CN109846728A - A kind of preparation method of the clean facial cleanser containing nano-graphene - Google Patents
A kind of preparation method of the clean facial cleanser containing nano-graphene Download PDFInfo
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- CN109846728A CN109846728A CN201910319620.4A CN201910319620A CN109846728A CN 109846728 A CN109846728 A CN 109846728A CN 201910319620 A CN201910319620 A CN 201910319620A CN 109846728 A CN109846728 A CN 109846728A
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Abstract
The invention belongs to facial cleanser technical fields, more particularly to a kind of preparation method of clean facial cleanser containing nano-graphene, quality formula is as follows: 5-10 parts of volcanic mud, 2-4 parts of nano-graphene, 10-15 parts of red wine, 20-25 parts of distilled water, 1-2 parts of Cocoamidopropyl betaine, 3-7 parts of peach blossom extracting solution, 3-5 parts of red sage root extract, 2-4 parts of ginger extract, 0.5-1.5 parts of hydroxyethyl cellulose, 2-5 parts of lauric acid.The present invention solves the problems, such as that existing product for resolving poxes is ineffective, by the Physical Absorption bactericidal effect of graphene and the efficient absorption effect of volcanic mud, forms the Adsorption and Sterilization effect of strength.
Description
Technical field
The invention belongs to facial cleanser technical fields, and in particular to a kind of preparation side of the clean facial cleanser containing nano-graphene
Method.
Background technique
Acne is also known as whelk, is a kind of chronic inflammatory skin of pilosebaceous unit, is mainly apt to occur in green few
Year, it is very big to teen-age psychology and social influence, but tend to nature after puberty and mitigate or fully recover.Clinical manifestation is with good hair
With the characteristics of the pleomorphism skin lesions such as acne, papule, warts, the tubercle of face.Mainly led with hypersteatosis, pilosebaceous follicle
The factors such as blockage, bacterium infection and inflammatory reaction are closely related.Adolesce androgen especially testosterone in descendant's body
It is horizontal to increase rapidly, promote sebaceous glands to develop and generate a large amount of sebums.The dyskeratosis of pilosebaceous duct causes to lead simultaneously
Blockage, dyssebacia form horn plug, that is, micro mist thorn.Multiple-microorganism especially propionibacterium acnes are a large amount of in hair follicle
Breeding, the lipase that propionibacterium acnes generate decompose sebum and generate free fatty acid, while chemotactic inflammatory cell and medium, finally
It induces and aggravates inflammatory reaction.Acne lesions are apt to occur in face and upper chest and back, show as acne, inflamed papules, secondary pustule,
The damage such as tubercle, often with seborrhea.It easily forms that pigmentation, pore be coarse or even scar etc. leaves illness, to the heart of patient
Reason and life cause serious influence.
Product for resolving poxes currently on the market also has much, but these product for resolving poxes add the fungicide of chemistry mostly, such as
Benasept, salicylic acid, benzoyl peroxide etc., irritation is big, some easily cause skin allergy, are not easy to absorb, for a long time
The disadvantages of using effect is not significant.
Summary of the invention
For the problems of the prior art, the present invention provides a kind of preparation side of clean facial cleanser containing nano-graphene
Method solves the problems, such as that existing product for resolving poxes is ineffective, passes through the Physical Absorption bactericidal effect of graphene and the height of volcanic mud
Adsorption effect is imitated, the Adsorption and Sterilization effect of strength is formed.
To realize the above technical purpose, the technical scheme is that
The quality formula of a kind of preparation method of the clean facial cleanser containing nano-graphene, the preparation method is as follows:
5-10 parts of volcanic mud, 2-4 parts of nano-graphene, 10-15 parts of red wine, 20-25 parts of distilled water, Cocoamidopropyl betaine
1-2 parts, 3-7 parts of peach blossom extracting solution, 3-5 parts of red sage root extract, 2-4 parts of ginger extract, 0.5-1.5 parts of hydroxyethyl cellulose,
2-5 parts of lauric acid.
Preparation method includes the following steps:
Step 1, hydroxyethyl cellulose is added and is stirred evenly into distilled water, obtain aqueous dispersion；
Step 2, Cocoamidopropyl betaine and lauric acid are added and are stirred evenly into aqueous dispersion, obtain mixed liquor A；
Step 3, nano-graphene and volcanic mud are put into wet ball grinding in ball-milling reaction machine and react 2-4h, it is equal that drying obtains partial size
Then even solid mixture is added into mixed liquor A constant temperature and stirs evenly, obtains mixed liquid B；
Step 4, vacuum distillation reaction 0.5-1.5h is added into vacuum distillation reaction kettle in mixed liquid B, obtains viscous paste；
Step 5, peach blossom extracting solution, red sage root extract and ginger extract are added and are stirred into red wine to being completely dissolved, then
Viscous paste sealing reaction 2-4h is added, obtains clean facial cleanser after cooling.
Mixing speed in the step 1 is 200-800r/min.
The liquid of wet ball grinding reaction in the step 3 uses dehydrated alcohol, and temperature is 20-40 DEG C, the drying
Temperature is 90-100 DEG C.
The temperature of constant temperature stirring in the step 3 is 60-70 DEG C, mixing speed 1000-2000r/min.
The pressure of vacuum distillation in the step 4 is the 70-80% of atmospheric pressure, and temperature is 100-110 DEG C, described sticky
The volume of slurry is the 5-10% of mixed liquid B.
The mixing speed of stirring in the step 5 is 1000-2000r/min, and the temperature of the sealing reaction is 100-
130 DEG C, pressure 0.2-0.5MPa.
Volcanic mud is the product in volcano, be with volcanic glass canescence as main component, it is dark-grey to black without stickiness
Mud.Volcanic mud becomes positively charged lotus or negative electrical charge after dissolving in water, thus the same electrically charged sebum dirt of absorption, therefore volcanic mud
Adsorption capacity be better than charcoal.Volcanic mud be rich in potassium, sodium, sulphur and a variety of natural minerals ingredients, can present outstanding moisturizing,
Elastic force and calmness are releived effect.
Nano-graphene sterilization ability is excellent, is the physics " antibiotic " of not drug resistance, can be thoroughly from facial pores
Depths bacteria removal, anti-acne effect can be better than similar cosmetics.Graphene have strong adsorption force, far infrared transmission, antibacterial bacteriostatic,
Generate the characteristics such as anion, natural environmental-protective.
Cocoamidopropyl betaine: being a kind of zwitterionic surfactant, all has under acid and alkaline condition
Excellent stability, presentation male and female is ionic respectively, is often used in combination with anions and canons and nonionic surfactant, compatibility
It is functional.Softness, conditioning and the low-temperature stability of washing class product can be significantly improved.This product irritation is small, performance is mild, bubble
Foam is more, strong detergency, and foam is fine and smooth and stablizes, and has excellent thickening property, flexibility, bactericidal properties, antistatic property, hard water resistance
Property, it is suitable for configuration shampoo, shower cream, facial cleanser etc., the flexibility to hair, skin can be enhanced.
Red wine is also referred to as red wine, has been studied confirmation and has contained multiple nutritional components.It is to take red grape and together with Portugal
Grape skin carries out soaking fermentation together and obtains, due to containing a large amount of polyphenol substance in grape, having oxidation resistance, therefore through extracting
Its extract oxidation resistance is stronger afterwards, and at it after fermenting and becoming grape wine, the content progress of polyphenol is improved, ingredient
It becomes more stable, anti-oxidation efficacy is greatly improved.Due to including a variety of anti-oxidizing compounds in red wine, so that
Red wine has surprising oxidation resistance, and procyanidins, catechin, quercetin, resveratrol etc. all have stronger
Antioxidation, oxidation resistance reach 50 times of vitamin E, reach ascorbic 25 times.Its procyanidins is anti-oxidant because having
Ability is very strong, therefore can reduce the injury of ultraviolet light, and can prevent collagen and elastic fibers from being destroyed.Red wine is more
Phenol can also maintain the complete of cell membrane and dermal composition to the infringement of antiactive oxygen;Inhibit collagen catabolic enzyme and other
All kinds of catabolic enzymes not only can be reduced injury caused by ultraviolet light and inflammatory response, and press down wherein being familiar with is catechin
Glue original protease, protects collagen not to be damaged.Red Wine Polyphenols can also reduce the stimulated caused inflammation of skin
Reaction;Inhibit Tyrosinase activity, reduces melanin production, allow skin brilliant white;Antiotasis is maintained, capilary varicose is prevented,
Promote the metabolism of fat with carbohydrate, eliminates tangerine hull constitution phenomenon.The resveratrol being wherein more typically in Red Wine Polyphenols,
It is also equipped with humectant properties, anti-inflammatory effect while having oxidation resistance, therefore good maintenance can be played the role of to skin, delays
The aging course of skin cell reduces melanin obvious effect to the activity for inhibiting Tyrosinase.
Contain the nutriments such as Kaempferol, coumarin, trifolin and vitamin A, B, C in peach blossom.These substances can expand
Blood vessel, promotion of blood circulation are opened, skin of moistening improves blood circulation, promotes skin-nourishing and oxygen supply, makes the rouge for promoting human senility
Brown quality accelerates excretion, prevents melanin chronic deposition in skin, so as to effectively prevent chloasma, freckle, blackspot, green
It is also rich in vegetable protein and the amino acid in free state in peach, is easy to be absorbed by the skin, to prevention and treatment dry skin, coarse and wrinkle
Line etc. effectively, can also enhance the disease resistance of skin, to prevent and treat skin disease, seborrhea, suppurative dermatitis, scurvy
Deng of great advantage to skin.
There is Salvia root P.E antioxidant contents, the danshinolic acids such as danshinolic acid and Rosmarinic acid to have very strong antioxidation,
Can effectively clear the intracorporal oxygen radical of people, anti-lipid peroxidation reaction improves human immunologic function, be currently known it is anti-
One of strongest natural products of oxidation.
Ginger has effects that relieving exterior syndrome and dispelling cold, warming middle energizer to arrest vomiting, warm lung cough-relieving, removing toxic substances, is usually used in anemofrigid cold, and taste are cold
Disease, gastrofrigid vomiting, lung cold cough, solving toxin of fish and crab.
From the above, it can be seen that the present invention has following advantages:
1. the present invention solves the problems, such as that existing product for resolving poxes is ineffective, pass through the Physical Absorption bactericidal effect and fire of graphene
The efficient absorption effect of minishanny forms the Adsorption and Sterilization effect of strength.
2. the present invention can not only be played using peach blossom extracting solution, red sage root extract and ginger extract as active constituent
Bactericidal effect, while good repairing effect can be played.
3. the present invention is combined using the negative ions of volcanic mud with the electric conductivity of graphene, forms uniform anion and inhale
It is attached, comprehensively killing, and promote the reparation characteristic of active constituent.
4. the present invention utilizes the grain effect of nano-graphene, ball effect can be formed in use, by each
Angle is adsorbed, and the making full use of of graphene, effective pollutant absorption and bacteria suppression effect are reached.
Specific embodiment
The present invention will be described in detail in conjunction with the embodiments, but does not do any restriction to claim of the invention.
Embodiment 1
The quality formula of a kind of preparation method of the clean facial cleanser containing nano-graphene, the preparation method is as follows:
5 parts of volcanic mud, 2 parts of nano-graphene, 10 parts of red wine, 20 parts of distilled water, 1 part of Cocoamidopropyl betaine, peach blossom mention
Take 3 parts of liquid, 3 parts of red sage root extract, 2 parts of ginger extract, 0.5 part of hydroxyethyl cellulose, 2 parts of lauric acid.
Preparation method includes the following steps:
Step 1, hydroxyethyl cellulose is added and is stirred evenly into distilled water, obtain aqueous dispersion；
Step 2, Cocoamidopropyl betaine and lauric acid are added and are stirred evenly into aqueous dispersion, obtain mixed liquor A；
Step 3, nano-graphene and volcanic mud are put into wet ball grinding in ball-milling reaction machine and react 2h, drying obtains uniform particle sizes
Solid mixture, constant temperature is then added into mixed liquor A and stirs evenly, obtains mixed liquid B；
Step 4, vacuum distillation reaction 0.5h is added into vacuum distillation reaction kettle in mixed liquid B, obtains viscous paste；
Step 5, peach blossom extracting solution, red sage root extract and ginger extract are added and are stirred into red wine to being completely dissolved, then
Viscous paste sealing reaction 2h is added, obtains clean facial cleanser after cooling.
Mixing speed in the step 1 is 200r/min.
The liquid of wet ball grinding reaction in the step 3 uses dehydrated alcohol, and temperature is 20 DEG C, the temperature of the drying
It is 90 DEG C.
The temperature of constant temperature stirring in the step 3 is 60 DEG C, mixing speed 1000r/min.
The pressure of vacuum distillation in the step 4 is the 70% of atmospheric pressure, and temperature is 100 DEG C, the body of the viscous paste
Product is the 5% of mixed liquid B.
The mixing speed of stirring in the step 5 is 1000r/min, and the temperature of the sealing reaction is 100 DEG C, pressure
For 0.2MPa.
Embodiment 2
The quality formula of a kind of preparation method of the clean facial cleanser containing nano-graphene, the preparation method is as follows:
10 parts of volcanic mud, 4 parts of nano-graphene, 15 parts of red wine, 25 parts of distilled water, 2 parts of Cocoamidopropyl betaine, peach blossom mention
Take 7 parts of liquid, 5 parts of red sage root extract, 4 parts of ginger extract, 1.5 parts of hydroxyethyl cellulose, 5 parts of lauric acid.
Preparation method includes the following steps:
Step 1, hydroxyethyl cellulose is added and is stirred evenly into distilled water, obtain aqueous dispersion；
Step 2, Cocoamidopropyl betaine and lauric acid are added and are stirred evenly into aqueous dispersion, obtain mixed liquor A；
Step 3, nano-graphene and volcanic mud are put into wet ball grinding in ball-milling reaction machine and react 4h, drying obtains uniform particle sizes
Solid mixture, constant temperature is then added into mixed liquor A and stirs evenly, obtains mixed liquid B；
Step 4, vacuum distillation reaction 1.5h is added into vacuum distillation reaction kettle in mixed liquid B, obtains viscous paste；
Step 5, peach blossom extracting solution, red sage root extract and ginger extract are added and are stirred into red wine to being completely dissolved, then
Viscous paste sealing reaction 4h is added, obtains clean facial cleanser after cooling.
Mixing speed in the step 1 is 800r/min.
The liquid of wet ball grinding reaction in the step 3 uses dehydrated alcohol, and temperature is 40 DEG C, the temperature of the drying
It is 100 DEG C.
The temperature of constant temperature stirring in the step 3 is 70 DEG C, mixing speed 2000r/min.
The pressure of vacuum distillation in the step 4 is the 80% of atmospheric pressure, and temperature is 110 DEG C, the body of the viscous paste
Product is the 10% of mixed liquid B.
The mixing speed of stirring in the step 5 is 2000r/min, and the temperature of the sealing reaction is 130 DEG C, pressure
For 0.5MPa.
Embodiment 3
The quality formula of a kind of preparation method of the clean facial cleanser containing nano-graphene, the preparation method is as follows:
8 parts of volcanic mud, 3 parts of nano-graphene, 12 parts of red wine, 23 parts of distilled water, 2 parts of Cocoamidopropyl betaine, peach blossom mention
Take 5 parts of liquid, 4 parts of red sage root extract, 3 parts of ginger extract, 1 part of hydroxyethyl cellulose, 3 parts of lauric acid.
Preparation method includes the following steps:
Step 1, hydroxyethyl cellulose is added and is stirred evenly into distilled water, obtain aqueous dispersion；
Step 2, Cocoamidopropyl betaine and lauric acid are added and are stirred evenly into aqueous dispersion, obtain mixed liquor A；
Step 3, nano-graphene and volcanic mud are put into wet ball grinding in ball-milling reaction machine and react 3h, drying obtains uniform particle sizes
Solid mixture, constant temperature is then added into mixed liquor A and stirs evenly, obtains mixed liquid B；
Step 4, vacuum distillation reaction 1h is added into vacuum distillation reaction kettle in mixed liquid B, obtains viscous paste；
Step 5, peach blossom extracting solution, red sage root extract and ginger extract are added and are stirred into red wine to being completely dissolved, then
Viscous paste sealing reaction 3h is added, obtains clean facial cleanser after cooling.
Mixing speed in the step 1 is 600r/min.
The liquid of wet ball grinding reaction in the step 3 uses dehydrated alcohol, and temperature is 30 DEG C, the temperature of the drying
It is 95 DEG C.
The temperature of constant temperature stirring in the step 3 is 65 DEG C, mixing speed 1500r/min.
The pressure of vacuum distillation in the step 4 is the 75% of atmospheric pressure, and temperature is 105 DEG C, the body of the viscous paste
Product is the 8% of mixed liquid B.
The mixing speed of stirring in the step 5 is 1500r/min, and the temperature of the sealing reaction is 120 DEG C, pressure
For 0.4MPa.
Performance detection
10% concentration product of the present invention is taken respectively, bactericidal effect is detected using conventional microbiological, test result shows that the present invention produces
Product bactericidal effect reaches 99% or more, and bactericidal effect is obvious.Microorganism selects Escherichia coli, salmonella, golden yellow common ball
Bacterium.
In conclusion the invention has the following advantages that
1. the present invention solves the problems, such as that existing product for resolving poxes is ineffective, pass through the Physical Absorption bactericidal effect and fire of graphene
The efficient absorption effect of minishanny forms the Adsorption and Sterilization effect of strength.
2. the present invention can not only be played using peach blossom extracting solution, red sage root extract and ginger extract as active constituent
Bactericidal effect, while good repairing effect can be played.
3. the present invention is combined using the negative ions of volcanic mud with the electric conductivity of graphene, forms uniform anion and inhale
It is attached, comprehensively killing, and promote the reparation characteristic of active constituent.
4. the present invention utilizes the grain effect of nano-graphene, ball effect can be formed in use, by each
Angle is adsorbed, and the making full use of of graphene, effective pollutant absorption and bacteria suppression effect are reached.
It is understood that being merely to illustrate the present invention above with respect to specific descriptions of the invention and being not limited to this
Technical solution described in inventive embodiments.Those skilled in the art should understand that still can be carried out to the present invention
Modification or equivalent replacement, to reach identical technical effect；As long as meet use needs, all protection scope of the present invention it
It is interior.
Claims (7)
1. a kind of preparation method of the clean facial cleanser containing nano-graphene, it is characterised in that: the quality of the preparation method is matched
Side is as follows:
5-10 parts of volcanic mud, 2-4 parts of nano-graphene, 10-15 parts of red wine, 20-25 parts of distilled water, Cocoamidopropyl betaine
1-2 parts, 3-7 parts of peach blossom extracting solution, 3-5 parts of red sage root extract, 2-4 parts of ginger extract, 0.5-1.5 parts of hydroxyethyl cellulose,
2-5 parts of lauric acid.
2. the preparation method of the clean facial cleanser according to claim 1 containing nano-graphene, it is characterised in that: including such as
Lower step:
Step 1, hydroxyethyl cellulose is added and is stirred evenly into distilled water, obtain aqueous dispersion；
Step 2, Cocoamidopropyl betaine and lauric acid are added and are stirred evenly into aqueous dispersion, obtain mixed liquor A；
Step 3, nano-graphene and volcanic mud are put into wet ball grinding in ball-milling reaction machine and react 2-4h, it is equal that drying obtains partial size
Then even solid mixture is added into mixed liquor A constant temperature and stirs evenly, obtains mixed liquid B；
Step 4, vacuum distillation reaction 0.5-1.5h is added into vacuum distillation reaction kettle in mixed liquid B, obtains viscous paste；
Step 5, peach blossom extracting solution, red sage root extract and ginger extract are added and are stirred into red wine to being completely dissolved, then
Viscous paste sealing reaction 2-4h is added, obtains clean facial cleanser after cooling.
3. the preparation method of the clean facial cleanser according to claim 2 containing nano-graphene, it is characterised in that: the step
Mixing speed in rapid 1 is 200-800r/min.
4. the preparation method of the clean facial cleanser according to claim 2 containing nano-graphene, it is characterised in that: the step
The liquid of wet ball grinding reaction in rapid 3 uses dehydrated alcohol, and temperature is 20-40 DEG C, and the temperature of the drying is 90-100 DEG C.
5. the preparation method of the clean facial cleanser according to claim 2 containing nano-graphene, it is characterised in that: the step
The temperature of constant temperature stirring in rapid 3 is 60-70 DEG C, mixing speed 1000-2000r/min.
6. the preparation method of the clean facial cleanser according to claim 2 containing nano-graphene, it is characterised in that: the step
The pressure of vacuum distillation in rapid 4 is the 70-80% of atmospheric pressure, and temperature is 100-110 DEG C, and the volume of the viscous paste is mixed
Close the 5-10% of liquid B.
7. the preparation method of the clean facial cleanser of Korea Spro's nano-graphene according to claim 2, it is characterised in that: the step
The mixing speed of stirring in rapid 5 is 1000-2000r/min, and the temperature of the sealing reaction is 100-130 DEG C, and pressure is
0.2-0.5MPa。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910319620.4A CN109846728A (en) | 2019-04-19 | 2019-04-19 | A kind of preparation method of the clean facial cleanser containing nano-graphene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910319620.4A CN109846728A (en) | 2019-04-19 | 2019-04-19 | A kind of preparation method of the clean facial cleanser containing nano-graphene |
Publications (1)
| Publication Number | Publication Date |
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| CN109846728A true CN109846728A (en) | 2019-06-07 |
Family
ID=66889321
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| CN201910319620.4A Withdrawn CN109846728A (en) | 2019-04-19 | 2019-04-19 | A kind of preparation method of the clean facial cleanser containing nano-graphene |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101550214B1 (en) * | 2014-02-27 | 2015-09-04 | 계명대학교 산학협력단 | Mask sheet having function of shape transformation and fixation and method thereof |
| CN105687029A (en) * | 2016-01-30 | 2016-06-22 | 范洲卫 | Facial cleanser for removing acnes and preparation method thereof |
| CN105997572A (en) * | 2016-05-19 | 2016-10-12 | 曾新民 | Cleansing milk containing nano graphene and preparation method thereof |
-
2019
- 2019-04-19 CN CN201910319620.4A patent/CN109846728A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101550214B1 (en) * | 2014-02-27 | 2015-09-04 | 계명대학교 산학협력단 | Mask sheet having function of shape transformation and fixation and method thereof |
| CN105687029A (en) * | 2016-01-30 | 2016-06-22 | 范洲卫 | Facial cleanser for removing acnes and preparation method thereof |
| CN105997572A (en) * | 2016-05-19 | 2016-10-12 | 曾新民 | Cleansing milk containing nano graphene and preparation method thereof |
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