CN106176495B - A kind of carefree shower cream and preparation method thereof - Google Patents

A kind of carefree shower cream and preparation method thereof Download PDF

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Publication number
CN106176495B
CN106176495B CN201610792799.1A CN201610792799A CN106176495B CN 106176495 B CN106176495 B CN 106176495B CN 201610792799 A CN201610792799 A CN 201610792799A CN 106176495 B CN106176495 B CN 106176495B
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China
Prior art keywords
parts
carefree
liquid
shower cream
reaction kettle
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CN106176495A (en
Inventor
张思明
吴刚
韦慧玉
邓燕
张小丽
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Double Needle (jiangsu) Industrial Co Ltd
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Double Needle (jiangsu) Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

Abstract

The present invention provides a kind of carefree shower creams and preparation method thereof, are related to technical field of daily necessities.The carefree shower cream includes the component of following parts by weight:50-60 parts of carefree liquid, 13-16 parts of hydroxypropyl celluloses, 10-12 parts of needle-shaped methyl sodiosul foaliphatates, MEA, 110-140 parts of fatty alcohol-ether sodium sulfates of 10-12 parts of coconut oleoyl amines, 40-55 parts of Cocoamidopropyl betaines, 10-12 parts of polyquaterniums -7,12-15 parts of glycol distearates, 14-16 parts of sodium chloride, 6-8 parts of essence, 1.2-3 parts of methylparabens, 0.1-0.2 parts of citric acids, water is solvent.Preparation method includes:Deionized water is added in reaction kettle and heats;The component of carefree shower cream is added and stirs evenly;Cool down to the substance in institute's reaction kettle;Adjust pH value;Carefree liquid is added into reaction kettle;Deionized water polishing quality is added;Vacuumize degassing.The present invention in shower cream by adding carefree liquid, to reach irritability of releiving, quickly eliminates the purpose of fatigue, has the characteristics that safe and efficient.

Description

A kind of carefree shower cream and preparation method thereof
Technical field
The present invention relates to technical field of daily necessities more particularly to a kind of carefree shower cream and preparation method thereof.
Background technique
Skin is the largest organ of human body, and the metabolism and body discharges for participating in entire human body absorb various elements Maximum gas tank, resist the first barrier of external various injuries.Skin is not only related with external environment, while also and in human body Various organ-tissues are tied in a hundred and one ways, particularly significant to human health.Research data shows:Contain 40 in skin histology Multiple element, the balanced of them has certain positive effect in the presence of to maintenance, the various normal functions for adjusting skin, if element Once it is unbalance, necessarily cause various dermatosis chronic diseases, causes greatly pain to patient, zinc, copper, iron content are more rich in skin Richness, skin are a tight seamless natural coats, human body are covered flawless, it is executed as the soldier of might again The defendance task of human body, protection and defence, secretion and excretion absorb and exhalation, participate in the small chemical plant of manufacture, while being again The special construction for adjusting internal water, salt, acid-base balance and barrier action skin, which plays the role of keeping out buffering, surrounds and annihilates, and becomes people Body the first line of defence, from top to bottom, inside and outside left and right, is not nowhere adjusted body temperature by skin sparing, utilizes radiation, convection current, evaporation etc. Mode radiates temperature adjustment, keeps the body temperature of people permanent constant within 37 DEG C of normal range (NR)s, and skin receives and the various senses of conduction by the light of nature Feel, such as touch, press, is hot, cold, pain, itch, feel specific function, make one to obtain invasion information in time, to prevent external infringement, protection is certainly Body health.
Therefore it needs to prepare a kind of carefree shower cream and at least mitigates or reduce drawbacks described above.
Summary of the invention
The object of the present invention is to provide a kind of carefree shower creams and preparation method thereof, by adding carefree liquid into shower cream With the irritability that achievees the purpose that releive, quickly eliminate fatigue.
The technical solution that the present invention solves above-mentioned technical problem is as follows:
In a first aspect, the carefree shower cream includes the group of following parts by weight the present invention provides a kind of carefree shower cream Part:50-60 parts of carefree liquid, 13-16 parts of hydroxypropyl celluloses, 10-12 parts of needle-shaped methyl sodiosul foaliphatates, 10-12 portions of cocounut oil MEA, 110-140 parts of fatty alcohol-ether sodium sulfates of amide, 40-55 parts of Cocoamidopropyl betaines, 10-12 parts of polyquaterniums -7, 12-15 parts of glycol distearates, 14-16 parts of sodium chloride, 6-8 parts of essence, 1.2-3 parts of methylparabens, 0.1-0.2 parts of lemons Lemon acid, water is solvent.
Optionally, the carefree liquid includes the component of following parts by weight:8-12 parts of radix bupleuri, 8-12 parts of Radix Paeoniae Alba, Radix Angelicae Sinensis 7-12 Part, 6-12 parts of Poria cocos, 5-12 parts of Rhizoma Atractylodis Macrocephalae, 5-12 parts of grapefruit skin, 3-9 parts of wild chrysanthemum, 12-20 parts of lotus leaf and 300-350 parts of water.
Second aspect, the present invention provides a kind of preparation methods of carefree shower cream, add into the shower cream carefree Liquid includes the following steps:
Deionized water is added in reaction kettle and is heated to 60 DEG C -80 DEG C;
Remaining component in addition to carefree liquid of carefree shower cream described in claim 1 is added into the reaction kettle simultaneously It stirs evenly;
Substance in the reaction kettle is carried out to be cooled to 40 DEG C -45 DEG C;
The pH value of substance in the reaction kettle is adjusted using citric acid, the pH value is adjusted to 6.5-8.0;
Carefree liquid is added into the reaction kettle, wherein the carefree liquid is prepared in following preparation process:By institute The all components for stating carefree liquid, which are placed under condition of negative pressure, to be boiled and keeps 2-2.5h to obtain carefree mixture, will be described carefree mixed It closes object and is filtered and obtains filtrate using the sieve that mesh number is at least 800 mesh, the filtrate is the carefree liquid, In, the condition of negative pressure is -0.075Mpa--0.060Mpa;
Deionized water polishing quality is added into the reaction kettle and is stirred to obtain feed liquid, wherein the stirring Revolving speed be 20-30 revs/min;
The feed liquid is put into vacuum emulsifying machine, by vacuumizing degassing, can be obtained final carefree shower cream.
Beneficial effects of the present invention:
Carefree shower cream of the invention, can effectively remove dirt and excess oil in skin pore, and delaying skin declines Old and reduction wrinkle of skin is formed.Carefree shower cream of the invention also has and moistens pure white skin, makes the delicate moist function of skin Effect.
The present invention in shower cream by adding carefree liquid, to reach irritability of releiving, quickly eliminates the purpose of fatigue, has Safe and efficient feature.
Detailed description of the invention
Fig. 1 is the process flow chart of the preparation method of the carefree shower cream of the embodiment of the present invention.
Specific embodiment
The principle and features of the present invention will be described below with reference to the accompanying drawings, and the given examples are served only to explain the present invention, and It is non-to be used to limit the scope of the invention.
The present invention provides a kind of carefree shower cream, the carefree shower cream includes the component of following parts by weight:50-60 parts Carefree liquid, 13-16 part hydroxypropyl cellulose, 10-12 parts of needle-shaped methyl sodiosul foaliphatates, 10-12 parts of coconut oleoyl amine MEA, 110-140 parts of fatty alcohol-ether sodium sulfates, 40-55 parts of Cocoamidopropyl betaines, 10-12 parts of polyquaterniums -7,12-15 parts of second Glycol distearate, 14-16 part sodium chloride, 6-8 parts of essence, 1.2-3 parts of methylparabens, 0.1-0.2 parts of citric acids, water are Solvent.
Fatty alcohol-ether sodium sulfate (AES) has good decontamination, foaming properties, and compatibility is good, resistance to hard water, low-temperature water-soluble The excellent comprehensive performance such as good.Fatty alcohol-ether sodium sulfate production be with fatty alcohol polyoxyethylene ether (AEO) be raw material through sulphation, It neutralizes and obtains.The starting material fatty alcohol of fatty alcohol-ether sodium sulfate can be divided into fat-based, petroleum base according to the difference of raw material sources With coal base three categories.Fatty alcohol-ether sodium sulfate is most important kind in alcohol system surfactant, and the country is mainly used in civilian The fields such as detergent (liquid detergent, dish washing detergent), personal-care supplies (shampoo, bath foam, hand cleanser).
Methyl sodiosul foaliphatate (MES) is always a hot spot of surfactant research and detergent industry.Fat Sour methyl ester sulfonate is based on natural material, mild, and low toxicity has good scourability, compatibility and biological degradability. Needle-shaped methyl sodiosul foaliphatate is easier to quantitative acquisition in process for preparation.
In the present invention, by 10-12 parts of needle-shaped methyl sodiosul foaliphatates and 110-140 parts of fatty alcohol-ether sodium sulfate additions Into carefree bath foam, good dirt-removing power can have, there are good foaming properties, and mild, low toxicity makes Carefree bath foam maintains good dirt-removing functions.
Polyquaternium -7 has that soluble easily in water, safe and nontoxic, hydrolytic stability is good, adaptable etc. excellent to pH value variation Point.In the present invention, 10-12 parts of polyquaterniums -7 are regard as cationic surfactant, can achieve good clean effect.
Coconut oleoyl amine MEA's is mainly used for making formula to become thickening and opaque, and enhances the master in surfactant The cleaning capacity for wanting cleansing is most commonly used to hair conditioner and shower cream etc. and washes in shield product.Although the foaming of coconut oleoyl amine MEA Ability is not to be directly used in cleaning skin or hair, it improves the working efficiency of both hands, and shower cream is made to be easy to be applied to table On face, take out stains to facilitate mechanicalness.It can also provide excellent moisturizing and conditioning to skin.In the present invention, will The cleaning capacity of principal cleaning ingredients can be enhanced as nonionic surfactant in 10-12 parts of coconut oleoyl amine MEA.
Cocoamidopropyl betaine is an extremely mild zwitterionic surfactant, to skin, eye mucous membrane without It stimulates, without allergic reaction, it can be with anionic surfactant, cationic surfactant and nonionic surfactant compatibility And transparent liquid or colloid is obtained, the foam of Cocoamidopropyl betaine is stablized fine and smooth.Meanwhile cocamidopropyl propyl amide beet Alkali is compounded with anionic surfactant, under suitable conditions, Material viscosity can be improved, thickening effect is obvious.Cocounut oil acyl Amine propyl betaine also has flexibility, bactericidal properties and antistatic property.In the present invention, by 40-55 parts of cocamidopropyl propyl amides Glycine betaine can be such that the clean effect of entire shower cream reaches most preferably as zwitterionic surfactant, and have excellent Security performance.
Glycol distearate dissolves after heating in surfactant complex or emulsification, can be precipitated in temperature-fall period Mirror flaky crystal, thus generate nacreous lustre.Using can produce apparent pearl effect in liquid washing products, and can increase The viscosity of product also has skin care, hair care hair care and antistatic property;With other types of surfactant intermiscibility It is good, and its stable pearl effect and thickening conditioning functions can be embodied;It is non-stimulated to skin, it is not damaged to hair;In contrast The pearly-lustre that ethylene glycol double stearate generates is stronger, and the pearly-lustre that ethylene glycol monostearate generates is finer and smoother.In the present invention, Using 12-15 parts of glycol distearates as emulsifier, shower cream can be made to generate preferable nacreous lustre, and can also increased Add the viscosity of shower cream.
The scientific name of methylparaben is to be compounded to carboxyl benzoic ether due to low with toxicity, nonirritant, efficiently easy, It is almost tasteless, nonirritant and the advantages that be able to maintain preferable antibacterial effect in wider pH value range, it becomes Wider food preservative is applied in food processing.In the present invention, using 1.2-3 parts of methylparaben as preservative, It is tasteless nonirritant and have preferable fungistatic effect so that the shower cream safety with higher in the present invention Energy.
Hydroxypropyl cellulose water-soluble and many organic solvent has moderate surface-active in aqueous solution, Thickening and stabilization are generated in aqueous dispersion.In the present invention, using 13-16 parts of hydroxypropyl celluloses as thickening Agent can make shower cream have good thickening effect.
Essence is by the concentration aromatic oil of artificial synthesized imitation fruit and natural perfume material smell, it is a kind of artificial musk Material, is chiefly used in food manufacturing.In the present invention, it is added in shower cream using 6-8 parts of essence, can plays and keep pure and fresh The effect of smell.
Citric acid is primarily present in lemon and citrus, cuticula can be made to fall off, and shallow-layer telangiectasis keeps skin thin Born of the same parents are metabolized enhancing, and moisture in corneocyte can also increased, makes skin moisturizing and high resilience.In the present invention, it uses 0.1-0.2 parts of citric acid can play the role of adjust shower cream pH value, other side effects will not be generated, can also with wash one's hair Other compositions in bath lotion are used together as antibacterial agent.
In the present invention, 14-16 parts of sodium chloride are added in shower cream, have and adjusts ion concentration, protects skin not The effect that can excessively absorb water.
Wherein, the carefree liquid includes the component of following parts by weight:8-12 parts of radix bupleuri, 8-12 parts of Radix Paeoniae Alba, 7-12 parts of Radix Angelicae Sinensis, 6-12 parts of Poria cocos, 5-12 parts of Rhizoma Atractylodis Macrocephalae, 5-12 parts of grapefruit skin, 3-9 parts of wild chrysanthemum, 12-20 parts of lotus leaf and 300-350 parts of water.
Radix bupleuri bitter, cold nature return liver, gallbladder channel, have evacuation to bring down a fever, liver of relaxing, the function of rising Yang.Radix Paeoniae Alba, which has, stabilizes liver The effect of sun, yin is received in blood-nourishing.Radix Angelicae Sinensis has benefiting blood and regulating blood circulation, menstruction regulating and pain relieving, moisturizing dryness and lubricating intestine, anticancer, anti-ageing anti-old, immune function Effect.Poria cocos has the effect of clearing damp and promoting diuresis, invigorating the spleen, tranquilizing the mind.Rhizoma Atractylodis Macrocephalae have air making-up and spleen enlivening, eliminate dampness and have diuretic effect, hidroschesis, miscarriage prevention function Effect.It is grapefruit skin acrid flavour bitter sweet, warm-natured, have the effect of resolving sputum, cough-relieving, qi-regulating, analgesic, cure mainly cough and asthma, the obstruction of the circulation of vital energy uncomfortable in chest, abdomen crymodynia, Food stagnation, hernia etc..Wild chrysanthemum cold nature has dispelling wind and heat from the body, subdhing swelling and detoxicating, it is red to treat furunculosis carbuncle swells, abscess of throat, wind fire The diseases such as eye, headache and dizziness.Lotus leaf clearing away summerheat, sending up the lucid yang, cooling blood and hemostasis are used for hot summer weather polydipsia, summer heat damp diarrhea, and spleen deficiency is let out It rushes down, blood-head tells nosebleed, uterine bleeding of having blood in stool, burnt FOLIUM NELUMBINIS inducing astrigency removing blood stasis and hemostasis.
Fig. 1 is the process flow chart of the preparation method of the carefree shower cream of the embodiment of the present invention.Referring to Fig. 1, the present invention is real It applies example and provides a kind of preparation method of carefree shower cream, carefree liquid is added into the shower cream, is included the following steps:
Deionized water is added in reaction kettle and is heated to 60 DEG C -80 DEG C for step 1.
Step 2, remaining in addition to carefree liquid that carefree shower cream described in claim 1 is added into the reaction kettle Component simultaneously stirs evenly.
Step 3 carries out the substance in the reaction kettle to be cooled to 40 DEG C -45 DEG C.
Step 4, the pH value that substance in the reaction kettle is adjusted using citric acid, the pH value are adjusted to 6.5-8.0.
Carefree liquid is added into the reaction kettle for step 5, wherein the carefree liquid prepared in following preparation process and At:The all components of the carefree liquid are placed under condition of negative pressure and boils and keeps 2-2.5h to obtain carefree mixture, by institute It states carefree mixture and is filtered and obtains filtrate using the sieve that mesh number is at least 800 mesh, the filtrate is described free and unfettered Distant liquid, wherein the condition of negative pressure is -0.075Mpa--0.060Mpa.
Deionized water polishing quality is added into the reaction kettle and is stirred to obtain feed liquid for step 6, wherein institute The revolving speed for stating stirring is 20-30 revs/min.
The feed liquid is put into vacuum emulsifying machine by step 7, by vacuumizing degassing, can be obtained final carefree wash one's hair Bath lotion.
Xiaoyao San in the present invention has carried out appropriate adjustment on the basis of traditional carefree powder formula, to carefree powder formula, To reach irritability of releiving, the purpose of fatigue is quickly eliminated.The carefree powder formula is added in shower cream by the present invention, can achieve It releives irritability, quickly eliminates the purpose of fatigue.
It below will be by specific embodiment come the present invention will be described.
Embodiment 1
In the present embodiment, carefree shower cream includes the component of following parts by weight:50 parts of carefree liquid, 13 parts of hydroxy propyl celluloses Element, 10 parts of needle-shaped methyl sodiosul foaliphatates, 10 parts of coconut oleoyl amine MEA, 110 parts of fatty alcohol-ether sodium sulfates, 40 parts of coconut oleoyl amines Propyl betaine, 10 parts of polyquaterniums -7,12 parts of glycol distearates, 14 parts of sodium chloride, 6 parts of essence, 1.2 parts of nipalgins Methyl esters, 0.1 part of citric acid, water is solvent.
Wherein, the carefree liquid includes the component of following parts by weight:8 parts of radix bupleuri, 8 parts of Radix Paeoniae Alba, 7 parts of Radix Angelicae Sinensis, 6 parts of Poria cocos, Rhizoma Atractylodis Macrocephalae part, 5 parts of grapefruit skin, 3 parts of wild chrysanthemum, 12 parts of lotus leaf and 300 parts of water.
The preparation method of the carefree shower cream of the present embodiment includes the following steps:
1, deionized water is added in reaction kettle and is heated to 60 DEG C.
2, anionic surfactant, cationic surfactant, non-ionic surface active are added into the reaction kettle Agent, zwitterionic surfactant, emulsifier, preservative, thickener, sodium chloride and essence simultaneously stir evenly.
3, the substance in the reaction kettle is carried out being cooled to 40 DEG C.
4, the pH value of substance in the reaction kettle is adjusted using citric acid, the pH value is adjusted to 6.5.
5, carefree liquid is added into the reaction kettle, wherein the carefree liquid is prepared in following preparation process:It will The all components of the carefree liquid, which are placed under condition of negative pressure, to be boiled and keeps 2h to obtain carefree mixture, by the carefree mixing Object is filtered and obtains filtrate using the sieve that mesh number is at least 800 mesh, and the filtrate is the carefree liquid, wherein The condition of negative pressure is -0.075Mpa.
6, deionized water polishing quality is added into the reaction kettle and is stirred to obtain feed liquid, wherein is described to stir The revolving speed mixed is 20 revs/min.
7, the feed liquid is put into vacuum emulsifying machine, by vacuumizing degassing, can be obtained final carefree shower cream.
Embodiment 2
In the present embodiment, carefree shower cream includes the component of following parts by weight:55 parts of carefree liquid, 15 parts of hydroxy propyl celluloses Element, 11 parts of needle-shaped methyl sodiosul foaliphatates, 11 parts of coconut oleoyl amine MEA, 125 parts of fatty alcohol-ether sodium sulfates, 50 parts of coconut oleoyl amines Propyl betaine, 11 parts of polyquaterniums -7,14 parts of glycol distearates, 15 parts of sodium chloride, 7 parts of essence, 2 parts of Metagins Ester, 0.15 part of citric acid, water is solvent.
Wherein, the carefree liquid includes the component of following parts by weight:10 parts of radix bupleuri, 10 parts of Radix Paeoniae Alba, 9 parts of Radix Angelicae Sinensis, Poria cocos 9 Part, 8 parts of Rhizoma Atractylodis Macrocephalae, 9 parts of grapefruit skin, 6 parts of wild chrysanthemum, 16 parts of lotus leaf and 325 parts of water.
The preparation method of the carefree shower cream of the present embodiment includes the following steps:
1, deionized water is added in reaction kettle and is heated to 70 DEG C.
2, anionic surfactant, cationic surfactant, non-ionic surface active are added into the reaction kettle Agent, zwitterionic surfactant, emulsifier, preservative, thickener, sodium chloride and essence simultaneously stir evenly.
3, the substance in the reaction kettle is carried out being cooled to 42 DEG C.
4, the pH value of substance in the reaction kettle is adjusted using citric acid, the pH value is adjusted to 7.0.
5, carefree liquid is added into the reaction kettle, wherein the carefree liquid is prepared in following preparation process:It will The all components of the carefree liquid, which are placed under condition of negative pressure, to be boiled and keeps 2h to obtain carefree mixture, by the carefree mixing Object is filtered and obtains filtrate using the sieve that mesh number is at least 800 mesh, and the filtrate is the carefree liquid, wherein The condition of negative pressure is -0.070Mpa.
6, deionized water polishing quality is added into the reaction kettle and is stirred to obtain feed liquid, wherein is described to stir The revolving speed mixed is 25 revs/min.
7, the feed liquid is put into vacuum emulsifying machine, by vacuumizing degassing, can be obtained final carefree shower cream.
Embodiment 3
In the present embodiment, carefree shower cream includes the component of following parts by weight:60 parts of carefree liquid, 16 parts of hydroxy propyl celluloses Element, 12 parts of needle-shaped methyl sodiosul foaliphatates, 12 parts of coconut oleoyl amine MEA, 140 parts of fatty alcohol-ether sodium sulfates, 55 parts of coconut oleoyl amines Propyl betaine, 12 parts of polyquaterniums -7,15 parts of glycol distearates, 16 parts of sodium chloride, 8 parts of essence, 3 parts of Metagins Ester, 0.2 part of citric acid, water is solvent.
Wherein, the carefree liquid includes the component of following parts by weight:12 parts of radix bupleuri, 12 parts of Radix Paeoniae Alba, 12 parts of Radix Angelicae Sinensis, Poria cocos 12 Part, 12 parts of Rhizoma Atractylodis Macrocephalae, 12 parts of grapefruit skin, 9 parts of wild chrysanthemum, 20 parts of lotus leaf and 350 parts of water.
The preparation method of the carefree shower cream of the present embodiment includes the following steps:
1, deionized water is added in reaction kettle and is heated to 80 DEG C.
2, anionic surfactant, cationic surfactant, non-ionic surface active are added into the reaction kettle Agent, zwitterionic surfactant, emulsifier, preservative, thickener, sodium chloride and essence simultaneously stir evenly.
3, the substance in the reaction kettle is carried out being cooled to 45 DEG C.
4, the pH value of substance in the reaction kettle is adjusted using citric acid, the pH value is adjusted to 8.0.
5, carefree liquid is added into the reaction kettle, the carefree liquid is prepared in following preparation process:It will be described The all components of carefree liquid, which are placed under condition of negative pressure, to be boiled and keeps 2.5h to obtain carefree mixture, by the carefree mixture Filtrate is filtered and obtained using the sieve that mesh number is at least 800 mesh, and the filtrate is the carefree liquid, wherein institute Stating condition of negative pressure is -0.060Mpa.
6, deionized water polishing quality is added into the reaction kettle and is stirred to obtain feed liquid, wherein is described to stir The revolving speed mixed is 30 revs/min.
7, the feed liquid is put into vacuum emulsifying machine, by vacuumizing degassing, can be obtained final carefree shower cream.
Fatigue is a kind of most common sub-health state, North American Nursing Diagnosis association (the north American Nursing diagnosis association, NANDA) it is defined as, one kind by individual itself perception is strong and lasting Taediumvitae and powerlessness when being engaged in mental and physical work, this feeling do not alleviate because of rest.The fatigue of duration is more It is a universal phenomenon, proportion is up to 10%-20% in general population.Fatigue has negatively the ability to work of individual It influences, is the risk factor that professional mistake occurs, it is unfavorable also to generate to the social life of individual.
The embodiment of the present invention, in order to verify whether the carefree shower cream has the effect of releive irritability, quickly elimination fatigue, Whether reach irritability of releiving after for a period of time using carefree shower cream of the invention by verifying user, quickly eliminate fatigue Effect.
One, 100 subjects are chosen, which has claimed below:
(1) be chief complaint with fatigue, and fatigue continue or recurrent exerbation 3 months or more, exclude may cause fatigue disease (including chronic fatigue syndrome, depression, anxiety disorder etc.), and nothing is detected with western medicine conventional physical examination method and index system It is obvious abnormal;
(2) it tests and assesses with Fatigue scale-14 (fatigue scale-14, FS-14), physical fatigue dimension score value reaches To 4 points or more and mental fatigue dimension score value is up to 3 points and the above person.
(3) the person that do not receive other treatment simultaneously;
(4) routine physical examination Non Apparent Abnormality and obvious heart and brain kidney and dysfunction of blood coagulation person;
(5) not using the pharmaceutical intervention measure for fatigue in nearly 1 month;
(6) age is 18-55 years old
(7) subject is voluntary and signs informed consent form.
Two, exclusion criteria
(1) gestational period, nursing period, menstrual period women or intended conception person in half a year;
(2) symptomatic confirmed fatigue person;
(3) there is the acute medical history person such as exogenous disease, wound in nearly 1 week.
Three, it is grouped
100 subjects are randomly divided into experimental group 50 and control group 50 using random digits table is looked into.Experimental group Middle male 25, female 25;Average age be (32 ± 10) year.Male 25, female 25 in control group;Average age is (30 ± 10) Year.Two groups of subject's genders and age compare, no significant difference (P>0.05) it, is comparable.
Four, process is tested
It is treated using health education and psychological counseling, specifically includes and subject is encouraged to form good living habit: After work, guarantees sufficient rest and sleep, carry out physical training appropriate, and pay attention to adequate nutrition and balanced diet;Draw Itself phychology should be rectified during working by leading subject, taken positive coping style to releive pressure, kept fit good Psychological condition.
50 subjects in experimental group use carefree shower cream of the invention, using once when having a bath daily, continuously make With three months.50 subjects in control group use common shower cream, using once when having a bath daily, are used continuously three Month.Experimental group is consistent using the amount of corresponding shower cream every time daily with the subject of control group.
Five, test index
(1)FS-14
FS-14 includes 14 projects altogether, wherein 8 reflection physical fatigues, 6 reflection mental fatigues.The score of the scale Mode is two point form point-score, that is, has the selection "Yes" of this symptom, counts 1 point, and the selection "No" without this symptom counts 0 point, In have 3 for reversed score, analysis indexes are respectively physical fatigue, mental fatigue and tired total score, and full marks are respectively 8 points, 6 points With 14 points, score value is higher, and expression degree of fatigue is heavier.
(2) Pittsburg Sleep Quality Index scale (Pittsburgh sleep quality index, PSQI)
By 19 self-appraisals and 5, he comments entry to constitute to PSQI content, wherein the l9 self-appraisal entry and 5 he comment entry not Participate in score.Participate in 18 white 7 factors for commenting entry to be combined into scale of score, respectively subjective sleep quality, sleep Incubation period, sleep continuity, habitual Sleep efficiency, it is sleep disordered, use sleep drug, daytime function obstacle.Each factor It scores by 0~3 point, adding up each factor score is PSQI total score, and total score range is 0~21 point, is allocated as with 7 as China adult sleep The reference dividing value of quality problems, total score≤4 point PSQI indicate that sleep quality is preferable:4 points<PSQI<8 points of expression sleep qualities one As:PSQI >=8 point indicate that sleep quality is poor.Score value is higher, shows that sleep quality is poorer.
1 experimental group of table and control group are compared using each item rating after corresponding shower cream
As can be seen from Table 1, control group and experimental group are after using common shower cream and carefree shower cream respectively, Fs 1 Each item rating of scale is below same group before use, two groups of prompt is made moderate progress using degree of fatigue after shower cream.With control group Compare, experimental group is lower using the scoring of rear physical fatigue and mental fatigue, prompts using carefree shower cream to physical fatigue Improvement is more significant, but slightly improves to mental fatigue curative effect.And from the point of view of PSQI scoring, experimental group is scored bright using rear PSQI It is aobvious to be lower than control group, prompt the sleep quality that can improve tested crowd using carefree shower cream, this may is that relieve fatigue because One of element.Meanwhile fatigue have invertibity, in time intervene can be effectively relieved, but if not drawing attention, pressure source not It releases in the case where even aggravating, degree of fatigue may also be further aggravated, and cause more serious consequence.
Pass through above test result, it is found that by using carefree extract of the invention, can have significantly It releives irritability, the effect that relieves fatigue.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (2)

1. a kind of carefree shower cream, which is characterized in that the carefree shower cream includes the component of following parts by weight:50-60 parts free and unfettered Distant liquid, 13-16 part hydroxypropyl cellulose, 10-12 parts of needle-shaped methyl sodiosul foaliphatates, 10-12 parts of coconut oleoyl amines MEA, 110- 140 parts of fatty alcohol-ether sodium sulfates, 40-55 parts of Cocoamidopropyl betaines, 10-12 parts of polyquaterniums -7,12-15 parts of ethylene glycol Distearate, 14-16 part sodium chloride, 6-8 parts of essence, 1.2-3 parts of methylparabens, 0.1-0.2 parts of citric acids, water are molten Agent;The carefree liquid includes the component of following parts by weight:8-12 parts of radix bupleuri, 8-12 parts of Radix Paeoniae Alba, 7-12 parts of Radix Angelicae Sinensis, Poria cocos 6-12 Part, 5-12 parts of Rhizoma Atractylodis Macrocephalae, 5-12 parts of grapefruit skin, 3-9 parts of wild chrysanthemum, 12-20 parts of lotus leaf and 300-350 parts of water.
2. carefree shower cream according to claim 1, which is characterized in that the preparation method of the carefree shower cream includes such as Lower step:
Deionized water is added in reaction kettle and is heated to 60 DEG C -80 DEG C;
Remaining component in addition to carefree liquid of carefree shower cream described in claim 1 is added into the reaction kettle and stirs Uniformly;
Substance in the reaction kettle is carried out to be cooled to 40 DEG C -45 DEG C;
The pH value of substance in the reaction kettle is adjusted using citric acid, the pH value is adjusted to 6.5-8.0;
Carefree liquid is added into the reaction kettle, wherein the carefree liquid is prepared in following preparation process:It will be described free and unfettered The all components of distant liquid, which are placed under condition of negative pressure, to be boiled and keeps 2-2.5h to obtain carefree mixture, by the carefree mixture Filtrate is filtered and obtained using the sieve that mesh number is at least 800 mesh, and the filtrate is the carefree liquid, wherein institute Stating condition of negative pressure is -0.075Mpa--0.060Mpa;
Deionized water polishing quality is added into the reaction kettle and is stirred to obtain feed liquid, wherein the stirring turns Speed is 20-30 revs/min;
The feed liquid is put into vacuum emulsifying machine, by vacuumizing degassing, can be obtained final carefree shower cream.
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CN107137275A (en) * 2017-05-22 2017-09-08 梁洁珍 A kind of gel-type shower cream and preparation method thereof
CN110373284A (en) * 2019-08-06 2019-10-25 两面针(江苏)实业有限公司 A kind of natural plant extracts perfumed soap and preparation method thereof

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CN102670452A (en) * 2012-05-31 2012-09-19 张红年 Artemisia argyi plant body wash and preparation method thereof
CN105168057A (en) * 2015-09-24 2015-12-23 湖北穆兰同大科技有限公司 Figwort root body wash
CN105362097A (en) * 2014-08-31 2016-03-02 李尧 Bath foam and preparation method thereof
CN105726391A (en) * 2016-02-29 2016-07-06 杭州木木生物科技有限公司 Dendrobium-officinale shower gel

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CN102670452A (en) * 2012-05-31 2012-09-19 张红年 Artemisia argyi plant body wash and preparation method thereof
CN105362097A (en) * 2014-08-31 2016-03-02 李尧 Bath foam and preparation method thereof
CN105168057A (en) * 2015-09-24 2015-12-23 湖北穆兰同大科技有限公司 Figwort root body wash
CN105726391A (en) * 2016-02-29 2016-07-06 杭州木木生物科技有限公司 Dendrobium-officinale shower gel

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