CN103385847B - Exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof - Google Patents
Exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof Download PDFInfo
- Publication number
- CN103385847B CN103385847B CN201310242394.7A CN201310242394A CN103385847B CN 103385847 B CN103385847 B CN 103385847B CN 201310242394 A CN201310242394 A CN 201310242394A CN 103385847 B CN103385847 B CN 103385847B
- Authority
- CN
- China
- Prior art keywords
- mali pumilae
- fructus mali
- spot
- exfoliated
- face mask
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 29
- QRYRORQUOLYVBU-VBKZILBWSA-N carnosic acid Chemical compound CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 claims abstract description 24
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 claims abstract description 18
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims abstract description 16
- NVNLLIYOARQCIX-MSHCCFNRSA-N Nisin Chemical compound N1C(=O)[C@@H](CC(C)C)NC(=O)C(=C)NC(=O)[C@@H]([C@H](C)CC)NC(=O)[C@@H](NC(=O)C(=C/C)/NC(=O)[C@H](N)[C@H](C)CC)CSC[C@@H]1C(=O)N[C@@H]1C(=O)N2CCC[C@@H]2C(=O)NCC(=O)N[C@@H](C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(NCC(=O)N[C@H](C)C(=O)N[C@H](CC(C)C)C(=O)N[C@H](CCSC)C(=O)NCC(=O)N[C@H](CS[C@@H]2C)C(=O)N[C@H](CC(N)=O)C(=O)N[C@H](CCSC)C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(N[C@H](C)C(=O)N[C@@H]3C(=O)N[C@@H](C(N[C@H](CC=4NC=NC=4)C(=O)N[C@H](CS[C@@H]3C)C(=O)N[C@H](CO)C(=O)N[C@H]([C@H](C)CC)C(=O)N[C@H](CC=3NC=NC=3)C(=O)N[C@H](C(C)C)C(=O)NC(=C)C(=O)N[C@H](CCCCN)C(O)=O)=O)CS[C@@H]2C)=O)=O)CS[C@@H]1C NVNLLIYOARQCIX-MSHCCFNRSA-N 0.000 claims abstract description 16
- 108010053775 Nisin Proteins 0.000 claims abstract description 16
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 16
- 239000011630 iodine Substances 0.000 claims abstract description 16
- 229910052740 iodine Inorganic materials 0.000 claims abstract description 16
- KRPAJLYSLFNDOA-UHFFFAOYSA-N mephenesin carbamate Chemical compound CC1=CC=CC=C1OCC(O)COC(N)=O KRPAJLYSLFNDOA-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229950006838 mephenesin carbamate Drugs 0.000 claims abstract description 16
- 239000004309 nisin Substances 0.000 claims abstract description 16
- 235000010297 nisin Nutrition 0.000 claims abstract description 16
- 239000003755 preservative agent Substances 0.000 claims abstract description 12
- 230000002335 preservative effect Effects 0.000 claims abstract description 12
- 150000001875 compounds Chemical class 0.000 claims abstract description 11
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 9
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 9
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims abstract description 9
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000011734 sodium Substances 0.000 claims abstract description 9
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 9
- 229940117986 sulfobetaine Drugs 0.000 claims abstract description 9
- 238000007796 conventional method Methods 0.000 claims abstract description 5
- 239000003643 water by type Substances 0.000 claims abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 6
- 235000013399 edible fruits Nutrition 0.000 abstract description 6
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 abstract description 4
- 229930003231 vitamin Natural products 0.000 abstract description 4
- 235000013343 vitamin Nutrition 0.000 abstract description 4
- 239000011782 vitamin Substances 0.000 abstract description 4
- 229940088594 vitamin Drugs 0.000 abstract description 4
- 150000003722 vitamin derivatives Chemical class 0.000 abstract description 4
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 abstract description 2
- 238000005562 fading Methods 0.000 abstract description 2
- 229920002674 hyaluronan Polymers 0.000 abstract description 2
- 229960003160 hyaluronic acid Drugs 0.000 abstract description 2
- 210000003491 skin Anatomy 0.000 description 35
- 230000000052 comparative effect Effects 0.000 description 29
- 230000001815 facial effect Effects 0.000 description 25
- 239000010408 film Substances 0.000 description 23
- 230000002421 anti-septic effect Effects 0.000 description 22
- 239000002537 cosmetic Substances 0.000 description 13
- WPTUPLITBGLORN-VOTSOKGWSA-N 2-amino-4-oxo-6-[(e)-2-phenylethenyl]-1,7-dihydropyrrolo[2,3-d]pyrimidine-5-carbonitrile Chemical compound N#CC=1C=2C(=O)NC(N)=NC=2NC=1\C=C\C1=CC=CC=C1 WPTUPLITBGLORN-VOTSOKGWSA-N 0.000 description 11
- 238000012360 testing method Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 244000005700 microbiome Species 0.000 description 8
- 239000000047 product Substances 0.000 description 7
- WYVVKGNFXHOCQV-UHFFFAOYSA-N 3-iodoprop-2-yn-1-yl butylcarbamate Chemical compound CCCCNC(=O)OCC#CI WYVVKGNFXHOCQV-UHFFFAOYSA-N 0.000 description 6
- 235000011187 glycerol Nutrition 0.000 description 6
- 230000035943 smell Effects 0.000 description 6
- 239000004094 surface-active agent Substances 0.000 description 6
- 241000220225 Malus Species 0.000 description 5
- 230000002159 abnormal effect Effects 0.000 description 5
- 239000002131 composite material Substances 0.000 description 5
- 239000003814 drug Substances 0.000 description 5
- 210000002615 epidermis Anatomy 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- 239000004567 concrete Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000011148 porous material Substances 0.000 description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 235000010987 pectin Nutrition 0.000 description 3
- 239000001814 pectin Substances 0.000 description 3
- 229920001277 pectin Polymers 0.000 description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 description 3
- 235000013824 polyphenols Nutrition 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- IXOCGRPBILEGOX-UHFFFAOYSA-N 3-[3-(dodecanoylamino)propyl-dimethylazaniumyl]-2-hydroxypropane-1-sulfonate Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC(O)CS([O-])(=O)=O IXOCGRPBILEGOX-UHFFFAOYSA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 241000745988 Phyllostachys Species 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005202 decontamination Methods 0.000 description 2
- 230000003588 decontaminative effect Effects 0.000 description 2
- SOROIESOUPGGFO-UHFFFAOYSA-N diazolidinylurea Chemical compound OCNC(=O)N(CO)C1N(CO)C(=O)N(CO)C1=O SOROIESOUPGGFO-UHFFFAOYSA-N 0.000 description 2
- 229960001083 diazolidinylurea Drugs 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 210000001061 forehead Anatomy 0.000 description 2
- 239000008233 hard water Substances 0.000 description 2
- 230000009931 harmful effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000004060 metabolic process Effects 0.000 description 2
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 2
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 2
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 2
- 229960002216 methylparaben Drugs 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- 230000035790 physiological processes and functions Effects 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 230000028327 secretion Effects 0.000 description 2
- ACZURWACGCXVLA-UHFFFAOYSA-M sodium;2-[2-[2-[2-[2-[2-[2-[2-(2-octoxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]acetate Chemical compound [Na+].CCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCC([O-])=O ACZURWACGCXVLA-UHFFFAOYSA-M 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 239000003053 toxin Substances 0.000 description 2
- 231100000765 toxin Toxicity 0.000 description 2
- 238000011282 treatment Methods 0.000 description 2
- 238000002137 ultrasound extraction Methods 0.000 description 2
- 229940099451 3-iodo-2-propynylbutylcarbamate Drugs 0.000 description 1
- 206010002198 Anaphylactic reaction Diseases 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 229920000832 Cutin Polymers 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 208000001840 Dandruff Diseases 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 241001530490 Salvia rosmarinus Species 0.000 description 1
- 206010039792 Seborrhoea Diseases 0.000 description 1
- 206010070834 Sensitisation Diseases 0.000 description 1
- 241000194017 Streptococcus Species 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 208000003455 anaphylaxis Diseases 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 239000004599 antimicrobial Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 235000008429 bread Nutrition 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 235000019985 fermented beverage Nutrition 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000834 fixative Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000019261 food antioxidant Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- WJRBRSLFGCUECM-UHFFFAOYSA-N hydantoin Chemical compound O=C1CNC(=O)N1 WJRBRSLFGCUECM-UHFFFAOYSA-N 0.000 description 1
- 229940091173 hydantoin Drugs 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 230000002503 metabolic effect Effects 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 230000035772 mutation Effects 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 230000037312 oily skin Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 238000011321 prophylaxis Methods 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000001223 reverse osmosis Methods 0.000 description 1
- 230000001835 salubrious effect Effects 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 230000008313 sensitization Effects 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 230000001052 transient effect Effects 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Abstract
The invention discloses a kind of exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof.Described exfoliated Fructus Mali pumilae spot-relieving face mask, be prepared from according to a conventional method by the raw material of following weight parts: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part cocamidopropyl propyl amide hydroxyl sulfo betaine, 4-6 part ethanol, 6-8 part capryl alcohol polyethers-9 carboxylic acid sodium, 0.8-2 part Fructus Mali pumilae extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters, described compound preservative, is made up of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.Exfoliated Fructus Mali pumilae spot-relieving face mask of the present invention, contains natural fruit and plant elite, hyaluronic acid, multiple vitamin, all uniform white colour of skin, check melanin, spot fading.
Description
Technical field
The present invention relates to facial film and preparation method thereof, be specifically related to a kind of exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof.
Background technology
Facial film is the important content in skin nursing, and for the regular application facial film of all kinds of skin characteristic, can make oily skin defat, thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.Facial film makes skin seem salubrious after using, smooth and pure white delicacy, this is because when facial film is coated on skin, facial film and skin produce affinity, along with the drying gradually of facial film, skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, the sebum of skin secretion and moisture reverse osmosis are in horny layer, epidermis softness is unfolded, pore instinct is opened, effective ingredient in facial film infiltrates skin and is absorbed, facial film is tightly connected with skin simultaneously, when removing facial film, aging cutin on skin, in pore deep layer dirt also by while leukorrhagia, make skin totally pure and fresh.
The principle of facial film, utilize the blink covering face exactly, the air that temporary transient isolation is extraneous and pollution, improve skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, the moisture in facial film infiltrates the horny layer of skin epidermis, skin becomes soft, and skin naturally light is flexible.
Along with the raising of people's quality of the life and people are to the pursuit of U.S., cosmetics kind is more and more various.At present, face mask of traditional Chinese medicine is one of beauty treatment educational circles effective whitening regime, and especially some Chinese medicine extraction liquid have the effect of good toxin expelling, speckle dispelling, reparation, skin care, also by being applied in facial film gradually.
But because facial film is liquid condition, Chinese medicine extraction liquid is easy to mould growth, a lot of face mask of traditional Chinese medicine antiseptic effects are in the market not good, and the shelf-life is short.Therefore all antiseptic can be added in a lot of face mask of traditional Chinese medicine.But a lot of antiseptic, while the microorganism such as kill bacteria, fungus, also can produce zest to skin, even causes erythema and erythra, Long Term Contact antiseptic, organism material sensitization can be increased, cause the danger of anaphylactic reaction.
Iodine propilolic alcohol butyl mephenesin Carbamate (being called for short IPBC) is a kind of novel cosmetic antiseptic, there is good fungistatic effect, and good dissolubility is had in surfactant, emulsifying agent, polar solvent, therefore be widely used in resident class and drip washing class cosmetic formulations, normal and other antiseptic such as diazolidinyl urea, hydantoin with the use of.In China's cosmetics health specification and European Union's regulatory affairs, regulation IPBC limits the use of antiseptic in components of cosmetics, and in cosmetics, maximum permission working concentration is 0.05%, and can not be used for oral hygiene and lip product.But in facial film, antiseptic effect when addition is less than 0.05% is also not obvious.Therefore, there is the little and problem that antiseptic effect is poor, the shelf-life is short of consumption in the antiseptic used in current facial film.Also there are the iodine propilolic alcohol butyl mephenesin Carbamate in partial face mask or other antiseptic large usage quantities, pessimal stimulation can be produced by skin, with rear needs cleaning face, use trouble.
Fructus Mali pumilae, deciduous tree, leaf is oval, and floral white is with blush.Fruit is circular, and taste is sweet or slightly sour, is Common Fruits, has abundant nutrition composition, have dietetic therapy, auxiliary treatment function.Fructus Mali pumilae is Rosaceae Maloideae Malus, deciduous tree.The fruit rich in mineral substances of Fructus Mali pumilae and vitamin are a kind of fruit that people are the most edible.Apple dietary fiber rich content, also containing a large amount of pectin, is very helpful for adjustment intestinal microbial population.Often eat and can make skin more water profit.
The pharmacological action of Fructus Mali pumilae extracting solution: Fructus Mali pumilae containing enriching saccharide, protein, fat, vitamin C, pectin, tannin, organic acid and calcium, phosphorus, ferrum, the mineral such as potassium.
Toxin expelling effect: Fructus Mali pumilae is of high nutritive value, good for health, always for people continue saying it with interest.In addition it also has eliminating salinity, reduces blood pressure, de-cholesterol, stimulates enterokinesia, the effects such as diuresis relieving constipation.Pectin in Fructus Mali pumilae can adjust human physiological functions.There is anti-oxidation function
Apple polyphenol have antioxidation, smelly eliminating effect, fresh-keeping, protect perfume, color fixative, prevent the effects such as vitamin loss, food quality deterioration can be prevented, therefore, can be used for aquatic products processing, meat products processing, bread, cake, oils and fats, the processing and manufacturing of oil-containing food and refreshment drink etc., can significantly improve its product quality and shelf-life.
Because apple polyphenol has plurality of health care functions, as caries prevention, prophylaxis of hypertension, Polyglucan reaction, antitumor; The physiological functions such as mutation, obstruction ultra-violet absorption, therefore can be used for the manufacture of health food and cosmetics.Apple polyphenol is as health care, functional food additives, and its use amount only needs 50-500PPm, can have sufficient effect.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention provides a kind of exfoliated Fructus Mali pumilae spot-relieving face mask.
Two of technical problem to be solved by this invention provides the preparation method of above-mentioned exfoliated Fructus Mali pumilae spot-relieving face mask.
The present invention seeks to be achieved through the following technical solutions:
A kind of exfoliated Fructus Mali pumilae spot-relieving face mask, is prepared from according to a conventional method by the raw material of following weight parts:
10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part cocamidopropyl propyl amide hydroxyl sulfo betaine, 4-6 part ethanol, 6-8 part capryl alcohol polyethers-9 carboxylic acid sodium, 0.8-2 part Fructus Mali pumilae extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
Wherein, described compound preservative, is made up of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
By carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, described compound preservative can be obtained.
Described exfoliated Fructus Mali pumilae spot-relieving face mask can adopt industry conventional method to be prepared from.
Further, present invention also offers a kind of preparation method of exfoliated Fructus Mali pumilae spot-relieving face mask, be made up of following step:
Polyvinyl alcohol is added in deionized water, be heated to 70-90 DEG C, dissolve, be cooled to 45-55 DEG C, add glycerol, cocamidopropyl propyl amide hydroxyl sulfo betaine, ethanol, the stirring of capryl alcohol polyethers-9 carboxylic acid sodium, be cooled to 40 DEG C, add Fructus Mali pumilae extracting solution and compound preservative, stir, described exfoliated Fructus Mali pumilae spot-relieving face mask can be obtained.
Concrete, in the present invention:
Described polyvinyl alcohol can select cosmetics-stage polyvinyl alcohol, specifically can select if the trade mark is the polyvinyl alcohol of PVA1788, PVA1799 or PVA2488.
Glycerol, has another name called: propylene glycol, English name: Glycerin, molecular formula C
3h
8o
3.
Cocamidopropyl propyl amide hydroxyl sulfo betaine, English name: COCAMIDOPROPYLHYDROXYSULTAINE, CAS accession number: 68139-30-0.There is excellent decontamination, emulsifying, foaming, steady bubble, antistatic, thickening capabilities.Gentle surfactant.The zest of other surfactants can be reduced.Resistance to hard water.Compatibility is good.
Capryl alcohol polyethers-9 carboxylic acid sodium, English name: SODIUM CAPRYLETH-9CARBOXYLATE, CAS accession number: 126646-15-9.There is excellent decontamination, emulsifying, dispersion, solubilising power.Low bubble, can be applicable to industrial spray cleaning.There is good lime soap dispersing power.Enduring high-concentration alkali.Oxidant can be tolerated.Resistance to hard water.High temperature resistant.Compatibility is good, can be composite with cationic surfactant, and is independent of each other.Mild surfactants, and the zest that can reduce other surfactants.
Fructus Mali pumilae extracting solution of the present invention can pass through commercially available and obtain.Also following method can be adopted to prepare and obtain: after Fructus Mali pumilae is pulverized, add the deionized water of 6-10 times of weight, soak 1-3 hour, ultrasonic extraction, 10-15 minute, filter, centrifugal, discard precipitation by supernatant concentration, obtained Fructus Mali pumilae extracting solution.Preferably, after concentrated, controlling Fructus Mali pumilae extracting solution density is 1.02-1.10g/cm
3.
Carnosic acid, molecular formula: C
20h
28o
4, No. CAS: 3650--09-7, source: Labiatae Rosmarinus plant rosemary Rosmarinus officinalis L.
AOB, No. CNS: 04.019, English name: antioxidant of bambooleaves.That AOB extracts from the tender leaf of Phyllostachys (phyllostachys) bamboo, with flavone and phenolic compound to be effective ingredient natural, nutrition, multi-functional food antioxidant.
Nisin, also claims nisin, English name: Nisin, a kind of polypeptide be made up of 34 aminoacid synthesized by streptococcus acidi lactici metabolism, molecular formula C
143h
228o
37n
42s
7molecular weight is 3348, and nisin is made up of water-wet side and hydrophobic side, is typical surfactant, efficient, nontoxic biological antiseptic, be widely used at present milk and milk products, fermented beverage, filling food, vegetable protein food, meat and its products anticorrosion.
Iodine propilolic alcohol butyl mephenesin Carbamate, English name: 3-Iodo-2-propynylbutylcarbamate, is abbreviated as IPBC, No. CAS: 55406-53-6, molecular formula: C
8h
12iNO
2, molecular weight is 281.10.
The present invention uses carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate composite as antiseptic, and antiseptic effect is significantly improved, the long shelf-life of facial film.And, use Compositional antiseptic agent, greatly reduce the consumption of iodine propilolic alcohol butyl mephenesin Carbamate, the consumption of iodine propilolic alcohol butyl mephenesin Carbamate is made to control below 0.03%, meet the IPBC specified in China's cosmetics health specification and European Union's regulatory affairs and limit the use of antiseptic in components of cosmetics, in cosmetics, maximum permission working concentration is 0.05%.Carnosic acid, AOB, nisin are nontoxic biological antiseptic, be widely used in food service industry, be diverted to cosmetic mask in the present invention, ill effect can't be brought to human body or skin, and harmful effect can not be produced to the stability of facial film.
The using method of exfoliated Fructus Mali pumilae spot-relieving face mask of the present invention is: before using facial film, first deeply clean facial, again facial film is coated on face, after 15-25 minute, facial film active substance is absorbed by the skin, and moisture evaporates, thin film is formed gradually at face, this thin film is peeled off from face, the dirt on skin of face, scurf also stick on thin film in company with and be eliminated, face seems clean, smooth.
Exfoliated Fructus Mali pumilae spot-relieving face mask of the present invention, can deep layer cleaning skin of face, and desalination facial lines, makes elasticity of skin compact, and water profit is plentiful.Continue to use, skin water profit is flexible, reproduces youthful vigor.
Exfoliated Fructus Mali pumilae spot-relieving face mask of the present invention, contains natural fruit and plant elite, hyaluronic acid, multiple vitamin, all uniform white colour of skin, check melanin, spot fading.
Exfoliated Fructus Mali pumilae spot-relieving face mask of the present invention, adopt the antiseptic that carnosic acid, AOB, nisin, iodine propilolic alcohol butyl mephenesin Carbamate are composite, shelf life of products is long, and can not produce harmful effect to skin.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
Take each raw material according to embodiment 1 data corresponding in table 1, by carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, described compound preservative can be obtained.
Polyvinyl alcohol is added in deionized water, be heated to 70-90 DEG C, dissolve, be cooled to 45-55 DEG C, add glycerol, cocamidopropyl propyl amide hydroxyl sulfo betaine, ethanol, the stirring of capryl alcohol polyethers-9 carboxylic acid sodium, be cooled to 40 DEG C, add Fructus Mali pumilae extracting solution and compound preservative, stir, described exfoliated Fructus Mali pumilae spot-relieving face mask can be obtained.
Wherein, the Fructus Mali pumilae extracting solution in embodiment 1 and comparative example 1-5 adopts following method to be prepared from: after Fructus Mali pumilae is pulverized, add the deionized water of 8 times of weight, soak 2 hours, ultrasonic extraction, 12 minutes, filters, centrifugal, discard precipitation by supernatant concentration, after concentrated, obtained density is 1.06g/cm
3fructus Mali pumilae extracting solution.
Table 1: face pack prescription list position: kilogram
| Embodiment 1 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | |
| Deionized water | 100 | 100 | 100 | 100 | 100 | 100 |
| PVA-124 88 | 12 | 12 | 12 | 12 | 12 | 12 |
| Glycerol | 10 | 10 | 10 | 10 | 10 | 10 |
| Cocamidopropyl propyl amide hydroxyl sulfo betaine | 1 | 1 | 1 | 1 | 1 | 1 |
| Ethanol | 5 | 5 | 5 | 5 | 5 | 5 |
| Capryl alcohol polyethers-9 carboxylic acid sodium | 7 | 7 | 7 | 7 | 7 | 7 |
| Fructus Mali pumilae extracting solution | 1 | 1 | 1 | 1 | 1 | 1 |
| Carnosic acid | 0.01 | / | / | / | / | / |
| AOB | 0.02 | 0.02 | 0.02 | 0.03 | / | / |
| Nisin | 0.01 | 0.01 | 0.02 | 0.01 | / | / |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.01 | 0.02 | 0.01 | 0.01 | / | / |
| Methyl parahydroxybenzoate | / | / | / | / | 0.05 | / |
Comparative example 1
Each raw material is taken according to comparative example 1 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Fructus Mali pumilae spot-relieving face mask of comparative example 1.
Comparative example 2
Each raw material is taken according to comparative example 2 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Fructus Mali pumilae spot-relieving face mask of comparative example 2.
Comparative example 3
Each raw material is taken according to comparative example 3 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Fructus Mali pumilae spot-relieving face mask of comparative example 3.
Comparative example 4
Each raw material is taken according to comparative example 4 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Fructus Mali pumilae spot-relieving face mask of comparative example 4.
Comparative example 5
Take each component according to comparative example 5 data corresponding in table 1, adopt method described in embodiment 1, namely obtain the exfoliated Fructus Mali pumilae spot-relieving face mask of comparative example 5.
Test case 1
Respectively by the exfoliated Fructus Mali pumilae spot-relieving face mask that embodiment 1 and comparative example 1-5 obtain, carry out fill with dark brown vial, open wide bottle cap, under being placed in ambient temperature 40 DEG C, relative humidity 85% environment, continuous observation is also tested, and concrete outcome sees the following form.Detect microorganism level, concrete test item, detection method and examination criteria carry out according to QB/T2872-2007.
| Observe phenomena | |
| Embodiment 1 | No abnormality seen after 60 days, pure in smell |
| Comparative example 1 | After 50 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative example 2 | After 40 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative example 3 | After 40 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative example 4 | After 40 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative example 5 | After 5 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
The antiseptic methyl parahydroxybenzoate used in comparative example 4 is one of the most frequently used cosmetics preservative in this area.Belong to antiseptic phenols, generally effective to mycete, yeast, antibacterial, there is the effect suppressing growth of microorganism, the shelf-life (under test condition of the present invention 40 days shelf-lifves) of cosmetics is effectively extended after adding, but long-term this antiseptic of excessive use, Diazolidinyl Urea epidermis cell, causes epidermis transition aging.
Can significantly be drawn by test data, the embodiment of the present invention 1 uses carnosic acid, AOB, nisin and the composite Synergistic of iodine propilolic alcohol butyl mephenesin Carbamate, and antiseptic effect (under test condition of the present invention 60 days shelf-lifves) is obviously better than comparative example 1-3 and only adopts AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate three composite (under test condition of the present invention less than 50 days shelf-life).
The accelerated test of facial film under opening is placed in ambient temperature 40 DEG C, relative humidity 85% environment of the embodiment of the present invention 1, can reach 60 days antiseptic effects, the long shelf-life of facial film, and shady and cool dry its shelf-life of place far surpasses 3 years in sealed states in conversion.
Test case 2
With CorneometerCM820 moisture of skin measuring instrument, carry out measurement skin surface moisture at tested position, tested position is respectively the abundant forehead of sebaceous gland.Operating ambient temperature is 22-24 DEG C, and relative humidity is 46%-55%, and the unit of skin moisture content is au (arbitraryunit).Use the female consumer forehead skin of the embodiment of the present invention 1 to test to one, concrete data see the following form.
| Before using, au | After using, au | Use latter 1 hour, au | |
| Embodiment 1 | 38.4 | 79.6 | 75.6 |
The above; be only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.
Claims (3)
1. an exfoliated Fructus Mali pumilae spot-relieving face mask, it is characterized in that, be prepared from according to a conventional method by the raw material of following weight parts: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part cocamidopropyl propyl amide hydroxyl sulfo betaine, 4-6 part ethanol, 6-8 part capryl alcohol polyethers-9 carboxylic acid sodium, 0.8-2 part Fructus Mali pumilae extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters;
Described compound preservative is made up of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
2. exfoliated Fructus Mali pumilae spot-relieving face mask as claimed in claim 1, is characterized in that, be prepared from according to a conventional method by the raw material of following weight:
Deionized water 100 kilograms;
PVA-124 88 12 kilograms;
Glycerol 10 kilograms;
Cocamidopropyl propyl amide hydroxyl sulfo betaine 1 kilogram;
Ethanol 5 kilograms;
Capryl alcohol polyethers-9 carboxylic acid sodium 7 kilograms;
Fructus Mali pumilae extracting solution 1 kilogram;
Carnosic acid 0.01 kilogram;
AOB 0.02 kilogram;
Nisin 0.01 kilogram;
Iodine propilolic alcohol butyl mephenesin Carbamate 0.01 kilogram.
3. the preparation method of exfoliated Fructus Mali pumilae spot-relieving face mask as claimed in claim 1, it is characterized in that, be made up of following step: polyvinyl alcohol is added in deionized water, be heated to 70-90 DEG C, dissolve, be cooled to 45-55 DEG C, add glycerol, cocamidopropyl propyl amide hydroxyl sulfo betaine, ethanol, the stirring of capryl alcohol polyethers-9 carboxylic acid sodium, be cooled to 40 DEG C, add Fructus Mali pumilae extracting solution and compound preservative, stir.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310242394.7A CN103385847B (en) | 2013-06-18 | 2013-06-18 | Exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310242394.7A CN103385847B (en) | 2013-06-18 | 2013-06-18 | Exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103385847A CN103385847A (en) | 2013-11-13 |
| CN103385847B true CN103385847B (en) | 2015-08-26 |
Family
ID=49530383
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310242394.7A Expired - Fee Related CN103385847B (en) | 2013-06-18 | 2013-06-18 | Exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103385847B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055263A (en) * | 2015-10-02 | 2015-11-18 | 王学建 | Traditional Chinese medicine mask with whitening and spot reducing effects and preparation method of traditional Chinese medicine mask |
| CN106974843A (en) * | 2016-11-01 | 2017-07-25 | 田鹏新 | A kind of exfoliated apple ferment facial mask and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101084869A (en) * | 2007-06-21 | 2007-12-12 | 上海利盛生化有限公司 | Method for extracting and purifying flavonoids from apple powder agent and application thereof |
| CN102366378A (en) * | 2011-09-21 | 2012-03-07 | 吴江市顺昌日用品有限公司 | Apple juice mask and its preparation method |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06158096A (en) * | 1992-05-07 | 1994-06-07 | Shiseido Co Ltd | Masking agent |
| JP2008174514A (en) * | 2007-01-22 | 2008-07-31 | Kao Corp | Water-in-oil type emulsified cosmetic |
| JP2010254667A (en) * | 2009-03-31 | 2010-11-11 | Fancl Corp | Collagen gel shrinking agent |
-
2013
- 2013-06-18 CN CN201310242394.7A patent/CN103385847B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101084869A (en) * | 2007-06-21 | 2007-12-12 | 上海利盛生化有限公司 | Method for extracting and purifying flavonoids from apple powder agent and application thereof |
| CN102366378A (en) * | 2011-09-21 | 2012-03-07 | 吴江市顺昌日用品有限公司 | Apple juice mask and its preparation method |
Non-Patent Citations (3)
| Title |
|---|
| Kim, Mi Young,et al.Clinical Effectiveness of Regular Use of Unripe Apple Mask Pack on Skin Status of Middle-aged Women.《Korean J Nutr》.2010,第43卷(第5期),第453-462页,尤其第453页摘要,第454页右栏第5-8行,第460页表 7. * |
| L.V. Thomas,et al.Nisin synergy with natural antioxidant extracts of the herb rosemary.《Proc IM IS on Natural Preserv. in Food Systems》.2006,第109-113页,第110页倒数第1-3段,第111页第1行,第8-10行,第112页表1-表3. * |
| 李东光等.第7节 面膜.《实用化妆品配方手册》.化学工业出版社,2009,(第2版),第106-108页. * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103385847A (en) | 2013-11-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103356420B (en) | Peel-off coix seed mask and preparation method of mask | |
| CN103356425B (en) | Peel-off ginseng mask and preparation method of mask | |
| CN103385824B (en) | Peel-off type red sage root mask and preparation method thereof | |
| CN103385826B (en) | Peel-off type mung bean acne-removing mask and preparation method thereof | |
| CN103405358B (en) | Stripping-type cherry firming facial mask and preparation method thereof | |
| CN103385847B (en) | Exfoliated Fructus Mali pumilae spot-relieving face mask and preparation method thereof | |
| CN103356468B (en) | Exfoliated bletilla face mask and preparation method thereof | |
| CN103356427B (en) | Peel-off type rhodiola rosea nourishing facial mask and preparation method thereof | |
| CN103356472B (en) | Peel-off type conyza blinii facial mask and preparation method thereof | |
| CN103356469B (en) | Peel-off type pomegranate facial mask and preparation method thereof | |
| CN103385840B (en) | Exfoliated Nidus collocaliae skin moistening facial film and preparation method thereof | |
| CN103356471B (en) | Peel-off pseudo-ginseng mask and preparation method of mask | |
| CN103356464B (en) | Peel-off type scutellaria baicalensis cleansing facial mask and preparation method thereof | |
| CN103356470B (en) | Exfoliated Herba Taraxaci skin cleaning mask and preparation method thereof | |
| CN103356435B (en) | Exfoliated ginkgo flour film and preparation method thereof | |
| CN103356433B (en) | Exfoliated green tea skin moistening facial film and preparation method thereof | |
| CN103356429B (en) | Peel-off type liquorice sterilizing facial mask and preparation method thereof | |
| CN103356473B (en) | Peel-off lavender refining mask and preparation method of mask | |
| CN103356463B (en) | Peel-off type radix saposhnikoviae anti-anaphylaxis facial mask and preparation method thereof | |
| CN103356422B (en) | Peel-off cornflower mask and preparation method of mask | |
| CN103356467B (en) | Peel-off type ganoderma lucidum facial mask and preparation method thereof | |
| CN103385825B (en) | Clean flour film of exfoliated yellow orange and preparation method thereof | |
| CN103356405B (en) | Exfoliated brown algae nutritive facial mask and preparation method thereof | |
| CN103356428B (en) | Exfoliated Fructus Forsythiae control pasta film and preparation method thereof | |
| CN103356423B (en) | Peel-off type tuckahoe facial mask and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Zhang Jilin Inventor before: Wang Feifen |
|
| COR | Change of bibliographic data | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160831 Address after: 225400 Jiangsu city of Taixing Province Branch Road, East high tech Industrial Park, No. 6 Patentee after: Impression of the emperor of Jiangsu biological Polytron Technologies Inc Address before: Room 2118 building four layer d441 No. third Shanghai 201111 Minhang District Guanghua Road Patentee before: Shanghai Zhenxin Chemical Co., Ltd. |
|
| CB03 | Change of inventor or designer information |
Inventor after: Zhang Jilin Inventor after: Xu Hui Inventor before: Zhang Jilin |
|
| CB03 | Change of inventor or designer information | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150826 Termination date: 20180618 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |