to profile bar shape, most of at present
Amino acid system mainly uses two methods of thickening method, crystallisation to prepare lotion.Crystallisation adds a large amount of powder of amino acids,
Cause lotion knot cream harder, lotion is coarse, makes troubles to production is filling, simultaneously because lotion is too hard, is not easy to squeeze out hose,
Influence the use feeling of consumer.The lotion prepared using thickening method, the phenomenon that often will appear low temperature jelly conglomeration, cryogenic conditions
Lower lotion meets water and is not easy to melt, and influences to blister, to influence the use feeling of consumer.
The stability of amino acid lotion is more difficult to control, and there are the test water outlet of room temperature shelf is thinning for general amino acid cleansing breast
The problem of, the problem of lotion is hardened under cryogenic conditions, jelly, conglomeration and it is heat-resisting after lotion layering, return thick problem.
The height of amino acid cleansing cream knot cream point influences production efficiency, and knot cream point is low (38 DEG C or less), and the time of cooling is long,
Especially in summer, the temperature of recirculated cooling water will make material body be cooled to 38 DEG C hereinafter, when cooling between 30-40 DEG C
Between it is longer, or by cooling water refrigeration need to consume more energy, cause production efficiency to reduce.
Invention content
Based on this, it is necessary in view of the above-mentioned problems, providing a kind of amino acid facial cleanser and preparation method thereof.
Specific technical solution is as follows：
A kind of amino acid facial cleanser, by percentage to the quality comprising following components：
The solid content of the methyl bay sodium acyl taurine is 50~60%.
Sorbierite used is the sorbitol solution of 69~71wt% in the present invention, for sorbierite in cosmetic industry production
Common form, as long as the amount of contained sorbierite is consistent with the present invention, it is also possible to which the sorbierite of other concentration or form substitutes.
Methyl bay sodium acyl taurine (50~60% solid content) used is methyl in cosmetic industry production in the present invention
The common type of bay sodium acyl taurine, as long as the amount of contained methyl bay sodium acyl taurine is consistent with the present invention, it is also possible to its
The methyl bay sodium acyl taurine of his purity substitutes.
In wherein some embodiments, by percentage to the quality, the amino acid facial cleanser includes following components：
In wherein some embodiments, by percentage to the quality, the amino acid facial cleanser includes following components：
In wherein some embodiments, the cocounut oil acyl glycine potassium, hydroxy stearic acid, tocopherol mixture quality
Percentage matches：Cocounut oil acyl glycine potassium 70~80%, hydroxy stearic acid 20~30%, tocopherol 0.5~1.0%, it is above-mentioned
Summation is 100%.
In wherein some embodiments, the polyquaternium cationoid surfactant is polyquaternium -7, polyquaternary amine
The mixture of salt -43 and water, mass percent proportioning are：It is polyquaternium -7 3~5%, polyquaternium -43 5~7%, remaining
Amount is water.
In wherein some embodiments, the emulsifier is the mixture of PEG-100 stearates and stearine,
Its mass percent matches：PEG-100 stearates 40~60%, stearine 40~60%.
In wherein some embodiments, the dispersant is that PEG/PPG-25/30 polymer and PEG/PPG-10/30 polymerize
The mixture of object, mass percent proportioning are：PEG/PPG-25/30 polymer 90~95%, PEG/PPG-10/30 polymer
5~10%.
Further include following components by percentage to the quality in wherein some embodiments：Essence 0.1~0.2% and
Preservative 0.1~0.2%.Further preferably preservative 0.1~0.15%.Still more preferably it is essence 0.18~0.2%
And preservative 0.1~0.12%.
The present invention also provides the preparation methods of above-mentioned amino acid facial cleanser, include the following steps：
Step A：Disinfection；
Step B：Weigh the cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3 butylene glycol,
PEG400, sorbierite, emulsifier, dispersant are dissolved by heating and are stirred evenly in main cooker；
Step C：The potassium hydroxide and appropriate amount of deionized water are weighed, stirring and dissolving is slowly added to main cooker while stirring, protects
Temperature stirring；
Step D：The sodium cocoyl glutamate, methyl bay sodium acyl taurine, lauryl hydroxyl sulfo betaine are weighed,
The sodium cocoyl glutamate is slowly first sprinkled into main cooker, agitating and heating dissolving sequentially adds clout, stir after heat preservation defoaming
Mix dissolving, stir evenly after begin to cool；
Step E：It weighs and main cooker is added after the sodium chloride appropriate amount of deionized water dissolves by heating completely, then by the poly- season
Ammonium salt cationoid surfactant is diluted with remaining deionized water, and main cooker is added, stirs evenly；
Step F：The essence, preservative are weighed, main cooker is sequentially added, after stirring evenly, stirring waits for that lotion is fine and smooth uniformly
After discharge.
In wherein some embodiments, the preparation method comprises the following steps：
Step A：Disinfection：The medicinal alcohol that volumetric concentration is 75% is taken to carry out vessel disinfection；
Step B：Weigh the cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3 butylene glycol,
PEG400, sorbierite, emulsifier, dispersant are heated to 70~85 DEG C and dissolve and stir evenly in main cooker；
Step C：Weigh the potassium hydroxide and appropriate amount of deionized water, stirring and dissolving and after being heated to 70~85 DEG C, while stirring
It mixes side and is slowly added to main cooker, 5~20min of insulated and stirred；
Step D：The sodium cocoyl glutamate, methyl bay sodium acyl taurine, lauryl hydroxyl sulfo betaine are weighed,
The sodium cocoyl glutamate is slowly first sprinkled into main cooker, agitating and heating dissolving sequentially adds clout, stir after heat preservation defoaming
Mix dissolving, stir evenly after begin to cool；
Step E：When main cooker is cooled to 50~65 DEG C, the sodium chloride is weighed, 50 are heated to appropriate amount of deionized water~
Main cooker is added after 65 DEG C of dissolvings completely, then the polyquaternium cationoid surfactant is dilute with remaining deionized water
It releases, main cooker is added, stirs evenly；
Step F：The essence, preservative are weighed, is sequentially added when main cooker is cooled to 40~45 DEG C, after stirring evenly,
Stirring discharges after lotion is fine and smooth uniformly.
The present invention compared with the prior art the advantages of and have the beneficial effect that：
The present inventor team breaches the technological difficulties of amino acid facial cleanser, with crystallization by largely studying
Based on method, it is aided with neutralisation and thickening method, prepares stable amino acid cleansing milk；The present invention lives amino acids table and other temperature
With surfactant carried out it is rational compounding form certain micellar concentration, and add polyquaternium cationoid reach foam enhancing and
The effect of foam stabilizing promotes foam total amount and quality so that product has abundant fine and smooth soft and smooth foam, improves amino acid and washes one's face
Milk reaches good and washes rear skin cleanliness factor to the cleaning force of skin.Rational surfactant and polyalcohol proportioning are taken simultaneously
Match, improve the knot cream point of amino acid lotion, improve the fine and smooth degree of lotion appearance, not adding pearling agent in the case of system
It is standby go out pearly-lustre fine and smooth lotion.
Amino acid facial cleanser prepared by the present invention is a amino acid facial cleanser for integrating many merits, in addition to temperature
With it is non-stimulated, pro-skin moisture retention is good etc., and most prominent feature is with abundant dense foam, and it is good to wash rear skin cleanliness factor, resistance to
The test of hot, cold-resistant, shelf is highly stable, and the molding of lotion appearance exquisiteness, no granular sensation, pearly-lustre exquisiteness is soft and smooth, and with best
Cream temperature is tied, between 38~45 DEG C, production is convenient for knot cream point control.
Specific implementation mode
It further illustrates the present invention with reference to embodiments.
Raw materials used in embodiment is commercially available common raw material, wherein：
Sodium cocoyl glutamate, trade name：HONDU SCG-95 are purchased from Shanghai Hong Du Fine Chemical Co., Ltd；
The mixture of cocounut oil acyl glycine potassium, hydroxy stearic acid, tocopherol, mass percent proportioning are：The sweet ammonia of cocounut oil acyl
Sour potassium 70~80%, hydroxy stearic acid 20~30%, tocopherol 0.5~1.0%, above-mentioned summation are 100%, trade name：
HONDU SCA-75 are purchased from Shanghai Hong Du Fine Chemical Co., Ltd；
Methyl bay sodium acyl taurine, trade name：HONDU LT-40, content are 50~60%, purchased from the macro degree essence in Shanghai
Thin Chemical Co., Ltd.；
The polyquaternium cationoid surfactant mixture of polyquaternium -43 and water (polyquaternium -7), quality
Percentage matches：Polyquaternium -7 3~5%, polyquaternium -43 5~7%, surplus are water, trade name：Supcare
620, it is purchased from Shanghai Hong Du Fine Chemical Co., Ltd；
Emulsifier：The mixture of PEG-100 stearates and stearine, mass percent proportioning are：PEG-100
Stearate 40-60%, stearine 40-60%, trade name：HONDU A-165 are purchased from the macro degree fine chemistry industry in Shanghai
Co., Ltd；
Dispersant：The mixture of PEG/PPG-25/30COPOLYMER and PEG/PPG-10/30COPOLYMER, quality hundred
Divide and is than proportioning：PEG/PPG-25/30 COPOLYMER 90~95%, PEG/PPG-10/30COPOLYMER 5~10%, quotient
The name of an article is：SAPPCHEM PC25 are purchased from Shanghai Hong Du Fine Chemical Co., Ltd；
Sorbierite, mass percent concentration are the sorbitol solution of 69~71wt%, are purchased from Luo Gaite；
Lauryl hydroxyl sulfo betaine is purchased from flower king；
Potassium hydroxide is purchased from excellent sharp moral.
Embodiment and comparative example
A kind of amino acid facial cleanser, by percentage to the quality, it includes component see the following table 1：
The formula table of table 1 Examples 1 to 3 and comparative example 1~4
Note："-" expression is not added
Preparation method is：
Step A：Disinfection：The medicinal alcohol that volumetric concentration is 75% is taken to carry out vessel disinfection；
Step B：Weigh cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3 butylene glycol, PEG400,
Sorbierite, emulsifier, dispersant are heated to 70~85 DEG C and dissolve and stir evenly in main cooker；
Step C：Weigh potassium hydroxide and appropriate amount of deionized water, stirring and dissolving and after being heated to 70~85 DEG C, while stirring
It is slowly added to main cooker, 5~20min of insulated and stirred；
Step D：Sodium cocoyl glutamate, methyl bay sodium acyl taurine, lauryl hydroxyl sulfo betaine are weighed, first will
Sodium cocoyl glutamate is slowly sprinkled into main cooker, and agitating and heating dissolving sequentially adds clout, stirring and dissolving is stirred after heat preservation defoaming
It is begun to cool after mixing uniformly；
Step E：When main cooker is cooled to 50~65 DEG C, sodium chloride is weighed, 50~65 DEG C are heated to appropriate amount of deionized water
Main cooker is added after dissolving completely, then adds after polyquaternium cationoid surfactant is stirred evenly with the dilution of remaining deionized water
Enter main cooker, stirs evenly；
Step F：Essence, preservative have been weighed, has been sequentially added when main cooker is cooled to 40~45 DEG C, after stirring evenly, in
Stirring at low speed discharges after lotion is fine and smooth uniformly.
Evaluation on probation is carried out to Examples 1 to 3 and 1~4 gained sample of comparative example, major embodiment is in use to bubble
The evaluation of foam, cleanliness factor, moisture feeling.
Specific method is：Sample is issued to 20 testers and compares use.Tester uses phase when using sample
Cleaned with method, each sample respectively use two weeks, tester according to oneself feel score.Scoring takes 10 points
System, 1 point worst, and 10 points best.
The specific clean method of tester is：It uses daily morning and evening, first drenches skin of face using clear water, use this hair
Bright product adds suitable quantity of water to be applied to face and circumference of eyes, and gently rub skin of face about one after rubbing blistering in the palm of the hand in right amount
Minute；Then it is rinsed well with clear water, is repeated the above steps daily morning and evening, per a sample using after two weeks, product is commented
Point, it the results are shown in Table 2.
1~4 evaluation table on probation of 2 Examples 1 to 3 of table and comparative example
| Test event | Lather quickness | Foaming abundancy degree | Wash rear cleanliness factor | Degree is moistened after washing |
| Embodiment 1 | 9.0 | 9.5 | 9.2 | 9.5 |
| Embodiment 2 | 8.8 | 8.9 | 9.2 | 9.0 |
| Embodiment 3 | 8.5 | 8.5 | 8.2 | 8.8 |
| Comparative example 1 | 8.3 | 8.4 | 8.0 | 8.5 |
| Comparative example 2 | 7.8 | 8.0 | 7.8 | 8.3 |
| Comparative example 3 | 8.3 | 8.3 | 9.0 | 8.5 |
| Comparative example 4 | 7.5 | 7.5 | 7.8 | 7.8 |
The experimental results showed that being added to cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, methyl bay
Sodium acyl taurine, lauryl hydroxyl sulfo betaine embodiment obtained by amino acid facial cleanser, blister in use
Speed, foaming abundancy degree, wash rear cleanliness factor, wash after moisten degree have promotion, it is better than comparative example.
The test of foaming power is carried out to facial cleanser lotion prepared by Examples 1 to 3 comparative example 1~4.Test method refers to
Ross-Miles methods, the measurement of GBT 13173.6-2000 detergent foaming powers.
Test condition is：0.25% deionized water solution, 40 ± 0.5 DEG C of experimental temperature test and read within 5 minutes foam height
Degree.Average test data such as table 3：
3 foaming power test result of table
| Test event | Average foam height (mm) |
| Embodiment 1 | 75 |
| Embodiment 2 | 68 |
| Embodiment 3 | 65 |
| Comparative example 1 | 45 |
| Comparative example 2 | 40 |
| Comparative example 3 | 42 |
| Comparative example 4 | 30 |
The experimental results showed that the mildy wash foaming power of embodiment is more preferable than the foaming power of the mildy wash of comparative example.In formula
Add cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, methyl bay sodium acyl taurine, lauryl hydroxyl sulphur
The foaming power of mildy wash can be made more preferable after base glycine betaine, polyquaternium -7 and polyquaternium -43.
The embodiment of the present invention 1~3 and comparative example 1~4 are carried out to wash rear cleanliness factor investigation, 20 testers is selected, makes
It is thick with equal area (2*3cm)/picture is smeared out on each tester's the back of the hand with BB frosts/eyeliner of equal amount (0.1 gram)
Elongated short identical lines weigh test sample (embodiment and comparative example sample) 0.2g, are applied at the back of the hand figure respectively, use
After a small amount of water soaks the back of the hand, 30s is softly cleaned, is rinsed with clear water, observed and clean effect.
Evaluation criterion：
Cleanliness factor is very good：BB frosts/eyeliner is rinsed well completely, does not see the marking.
Cleanliness factor is general：BB frosts/eyeliner is not rinsed well completely, still there is the unobvious marking.
Cleanliness factor is poor：BB frosts/eyeliner is not rinsed well completely, still there is the apparent marking of residual.
Experimental result is shown in Table 4：
Table 4 washes rear cleanliness factor test result
| Test event | Cleanliness factor is very good (%) | Cleanliness factor is general (%) | Cleanliness factor is poor (%) |
| Embodiment 1 | 95% | 5% | 0 |
| Embodiment 2 | 90% | 10% | 0 |
| Embodiment 3 | 80% | 20% | 0 |
| Comparative example 1 | 45% | 35% | 20% |
| Comparative example 2 | 10% | 45% | 40% |
| Comparative example 3 | 70% | 20% | 10% |
| Comparative example 4 | 10% | 50% | 40% |
Experimental result：Cleanliness factor after mildy wash prepared by the formula in scope of embodiments is washed is preferable.Illustrate in formula
Add cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, methyl bay sodium acyl taurine, lauryl hydroxyl sulphur
Base glycine betaine has remarkable result to the promotion for being formulated cleannes.
The knot cream point of Examples 1 to 3 and comparative example 1~4 is compared, see table 5：
5 knot cream temperature comparisons' result of table
The experimental results showed that the knot cream temperature of amino acid facial cleanser obtained by embodiment is higher than the knot cream temperature of comparative example,
Cocounut oil acyl glycine potassium hydroxy stearic acid tocopherol, methyl bay sodium acyl taurine, lauryl weight ratio are added in formula
The promotion with comparison gained facial cleanser knot cream point of glycine betaine and polyalcohol has significant effect.
To the appearance, smear and stability contrast of Examples 1 to 3 and comparative example 1~4, see table 6,7：
6 appearance of table, smear result
| Test event | Prepare appearance after discharging 24 hours, smear evaluation |
| Embodiment 1 | Appearance is fine and smooth, soft and smooth pearly-lustre is presented, is easily spread, smear is good |
| Embodiment 2 | Appearance is fine and smooth, it is soft, soft and smooth pearly-lustre is presented, easily sprawls, smear it is good |
| Embodiment 3 | Appearance is fine and smooth, it is soft, soft and smooth pearly-lustre is presented, easily sprawls, smear it is good |
| Comparative example 1 | Appearance powdery has fine grained, is partially hard, not easy to apply |
| Comparative example 2 | Appearance is not coarse, easy to apply |
| Comparative example 3 | Appearance it is dilute it is soft, coarse, be not molded |
| Comparative example 4 | Appearance is coarse, it is hard, without pearly-lustre, be not easy to smear |
The experimental results showed that the lotion of the amino acid facial cleanser prepared by embodiment, appearance is fine and smooth soft, easily sprawl,
Smear is good, and use feeling is more preferably.
7 stability test result of table
The experimental results showed that the stability of the amino acid facial cleanser obtained by embodiment is got well than comparative example.
Each technical characteristic of embodiment described above can be combined arbitrarily, to keep description succinct, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, it is all considered to be the range of this specification record.
Several embodiments of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection of the present invention
Range.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of amino acid facial cleanser, which is characterized in that by percentage to the quality comprising following components：
The solid content of the methyl bay sodium acyl taurine is 50~60%.
2. amino acid facial cleanser according to claim 1, which is characterized in that by percentage to the quality comprising with the following group
Point：
3. amino acid facial cleanser according to claim 2, which is characterized in that by percentage to the quality comprising with the following group
Point：
4. according to claims 1 to 3 any one of them amino acid facial cleanser, which is characterized in that the cocounut oil acyl glycine potassium,
Hydroxy stearic acid, tocopherol mixture mass percent proportioning be：Cocounut oil acyl glycine potassium 70~80%, hydroxy stearic acid
20~30%, tocopherol 0.5~1.0%, above-mentioned summation are 100%.
5. according to claims 1 to 3 any one of them amino acid facial cleanser, which is characterized in that the polyquaternary amine salt sun from
Sub- surfactant is the mixture of polyquaternium -7, polyquaternium -43 and water, and mass percent proportioning is：Polyquaternium-
7 3~5%, polyquaternium -43 5~7%, surplus are water.
6. according to claims 1 to 3 any one of them amino acid facial cleanser, which is characterized in that the emulsifier is PEG-100
The mixture of stearate and stearine, mass percent proportioning are：It is PEG-100 stearates 40~60%, sweet
Oleostearin acid esters 40~60%.
7. according to claims 1 to 3 any one of them amino acid facial cleanser, which is characterized in that the dispersant is PEG/
The mixture of PPG-25/30 polymer and PEG/PPG-10/30 polymer, mass percent proportioning are：PEG/PPG-25/30
Polymer 90~95%, PEG/PPG-10/30 polymer 5~10%.
8. according to claims 1 to 3 any one of them amino acid facial cleanser, which is characterized in that further include with mass percent
The following components of meter：Essence 0.1~0.2% and preservative 0.1~0.2%.
9. a kind of preparation method of amino acid facial cleanser according to any one of claims 8, which is characterized in that include the following steps：
Step A：Disinfection；
Step B：Weigh the cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3 butylene glycol, PEG400,
Sorbierite, emulsifier, dispersant are dissolved by heating and are stirred evenly in main cooker；
Step C：The potassium hydroxide and appropriate amount of deionized water are weighed, stirring and dissolving is slowly added to main cooker while stirring, and heat preservation is stirred
It mixes；
Step D：The sodium cocoyl glutamate, methyl bay sodium acyl taurine, lauryl hydroxyl sulfo betaine are weighed, first will
The sodium cocoyl glutamate is slowly sprinkled into main cooker, and agitating and heating dissolving after heat preservation defoaming, sequentially adds clout, and stirring is molten
Solve, stir evenly after begin to cool；
Step E：It weighs and main cooker is added after the sodium chloride appropriate amount of deionized water dissolves by heating completely, then by the polyquaternium
Cationoid surfactant is diluted with remaining deionized water, and main cooker is added, stirs evenly；
Step F：The essence, preservative are weighed, main cooker is sequentially added, after stirring evenly, stirring goes out after lotion is fine and smooth uniformly
Material.
10. the preparation method of amino acid facial cleanser according to claim 9, which is characterized in that include the following steps：
Step A：Disinfection：The medicinal alcohol that volumetric concentration is 75% is taken to carry out vessel disinfection；
Step B：Weigh the cocounut oil acyl glycine potassium, hydroxy stearic acid, the mixture of tocopherol, 1,3 butylene glycol, PEG400,
Sorbierite, emulsifier, dispersant are heated to 70~85 DEG C and dissolve and stir evenly in main cooker；
Step C：Weigh the potassium hydroxide and appropriate amount of deionized water, stirring and dissolving and after being heated to 70~85 DEG C, while stirring
It is slowly added to main cooker, 5~20min of insulated and stirred；
Step D：The sodium cocoyl glutamate, methyl bay sodium acyl taurine, lauryl hydroxyl sulfo betaine are weighed, first will
The sodium cocoyl glutamate is slowly sprinkled into main cooker, and agitating and heating dissolving after heat preservation defoaming, sequentially adds clout, and stirring is molten
Solve, stir evenly after begin to cool；
Step E：When main cooker is cooled to 50~65 DEG C, the sodium chloride is weighed, 50~65 DEG C are heated to appropriate amount of deionized water
Main cooker is added after dissolving completely, then the remaining deionized water of polyquaternium cationoid surfactant is diluted, adds
Enter main cooker, stirs evenly；
Step F：The essence, preservative are weighed, is sequentially added when main cooker is cooled to 40~45 DEG C, after stirring evenly, stirring
It discharges after lotion is fine and smooth uniformly.
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| CN110638679B (en) * | 2019-10-29 | 2022-08-16 | 广州市娇兰化妆品有限公司 | Amino acid cleansing cream compounded by amino acid potassium salt and amino acid sodium salt and preparation method thereof |
| CN110742819B (en) * | 2019-12-10 | 2023-04-25 | 广州瑞誉化工科技有限公司 | Amino acid facial cleaning honey |
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| CN113925804A (en) * | 2021-09-03 | 2022-01-14 | 太和康美(北京)中医研究院有限公司 | Amino acid facial cleanser |
| CN113693956B (en) * | 2021-09-23 | 2023-09-26 | 韩佛化妆品(湖州)有限公司 | Facial cleanser composition |
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