CN106901998B - Bath foam - Google Patents
Bath foam Download PDFInfo
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- CN106901998B CN106901998B CN201510981621.7A CN201510981621A CN106901998B CN 106901998 B CN106901998 B CN 106901998B CN 201510981621 A CN201510981621 A CN 201510981621A CN 106901998 B CN106901998 B CN 106901998B
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- surfactant
- amphoteric surfactant
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Biophysics (AREA)
- Molecular Biology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses bath foam. It comprises an anionic surfactant, an amphoteric surfactant, a nonionic surfactant and a thickening agent; the weight percentage of the anionic surfactant is 2-6%, and the anionic surfactant mainly comprises any one or the combination of alkyl ether carboxylate, phosphate ester type anionic surfactant and fatty acyl amino acid salt; the weight percentage of the amphoteric surfactant is 5-12%, and the amphoteric surfactant mainly comprises any one or the combination of a betaine amphoteric surfactant, sodium lauroamphoacetate and an amine oxide amphoteric surfactant; the weight percentage of the nonionic surfactant is 1-4%, and the nonionic surfactant consists of alkyl polyglycoside surfactant and PEG-8 sorbitan laurate; the thickener is a non-alkanolamide thickener. The invention has no sulfate and adopts a non-alkanolamide thickening system, so that the formula is milder and safer, and the risk substances in the product are lower.
Description
Technical Field
The invention belongs to the technical field of daily chemical articles, and particularly relates to bath foam.
Background
The common non-soap-based shower gel generally uses fatty alcohol-polyoxyethylene ether sodium sulfate or fatty alcohol-polyoxyethylene ether ammonium sulfate as a main surfactant. However, sodium fatty alcohol polyoxyethylene ether sulphate or ammonium fatty alcohol polyoxyethylene ether sulphate both suffer from two major problems, namely dioxane and sulphate groups. The fatty alcohol polyoxyethylene ether sulfate can generate a byproduct dioxane in the sulfonation process. Dioxane is an organic compound, namely dioxane, 1, 4-dioxane, belonging to a micro-toxic class, is irritant to the skin, eyes and respiratory system and may cause damage to the liver, kidneys and nervous system, and acute poisoning may lead to death. Therefore, the use of the fatty alcohol polyoxyethylene ether sulfate introduces dioxane into the product, and poses a threat to the health of consumers. Also, sulfates can irritate the eyes and dry hair and skin.
In addition, most body washes employ alkanolamides as thickeners, and most of the prior alkanolamides contain free amines as impurities. Free amine is a potential source of nitrosamine and has carcinogenic effect on human body.
Disclosure of Invention
The invention aims to provide bath foam to overcome the defects in the prior art.
In order to achieve the purpose, the invention adopts the following technical scheme:
a bath lotion comprises anionic surfactant, amphoteric surfactant, nonionic surfactant and thickener; the weight percentage of the anionic surfactant is 2-6%, and the anionic surfactant mainly comprises any one or the combination of alkyl ether carboxylate, phosphate ester type anionic surfactant and fatty acyl amino acid salt; the weight percentage of the amphoteric surfactant is 5-12%, and the amphoteric surfactant mainly comprises any one or the combination of a betaine amphoteric surfactant, sodium lauroamphoacetate and an amine oxide amphoteric surfactant; the weight percentage of the nonionic surfactant is 1-4%, and the nonionic surfactant consists of alkyl polyglycoside surfactant and PEG-8 sorbitan laurate; the thickener is a non-alkanolamide thickener.
Further, the weight percentage of the anionic surfactant is as follows:
0 to 2 percent of alkyl ether carboxylate
0 to 3 percent of phosphate type anionic surfactant
0-3% of fatty acyl amino acid salt.
Preferably, the alkyl ether carboxylate consists of a fatty alcohol polyoxyethylene ether carboxylate and/or an alkanolamide ether carboxylate, wherein: the fatty alcohol-polyoxyethylene ether carboxylate has a structure of R (OCH)2CH2)nOCH2COONa, R being C10～14N is 2 to 9; the alkanol amide ether carboxylate is RCONH (CH)2CH2O)nCH2CH2COONa, R being C10～14Wherein n is 2 to 9.
Preferably, the phosphate type anionic surfactant is any one of or a combination of potassium lauryl phosphate and potassium lauryl ether phosphate.
Preferably, the fatty acyl amino acid salt is any one of sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium cocoyl sarcosinate and sodium cocoyl glutamate, or a combination thereof.
Preferably, the weight percentage of the amphoteric surfactant is as follows:
2 to 8 percent of betaine amphoteric surfactant
2-8% of imidazoline type amphoteric surfactant
0-8% of amine oxide type amphoteric surfactant.
Preferably, the betaine type amphoteric surfactant is any one or combination of cocobetaine, lauramidopropyl betaine, cocamidopropyl betaine and oleamidopropyl betaine; the imidazoline type amphoteric surfactant is sodium rosaceous amphoacetate; the amine oxide type amphoteric surfactant is any one or combination of cocamidopropyl amine oxide, cocamine oxide, lauramidopropyl amine oxide and lauramidopropyl amine oxide.
Preferably, the thickener is a polyethylene glycol polymer thickener. Further, the thickener is selected from the group consisting of PEG-80 glyceryl tallowate, PEG-n (n ═ 6, 8, 12) beeswax, PEG-4 isostearate, PEG-n (n ═ 3, 4, 8, 150) distearate, PEG-18 glyceryl oleate/cocoate, PEG-8 dioleate, PEG-200 glyceryl stearate, PEG-n (n ═ 28, 200) glyceryl tallowate, PEG-7 hydrogenated castor oil, PEG-40 jojoba oil, PEG-2 laurate, PEG-120 methyl glucose dioleate, PEG-150 pentaerythrityl tetrastearate, PEG-55 propylene glycol oleate, PEG-160 sorbitan triisostearate, PEG-n (n ═ 8, 75, 100) stearate, PEG-90 diisostearate, PEG-8-3 dilaurate, PEG-PPG-8-3 dilaurate, PEG-200 glyceryl monostearate, PEG-methyl glyceryl stearate, PEG-2 glyceryl stearate, PEG-7 sorbitan triisostearate, PEG-8, PEG-75, 100 distearate, PEG-90 diisostearate, PEG, PEG-120 methyl glucose trioleate, PEG-200 hydrogenated glycerol palmitoleate, PEG-7 glycerol cocoate, PEG-90 glycerol isostearate, laureth-2, laureth-3 and laureth-4.
The invention also comprises a humectant, emollient oil, citric acid, a preservative and essence.
The invention has no sulfate and adopts a non-alkanolamide thickening system, so that the formula is milder and safer, natural oil of skin can not be excessively removed, and the risk substances in the product are lower. The invention is not only suitable for general bath foam, but also suitable for cleaning the whole body of infants.
Detailed Description
The total active substances of the bath foam mainly comprise an anionic surfactant, an amphoteric surfactant, a nonionic surfactant, a humectant, emollient oil, citric acid, a preservative, a thickening agent and essence. Wherein:
the anionic surfactant is one or the combination of alkyl ether carboxylate, phosphate ester type anionic surfactant and fatty acyl amino acid salt. Wherein: the alkyl ether carboxylate is one or two of fatty alcohol-polyoxyethylene ether carboxylate and alkanolamide ether carboxylate, and the structure of the fatty alcohol-polyoxyethylene ether carboxylate is R (OCH)2CH2)nOCH2COONa, R being C10～14N is 2 to 9; the alkanolamide ether carboxylate is RCONH (CH)2CH2O)nCH2CH2COONa, R being C10～14Wherein n is 2 to 9. The phosphate type anionic surfactant is preferably one or a combination of potassium lauryl phosphate and potassium lauryl phosphate. The fatty acyl amino acid salt is selected from one or the combination of sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium cocoyl sarcosinate and sodium cocoyl glutamate.
The amphoteric surfactant is selected from one or the combination of betaine amphoteric surfactant, imidazoline amphoteric surfactant and amine oxide amphoteric surfactant. Wherein: the betaine type amphoteric surfactant is selected from one or combination of cocobetaine, lauramidopropyl betaine, cocoamidopropyl betaine and oleamidopropyl betaine; the imidazoline surfactant is preferably sodium lauroamphoacetate; the amine oxide type amphoteric surfactant is selected from one or a combination of cocamidopropyl amine oxide, cocamine oxide, lauramidopropyl amine oxide and lauramine oxide.
The nonionic surfactant preferably comprises alkyl polyglycoside surfactant and PEG-80 sorbitan laurate.
The thickener is a polyethylene glycol-based polymer thickener, preferably PEG-80 glyceryl tallowate, PEG-n (n ═ 6, 8, 12) beeswax, PEG-4 isostearate, PEG-n (n ═ 3, 4, 8, 150) distearate, PEG-18 glyceryl oleate/cocoate, PEG-8 dioleate, PEG-200 glyceryl stearate, PEG-n (n ═ 28, 200) glyceryl tallowate, PEG-7 hydrogenated castor oil, PEG-40 jojoba oil, PEG-2 laurate, PEG-120 methyl glucose dioleate, PEG-150 pentaerythretetrastearate, PEG-55 propylene glycol oleate, PEG-160 sorbitan triisostearate, PEG-n (n ═ 8, 75, 100) stearate, PEG-90 diisostearate, PEG-8 glyceryl stearate, PEG-4 glyceryl stearate, PEG-200 glyceryl stearate, PEG-4 glyceryl stearate, PEG-200 glyceryl stearate, PEG-28 sorbitan triisostearate, PEG-8, 75, 100 stearate, PEG-100 glyceryl stearate, and PEG, PEG-8PPG-3 dilaurate, PEG-120 methyl glucose trioleate, PEG-200 hydrogenated glycerol palmitoleate, PEG-7 glycerol cocoate and PEG-90 glycerol isostearate, and is compounded with laureth-2, laureth-3 and laureth-4.
The humectant is selected from glycerol, 1, 3-propylene glycol, glyceryl polyether-26, diglycerol, sodium hyaluronate, sodium alginate, β -dextran
The skin moistening oil can be natural oil or synthetic oil.
The preservative and the essence are common raw materials of the bath foam.
Examples
The bath foam is prepared by a conventional preparation method of the bath foam, the total active substances in the examples 1-12 are 10-20% by weight, and the composition distribution is as follows:
examples 1 to 12
Skin irritation test
The invention uses Zein (Zein) method to test the irritability of the above examples 1-12, the total active matter weight percentage content in the tested sample concentration is 1%, the result is as follows:
| examples | Zein (g)/g surfactant |
| 1 | 0.2231 |
| 2 | 0.0521 |
| 3 | 0.1065 |
| 4 | 0.2433 |
| 5 | 0.1007 |
| 6 | 0.1635 |
| 7 | 0.0976 |
| 8 | 0.0671 |
| 9 | 0.2318 |
| 10 | 0.0334 |
| 11 | 0.2177 |
| 12 | 0.1063 |
Comparative example
| Comparative active composition | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Sodium fatty alcohol Ether sulfate | 10 | 8 | 8 | 6 |
| Sodium fatty alcohol sulfate | 0 | 2 | 0 | 2 |
| Lauramidopropyl betaine | 0 | 0 | 2 | 2 |
| Alkanolamides | 1 | 1 | 1 | 1 |
| Glycerol | 2 | 2 | 2 | 2 |
| Zein (g)/g surfactant | 1.7176 | 2.0311 | 1.3988 | 0.7916 |
As can be seen from the above two tables, the skin irritation of the present invention is significantly lower, and the product formulation is milder and safer.
Claims (5)
1. A bath foam comprising an anionic surfactant, an amphoteric surfactant, a nonionic surfactant and a thickener, characterized in that,
the weight percentage of the anionic surfactant is 2-6%, and the anionic surfactant is composed of any one or the combination of alkyl ether carboxylate, phosphate ester type anionic surfactant and fatty acyl amino acid salt;
the weight percentage of the amphoteric surfactant is 5-12%, and the amphoteric surfactant comprises any one or combination of betaine amphoteric surfactant, sodium lauroamphoacetate and amine oxide amphoteric surfactant;
the weight percentage of the nonionic surfactant is 1-4%, and the nonionic surfactant consists of alkyl polyglycoside surfactant and PEG-8 sorbitan laurate;
the thickening agent is a non-alkanol amide type thickening agent;
the anionic surfactant comprises the following components in percentage by weight:
the alkyl ether carboxylate is more than 0 and less than or equal to 2 percent
0 to 3 percent of phosphate type anionic surfactant
0-3% of fatty acyl amino acid salt;
the alkyl ether carboxylate consists of fatty alcohol polyoxyethylene ether carboxylate and/or alkanol amide ether carboxylate, wherein: what is needed isThe fatty alcohol-polyoxyethylene ether carboxylate has a structure of R (OCH)2CH2)nOCH2COOM, R is C10～14N is 2 to 9; the alkanol amide ether carboxylate is RCONH (CH)2CH2O)nCH2CH2COOM, R is C10～14N is 2 to 9;
the phosphate type anionic surfactant is any one or combination of potassium lauryl phosphate and potassium lauryl ether phosphate;
the fatty acyl amino acid salt is any one or combination of sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium cocoyl sarcosinate and sodium cocoyl glutamate;
the weight percentage of the amphoteric surfactant is as follows:
2 to 8 percent of betaine amphoteric surfactant
2-8% of imidazoline type amphoteric surfactant
0-8% of amine oxide type amphoteric surfactant.
2. The bath foam according to claim 1, wherein said betaine-type amphoteric surfactant is any one or combination of cocobetaine, lauramidopropyl betaine, cocamidopropyl betaine, and oleamidopropyl betaine; the imidazoline type amphoteric surfactant is sodium rosaceous amphoacetate; the amine oxide type amphoteric surfactant is any one or combination of cocamidopropyl amine oxide, cocamine oxide, lauramidopropyl amine oxide and lauramidopropyl amine oxide.
3. The body wash of claim 1, wherein said thickener is a polyethylene glycol based polymeric thickener.
4. The body wash of claim 3, wherein the thickening agent is selected from the group consisting of PEG-80 glyceryl tallowate, PEG-n beeswax, PEG-4 isostearate, PEG-n distearate, PEG-18 glyceryl oleate/cocoate, PEG-8 dioleate, PEG-200 glyceryl stearate, PEG-n glyceryl tallowate, PEG-7 hydrogenated castor oil, PEG-40 jojoba oil, PEG-2 laurate, PEG-120 methyl glucose dioleate, PEG-150 pentaerythrityl tetrastearate, PEG-55 propylene glycol oleate, PEG-160 sorbitan triisostearate, PEG-n stearate, PEG-90 diisostearate, PEG-8PPG-3 dilaurate, PEG-120 methyl glucose trioleate, PEG-200 hydrogenated glycerol palmitoleate, PEG-7 glycerol cocoate, PEG-90 glycerol isostearate, laureth-2, laureth-3 and laureth-4.
5. The body wash of claim 1, further comprising a humectant, emollient oils, citric acid, a preservative, and a fragrance.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510981621.7A CN106901998B (en) | 2015-12-22 | 2015-12-22 | Bath foam |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510981621.7A CN106901998B (en) | 2015-12-22 | 2015-12-22 | Bath foam |
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| Publication Number | Publication Date |
|---|---|
| CN106901998A CN106901998A (en) | 2017-06-30 |
| CN106901998B true CN106901998B (en) | 2020-06-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510981621.7A Active CN106901998B (en) | 2015-12-22 | 2015-12-22 | Bath foam |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107648096A (en) * | 2017-09-22 | 2018-02-02 | 拉芳家化股份有限公司 | A kind of children's adacrya hair washing bath foam composition |
| CN108754046B (en) * | 2018-06-04 | 2020-12-11 | 嘉兴学院 | Leather softener and preparation method thereof |
| CN109172409B (en) * | 2018-09-20 | 2021-07-27 | 洛娃日化(江苏)股份有限公司 | Thickener aiming at amino acid surfactant, application thereof and shampoo |
| CN111437219B (en) * | 2019-10-31 | 2022-12-20 | 上海新如生物科技有限公司 | Weakly acidic body wash and preparation method thereof |
| CN113018207A (en) * | 2019-12-24 | 2021-06-25 | 上海家化联合股份有限公司 | Self-thickening composition of amino acid surfactants |
| CN111621064A (en) * | 2020-05-29 | 2020-09-04 | 宁夏共享化工有限公司 | Binder for 3D ink-jet printing |
| DE102022208941A1 (en) * | 2022-08-29 | 2024-02-29 | Beiersdorf Aktiengesellschaft | Cleansing preparation for shaving preparation and facial cleansing |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2916629A1 (en) * | 2007-05-30 | 2008-12-05 | Lvmh Rech | Cleaning cosmetic composition, useful e.g. as shampoo composition/shower gel, for skin, preferably face, body/hair, comprises primary anionic surfactant with cleaning action, and crosslinked polymer/crosslinked super absorbent copolymer |
| CN101342120A (en) * | 2008-09-02 | 2009-01-14 | 广东拉芳日化有限公司 | Shower cream |
| CN103705404A (en) * | 2013-12-31 | 2014-04-09 | 汕头市大千高新科技研究中心有限公司 | Emulsion bath foam containing natural oil and preparation method thereof |
| CN104940042A (en) * | 2015-06-18 | 2015-09-30 | 杭州孔凤春化妆品有限公司 | Low-irritation bath product formula composition and preparation method thereof |
-
2015
- 2015-12-22 CN CN201510981621.7A patent/CN106901998B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2916629A1 (en) * | 2007-05-30 | 2008-12-05 | Lvmh Rech | Cleaning cosmetic composition, useful e.g. as shampoo composition/shower gel, for skin, preferably face, body/hair, comprises primary anionic surfactant with cleaning action, and crosslinked polymer/crosslinked super absorbent copolymer |
| CN101342120A (en) * | 2008-09-02 | 2009-01-14 | 广东拉芳日化有限公司 | Shower cream |
| CN103705404A (en) * | 2013-12-31 | 2014-04-09 | 汕头市大千高新科技研究中心有限公司 | Emulsion bath foam containing natural oil and preparation method thereof |
| CN104940042A (en) * | 2015-06-18 | 2015-09-30 | 杭州孔凤春化妆品有限公司 | Low-irritation bath product formula composition and preparation method thereof |
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Effective date of registration: 20230616 Address after: 511455 No. 8 Xiaohu South Third Road, Xiaohu Island, Huangge Town, Nansha District, Guangzhou City, Guangdong Province Patentee after: GUANGZHOU LANGQI DAILY NECESSITIES CO.,LTD. Patentee after: GUANGZHOU DAILY CHEMICAL INDUSTRY RESEARCH INSTITUTE CO.,LTD. Address before: 510660 No. 128, Whampoa Avenue, Guangzhou, Guangdong Patentee before: GUANGZHOU LONKEY INDUSTRIAL Co.,Ltd. Patentee before: GUANGZHOU DAILY CHEMICAL INDUSTRY RESEARCH INSTITUTE CO.,LTD. |
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