CN103705404B - A kind of containing natural oil emulsus bath foam and preparation method thereof - Google Patents
A kind of containing natural oil emulsus bath foam and preparation method thereof Download PDFInfo
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- CN103705404B CN103705404B CN201310752606.6A CN201310752606A CN103705404B CN 103705404 B CN103705404 B CN 103705404B CN 201310752606 A CN201310752606 A CN 201310752606A CN 103705404 B CN103705404 B CN 103705404B
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Abstract
The invention provides a kind of emulsus bath foam containing natural oil, this bath foam comprises surfactant, thickening agent, additive and deionized water, surfactant is made up of a certain proportion of anion surfactant and amphoteric surfactant, thickening agent is macromolecule washing thickening agent, this macromolecule washing thickening agent is made up of with mass ratio 1:1 acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer and Merquat 280/C13-16 isoparaffin/laureth-25 mixture, additive comprises antiseptic, acidity regulator and spice regulator, this bath foam also includes natural oil.Bath foam of the present invention, formula is reasonable, character is gentle, foaming abundancy during use, can not only cleaning skin very well, can also supplement rapidly the oil content that skin loses, effectively prevent xerosis cutis after shower, and not stratified in storage process, do not analyse oil.Present invention also offers the above-mentioned preparation method containing natural oil emulsus bath foam.
Description
Technical field
The present invention relates to a kind of skin cleaning articles for use, particularly relate to a kind of bath foam, more specifically relate to a kind of emulsus bath foam containing natural oil.The invention still further relates to this preparation method containing natural oil emulsus bath foam.
Background technology
Probably three types is had on the market at present for the bath foam that skin is clean, be all transparent type or semitransparent type product: one is soap base type, it be based on fancy soap composition improvement form, great majority are main component with soap, this series products alkalescence is comparatively strong, zest is comparatively large, and soap series products is easily deposited on skin when taking a shower, blocking pore, hinder breathing and the metabolism of skin, after taking a shower, skin can feel dry and astringent; Two is surfactant type, and it is mainly formed by the surfactant compound with cleaning function, more satiny during product washing, but has kind of the sordid sensation of bath; Three is the bath foam being added with natural oil, because the bath foam being added with natural oil can clean up the antibacterial on skin, Glycerin can be doubled again in the season of drying, thus the favor of consumer is more and more obtained, but the composition and engineering more complicated of this bath foam, if other composition interworkings of natural oil and product are bad, then product can be made to occur thinning, layering, analyse the situation such as oil, non-foam.
Along with improving constantly of people's living standard, consumer also proposes higher requirement to the quality of bath product, if outward appearance should be emulsus, the foam performance of product, the moist performance of product should be all good etc., therefore, research and develop a kind of containing natural oil and the bath product of stable system is those skilled in the art endeavour study problem.
Summary of the invention
For solving above Problems existing, the object of this invention is to provide a kind of emulsus bath foam containing natural oil, this body wash liquid formula is reasonable, technique simple, not stratified in storage process, do not analyse oil, has again abundant foam during use.
Another object of the present invention is to provide a kind of preparation method of above-mentioned emulsus bath foam.
For realizing above object, of the present invention containing natural oil emulsus bath foam, comprise surfactant, thickening agent, additive and deionized water, it is characterized in that: described surfactant is made up of anion surfactant and amphoteric surfactant, anion surfactant is ammonium lauryl sulfate, polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, amide groups polyoxyethylene ether magnesium sulfate, one or more in SAS, amphoteric surfactant is cocamido propyl betaine, empgen BB, dodecyl CAB, dimethyl dodecyl amine oxide, cocoamidopropyl dimethyl betanin, cocamidopropyl propyl amide hydroxyl sulphonic acid betaine, coco imidoazolinium, one or more in fatty alcohol-polyoxyethylene ether disodium sulfosuccinate salt, their mass ratioes in bath foam are anion surfactant 15-25%, amphoteric surfactant 1-6%, described thickening agent is macromolecule washing thickening agent, and this macromolecule washing thickening agent is by acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer and Merquat 280/C
13-16isoparaffin/laureth-25 mixture forms, and their mass ratioes in bath foam are acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer 2-4%, Merquat 280/C
13-16isoparaffin/laureth-25 mixture 2-4%, described additive comprises antiseptic, acidity regulator and spice regulator, described bath foam also includes natural oil, and the mass ratio of natural oil in bath foam is 1-2%.
The model produced in the preferred Shantou City Daqian High and New Technology Research Center Co., Ltd of aforesaid propylene acid/acrylamide group methyl propane sulfonic acid copolymer is the macromolecule washing thickening agent of T-02; Merquat 280/C
13-16the model produced in the preferred Shantou City Daqian High and New Technology Research Center Co., Ltd of isoparaffin/laureth-25 mixture is the macromolecule washing thickening agent of T-03B.
Above-mentioned anion surfactant is preferably made up of with the ratio of mass ratio 1 ︰ 1 70% polyoxyethylenated alcohol sodium sulfate and 70% ammonium lauryl sulfate; Above-mentioned amphoteric surfactant is 35% cocoamidopropyl dimethyl betanin preferably.
Above-mentioned natural oil is one or both in Oleum Ricini, rapeseed oil, Testa oryzae oil, soybean oil, Oleum Arachidis hypogaeae semen, Petiolus Trachycarpi oil, palm-kernel oil, olive oil, aloe, Jojoba oil, almond oil, macadamia nut oil, sunflower seed oil, tocopherol, Vc acetate.
In order to increase skin clean after lubrication sense, above-mentioned bath foam also comprises cation guar gum, the Merquat 280 with conditioning skin moistening effect, has the lauric acid of skin moistening interception, stearic acid and has the disodiumedetate of softening of water effect; The mass ratio of each component in bath foam is cation guar gum is 0.2-0.8%, Merquat 280 is 0.5-1.5%, lauric acid is 1-2%, stearic acid is 1-2%, disodiumedetate is 0.2-0.8%.
The preferred methyl hydroxybenzoate of foregoing preservatives, acidity regulator optimization citric acid, the preferred spice of spice regulator, their mass ratioes in bath foam are methyl hydroxybenzoate 0.2-0.3%, citric acid 0.2-0.25%, spice 0.1-0.3%.
In order to make bath foam, in use foam is abundanter, and above-mentioned surfactant also comprises cocos nucifera oil acyl glycine potassium, and the mass ratio of cocos nucifera oil acyl glycine potassium in bath foam is 3-6%.
Emulsus bath foam containing natural oil of the present invention, a certain proportion of anion surfactant and amphoteric surfactant is adopted to combine as dual surfactant, utilize the water suction skin moistening moisture-keeping function of natural oil, again coordinate have special construction macromolecule washing thickening agent, make whole system not stratified in storage process, do not analyse oil.Bath foam of the present invention, formula is reasonable, character is gentle, foaming abundancy during use, can not only cleaning skin very well, can also supplement rapidly the oil content that skin loses, effectively prevent xerosis cutis after shower, and product stability and adaptability good.
The present invention also provides a kind of above-mentioned preparation method containing natural oil emulsus bath foam, and this preparation method in turn includes the following steps:
(1) deionized water is added reaction pot, be warming up to 60-62 DEG C and constant temperature, slowly add acidity regulator, stir 10-15 minute;
(2) open homogenizing and drop into Merquat 280/C13-16 isoparaffin/laureth-25 mixture fast, homogenizing 30-60 second, open to stir and continue dispersion, anion surfactant, amphoteric surfactant, acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer, natural oil is added successively after it stirs, antiseptic, stirring, be warming up to 75-85 DEG C, dispersed with stirring is even;
(3) treat that material body is all uniformly dispersed, constant temperature is lowered the temperature after half an hour; Be cooled to less than 40 DEG C and add spice regulator, stir, be i.e. obtained bath oil.
In above-mentioned preparation method, step (1) first adds the disodiumedetate with softening of water effect in deionized water, stirring and dissolving before intensification, then adds the cation guar gum with the effect of conditioning skin moistening and disperse; Step (2) adds cocos nucifera oil acyl glycine potassium, Merquat 280, lauric acid, stearic acid while adding natural oil.
The preparation method of emulsus bath foam of the present invention, according to the difference of each constitutive property, carries out successively adding and disperseing, thus obtains the stable system of character.Preparation method of the present invention, technique is simple, and parameter is easy to control, and is suitable for size producer and promotes the use of.
Detailed description of the invention
Here is specific embodiments of the invention, and these embodiments just to containing the several formula of bath foam of natural oil and illustrating of preparation method, and are not used to limit the scope of the invention.
1, containing the formula of the bath oil of natural oil
2, containing the preparation method of the bath oil of natural oil
1) in proportion above-mentioned deionized water and disodiumedetate are added reaction pot stirring and dissolving, continue to add cation guar gum C-14S and disperse, be warming up to 60 DEG C and constant temperature, slowly add citric acid and stir 10-15 minute;
2) open homogenizing and drop into macromolecule washing thickening agent T-03B fast, homogenizing 30-60 second, open to stir and continue dispersion, polyoxyethylenated alcohol sodium sulfate, ammonium lauryl sulfate, cocoamidopropyl dimethyl betanin, cocos nucifera oil acyl glycine potassium, macromolecule washing thickening agent T-02, polyquaternary ammonium salt, methyl hydroxybenzoate, lauric acid, stearic acid, olive oil and/soybean oil is added successively after it stirs, stir, be warming up to 75-85 DEG C, dispersed with stirring is even;
3) treat that material body is all uniformly dispersed, constant temperature is lowered the temperature after half an hour, is cooled to less than 40 DEG C and adds essence, stir, namely obtain product bath oil.
3, Performance Detection
After testing, indices meets the requirement of GB " QB1994-2004 bath shampoo " to the bath oil containing natural oil that each formula above-mentioned obtains, and the test result of its stability is as following table:
Claims (9)
1. one kind contains natural oil emulsus bath foam, comprise surfactant, thickening agent, additive and deionized water, it is characterized in that: described surfactant is made up of anion surfactant and amphoteric surfactant, anion surfactant is ammonium lauryl sulfate, polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, amide groups polyoxyethylene ether magnesium sulfate, one or more in SAS, amphoteric surfactant is cocamido propyl betaine, empgen BB, dodecyl CAB, dimethyl dodecyl amine oxide, cocoamidopropyl dimethyl betanin, cocamidopropyl propyl amide hydroxyl sulphonic acid betaine, coco imidoazolinium, one or more in fatty alcohol-polyoxyethylene ether disodium sulfosuccinate salt, their mass ratioes in bath foam are anion surfactant 15-25%, amphoteric surfactant 1-6%, described thickening agent is macromolecule washing thickening agent, and this macromolecule washing thickening agent is by acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer and Merquat 280/C
13-16isoparaffin/laureth-25 mixture forms, and their mass ratioes in bath foam are acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer 2-4%, Merquat 280/C
13-16isoparaffin/laureth-25 mixture 2-4%, described additive comprises antiseptic, acidity regulator and spice regulator, described bath foam also includes natural oil, and the mass ratio of natural oil in bath foam is 1-2%.
2. according to claim 1 containing natural oil emulsus bath foam, it is characterized in that: the macromolecule washing thickening agent of described acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer to be the model produced in Shantou City Daqian High and New Technology Research Center Co., Ltd be T-02; Merquat 280/C
13-16isoparaffin/laureth-25 mixture be Shantou City Daqian High and New Technology Research Center Co., Ltd produce model be T-03B macromolecule washing thickening agent.
3. according to claim 2 containing natural oil emulsus bath foam, it is characterized in that: described anion surfactant by content be 70% polyoxyethylenated alcohol sodium sulfate and content be 70% ammonium lauryl sulfate form with the ratio of mass ratio 1:1; Described amphoteric surfactant to be content be 35% cocoamidopropyl dimethyl betanin.
4. according to Claims 2 or 3 containing natural oil emulsus bath foam, it is characterized in that: described natural oil is olive oil and/or soybean oil.
5. according to Claims 2 or 3 containing natural oil emulsus bath foam, it is characterized in that: described bath foam also comprises cation guar gum, the Merquat 280 with conditioning skin moistening effect there is the lauric acid of skin moistening interception, stearic acid and there is the disodiumedetate of softening of water effect; The mass ratio of each component in bath foam is cation guar gum is 0.2-0.8%, Merquat 280 is 0.5-1.5%, lauric acid is 1-2%, stearic acid is 1-2%, disodiumedetate is 0.2-0.8%.
6. according to Claims 2 or 3 containing natural oil emulsus bath foam, it is characterized in that: described antiseptic is methyl hydroxybenzoate, acidity regulator is citric acid, spice regulator is spice, their mass ratioes in bath foam are methyl hydroxybenzoate 0.2-0.3%, citric acid 0.2-0.25%, spice 0.1-0.3%.
7. according to Claims 2 or 3 containing natural oil emulsus bath foam, it is characterized in that: described surfactant also comprises cocos nucifera oil acyl glycine potassium, the mass ratio of cocos nucifera oil acyl glycine potassium in bath foam is 3-6%.
8. contain a preparation method for natural oil emulsus bath foam described in claim 1, this preparation method in turn includes the following steps:
(1) deionized water is added reaction pot, be warming up to 60-62 DEG C and constant temperature, slowly add acidity regulator, stir 10-15 minute;
(2) open homogenizing and drop into Merquat 280/C13-16 isoparaffin/laureth-25 mixture fast, homogenizing 30-60 second, open to stir and continue dispersion, anion surfactant, amphoteric surfactant, acrylic acid/acrylamide ylmethyl propane sulfonic acid copolymer, natural oil is added successively after it stirs, antiseptic, stirring, be warming up to 75-85 DEG C, dispersed with stirring is even;
(3) treat that material body is all uniformly dispersed, constant temperature is lowered the temperature after half an hour, is cooled to less than 40 DEG C and adds spice regulator, stir, i.e. obtained bath oil.
9. according to claim 8 containing the preparation method of natural oil emulsus bath foam, it is characterized in that: described step (1) first adds the disodiumedetate with softening of water effect in deionized water before intensification, stirring and dissolving, then add the cation guar gum with conditioning skin moistening effect and disperse; Described step (2) adds cocos nucifera oil acyl glycine potassium, Merquat 280, lauric acid, stearic acid while adding natural oil.
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| DE102014207421A1 (en) * | 2014-04-17 | 2015-10-22 | Evonik Degussa Gmbh | Surfactant compositions and high oily formulations containing these |
| CN106901998B (en) * | 2015-12-22 | 2020-06-12 | 广州市浪奇实业股份有限公司 | Bath foam |
| CN106511140B (en) * | 2016-01-04 | 2019-08-16 | 无限极（中国）有限公司 | A kind of bath oil and preparation method thereof |
| CN106109275B (en) * | 2016-07-20 | 2019-08-06 | 珠海伊斯佳科技股份有限公司 | A kind of foaming bath oil and preparation method thereof rich in vegetable oil |
| CN106309234A (en) * | 2016-09-22 | 2017-01-11 | 佛山慧创正元新材料科技有限公司 | Weak-acid bath wash for baby |
| CN108420774A (en) * | 2018-05-29 | 2018-08-21 | 北京明弘科贸有限责任公司 | A kind of moist shower cream and preparation method thereof |
| CN116390708A (en) * | 2020-09-23 | 2023-07-04 | 莱雅公司 | Composition for cleansing and/or removing cosmetics from keratin materials |
| CN116407465A (en) * | 2023-06-10 | 2023-07-11 | 汕头市深泰新材料科技发展有限公司 | Application of high molecular polymer in improving stability of toothpaste product |
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| CN101342120A (en) * | 2008-09-02 | 2009-01-14 | 广东拉芳日化有限公司 | Shower cream |
| CN103108674A (en) * | 2010-06-08 | 2013-05-15 | 欧莱雅 | Colored aqueous cosmetic compositions |
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| US9381150B2 (en) * | 2008-03-07 | 2016-07-05 | Kimberly-Clark Worldwide, Inc. | Alcohol antimicrobial skin sanitizing compositions including cationic compatible thickeners |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101342120A (en) * | 2008-09-02 | 2009-01-14 | 广东拉芳日化有限公司 | Shower cream |
| CN103108674A (en) * | 2010-06-08 | 2013-05-15 | 欧莱雅 | Colored aqueous cosmetic compositions |
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