CN103961271A - Cleansing cream and preparation method thereof - Google Patents

Cleansing cream and preparation method thereof Download PDF

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Publication number
CN103961271A
CN103961271A CN201410008508.6A CN201410008508A CN103961271A CN 103961271 A CN103961271 A CN 103961271A CN 201410008508 A CN201410008508 A CN 201410008508A CN 103961271 A CN103961271 A CN 103961271A
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preparation
surfactant
raw material
polyhydric alcohol
sulfosuccinic acid
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CN103961271B (en
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陈超
林艺青
黄进明
洪绯
廖立平
颜森泉
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Pientzehuang (shanghai) Biological Technology Development Co Ltd
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Pientzehuang (shanghai) Biological Technology Development Co Ltd
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Abstract

The invention discloses a preparation method of cleansing cream and a product prepared with the method. The cleansing cream comprises raw materials as follows: 5.0%-20% of a sulfosuccinate type surfactant, 20.0%-60.0% of an N-fatty acylamino acid surfactant, 0.1%-2.0% of an emulsifier, 10.0%-40.0% of polyhydric alcohol and water, wherein themolecular formula of the polyhydric alcohol is CnH2n+2-x(OH)x, n is in a range of 3-5, and x is in a range of 2-4. The preparation method comprises the steps as follows: the raw materials are evenly mixed, heated to 75-100 DEG C and cooled to 38-50 DEG C after being completelydissolved. The cleansing cream prepared with the preparation method is excellent in foam characteristic, good in cleansing performance, low in alkalinity, low in irritation, easy to wash, free of residues after being washed, good in moisture retention and free from phenomena such as stickiness, greasiness, dryness, tightness and the like after being used, and the skin is free from the dehydration phenomenon after being washed.

Description

A kind of facial cleaning cream and preparation method thereof
Technical field
The present invention relates to a kind of facial cleaning cream and preparation method thereof.
Background technology
The kind that the national standard of individual's facial cleansing series products is filled a prescription selected cleansing according to it is divided into two class soap types and the large class of surfactant type two.
Traditional soap type facial cleansing series products is that its degreasing power is strong, after use, will make the excessive loss of facial sebum using the fatty acid after highly basic saponification as main clean constituents, causes the excessive dehydration of skin and dry and astringent tight; Alkalescence is higher, and skin acid environment is damaged, and face is had to stronger zest.
In surfactant type facial cleansing series products, anion surfactant type facial cleansing series products, the general polymer that adopts carrys out the clean constituents of thickening surfactant, though this product is low compared to traditional soap type facial cleansing series products zest, but its foaminess is bad, be difficult for rinsing, after washing, residue in facial polymer viscosifier and will cause the sticky tight of face, make consumer produce sense of discomfort.
The Cleasing compositions of above-mentioned two large classes has shortcoming separately, has limited its industrialized application development.This phenomenon is urgently to be resolved hurrily.
Summary of the invention
Technical problem to be solved by this invention is that to overcome existing surfactant type facial cleansing series products foaminess bad, is difficult for rinsing, and washes the sticky tight of rear face, makes consumer produce the defect of sense of discomfort, and a kind of facial cleaning cream and preparation method thereof is provided.Facial cleaning cream foam characteristic excellence that described preparation method makes, clean-up performance is good, alkalescence is low, zest is little, easily flushing, and further wash rear noresidue, wash rear skin and there will not be phenomenon of losing water, performance of keeping humidity is good, and uses the phenomenons such as can be sticky, not dry and astringent not tight.
One of object of the present invention is: the preparation method that a kind of facial cleaning cream is provided;
Described facial cleaning cream comprises the 2-Sulfosuccinic acid esters surfactant of following raw material: 5.0%-20%, the N-fatty acyl group amino acid surfactant of 20.0%-60.0%, the emulsifying agent of 0.1%-2.0%, the polynary alcohol and water of 10.0%-40.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4;
Described preparation method comprises the following steps: by described raw material mix homogeneously, is heated to 75-100 DEG C, after it dissolves completely, is cooled to 38-50 DEG C.
Do following specific description for the preparation method of facial cleaning cream of the present invention below:
In the present invention, described 2-Sulfosuccinic acid esters surfactant is a kind of anion surfactant.Described 2-Sulfosuccinic acid esters surfactant preferably comprises one or more in 2-Sulfosuccinic acid diisobutyl ester sodium, 2-Sulfosuccinic acid dihexyl sodium, lauryl alcohol sulfosuccinate disodium and 2-Sulfosuccinic acid lauroyl amido ethyl ester disodium, is more preferably lauryl alcohol sulfosuccinate disodium.The structural formula of described lauryl alcohol sulfosuccinate disodium is as follows:
In the present invention, the addition of described 2-Sulfosuccinic acid esters surfactant is preferably 8.0%-15%, and described percentage ratio is the mass percent that accounts for described raw material.
Described N-fatty acyl group amino acid surfactant is the surfactant of this area routine.Described N-fatty acyl group amino acid surfactant preferably comprises one or more in sodium lauroyl sarcosine, KORANTIN SH sodium, sodium methyl cocoyl taurate and sodium lauroyl glutamate, is more preferably sodium methyl cocoyl taurate.The addition of described N-fatty acyl group amino acid surfactant is preferably 30%-50%, and described percentage ratio is the mass percent that accounts for described raw material.
In the present invention, described emulsifying agent is the emulsifying agent of this area routine.Described emulsifying agent preferably comprises one or more in glyceryl stearate, Natrulon H-10 myristinate, ceteareth-20, polysorbate-20, is more preferably Natrulon H-10 myristinate.The addition of described emulsifying agent is preferably 0.2%-1.5%, and described percentage ratio is the mass percent that accounts for described raw material.
In the present invention, described polyhydric alcohol is preferably hydroxyl value 1400-2500mgKOH/g, degree of functionality 2-5, the viscosity 100-1500mPas at 25 DEG C and the polyhydric alcohol of molal weight 76-152.Described polyhydric alcohol preferably comprises: one or more in glycerol, propylene glycol, 1,3 butylene glycol and diethylene glycol are more preferably glycerol.The addition of described polyhydric alcohol is preferably 15.0%-35.0%, and described percentage ratio is the mass percent that accounts for described raw material.
In the present invention, the raw material of described facial cleaning cream is preferably: the 2-Sulfosuccinic acid esters surfactant of 5.0%-20%, the N-fatty acyl group amino acid surfactant of 20.0%-60.0%, the emulsifying agent of 0.1%-2.0%, the polynary alcohol and water of 10.0%-40.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4.
In the present invention, the raw material of described facial cleaning cream is more preferably: the 2-Sulfosuccinic acid esters surfactant of 8.0%-15%, the N-fatty acyl group amino acid surfactant of 30%-50%, the emulsifying agent of 0.2%-1.5%, the polynary alcohol and water of 15.0%-35.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4.
In the present invention, the raw material of described facial cleaning cream is more preferably: the lauryl alcohol sulfosuccinate disodium of 5.0%-20%, the sodium methyl cocoyl taurate of 20.0%-60.0%, the Natrulon H-10 myristinate of 0.1%-2.0%, the G & W of 10.0%-40.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4.
In the present invention, the method for described mix homogeneously is the method for this area routine.Described mix homogeneously be preferably first described 2-Sulfosuccinic acid esters surfactant by with described polyhydric alcohol mix homogeneously, then mix homogeneously with described N-fatty acyl group amino acid surfactant, described emulsifying agent and described water.
In the present invention, described heating is preferably for being heated to 80-85 DEG C; The time of described heating is preferably 20-30min, is more preferably 20min.
When described heating, preferably stir material; The speed of described stirring is preferably 30-50rpm, is more preferably 40rpm.
After described heating, preferably insulation; The time of described insulation is preferably 15-30min, is more preferably 15-20min.
In the present invention, described cooling is preferably for being cooled to 38 DEG C; The time of described cooling is preferably 30-50min.Described cooling is preferably for stirring cooling.The mixing speed of described stirring cooling is preferably 20-30rpm, is more preferably 25rpm.
In the present invention, preferably, in the time of described cooling, also can add one or more in antiseptic, pH adjusting agent and essence.
Described antiseptic and/or the selection of essence, meet the regulation of hygienic standards for cosmetics, selects safe raw material.Described antiseptic is the antiseptic of this area routine, and described antiseptic is preferably one or more in phenoxyethanol, methyl hydroxybenzoate and propyl hydroxybenzoate.The addition of described antiseptic is preferably 0.4%-0.8%, is more preferably 0.6%; Described percentage ratio is the mass percent that accounts for described raw material.Described essence is the essence of this area routine, and the addition of described essence is preferably 0.1%-0.3%, is more preferably 0.2%; Described percentage ratio is the mass percent that accounts for described raw material.
In the time adding described antiseptic and/or essence, preferably in the time that being down to 45-55 DEG C, temperature adds; More preferably, in the time that being down to 50 DEG C, temperature adds.
Described pH adjusting agent is the pH adjusting agent of this area routine, is preferably citric acid and/or phosphoric acid, is more preferably citric acid.After described pH adjusting agent regulates, the pH value of described product is preferably 5.5-8.0, is more preferably 6.0-7.0.
In the time adding described pH adjusting agent, preferably in the time that being down to 60-70 DEG C, temperature adds.
In the present invention, preferably in a technical scheme, do not contain the thickening agent of this area routine.Described thickening agent can be carbomer.
Two of object of the present invention is, the facial cleaning cream that provides above-mentioned preparation method to make.
In the present invention, the preparation method of described facial cleaning cream is by each raw material and addition thereof, and the overall coordination effect of preparation technology and condition, on the basis of good foam, the resistance to hard water characteristic of oil resistant, reduce zest and improve foam performance, reduce absorption affinity, the product making more easily rinses, and can suppress potential zest solute penetration skin, reduce the dehydration of skin, play certain moisture-keeping efficacy, meanwhile, avoided skin to cause sticky tight sense.
Meeting on the basis of this area general knowledge, above-mentioned each optimum condition, can combination in any, obtains the preferred embodiments of the invention.
Agents useful for same of the present invention and raw material be commercially available obtaining all.
Positive progressive effect of the present invention is: facial cleaning cream alkalescence of the present invention is low, zest is little, wash rear skin there will not be dehydration or the dry and astringent phenomenon such as tight, easily rinse simultaneously, and further can be because of not residual and cause the sticky tight sense of face, and foam characteristic excellence, clean-up performance good, wash rear noresidue, performance of keeping humidity is good.
Detailed description of the invention
Mode below by embodiment further illustrates the present invention, but does not therefore limit the present invention among described scope of embodiments.The experimental technique of unreceipted actual conditions in the following example, according to conventional method and condition, or selects according to catalogue.
Embodiment 1
Raw material is as shown in the table:
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 40rpm) and is heated to 85 DEG C, and insulation 20min, after it dissolves completely, the cooling of (speed 25rpm) limit is stirred on limit, is cooled to 70 DEG C, adds pH adjusting agent and regulates pH value to 7.0, be cooled to again 50 DEG C, add antiseptic and essence, be further cooled to 38 DEG C.
Embodiment 2
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 40rpm) and is heated to 80 DEG C, and insulation 20min, after it dissolves completely, the cooling of (speed 25rpm) limit is stirred on limit, is cooled to 60 DEG C, adds pH adjusting agent and regulates pH value to 6.0, be cooled to again 50 DEG C, add antiseptic and essence, be further cooled to 38 DEG C.
Embodiment 3
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 40rpm) and is heated to 80 DEG C, and insulation 20min, after it dissolves completely, the cooling of (speed 25rpm) limit is stirred on limit, is cooled to 60 DEG C, adds pH adjusting agent and regulates pH value to 6.0, be cooled to again 50 DEG C, add antiseptic and essence, be further cooled to 38 DEG C.
Embodiment 4
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 50rpm) and is heated to 100 DEG C, and insulation 20min, after it dissolves completely, is cooled to 70 DEG C, adds pH adjusting agent and regulates pH value to 8.0, then be cooled to 45 DEG C, adds antiseptic and essence, is further cooled to 38 DEG C.
Embodiment 5
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 50rpm) and is heated to 75 DEG C, and insulation 30min, after it dissolves completely, the cooling of (speed 30rpm) limit is stirred on limit, is cooled to 70 DEG C, adds pH adjusting agent and regulates pH value to 5.5, be cooled to again 55 DEG C, add antiseptic and essence, be further cooled to 50 DEG C.
Embodiment 6
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 50rpm) and is heated to 75 DEG C, and insulation 30min, after it dissolves completely, the cooling of (speed 30rpm) limit is stirred on limit, is cooled to 65 DEG C, adds pH adjusting agent and regulates pH value to 7.0, be cooled to again 50 DEG C, add antiseptic and essence, be further cooled to 40 DEG C.
Embodiment 7
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 50rpm) and is heated to 100 DEG C, and insulation 20min, after it dissolves completely, is cooled to 38 DEG C.
Embodiment 8
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 50rpm) and is heated to 75 DEG C, insulation 30min, and after it dissolves completely, the cooling of (speed 30rpm) limit is stirred on limit, is cooled to 50 DEG C.
Embodiment 9
Preparation method comprises the following steps:
(1) by 2-Sulfosuccinic acid esters surfactant will with polyhydric alcohol mix homogeneously, then mix homogeneously with N-fatty acyl group amino acid surfactant, emulsifying agent and water;
(2) limit is stirred (speed 30rpm) and is heated to 100 DEG C, insulation 15min, and after it dissolves completely, limit is stirred (speed 20rpm) limit and is cooled to 45 DEG C.
Embodiment 10
Raw material: the carbomer that contains 0.2g, as thickening agent, reduce the amount of water, all the other are with the embodiment of the present invention 1.
Comparative example 1
The addition of 2-Sulfosuccinic acid esters surfactant is 30%, and the amount of water reduces, and all the other are with the embodiment of the present invention 1.
Comparative example 2
The addition of N-fatty acyl group amino acid surfactant is 15%, and water is supplied surplus, and all the other are with the embodiment of the present invention 1.
Comparative example 3
The addition of polyhydric alcohol is 50%, and the amount of water reduces, and all the other are with the embodiment of the present invention 1.Product appearance is coarse, affects lather quickness and use sense, cannot investigate by product stability.
Comparative example 4
The addition of polyhydric alcohol is 5%, and the amount of water reduces, and all the other are with the embodiment of the present invention 1.Product cannot form paste structure, is emulsion form quality, and outward appearance is not good and affect use sense, cannot investigate by product stability.
Effect embodiment 1
The detection of spumescence.Get product and commercially available prod in product and the comparative example that the present invention makes, carry out the detection of spumescence under equal conditions.
Wherein, the name of commercially available prod A is called: the soft pearl Cleansing Foam of Neutrogena deep layer; Manufacturer is: company limited of Johnson & Johnson (China);
The name of commercially available prod B is called: the tender white facial milk cleanser of Olay emulsion; Manufacturer is: P&G (Guangzhou) Co. Ltd;
The name of commercially available prod C is called: the man of L'Oreal strength energy deep layer purifies facial cleaning cream; Manufacturer is: Suzhou Shang Mei international cosmetic company limited.
Detection method is with reference to Ross-Miles method.Testing result is as shown in table 1:
Table 1 product foam height testing result
Group Foam height (mm)
Embodiment 1 144
Embodiment 2 147
Embodiment 3 137
Embodiment 10 135
Comparative example 2 131
Comparative example 3 124
Commercially available prod A 112
Commercially available prod B 97
Commercially available prod C 122
As shown in Table 1: the foam height of product of the present invention is far away higher than comparative example and commercially available prod, the foam performance excellence of product of the present invention.
Effect embodiment 2
The detection of performance of keeping humidity.
The detection of spumescence.Get product and commercially available prod in product and the comparative example that the present invention makes, carry out the detection of performance of keeping humidity under equal conditions.
Wherein, the name of commercially available prod A is called: the soft pearl Cleansing Foam of Neutrogena deep layer; Manufacturer is: company limited of Johnson & Johnson (China);
The name of commercially available prod B is called: the tender white facial milk cleanser of Olay emulsion; Manufacturer is: P&G (Guangzhou) Co. Ltd;
The name of commercially available prod C is called: the man of L'Oreal strength energy deep layer purifies facial cleaning cream; Manufacturer is: Suzhou Shang Mei international cosmetic company limited.
Detection method: measure the water content of 10 experimenters skin of different time after using before facial cleansing product and using the clean face of different product facial cleansing product of same amount, calculate the average of moisture of skin addition (MMV).The detecting instrument of moisture of skin addition is: the public skin test instrunment of Corneometer CM825+ Germany CK.
Testing result is as shown in table 2:
The performance of keeping humidity testing result of the each product of table 2
As shown in Table 2: the performance of keeping humidity of product of the present invention is far away higher than the product in comparative example and commercially available prod.The product that method of the present invention makes has obvious beneficial effect.

Claims (10)

1. a preparation method for facial cleaning cream, is characterized in that: described facial cleaning cream comprises the 2-Sulfosuccinic acid esters surfactant of following raw material: 5.0%-20%, the N-fatty acyl group amino acid surfactant of 20.0%-60.0%, the emulsifying agent of 0.1%-2.0%, the polynary alcohol and water of 10.0%-40.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4; Described preparation method comprises the following steps: by described raw material mix homogeneously, is heated to 75-100 DEG C, after it dissolves completely, is cooled to 38-50 DEG C.
2. preparation method as claimed in claim 1, is characterized in that: the raw material of described facial cleaning cream is: the 2-Sulfosuccinic acid esters surfactant of 5.0%-20%, the N-fatty acyl group amino acid surfactant of 20.0%-60.0%, the emulsifying agent of 0.1%-2.0%, the polynary alcohol and water of 10.0%-40.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4.
3. preparation method as claimed in claim 1 or 2, is characterized in that: described 2-Sulfosuccinic acid esters surfactant comprises one or more in 2-Sulfosuccinic acid diisobutyl ester sodium, 2-Sulfosuccinic acid dihexyl sodium, lauryl alcohol sulfosuccinate disodium and 2-Sulfosuccinic acid lauroyl amido ethyl ester disodium; The addition of described 2-Sulfosuccinic acid esters surfactant is preferably 8.0%-15%;
Described N-fatty acyl group amino acid surfactant comprises one or more in sodium lauroyl sarcosine, KORANTIN SH sodium, sodium methyl cocoyl taurate and sodium lauroyl glutamate; The addition of described N-fatty acyl group amino acid surfactant is preferably 30%-50%;
Described emulsifying agent comprises one or more in glyceryl stearate, Natrulon H-10 myristinate, ceteareth-20, polysorbate-20; The addition of described emulsifying agent is preferably 0.2%-1.5%;
Described polyhydric alcohol is hydroxyl value 1400-2500mgKOH/g, degree of functionality 2-5, the viscosity 100-1500mPas at 25 DEG C and the polyhydric alcohol of molal weight 76-152; Described polyhydric alcohol preferably comprises: one or more in glycerol, propylene glycol, 1,3 butylene glycol and diethylene glycol; The addition of described polyhydric alcohol is preferably 15.0%-35.0%;
Described percentage ratio is the mass percent that accounts for described raw material.
4. preparation method as claimed in claim 1 or 2, is characterized in that: the raw material of described facial cleaning cream is: the 2-Sulfosuccinic acid esters surfactant of 8.0%-15%, the N-fatty acyl group amino acid surfactant of 30%-50%, the emulsifying agent of 0.2%-1.5%, the polynary alcohol and water of 15.0%-35.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4.
5. preparation method as claimed in claim 1 or 2, is characterized in that: the raw material of described facial cleaning cream is: the lauryl alcohol sulfosuccinate disodium of 5.0%-20%, the sodium methyl cocoyl taurate of 20.0%-60.0%, the Natrulon H-10 myristinate of 0.1%-2.0%, the G & W of 10.0%-40.0%; Described percentage ratio is the mass percent that accounts for described raw material; Described polyhydric alcohol is that molecular formula is C nh 2n+2-x(OH) x, wherein, n is that 3-5 and x are 2-4.
6. preparation method as claimed in claim 1 or 2, it is characterized in that: described mix homogeneously is first by described 2-Sulfosuccinic acid esters surfactant and described polyhydric alcohol mix homogeneously, then mix homogeneously with described N-fatty acyl group amino acid surfactant, described emulsifying agent and described water;
Described being heated to be is heated to 80-85 DEG C; The time of described heating is preferably 20-30min, is more preferably 20min; When described heating, preferably stir material; The speed of described stirring is preferably 30-50rpm, is more preferably 40rpm; After described heating, preferably insulation; The time of described insulation is preferably 15-30min, is more preferably 15-20min.
7. preparation method as claimed in claim 1 or 2, is characterized in that: described cooling is for being cooled to 38 DEG C; The time of described cooling is preferably 30-50min; Described cooling is preferably for stirring cooling; The mixing speed of described stirring cooling is preferably 20-30rpm, is more preferably 25rpm.
8. preparation method as claimed in claim 1 or 2, is characterized in that: in the time of described cooling, also add one or more in antiseptic, pH adjusting agent and essence;
Described antiseptic is preferably one or more in phenoxyethanol, methyl hydroxybenzoate and propyl hydroxybenzoate; The addition of described antiseptic is preferably 0.4%-0.8%, is more preferably 0.6%;
The addition of described essence is preferably 0.1%-0.3%, is more preferably 0.2%;
In the time adding described antiseptic and/or essence, preferably in the time that being down to 45-55 DEG C, temperature adds; More preferably, in the time that being down to 50 DEG C, temperature adds; Described pH adjusting agent is citric acid and/or phosphoric acid; After described pH adjusting agent regulates, the pH value of described product is preferably 5.5-8.0, is more preferably 6.0-7.0; In the time adding described pH adjusting agent, preferably in the time that being down to 60-70 DEG C, temperature adds.
9. preparation method as claimed in claim 1, is characterized in that: in described raw material, do not contain thickening agent.
10. the facial cleaning cream that preparation method makes as claimed in any one of claims 1-9 wherein.
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CN107260609A (en) * 2017-06-30 2017-10-20 广州澳希亚实业有限公司 A kind of pure crystal type anti-acne amino acid cleansing cream and preparation method thereof
CN107638341A (en) * 2017-08-25 2018-01-30 广州仙施生物科技有限公司 A kind of amino acid cleansing cream and preparation method thereof
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CN105997572A (en) * 2016-05-19 2016-10-12 曾新民 Cleansing milk containing nano graphene and preparation method thereof
CN105997572B (en) * 2016-05-19 2021-02-02 广州靓美莲美容科技有限公司 Facial cleanser containing nano graphene and preparation method thereof
CN107260609A (en) * 2017-06-30 2017-10-20 广州澳希亚实业有限公司 A kind of pure crystal type anti-acne amino acid cleansing cream and preparation method thereof
CN107260609B (en) * 2017-06-30 2020-06-19 广州澳希亚实业有限公司 Pure crystalline acne-removing amino acid facial cleanser and preparation method thereof
CN107638341A (en) * 2017-08-25 2018-01-30 广州仙施生物科技有限公司 A kind of amino acid cleansing cream and preparation method thereof
CN110638715A (en) * 2019-11-14 2020-01-03 广州一一生物技术有限公司 Male facial cleanser and preparation method thereof
CN112957289A (en) * 2021-02-05 2021-06-15 克利黛尔生物科技(杭州)有限公司 Formula, production process and product of thickener-free cleansing cream

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