CN103961271B - Cleansing cream and preparation method thereof - Google Patents
Cleansing cream and preparation method thereof Download PDFInfo
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- CN103961271B CN103961271B CN201410008508.6A CN201410008508A CN103961271B CN 103961271 B CN103961271 B CN 103961271B CN 201410008508 A CN201410008508 A CN 201410008508A CN 103961271 B CN103961271 B CN 103961271B
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Abstract
The invention discloses a preparation method of cleansing cream and a product prepared with the method. The cleansing cream comprises raw materials as follows: 5.0%-20% of a sulfosuccinate type surfactant, 20.0%-60.0% of an N-fatty acylamino acid surfactant, 0.1%-2.0% of an emulsifier, 10.0%-40.0% of polyhydric alcohol and water, wherein themolecular formula of the polyhydric alcohol is CnH2n+2-x(OH)x, n is in a range of 3-5, and x is in a range of 2-4. The preparation method comprises the steps as follows: the raw materials are evenly mixed, heated to 75-100 DEG C and cooled to 38-50 DEG C after being completelydissolved. The cleansing cream prepared with the preparation method is excellent in foam characteristic, good in cleansing performance, low in alkalinity, low in irritation, easy to wash, free of residues after being washed, good in moisture retention and free from phenomena such as stickiness, greasiness, dryness, tightness and the like after being used, and the skin is free from the dehydration phenomenon after being washed.
Description
Technical field
The present invention relates to a kind of face cleaning cream and preparation method thereof.
Background technology
The national standard of personal facial cleansing class product is divided into two classes according to the kind of the selected cleansing of its formula
Aliphatic acid salt form and surfactant type two big class.
Traditional aliphatic acid salt form facial cleansing class product is using the aliphatic acid after highly basic saponification as main cleaning class
Composition, its degreasing power is strong, will make the excessive loss of facial sebum after use, causes the excessive dehydration of skin and dry and astringent tight；Alkali
Property is higher, skin acid environment is damaged, has stronger excitant to face.
In surfactant type facial cleansing class product, anion surfactant type facial cleansing class product, typically adopt
Clean constituents with polymer come thickening surfactant, though this product produces compared to traditional aliphatic acid salt form facial cleansing class
Product excitant is low, but its foaminess is bad, is difficult to rinse, and the polymer viscosifier residuing in face after washing will result in the viscous of face
Greasy tight, make consumer produce sense of discomfort.
The Cleasing compositions of above-mentioned two big class have respective shortcoming, limit its industrialized application development.This phenomenon
Urgently to be resolved hurrily.
Content of the invention
The technical problem to be solved is to overcome existing surfactant type facial cleansing class product foaminess not
Good, it is difficult to rinse, washes the sticky tight of rear face, make consumer produce the defect of sense of discomfort, a kind of face cleaning cream and its system are provided
Preparation Method.The face cleaning cream foam characteristic that described preparation method is obtained is excellent, clean-up performance is good, alkalescence is low, excitant is little, easy
Rinse, and further wash rear noresidue, to wash rear skin be not in phenomenon of losing water, performance of keeping humidity is good, and using will not
Sticky, the dry and astringent phenomenon such as tight.
An object of the present invention is: provides a kind of preparation method of face cleaning cream；
Described face cleaning cream includes the sulfosuccinic acid esters surfactant of following raw material: 5.0%-20%, 20.0%-
60.0% n- fatty acid acylamino acid surfactant, the emulsifying agent of 0.1%-2.0%, the polynary alcohol and water of 10.0%-40.0%；
Described percentage is the mass percent accounting for described raw material；Described polyalcohol is c for molecular formulanh2n+2-x(oh)x, wherein, n
It is 2-4 for 3-5 and x；
Described preparation method comprises the following steps: described raw material is mixed, is heated to 75-100 DEG C, treat that it is complete
After CL, it is cooled to 38-50 DEG C, you can.
Preparation method below for the face cleaning cream of the present invention does following specific description:
In the present invention, described sulfosuccinic acid esters surfactant is a kind of anion surfactant.Described
Sulfosuccinic acid esters surfactant is preferably comprised sulfosuccinic acid diisobutyl ester sodium, sulfosuccinic acid dihexyl sodium, the moon
One or more of cinnamic alcohol sulfosuccinate disodium and sulfosuccinic acid lauroyl aminoethyl disodium, more preferably for bay
Alcohol sulfosuccinate disodium.The structural formula of described laruyl alcohol sulfosuccinate disodium is as follows:
In the present invention, the addition of described sulfosuccinic acid esters surfactant is preferably 8.0%-15%, described
Percentage is the mass percent accounting for described raw material.
Described n- fatty acid acylamino acid surfactant is the conventional surfactant in this area.Described n- fat
Acyl amino acid surfactant is preferably comprised sodium lauroyl sarcosine, n- oleoyl sarcosine sodium, methyl cocoyl ox sulphur
One or more of sour sodium and sodium lauroyl glutamate, more preferably for sodium methyl cocoyl taurate.Described n- fat
The addition of fat acyl amino acid surfactant is preferably 30%-50%, and described percentage is the quality accounting for described raw material
Percentage.
In the present invention, described emulsifying agent is the conventional emulsifying agent in this area.Described emulsifying agent is preferably comprised glycerine
One or more of stearate, Natrulon H-10 myristinate, ceteareth -20, polysorbate -20, more
It is Natrulon H-10 myristinate goodly.The addition of described emulsifying agent is preferably 0.2%-1.5%, and described percentage is
Account for the mass percent of described raw material.
In the present invention, described polyalcohol is preferably hydroxyl value 1400-2500mgkoh/g, and degree of functionality 2-5, at 25 DEG C
Viscosity 100-1500mpa s and the polyalcohol of molal weight 76-152.Described polyalcohol is preferably comprised: glycerine, the third two
One or more of alcohol, 1,3-BDO and diethylene glycol (DEG), more preferably for glycerine.The addition of described polyalcohol is preferably
15.0%-35.0%, described percentage is the mass percent accounting for described raw material.
In the present invention, the raw material of described face cleaning cream is preferably: the sulfosuccinic acid esters surface-active of 5.0%-20%
Agent, the n- fatty acid acylamino acid surfactant of 20.0%-60.0%, the emulsifying agent of 0.1%-2.0%, 10.0%-40.0% many
First alcohol and water；Described percentage is the mass percent accounting for described raw material；Described polyalcohol is c for molecular formulanh2n+2-x
(oh)x, wherein, n is 3-5 and x is 2-4.
In the present invention, the raw material of described face cleaning cream is more preferably: the sulfosuccinic acid esters surface-active of 8.0%-15%
Agent, the n- fatty acid acylamino acid surfactant of 30%-50%, the emulsifying agent of 0.2%-1.5%, the polyalcohol of 15.0%-35.0%
And water；Described percentage is the mass percent accounting for described raw material；Described polyalcohol is c for molecular formulanh2n+2-x(oh)x,
Wherein, n is 3-5 and x is 2-4.
In the present invention, the raw material of described face cleaning cream is more preferably: the laruyl alcohol sulfosuccinate disodium of 5.0%-20%,
The sodium methyl cocoyl taurate of 20.0%-60.0%, the Natrulon H-10 myristinate of 0.1%-2.0%, 10.0%-40.0%
G ＆ W；Described percentage is the mass percent accounting for described raw material；Described polyalcohol is c for molecular formulanh2n+2-x
(oh)x, wherein, n is 3-5 and x is 2-4.
In the present invention, the described method mixing is the conventional method in this area.Described mixes preferably
Sulfosuccinic acid esters surfactant described in elder generation will mix with described polyalcohol, then with described n- fatty acyl
Base amino acid surfactant, described emulsifying agent and described water mix.
In the present invention, described heating is preferably heated to 80-85 DEG C；The time of described heating is preferably 20-
30min, more preferably for 20min.
Material is preferably stirred during described heating；The speed of described stirring is preferably 30-50rpm, more preferably for
40rpm.
After described heating, preferably it is incubated；The time of described insulation is preferably 15-30min, more preferably for 15-
20min.
In the present invention, described cooling is preferably cooled to 38 DEG C；The time of described cooling is preferably 30-
50min.Cooling is preferably stirred in described cooling.The mixing speed of described stirring cooling is preferably 20-30rpm, more
It is 25rpm goodly.
In the present invention, it is preferred that in described cooling, one of preservative, ph conditioning agent and essence also can be added
Or it is multiple.
Described preservative and/or the selection of essence, meet the regulation of hygienic standards for cosmetics, from safe raw material.
Described preservative is the conventional preservative in this area, and described preservative is preferably Phenoxyethanol, methyl hydroxybenzoate and oxybenzene
One or more of propyl ester.The addition of described preservative is preferably 0.4%-0.8%, more preferably for 0.6%；Described hundred
Divide than the mass percent for accounting for described raw material.Described essence is the conventional essence in this area, the interpolation of described essence
Amount is preferably 0.1%-0.3%, more preferably for 0.2%；Described percentage is the mass percent accounting for described raw material.
When adding described preservative and/or essence, preferably add when temperature is down to 45-55 DEG C；More preferably, exist
Temperature is down to and is added when 50 DEG C.
Described ph conditioning agent is the conventional ph conditioning agent in this area, preferably citric acid and/or phosphoric acid, more preferably for
Citric acid.After described ph conditioning agent is adjusted, the ph value of described product is preferably 5.5-8.0, more preferably for 6.0-7.0.
When adding described ph conditioning agent, preferably add when temperature is down to 60-70 DEG C.
In the present invention, preferably in a technical scheme, do not contain the conventional thickener in this area.Described thickener is permissible
For Carbomer.
The second object of the present invention is, provides the face cleaning cream that above-mentioned preparation method is obtained.
In the present invention, the preparation method of described face cleaning cream passes through each raw material and its addition, and preparation technology and bar
The overall coordination effect of part, on the basis of good foam, oil resistant resistance to hard water characteristic, reduces excitant and improves foam performance,
Reduce absorption affinity, prepared product is more easy to rinse, and can suppress potential excitant solute penetration skin, reduces the dehydration of skin,
Play certain moisture-keeping efficacy, simultaneously, it is to avoid skin causes sticky tight feeling.
On the basis of meeting common sense in the field, above-mentioned each optimum condition, can be combined, obtain final product each preferable reality of the present invention
Example.
Agents useful for same of the present invention and raw material are all commercially available.
The positive effect of the present invention is: the face cleaning cream alkalescence of the present invention is low, excitant is little, wash rear skin will not go out
Existing dehydration or the dry and astringent phenomenon such as tight, easily rinse simultaneously, and face further will not be caused because of residual sticky tight
Taut sense, and foam characteristic is excellent, clean-up performance is good, wash rear noresidue, performance of keeping humidity is good.
Specific embodiment
Further illustrate the present invention below by the mode of embodiment, but therefore do not limit the present invention to described reality
Apply among a scope.The experimental technique of unreceipted actual conditions in the following example, conventionally and condition, or according to business
Product specification selects.
Embodiment 1
Raw material is as shown in the table:
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 40rpm) is heated to 85 DEG C, is incubated 20min, and after it is completely dissolved, (speed is stirred on side
25rpm) side cooling, is cooled to 70 DEG C, interpolation ph conditioning agent regulation ph value to 7.0, then is cooled to 50 DEG C, adds preservative and perfume (or spice)
Essence, is cooled to 38 DEG C further.
Embodiment 2
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 40rpm) is heated to 80 DEG C, is incubated 20min, and after it is completely dissolved, (speed is stirred on side
25rpm) side cooling, is cooled to 60 DEG C, interpolation ph conditioning agent regulation ph value to 6.0, then is cooled to 50 DEG C, adds preservative and perfume (or spice)
Essence, is cooled to 38 DEG C further.
Embodiment 3
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 40rpm) is heated to 80 DEG C, is incubated 20min, and after it is completely dissolved, (speed is stirred on side
25rpm) side cooling, is cooled to 60 DEG C, interpolation ph conditioning agent regulation ph value to 6.0, then is cooled to 50 DEG C, adds preservative and perfume (or spice)
Essence, is cooled to 38 DEG C further.
Embodiment 4
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 50rpm) is heated to 100 DEG C, is incubated 20min, after it is completely dissolved, is cooled to 70 DEG C,
Add ph conditioning agent and adjust ph value to 8.0, then be cooled to 45 DEG C, add preservative and essence, be cooled to 38 DEG C further.
Embodiment 5
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 50rpm) is heated to 75 DEG C, is incubated 30min, and after it is completely dissolved, (speed is stirred on side
30rpm) side cooling, is cooled to 70 DEG C, interpolation ph conditioning agent regulation ph value to 5.5, then is cooled to 55 DEG C, adds preservative and perfume (or spice)
Essence, is cooled to 50 DEG C further.
Embodiment 6
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 50rpm) is heated to 75 DEG C, is incubated 30min, and after it is completely dissolved, (speed is stirred on side
30rpm) side cooling, is cooled to 65 DEG C, interpolation ph conditioning agent regulation ph value to 7.0, then is cooled to 50 DEG C, adds preservative and perfume (or spice)
Essence, is cooled to 40 DEG C further.
Embodiment 7
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 50rpm) is heated to 100 DEG C, is incubated 20min, after it is completely dissolved, is cooled to 38 DEG C.
Embodiment 8
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 50rpm) is heated to 75 DEG C, is incubated 30min, and after it is completely dissolved, (speed is stirred on side
30rpm) side cooling, is cooled to 50 DEG C.
Embodiment 9
Preparation method comprises the following steps:
(1) sulfosuccinic acid esters surfactant will be mixed with polyalcohol, then with n- fatty acid acylamino acid
Surfactant, emulsifying agent and water mix；
(2) side stirring (speed 30rpm) is heated to 100 DEG C, is incubated 15min, and after it is completely dissolved, (speed is stirred on side
20rpm) side is cooled to 45 DEG C.
Embodiment 10
Raw material: the Carbomer containing 0.2g, as thickener, reduces the amount of water, remaining is with the embodiment of the present invention 1.
Comparative example 1
The addition of sulfosuccinic acid esters surfactant is 30%, and the amount of water reduces, and remaining is with the embodiment of the present invention 1.
Comparative example 2
The addition of n- fatty acid acylamino acid surfactant is 15%, supplies surplus with water, and remaining is implemented with the present invention
Example 1.
Comparative example 3
The addition of polyalcohol is 50%, and the amount of water reduces, and remaining is with the embodiment of the present invention 1.Product appearance is coarse, impact
Lather quickness and use feeling are it is impossible to be investigated by product stability.
Comparative example 4
The addition of polyalcohol is 5%, and the amount of water reduces, and remaining is with the embodiment of the present invention 1.Product cannot form paste knot
Structure, is emulsion form quality, and outward appearance is not good and affects use feeling it is impossible to investigate by product stability.
Effect example 1
The detection of spumescence.Take the product in the product that the present invention is obtained and comparative example and commercially available prod, carry out equal bar
The detection of spumescence under part.
Wherein, commercially available prod a's is entitled: Neutrogena deep layer soft pearl Cleansing Foam；Manufacturer is: Johnson ＆ Johnson (Chinese) is limited
Company；
Commercially available prod b's is entitled: the tender white mildy wash of yulan fat liquor；Manufacturer is: P＆G (Guangzhou) Co. Ltd；
Commercially available prod c's is entitled: L'Oreal man strength energy deep layer purifies face cleaning cream；Manufacturer is: the Suzhou still U.S.
Border cosmetics Co., Ltd.
Detection method is with reference to ross miles method.Testing result is as shown in table 1:
Table 1 product foam height testing result
| Group | Foam height (mm) |
| Embodiment 1 | 144 |
| Embodiment 2 | 147 |
| Embodiment 3 | 137 |
| Embodiment 10 | 135 |
| Comparative example 2 | 131 |
| Comparative example 3 | 124 |
| Commercially available prod a | 112 |
| Commercially available prod b | 97 |
| Commercially available prod c | 122 |
As shown in Table 1: the foam height of the product of the present invention is significantly larger than comparative example and commercially available prod, the product of the present invention
Foam performance excellent.
Effect example 2
The detection of performance of keeping humidity.
The detection of spumescence.Take the product in the product that the present invention is obtained and comparative example and commercially available prod, carry out equal bar
The detection of performance of keeping humidity under part.
Wherein, commercially available prod a's is entitled: Neutrogena deep layer soft pearl Cleansing Foam；Manufacturer is: Johnson ＆ Johnson (Chinese) is limited
Company；
Commercially available prod b's is entitled: the tender white mildy wash of yulan fat liquor；Manufacturer is: P＆G (Guangzhou) Co. Ltd；
Commercially available prod c's is entitled: L'Oreal man strength energy deep layer purifies face cleaning cream；Manufacturer is: the Suzhou still U.S.
Border cosmetics Co., Ltd.
Detection method: measure the different product face before using facial cleansing product with using same amount for 10 experimenters
After portion's cleaning products cleaning face, the water content of the skin of different time, calculates the average of moisture of skin addition (mmv).Skin
The detecting instrument of moisture addition is: corneometer cm825+ Germany ck public affairs skin tester.
Testing result is as shown in table 2:
The performance of keeping humidity testing result of each product of table 2
As shown in Table 2: the performance of keeping humidity of the product of the present invention is significantly larger than product and commercially available prod in comparative example.This
The product that bright method is obtained has obvious beneficial effect.
Claims (14)
1. a kind of preparation method of face cleaning cream it is characterised in that: described face cleaning cream includes the sulphur of following raw material: 5.0%-20%
Base succinate compound surfactant, the n- fatty acid acylamino acid surfactant of 20.0%-60.0%, 0.1%-2.0%
Emulsifying agent, the polynary alcohol and water of 10.0%-40.0%；Described percentage is the mass percent accounting for described raw material；Described
Polyalcohol for molecular formula be cnh2n+2-x(oh)x, wherein, n is 3-5 and x is 2-4；Described preparation method comprises the following steps:
Described raw material is mixed, is heated to 75-100 DEG C, after it is completely dissolved, be cooled to 38-50 DEG C, you can；Described
Sulfosuccinic acid esters surfactant includes sulfosuccinic acid diisobutyl ester sodium, sulfosuccinic acid dihexyl sodium, laruyl alcohol sulphur
One or more of base succinate disodium and sulfosuccinic acid lauroyl aminoethyl disodium；Described n- fatty acyl group ammonia
Base acid surfaces activating agent includes sodium lauroyl sarcosine, n- oleoyl sarcosine sodium, sodium methyl cocoyl taurate and lauroyl
One or more of base sodium glutamate.
2. preparation method as claimed in claim 1 it is characterised in that: the raw material of described face cleaning cream is: 5.0%-20%'s
Sulfosuccinic acid esters surfactant, the n- fatty acid acylamino acid surfactant of 20.0%-60.0%, 0.1%-
2.0% emulsifying agent, the polynary alcohol and water of 10.0%-40.0%；Described percentage is the mass percent accounting for described raw material；
Described polyalcohol is c for molecular formulanh2n+2-x(oh)x, wherein, n is 3-5 and x is 2-4.
3. preparation method as claimed in claim 1 or 2 it is characterised in that: described emulsifying agent includes stearine, poly-
One or more of glycerine -10 myristinate, ceteareth -20, polysorbate -20；Described polyalcohol
For hydroxyl value 1400-2500mgkoh/g, degree of functionality 2-5, the viscosity 100-1500mpa s at 25 DEG C and molal weight 76-152
Polyalcohol.
4. preparation method as claimed in claim 3 it is characterised in that: the adding of described sulfosuccinic acid esters surfactant
Dosage is 8.0%-15%；The addition of described n- fatty acid acylamino acid surfactant is 30%-50%；Described breast
The addition of agent is 0.2%-1.5%；Described polyalcohol includes: in glycerine, propane diols, 1,3 butylene glycol and diethylene glycol (DEG)
One or more；The addition of described polyalcohol is 15.0%-35.0%；Described percentage is the quality accounting for described raw material
Percentage.
5. preparation method as claimed in claim 1 or 2 it is characterised in that: the raw material of described face cleaning cream is: 8.0%-15%
Sulfosuccinic acid esters surfactant, the n- fatty acid acylamino acid surfactant of 30%-50%, 0.2%-1.5%
Emulsifying agent, the polynary alcohol and water of 15.0%-35.0%；Described percentage is the mass percent accounting for described raw material；Described
Polyalcohol for molecular formula be cnh2n+2-x(oh)x, wherein, n is 3-5 and x is 2-4.
6. preparation method as claimed in claim 1 or 2 it is characterised in that: the raw material of described face cleaning cream is: 5.0%-20%
Laruyl alcohol sulfosuccinate disodium, the sodium methyl cocoyl taurate of 20.0%-60.0%, 0.1%-2.0% poly-
Glycerine -10 myristinate, the G ＆ W of 10.0%-40.0%；Described percentage is the percent mass accounting for described raw material
Than；Described polyalcohol is c for molecular formulanh2n+2-x(oh)x, wherein, n is 3-5 and x is 2-4.
7. preparation method as claimed in claim 1 or 2 it is characterised in that: described mixes as first by described sulfo group
Succinate compound surfactant and described polyalcohol mix, then with described n- fatty acid acylamino acid surface-active
Agent, described emulsifying agent and described water mix；Described being heated to be is heated to 80-85 DEG C；The time of described heating
For 20-30min；Material is stirred during described heating；The speed of described stirring is 30-50rpm；After described heating, insulation；
The time of described insulation is 15-30min.
8. preparation method as claimed in claim 7 it is characterised in that: the described heat time be 20min；Described stirring
Speed is 40rpm；The time of described insulation is 15-20min.
9. preparation method as claimed in claim 1 or 2 it is characterised in that: described cooling be cooled to 38 DEG C；Described fall
The time of temperature is 30-50min；Described cooling is stirring cooling；The mixing speed of described stirring cooling is 20-30rpm.
10. preparation method as claimed in claim 9 it is characterised in that: the mixing speed of described cooling be 25rpm.
11. preparation methods as claimed in claim 1 it is characterised in that: in described cooling, be additionally added preservative, ph adjust
Section one or more of agent and essence；
Described preservative is one or more of Phenoxyethanol, methyl hydroxybenzoate and Nipasol；The adding of described preservative
Dosage is 0.4%-0.8%；
The addition of described essence is 0.1%-0.3%；
When adding described preservative and/or essence, add when temperature is down to 45-55 DEG C；Described ph conditioning agent is lemon
Lemon acid and/or phosphoric acid；After described ph conditioning agent is adjusted, ph value is 5.5-8.0；When adding described ph conditioning agent, in temperature
Degree is down to and is added when 60-70 DEG C.
12. preparation methods as claimed in claim 11 it is characterised in that: the addition of described preservative be 0.6%；Described
Essence addition be 0.2%；When described interpolation preservative and/or essence, add when temperature is down to 50 DEG C；Ph value is
6.0-7.0.
13. preparation methods as claimed in claim 1 it is characterised in that: in described raw material do not contain thickener.
The face cleaning cream that 14. preparation methods as any one of claim 1-13 are obtained.
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| CN105997572B (en) * | 2016-05-19 | 2021-02-02 | 广州靓美莲美容科技有限公司 | Facial cleanser containing nano graphene and preparation method thereof |
| CN107260609B (en) * | 2017-06-30 | 2020-06-19 | 广州澳希亚实业有限公司 | Pure crystalline acne-removing amino acid facial cleanser and preparation method thereof |
| CN107638341A (en) * | 2017-08-25 | 2018-01-30 | 广州仙施生物科技有限公司 | A kind of amino acid cleansing cream and preparation method thereof |
| CN110638715B (en) * | 2019-11-14 | 2022-06-21 | 广州一一生物技术有限公司 | Men's facial cleanser and preparation method thereof |
| CN112957289A (en) * | 2021-02-05 | 2021-06-15 | 克利黛尔生物科技(杭州)有限公司 | Formula, production process and product of thickener-free cleansing cream |
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| CN1683484A (en) * | 2004-04-16 | 2005-10-19 | 上海宏略实业有限公司 | Cleaning composition and its use |
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| CN103961271A (en) | 2014-08-06 |
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