CN105997572A - Cleansing milk containing nano graphene and preparation method thereof - Google Patents
Cleansing milk containing nano graphene and preparation method thereof Download PDFInfo
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- CN105997572A CN105997572A CN201610333689.9A CN201610333689A CN105997572A CN 105997572 A CN105997572 A CN 105997572A CN 201610333689 A CN201610333689 A CN 201610333689A CN 105997572 A CN105997572 A CN 105997572A
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- graphene
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
Abstract
The invention provides cleansing milk which contains nano graphene, has fine foam, removes acne and eliminates inflammation and a preparation method thereof. The cleansing milk containing nano graphene comprises, by weight proportion, 0.05-0.1 part of nano graphene and 2-5 parts of sodium lauroyl taurate. According to the cleansing milk containing nano graphene and the preparation method thereof, the nano graphene physical sterilization component and sodium lauroyl taurate are added, and the cleansing milk is safe and free of stimulation and has surface activity performance of fine foam. The cleansing milk further prevents and removes acne while cleaning the face thoroughly, has a very good acne removal and inflammation diminishing effect on the skin, and is suitable for all skin types.
Description
Technical field
The present invention relates to a kind of cleansing milk and preparation method thereof, especially a kind of nano-graphene that contains is washed one's face
Milk and preparation method thereof.
Background technology
The PH of soap base cleansing milk in the market is much larger than 7, belongs to alkalescence, and zest is the biggest；Meanwhile,
Also have a lot of anti-acne facial cleanser products often to contain ethanol, chloromycetin etc. and illegally add antibiotic, to human body
Can produce drug resistance, some is also added with coloured Chinese medicine powder and increases deep skin color, the most unsightly.
Summary of the invention
For above-mentioned technological deficiency with not enough, the invention provides a kind of zest is little, foam is fine and smooth and
Cleansing milk containing nano-graphene with acne-removing inflammation-diminishing effect and preparation method thereof.
The technical scheme is that the present invention proposes a kind of cleansing milk containing nano-graphene, including
Weight ratio: nano-graphene 0.05-0.1 part and lauroyl sodium taurocholate 2-5 part.
Preferential as technique scheme, also includes sodium lauroyl sarcosine 2.5-3.5 part and cocos nucifera oil
Amido propyl betaine 2-3 part.
Preferential as technique scheme, also includes laureth sulfosuccinate disodium
15-30 part.
Preferential as technique scheme, also includes hyaluronate sodium 0.1 part and deionized water 46-58
Part.
Preferential as technique scheme, also includes glycerol 5-7 part and 1.3 butanediol 2-4 parts.
Preferential as technique scheme, also includes 1.0-2.0 carbomer and methylcellulose
1.0-1.5 part.
Preferential as technique scheme, also includes sodium chloride 1.5-2.0 part and triethanolamine regulation
Mastic 0.8-1.2 part, described triethanolamine regulation mastic pH value is between 5.5-6.0.
Preferential as technique scheme, also includes Methylisothiazolinone 0.3-0.4 part, essence
0.3-0.5 part.
A kind of preparation method containing nano-graphene cleansing milk, comprises the steps:
(1) it is 0.05-0.1 part nano-graphene, 0.1 part of hyaluronate sodium and 1.0-2.0 by weight portion
Carbomer joins in the deionized water of 46-58 part, homogenizing 5-8 minute；It is separately added into 5-7 part again
Glycerol, 2-4 part 1.3 butanediol and 1.0-1.5 part methylcellulose are heated to 80-85 DEG C and are sufficiently stirred for
Dissolve transparent；
(2) it is 2-5 part lauroyl sodium taurocholate, 2.5-3.5 part Hamposyl L by weight portion
Sodium, 2-3 part cocamido propyl betaine and 15-30 part laureth sulfosuccinate disodium
Stirring is separately added into, and maintains about 75 DEG C to be less than positive and negative 1 degree, fully dissolves；
(3) it is cooled to 45 degree, is 1.5-2.0 part sodium chloride and triethanolamine regulation cream by weight portion
Body (regulation mastic pH value is between 5.5-6.0) is separately added into and uniform stirring.
Preferential as technique scheme, described step (1) heating-up temperature is 80 DEG C, step (2)
In maintenance temperature be 75 DEG C.
Preferential as technique scheme, it is characterised in that: also include step (4): be heated to 80 DEG C
Be completely dissolved, after be cooled to 45 DEG C, then be cooled to 40 degree, by different for weight portion 0.3-0.4 part methyl
Thiazolinone and 0.3-0.5 part essence are separately added into, and stir, ageing, obtain containing nano-graphite
The cleansing milk of alkene..
Having the beneficial effect that of the cleansing milk of the present invention and preparation method thereof:
The present invention propose containing nano-graphene cleansing milk and preparation method thereof, with the addition of nano-graphene
Physical sterilization composition, allows antibacterial will not produce drug resistance, has good acne-removing inflammation-diminishing effect to skin；
Comedo teen-age to chronic inflammation (being also acne) has good effect.Its nano-graphene
Can kill 10 various bacteria such as bacillus pyocyaneus, escherichia coli, its nano-graphene itself is to be linked to be one
The carbon atom of string, just as one layer of the most closely knit cloth the thinnest, they tackle the mode of antibacterial 3 kinds: the
One is directly to cut, and owing to Graphene is nano level, and antibacterial is micron order, and the former is less than the latter
1000 times, Graphene, as same cutter the sharpest, is directly cut antibacterial to death；The second is hungry to death
Antibacterial, antibacterial can be wrapped up as cloth by nano level Graphene closely, makes antibacterial absorb
Less than nutrition, die of starvation；The third is slowly to wither away, and owing to Graphene is the least, antibacterial can be by stone
Ink alkene gulps down enter " tripe " inner, can suffer from diarrhea uncomfortable just as people has eaten foreign body, cause antibacterial slowly to be withered away,
Exactly because this physical sterilization method of Graphene, allow antibacterial will not produce drug resistance, skin is had
Well acne-removing inflammation-diminishing effect.
Meanwhile, use natural amino acid surfactant can also whitening nutrition flesh while cleaning skin
Skin, its lauroyl sodium taurocholate is a kind of safe and non-stimulating surfactant, has good going
Dirty power and emulsifying capacity；Meanwhile, lauroyl sodium taurocholate is a kind of safe and non-stimulating surface activity
Agent, has good detergency and emulsifying capacity, and abundant fine and smooth foam can give skin gentleness, grow
Profit, salubrious sensation, good stability, non-stimulated to eyes, and with sodium lauroyl sarcosine compound right
Skin irritation is less, belongs to standard amino acid solution surfactant；
Cocamido propyl betaine and laureth sulfosuccinate disodium compound, and have good
Cleaning, foaming, opsonic action, zest is little, foaming abundancy is fine and smooth and stable.
This cleansing milk preparation method is simple, economical and efficient, manufacturing cycle are short, natural pollution-free, product
Stable in properties, emulsifying effectiveness are good.
Detailed description of the invention
Embodiment 1
The preparation method containing nano-graphene cleansing milk of the present embodiment, comprises the following steps:
A) it is 0.06 part of nano-graphene, 1.5 parts of carbomers and 0.1 part of hyaluronic acid by weight portion
Sodium joins in 46-58 part deionized water of 58 parts, homogenizing 5 minutes；Be separately added into again 5 parts of glycerol,
4 part of 1.3 butanediol and 1.5 parts of methylcellulose are heated to 80-85 DEG C and are sufficiently stirred for dissolving transparent；
Hyaluronate sodium at such a temperature, can ensure the abundant sterilizing of product, and solution temperature is less than
80 DEG C, sterilizing is incomplete, and temperature is higher than 85 DEG C, uprises for horsepower requirements, is also easily destroyed each
The stability of composition.Nano-graphene physical sterilization composition, allows antibacterial will not produce drug resistance, to skin
Skin has good acne-removing inflammation-diminishing effect；Glycerol and 1.3 butanediols have a good moisture-keeping function, carbomer,
Methyl cellulose have good thickening lubricant effect.
B) it is 2 parts of lauroyl sodium taurocholates, 3 portions of sodium lauroyl sarcosines, 2 portions of coconut palms by weight portion
Oleamide CAB and 20 parts of laureth sulfosuccinate disodium stirrings are separately added into also
Maintain about 75 DEG C to be less than positive and negative 1 degree, fully dissolve；
Lauroyl sodium taurocholate is a kind of safe and non-stimulating surfactant, has good decontamination
Power and emulsifying capacity, abundant fine and smooth foam can give the sensation that skin is gentle, moist, salubrious, surely
Qualitative good, non-stimulated to eyes and compounding with sodium lauroyl sarcosine less to skin irritation, belong to
In standard amino acid solution surfactant；Cocamido propyl betaine and laureth sulfosuccinic
Acid esters disodium compounds, and has good cleaning, foaming, opsonic action, and zest is little, foaming abundancy
Fine and smooth and stable.
C) it is cooled to 45 degree, is 1.5 parts of sodium chloride and 0.8 triethanolamine regulation mastic by weight portion
It is separately added into and uniform stirring.
D) 0.3 part of Methylisothiazolinone of weight portion and 0.3 part of essence are separately added into, stir,
Ageing, obtains the cleansing milk containing nano-graphene.
Embodiment 2
The preparation method of the pectin mastic facial film of the present embodiment, comprises the following steps:
A) it is 0.06 part of nano-graphene, 2 parts of carbomers and 0.1 part of hyaluronate sodium by weight portion
Join in the deionized water of 51 parts, homogenizing 5 minutes；Be separately added into again 5 parts of glycerol, 4 part 1.3
Butanediol and 1.5 parts of methylcellulose are heated to 80-85 DEG C and are sufficiently stirred for dissolving transparent；
B) it is 3 parts of lauroyl sodium taurocholates, 3 parts of sodium lauroyl sarcosines and 2 portions of coconut palms by weight portion
Oleamide CAB and 25 parts of laureth sulfosuccinate disodium stirrings are separately added into also
Maintain about 75 DEG C to be less than positive and negative 1 degree, fully dissolve；
C) it is cooled to 45 degree, is 1.5 parts of sodium chloride and 1.2 parts of triethanolamine regulation cream by weight portion
Body is separately added into and uniform stirring.
D) 0.3 part of Methylisothiazolinone of weight portion and 0.3 part of essence are separately added into, stir,
Ageing, obtains the cleansing milk containing nano-graphene.
Embodiment 2 is thicker than embodiment 1 mastic, and foam is more and fine and smooth, and embodiment 1 mastic also has
Mobility.
Embodiment 3
The preparation method of the pectin mastic facial film of the present embodiment, comprises the following steps:
A) it is that 0.1 part of nano-graphene, 2 parts of carbomers and 0.1 part of hyaluronate sodium add by weight portion
Enter in the deionized water of 46 parts, homogenizing 5 minutes；It is separately added into 6 parts of glycerol, 2 part of 1.3 fourth again
Glycol and 2 parts of methylcellulose are heated to 80-85 DEG C and are sufficiently stirred for dissolving transparent；
B) it is 4 parts of lauroyl sodium taurocholates, 3 parts of sodium lauroyl sarcosines and 3 portions of coconut palms by weight portion
Oleamide CAB and 30 parts of laureth sulfosuccinate disodium stirrings are separately added into also
Maintain about 75 DEG C to be less than positive and negative 1 degree, fully dissolve；
C) it is cooled to 45 degree, is 2.0 parts of sodium chloride and 1.0 parts of triethanolamine regulation cream by weight portion
Body is separately added into and uniform stirring.
D) 0.3 part of Methylisothiazolinone of weight portion and 0.5 part of essence are separately added into, stir,
Ageing, obtains the cleansing milk containing nano-graphene.
Embodiment 3 is thicker than embodiment 2 mastic, the more rich exquisiteness of foam.
Under by test illustrate above-mentioned cleansing milk good result.
Each process selects face's corse sweat pore respectively, the volunteer 30 of acne is tested, point
Not Yong the cleansing milk for preparing of embodiment 1-3, sooner or later wash one's face for twice every day, unite after using 50 days continuously
Meter improvement rate (%).Treatment standard: be obviously improved: washed skin moisturizing is moist, corse sweat pore,
Acne phenomenon alleviates significantly or disappears；Alleviate: corse sweat pore, acne phenomenon are to a certain degree
Alleviate or disappear；Invalid: face's pore, acne phenomenon are the most clearly.Result of the test see table:
Experimental result is shown in Table 1:
Table 1 result shows: embodiment 1-3 has preferably effect to corse sweat pore, Cuo acne-removing inflammation-diminishing
Really.
Embodiment described above is only to be described the preferred embodiment of the present invention, the most right
The scope of the present invention is defined, under design spirit premise without departing from the present invention, and this area unskilled labor
Various deformation that technical solution of the present invention is made by journey technical staff and improvement, all should fall into the present invention's
In the protection domain that claims determine.
Claims (10)
1. the cleansing milk containing nano-graphene, including weight ratio: nano-graphene
0.05-0.1 part and lauroyl sodium taurocholate 2-5 part.
Cleansing milk containing nano-graphene the most according to claim 1, it is characterised in that: also wrap
Include sodium lauroyl sarcosine 2.5-3.5 part and cocamido propyl betaine 2-3 part.
Cleansing milk containing nano-graphene the most according to claim 1, it is characterised in that: also wrap
Include laureth sulfosuccinate disodium 15-30 part.
Cleansing milk containing nano-graphene the most according to claim 1, it is characterised in that: also wrap
Include hyaluronate sodium 0.1 part, deionized water 46-58 part, glycerol 5-7 part and 1.3 butanediol 2-4
Part.
Cleansing milk containing nano-graphene the most according to claim 1, it is characterised in that: also wrap
Include 1.0-2.0 carbomer and methylcellulose 1.0-1.5 part.
Cleansing milk containing nano-graphene the most according to claim 1, it is characterised in that: also wrap
Including sodium chloride 1.5-2.0 part and triethanolamine regulation mastic 0.8-1.2 part, described triethanolamine regulates
Mastic pH value is at 5.5-6.0.
7. according to the arbitrary described cleansing milk containing nano-graphene of claim 1-6, it is characterised in that:
Also include Methylisothiazolinone 0.3-0.4 part, essence 0.3-0.5 part.
8. the preparation method containing nano-graphene cleansing milk, comprises the steps:
(1) it is 0.05-0.1 part nano-graphene, 0.1 part of hyaluronate sodium and 1.0-2.0 by weight portion
Carbomer joins in the deionized water of 46-58 part, homogenizing 5-8 minute；It is separately added into 5-7 part again
Glycerol, 2-4 part 1.3 butanediol and 1.0-1.5 part methylcellulose are heated to 80-85 DEG C and are sufficiently stirred for
Dissolve transparent；
(2) it is 2-5 part lauroyl sodium taurocholate, 2.5-3.5 part Hamposyl L by weight portion
Sodium, 2-3 part cocamido propyl betaine and 15-30 part laureth sulfosuccinate disodium
Stirring is separately added into, and maintains about 75 DEG C to be less than positive and negative 1 degree, fully dissolves；
(3) it is cooled to 45 degree, is 1.5-2.0 part sodium chloride and 0.8-1.2 part three second by weight portion
Hydramine regulation mastic, is separately added into and uniform stirring, and described triethanolamine regulation mastic pH value exists
5.5-6.0。
The preparation method of pectin mastic facial film the most according to claim 8, it is characterised in that: institute
Stating step (1) heating-up temperature is 80 DEG C, and the maintenance temperature in step (2) is 75 DEG C.
The preparation method of the cleansing milk of nano-graphene the most according to claim 8 or claim 9, its
Be characterised by: also include step (4): be heated to 80 DEG C and be completely dissolved, after be cooled to 45 DEG C, then drop
Weight portion 0.3-0.4 part Methylisothiazolinone and 0.3-0.5 part essence, to 40 degree, are added by temperature respectively
Enter, stir, ageing, obtain the cleansing milk containing nano-graphene.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610333689.9A CN105997572B (en) | 2016-05-19 | 2016-05-19 | Facial cleanser containing nano graphene and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610333689.9A CN105997572B (en) | 2016-05-19 | 2016-05-19 | Facial cleanser containing nano graphene and preparation method thereof |
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| CN105997572A true CN105997572A (en) | 2016-10-12 |
| CN105997572B CN105997572B (en) | 2021-02-02 |
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Cited By (7)
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| CN106491375A (en) * | 2016-12-14 | 2017-03-15 | 拜东辰 | A kind of feature Graphene handwashing liquid and preparation method thereof |
| CN107057880A (en) * | 2017-04-14 | 2017-08-18 | 南通强生石墨烯科技有限公司 | Graphene antibiosis complex liquid and preparation method thereof |
| CN107157781A (en) * | 2017-06-18 | 2017-09-15 | 黑龙江嘉能高科技开发有限责任公司 | A kind of single-layer graphene repair membrane and preparation method |
| CN107822979A (en) * | 2017-11-30 | 2018-03-23 | 宁波秋日小城智能科技有限公司 | A kind of preparation method of the freeze-dried powder of the composition with acne-removing |
| CN107875059A (en) * | 2017-11-30 | 2018-04-06 | 宁波秋日小城智能科技有限公司 | A kind of composition with acne-removing |
| CN109846728A (en) * | 2019-04-19 | 2019-06-07 | 泉州市福勤科技推广有限公司 | A kind of preparation method of the clean facial cleanser containing nano-graphene |
| CN112057396A (en) * | 2020-09-11 | 2020-12-11 | 广东墨睿科技有限公司 | Graphene-containing mild cleansing facial cleanser |
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| CN112057396A (en) * | 2020-09-11 | 2020-12-11 | 广东墨睿科技有限公司 | Graphene-containing mild cleansing facial cleanser |
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| Publication number | Publication date |
|---|---|
| CN105997572B (en) | 2021-02-02 |
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