CN106974843A

CN106974843A - A kind of exfoliated apple ferment facial mask and preparation method thereof

Info

Publication number: CN106974843A
Application number: CN201610934785.9A
Authority: CN
Inventors: 田鹏新
Original assignee: Individual
Current assignee: Individual
Priority date: 2016-11-01
Filing date: 2016-11-01
Publication date: 2017-07-25

Abstract

The present invention relates to cosmetic field, and in particular to a kind of exfoliated apple ferment facial mask and preparation method thereof, and its component is film forming agent：5 10 parts of polyvinyl alcohol, 15 parts of PVP, 0.3 1 parts of ethylene glycol dilaurate, 58 parts of chitosan, 13 parts of carboxy-propyl cellulose；Oil：1.5 2.5 parts of jojoba oil, 1.5 3.5 parts of evening primrose oil, 24 parts of olive oil；NMF：35 parts of 5 10 parts of glycerine, hyaluronic acid or Sodium Hyaluronate, 25 parts of sorbierite；Pulvis：12 parts of kaolin, 12 parts of zinc oxide；Alcohols：10 15 parts of C1 C4 lower alcohol；Surfactant：12 parts of polyglyceryl fatty acid ester；12 parts of polyoxyethylene hardened castor oil；Apple ferment：10 25 parts, the speed of its film forming, gas permeability, tension force are strong and weak, fissility is more excellent, and its ferment composition is retained, with to the preferable moisten effect of skin.

Description

A kind of exfoliated apple ferment facial mask and preparation method thereof

Technical field：

The present invention relates to cosmetic field, and in particular to a kind of exfoliated apple ferment facial mask and preparation method thereof.

Background technology：

Facial mask is a kind of multipurpose cosmetics for integrating cleaning, skin care and beauty, using the of short duration time for being covered in face, Air and the pollution in the external world are temporarily isolating, skin temperature is improved, the pore expansion of skin promotes sweat gland secretion and metabolism, For the regular application facial mask of all kinds of skin characteristics, Oily degreasing can be made, thick pore is restrained, dry up gauffer Skin recovers gloss, and the inflammation of dark sore skin is inhibited.

The species of facial mask is a lot, can generally be divided into four classes, that is, peels off facial mask, powder face pack, cream pack and forming surface Film.And peel off facial mask and be generally ointment shape and gel, facial mask is coated on face when using, thrown off after dry, face Dirt, scurf be also adhered on facial mask while be broken away, reach the purpose of cleaning skin.

Cosmetics of the prior art in the skin care item of gypsum shape or the skin care item of liquid, are made to the application majority of ferment Film forming into facial mask is poor, is suitable as powder face pack, cream pack and is coated on the face, is rinsed after facial mask has been applied with clear water The mode of removing cleans face, weaker for the removal ability of facial dirt, scurf for facial mask is peeled off.

For peel off facial mask film forming for, it is necessary to consider the speed of film forming, the gas permeability of film forming, film forming tension force it is strong Weak, film forming fissility this four key points of quality, and ferment is made and peels off facial mask, also need to consider that film forming agent addition lives to ferment The influence of property.

The content of the invention

Present disclosure is to provide a kind of exfoliated apple ferment facial mask, the speed of its film forming, the gas permeability of film forming, The tension force of film forming is strong and weak, film forming fissility is more excellent, and the ferment composition in facial mask is retained, with preferably moist to skin Effect.

To achieve the above object, inventor is by reducing the addition of synthesis type film forming agent into facial mask, and is gathered using shell Sugar lifts the tension force of peel off pack as the supplement of film forming agent, and the facial mask prepared with apple ferment can retain excellent Enzyme activity, is used for a long time, and has good effect for facial skin whitening, moisturizing, oil-control, desalination scar.

The component of the present invention is specific as follows：

Film forming agent：5-10 parts of polyvinyl alcohol, 1-5 parts of PVP, 0.3-1 parts of ethylene glycol dilaurate, chitosan 5-8 parts, 1-3 parts of carboxy-propyl cellulose；

Oil：1.5-2.5 parts of jojoba oil, 1.5-3.5 parts of evening primrose oil, 2-4 parts of olive oil；

NMF：3-5 parts of 5-10 parts of glycerine, hyaluronic acid or Sodium Hyaluronate, 2-5 parts of sorbierite；

Pulvis：1-2 parts of kaolin, 1-2 parts of zinc oxide；

Alcohols：C₁-C₄10-15 parts of lower alcohol；

Surfactant：1-2 parts of polyglyceryl fatty acid ester；1-2 parts of polyoxyethylene hardened castor oil；

Apple ferment：10-25 parts.

The homogeneous components being mixed to form with 0.8-1.2 times of deionized water of said components total amount.

By being fermented to apple, containing abundant enzyme system, these enzymes can decompose face's grease, cutin-softening layer, Make skin more clean tender.Meanwhile, apple is in the presence of microorganism and enzyme, and protein-based nutriment can be broken down into small The nutrient such as molecular peptide or amino acid, vitamin, mineral matter, EGF can be discharged fully, natural anthocyanidin, polysaccharide, flavones Also it is dissolved in zymotic fluid Deng some natural anti-oxidation products, these compositions can directly be absorbed by skin, for cosmetics In, accelerate skin and mucous membrane wound healing, anti-inflammatory analgesic, prevent wound form a scab trace and play significant moisturizing, nti-freckle and Effect of anti-aging.

Rich in amylaceous apple, the apple ferment made by particular form can possess appropriate starchiness, and in face Appropriate thickening effect is produced in film system, the use of thickener can be reduced to a certain degree；

By to using natural, xanthans, chitosan with good filming effect as film forming agent, reduce it is artificial synthesized into The use of film, has higher security for the nursing of facial skin；And there is excellent fit 5 to most of active materials Property；Obtained facial mask film forming is good, and the speed of film forming, the gas permeability of film forming, the tension force power of film forming, film forming fissility have There is gratifying effect.

Further, calculate as mass fraction, also comprising 6-10 parts of functional components；Preferably, described feature Composition is anti-inflammatory composition, and plant extracts, whitening composition presses 0-1:0-3:0-2 ratio is mixed.

Wherein, anti-inflammatory composition is any one in enoxolone, allantoin, ammonium ichthosulfonate or two or more mixing.

Enoxolone has inhibitory action to various acute inflammation, the anti-inflammatory with similar phenylbutazone or hydrocortisone sample Effect, to people's multiple type nuclear leukocyte（PMN）The oxygen radical of release has obvious scavenging action, acts on inflammation part, has Excellent anti-inflammatory efficacy；

Allantoin, which has, promotes cell growth, quickening wound healing, and the physiological function such as cutin-softening albumen, is the good of skin trauma Good consolidant and antiulcer agents.It is added in facial mask, facial skin drying can be alleviated, contribute to hyaluronic acid/hyaluronic acid The performance of sodium moisture-retaining capacity, shines the jade-like stone profit texture of facial skin；

For the redness in facial skin hair follicle portion, and for fat granule, extrude these inflammation parts and easily leave scar, pass through Using the facial mask added with ammonium ichthosulfonate, such red and swollen, intensification of fat granule can be prevented, in the promotion cell growth of apple ferment Under effect, inflammation part is set to be converted into normal condition, it is to avoid the further intensification of inflammation part.

Plant extracts is more than one or both of camomile extract, pot marigold extract, aloe extract Mixing.

Camomile extract can not only balanced fat secretion, press down fat anti-acne, prevent acne, eliminate blackspot, skin whitening, and And there is suppression and bactericidal action to some skin pathogenicity fungies.The mildy wash that makes an addition in cosmetics, face cream, massage There is good skin care, beautifying skin and treating to act in cream, facial mask；

Contain lutein in pot marigold, medical experiment proves that natural carotenol contained in plant is a kind of antioxygen of excellent performance Agent, by being used for skin, mucous membrane outside, can eliminate various inflammation, and accelerate blood clotting, promote wound incrustation, and prevent from staying scar Effect；

Anthracene ketone compounds in aloe have the effects such as sterilization, antibacterial, anti-inflammatory, removing toxic substances, promotion wound healing, research hair mostly Existing Aloesin and Barbaloin are respectively provided with sterilization, antiinflammation, and the sterilization of aloe, inflammation-diminishing function can effectively eliminate powder Thorn, acne, are used clinically for treating inflammation, evident in efficacy.

Whitening composition is more than one or both of four hexyl decyl alcohol acid ascorbyl esters, azelaic acid, hydroquinones, tartaric acid Mixing.

Four hexyl decyl alcohol acid ascorbyl esters, hydroquinones have good anti-oxidant and white-skinned face function, for suppressing junket ammonia The activity of sour enzyme, it is to avoid melanin deposition has excellent effect, is added in all kinds of cosmetics frequently as whitening composition, addition Be conducive to improving the white-skinned face function of its this product into this product.

The generation and effect of azelaic acid energy inhibitory activity oxygen groups, this result is beneficial to the anti-inflammatory of medicine and a variety of treatments are made With its security is good nontoxic without teratogenesis, by reducing the synthesis of thread keratin, is added in facial mask, contributes to The permeability of apple ferment is lifted, and reduces the skin problem of follicular hyperkeratosis.

Tartaric acid can accelerate the renewal of cell, remove unhealthy and abnormal epidermal cell, thus improve skin appearance with Function, makes the colour of skin comprehensively be improved.Also studies have found that, the hydroxyacetic acid such as lactic acid in addition to the effect for having exfoliating, also The synthesis of melanin can be suppressed, used cooperatively with four hexyl decyl alcohol acid ascorbyl esters, azelaic acid, hydroquinones, moreover it is possible to lifted Its whitening effect.

Another object of the present invention is to provide the manufacture method of the exfoliated apple ferment facial mask, comprise the following steps that：

（1）Apple is cleaned and is enucleated, is crushed, after carrying out fermentation 5-10 days under the conditions of lucifuge, by the apple after fermentation with not sending out The apple of ferment presses 1:3 ratio mixed fermentations 10-25 days, and circulating fermentation；The circulating fermentation zymotic fluid of 30-45 days is entered with apple Row pulverization process, is filtered off after insoluble matter, after ferment clear liquid is sterilized, and is carried out freeze-drying process, is prepared as apple ferment Powder；

（2）Xanthans, chitosan are dissolved in deionized water in proportion, 50-60 DEG C is cooled to again after being heated to boiling, addition is removed Stirred after remaining components outside apple ferment powder, be cooled to addition apple ferment powder after normal temperature；Obtain apple ferment facial mask.

By the way that xanthans, chitosan are carried out into maturation process, the film forming speed of end article of the present invention, Yi Jicheng can be improved Film-strength；50-60 DEG C is then cooled to, functional components are dissolved, while can preventing that functional components from destroying, each component is obtained Sufficiently effectively dissolving；Apple ferment powder is dissolved at normal temperatures, can be possessed active component therein.

For step（1）Sterilization process therein, can be set to UHT sterilizations by the optimization of process；And at -18 ~ -35 DEG C, Vacuum is progress vacuum freeze drying processing under conditions of 10-15Pa.Activity for apple ferment is kept with better Good effect.

Embodiment

In order that the objects, technical solutions and advantages of the present invention are more easily understood, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.

Embodiment 1

A kind of exfoliated apple ferment facial mask, is calculated as mass fraction, with getting following material ready：

Film forming agent：5 parts of polyvinyl alcohol, 3 parts of PVP, 0.5 part of ethylene glycol dilaurate, 7 parts of chitosan, carboxylic third 2 parts of base cellulose；

Oil：2 parts of jojoba oil, 2.5 parts of evening primrose oil, 2 parts of olive oil；

NMF：5 parts of 5 parts of glycerine, hyaluronic acid or Sodium Hyaluronate, 5 parts of sorbierite；

Pulvis：2 parts of kaolin, 1 part of zinc oxide；Alcohols：10 parts of ethanol；

Surfactant：1 part of polyglyceryl fatty acid ester；2 parts of polyoxyethylene hardened castor oil；15 parts of apple ferment；Deionized water 80 parts；

It is prepared according to the following steps this product：

Embodiment 2

Film forming agent：8 parts of polyvinyl alcohol, 4 parts of PVP, 0.8 part of ethylene glycol dilaurate, 7 parts of chitosan, carboxylic third 2 parts of base cellulose；

Oil：2 parts of jojoba oil, 3 parts of evening primrose oil, 3 parts of olive oil；

NMF：3 parts of 8 parts of glycerine, hyaluronic acid or Sodium Hyaluronate, 3 parts of sorbierite；

Pulvis：1 part of kaolin, 2 parts of zinc oxide；Alcohols：8 parts of ethanol, 3 parts of isopropanol；

Surfactant：1.5 parts of polyglyceryl fatty acid ester；1.5 parts of polyoxyethylene hardened castor oil；20 parts of apple ferment；Go from Sub- 100 parts of water；

1 part of enoxolone, 0.5 part of ammonium ichthosulfonate, 2 parts of camomile extract, 1 part of aloe extract, four hexyl decyl alcohol ascorbic acid 3 parts of ester, 1 part of azelaic acid.

It is prepared according to the following steps this product：

（1）Apple is cleaned and is enucleated, is crushed, after carrying out fermentation 5-10 days under the conditions of lucifuge, by the apple after fermentation with not sending out The apple of ferment presses 1:3 ratio mixed fermentations 10-25 days, and circulating fermentation；The circulating fermentation zymotic fluid of 30-45 days is entered with apple Row pulverization process, is filtered off after insoluble matter, and ferment clear liquid is carried out after UHT sterilizations, and at -18 DEG C, vacuum is under conditions of 13Pa Vacuum freeze drying processing is carried out, apple ferment powder is prepared as；

（2）Xanthans, chitosan are dissolved in deionized water in proportion, is heated to after boiling being cooled to 60 DEG C again, adds and remove apple Stirred after remaining components outside fruit ferment powder, be cooled to addition apple ferment powder after normal temperature；Obtain apple ferment facial mask.

Embodiment 3

Film forming agent：7 parts of polyvinyl alcohol, 5 parts of PVP, 1 part of ethylene glycol dilaurate, 5 parts of chitosan, carboxylic propyl group 3 parts of cellulose；

Oil：1.5 parts of jojoba oil, 1.8 parts of evening primrose oil, 3.2 parts of olive oil；

NMF：5 parts of 6 parts of glycerine, hyaluronic acid or Sodium Hyaluronate, 4 parts of sorbierite；

Pulvis：1.5 parts of kaolin, 1.5 parts of zinc oxide；

Alcohols：9 parts of ethanol, 1 part of isopropanol, 1 part of isobutanol；

Surfactant：1.5 parts of polyglyceryl fatty acid ester；1.5 parts of polyoxyethylene hardened castor oil；

23 parts of apple ferment, 108 parts of deionized water；

0.5 part of enoxolone, 0.5 part of allantoin, 1 part of camomile extract, 0.8 part of pot marigold extract, aloe extract 1.2 Part, 0.5 part of four hexyl decyl alcohol acid ascorbyl ester, 0.5 part of azelaic acid, 0.5 part of hydroquinones, 0.5 part of tartaric acid.

（1）Apple is cleaned and is enucleated, is crushed, after fermentation being carried out under the conditions of the lucifuge 5-10 days, by the apple after fermentation and Unfermentable apple presses 1:3 ratio mixed fermentations 10-25 days, and circulating fermentation；By the circulating fermentation zymotic fluid and apple of 30-45 days Fruit carries out pulverization process, filters off after insoluble matter, and ferment clear liquid is carried out after UHT sterilizations, and at -25 DEG C, vacuum is 10Pa bar Vacuum freeze drying processing is carried out under part, apple ferment powder is prepared as；

（2）Xanthans, chitosan are dissolved in deionized water in proportion, is heated to after boiling being cooled to 55 DEG C again, adds and remove apple Stirred after remaining components outside fruit ferment powder, be cooled to addition apple ferment powder after normal temperature；Obtain apple ferment facial mask.

Test case

According to above-described embodiment 1 make facial mask, be respectively adopted only save xanthans, only save chitosan, save xanthans and The mode of chitosan, carries out the production of facial mask, is contrasted evaluate with test case 1-3 and embodiment 1-3 respectively；

20 female subjects each to 6 groups carry out skin test, and by raw material on facial skin, half an hour after to be dried takes Under, it is strong to the tension force of the speed of the film forming of product in each embodiment, the gas permeability of film forming, film forming according to the impression standard of subject Weak, film forming tension force is strong and weak, cuticula removes speed, skin smoothness and evaluated, the results detailed in Table 1.

Evaluation criterion：

□：Have in 20 people and more than 18 people think to work well.

○：Have in 20 people and more than 15-17 people think to work well.

△：Have in 20 people and more than 10-14 people think to work well.

×：Have in 20 people less than more than 10 people thinking to work well.

The evaluation result of table 1

The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, it is any Those familiar with the art the invention discloses technical scope in, the change or replacement that can be readily occurred in, all should It is included within the scope of the present invention.Therefore, protection scope of the present invention should be defined by scope of the claims.

Claims

1. a kind of exfoliated apple ferment facial mask, it is characterised in that calculate as mass fraction, include following material：

Pulvis：1-2 parts of kaolin, 1-2 parts of zinc oxide；

Alcohols：C₁-C₄10-15 parts of lower alcohol；

Apple ferment：10-25 parts；

2. a kind of exfoliated apple ferment facial mask as claimed in claim 1, it is characterised in that calculate, also wrap as mass fraction 6-10 containing functional components parts.

3. a kind of exfoliated apple ferment facial mask as claimed in claim 2, it is characterised in that described functional components are anti- Inflammatory components, plant extracts, whitening composition presses 0-1:0-3:0-2 ratio is mixed.

4. a kind of exfoliated apple ferment facial mask as claimed in claim 3, it is characterised in that described anti-inflammatory composition is sweet Any one in careless hypo acid, allantoin, ammonium ichthosulfonate or two or more mixing.

5. a kind of exfoliated apple ferment facial mask as claimed in claim 3, it is characterised in that described plant extracts is ocean Mixing more than one or both of Flos Chrysanthemi extract, pot marigold extract, aloe extract.

6. a kind of exfoliated apple ferment facial mask as claimed in claim 3, it is characterised in that described whitening composition be four oneself Mixing more than one or both of base decyl alcohol acid ascorbyl ester, azelaic acid, hydroquinones, tartaric acid.

7. a kind of preparation method of exfoliated apple ferment facial mask as described in claim 1-6 any one, its feature exists In following steps：

Apple is cleaned and is enucleated, is crushed, after fermentation being carried out under the conditions of the lucifuge 5-10 days, by the apple after fermentation with it is unfermentable Apple presses 1:3 ratio mixed fermentations 10-25 days, and circulating fermentation；The circulating fermentation zymotic fluid of 30-45 days and apple are subjected to powder Broken processing, is filtered off after insoluble matter, after ferment clear liquid is sterilized, and is carried out freeze-drying process, is prepared as apple ferment powder；

Xanthans, chitosan are dissolved in deionized water in proportion, is heated to after boiling being cooled to 50-60 DEG C again, adds and remove apple Stirred after remaining components outside fruit ferment powder, be cooled to addition apple ferment powder after normal temperature；Obtain apple ferment facial mask.

8. a kind of preparation method of exfoliated apple ferment facial mask as claimed in claim 7, it is characterised in that：

Step（1）Described in sterilization process be UHT sterilization；And at -18 ~ -35 DEG C, vacuum is to enter under conditions of 10-15Pa The processing of row vacuum freeze drying.