CN103405358A - Stripping-type cherry firming facial mask and preparation method thereof - Google Patents
Stripping-type cherry firming facial mask and preparation method thereof Download PDFInfo
- Publication number
- CN103405358A CN103405358A CN2013102432560A CN201310243256A CN103405358A CN 103405358 A CN103405358 A CN 103405358A CN 2013102432560 A CN2013102432560 A CN 2013102432560A CN 201310243256 A CN201310243256 A CN 201310243256A CN 103405358 A CN103405358 A CN 103405358A
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- skin
- facial mask
- stripping
- cherry
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Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a stripping-type cherry firming facial mask and a preparation method thereof. The stripping-type cherry firming facial mask is prepared from the following materials by using a conventional method in parts by weight: 10-14 parts of polyvinyl alcohol, 8-12 parts of glycerol, 0.8-1.2 parts of hydrolyzed extensin, 4-6 parts of ethanol, 6-8 parts of cetyl lycine, 0.8-2 parts of cherry extract, 0.03-0.08 parts of a compound preservative and 100 parts of deionized water, wherein the compound preservative is prepared from the following components in parts by weight: 1-3 parts of carnosic acid, 3-5 parts of antioxidant of bamboo leaves, 1-3 parts of nisin and 1-3 parts of iodine propiolic alcohol butyl ammonia formate. By adopting the stripping-type cherry firming facial mask disclosed by the invention, the nutritional ingredients such as vitamin C being in gradual shortage in the skin can be supplied; pores can be closed; the stripping-type cherry firming facial mask contains a plurality of active ingredients such as vitamins, and arginin, so that dark and matte skin is prevented; the skin is compact; the elasticity is restored.
Description
Technical field
The present invention relates to facial film and preparation method thereof, be specifically related to a kind of exfoliated Fructus Pruni pseudocerasi extra firming facial mask and preparation method thereof.
Background technology
Facial film is the important content in skin nursing, for the regular application facial film of all kinds of skin characteristics, can make the oily skin defat, and thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.Facial film makes skin seem salubrious after using, smooth and pure white delicacy, this is because when facial film is coated on skin, facial film and skin produce affinity, drying gradually along with facial film, the skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, the sebum of skin secretion and moisture reverse osmosis are in horny layer, the epidermis softness is unfolded, the pore instinct is opened, effective ingredient in facial film infiltrates skin and is absorbed, facial film tightly is connected with skin simultaneously, when removing facial film, aging cutin on skin, in pore, the deep layer dirt is also by the while leukorrhagia, make skin pure and fresh clean.
The principle of facial film, utilize exactly the blink that covers face, extraneous air and the pollution of temporary transient isolation, improve the skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to the oil substances that skin is got rid of the metabolic product of epidermis cell and accumulation, the moisture in facial film infiltrates the horny layer of skin epidermis, it is soft that skin becomes, and skin light naturally is flexible.
To beautiful pursuit, the cosmetics kind is more and more various along with the raising of people's quality of the life and people.At present, face mask of traditional Chinese medicine is one of beauty treatment educational circles effective whitening scheme, and especially some Chinese medicine extraction liquid have the effect of toxin expelling, speckle dispelling, reparation, skin care preferably, also by being applied in facial film gradually.
But because facial film is liquid condition, Chinese medicine extraction liquid is easy to grow mycete, a lot of face mask of traditional Chinese medicine antiseptic effects in the market are not good, and the shelf-life is short.In therefore a lot of face mask of traditional Chinese medicines, all can add antiseptic.Yet a lot of antiseptic, in the microorganisms such as kill bacteria, fungus, also can produce zest to skin, even cause erythema and erythra, the Long Term Contact antiseptic, can increase organism material sensitization, cause the danger of anaphylactic reaction.
Iodine propilolic alcohol butyl mephenesin Carbamate (being called for short IPBC) is a kind of novel cosmetic antiseptic, has good fungistatic effect, and dissolubility preferably arranged in surfactant, emulsifying agent, polar solvent, therefore be widely used in resident class and drip washing class cosmetic formulations, other antiseptic such as normal and diazolidinyl urea, hydantoin are used in conjunction with.In China's cosmetics health standard and European Union's regulatory affairs, regulation IPBC limits the use of antiseptic in components of cosmetics, and maximum permission working concentration is 0.05% in cosmetics, and can not be for oral hygiene and lip product.But in facial film, antiseptic effect not obvious when addition is less than 0.05%.Therefore, there is little and antiseptic effect is poor, the shelf-life the is short problem of consumption in the antiseptic used in current facial film.Iodine propilolic alcohol butyl mephenesin Carbamate or other antiseptic large usage quantities in the part facial film are also arranged, can be produced pessimal stimulation by skin, with after need to clean facial, use and bother.
Fructus Pruni pseudocerasi, be the fruit of rosaceous plant Fructus Pruni pseudocerasi Prunus pseudocerasus.Another name: car li son, Zhu fruit, cherry apple, family's Fructus Pruni pseudocerasi, Ying peach, Oriolus chinensis diffusus peach, tassel peach, cherry pearl, wedge peach, Ying Tao, Jing Tao, Niu Tao, Ling English, Zhu Ying, Mai Ying, precipice honey, cherry, Nanking cherry, Prunus avium, sour cherry.Nature and flavor: tepor, sweet, sour.Function: strengthening the spleen nourishing the stomach, arresting seminal emission antidiarrheal.Composition: edible part 80%.Energy content 192kj in every 100g, moisture 88g, protein 1.1g, fatty 0.2g, dietary fiber 0.3g, carbohydrate 9.9g, carotene 210 μ g, retinol equivalent 35 μ g, thiamine 0.02mg, riboflavin 0.02mg, nicotinic acid 0.6mg; Vitamin C 10mg, vitamin E2 .22mg, potassium 232mg, sodium 8mg, calcium 11mg, magnesium 12mg, ferrum 0.4mg, manganese 0.07mg, zinc 0.23mg, copper 0.10mg, phosphorus 27mg, selenium 0.21 μ g.
Cherry i s of high nutrition, contained protein, sugar, phosphorus, carotene, vitamin C are high, and especially iron-holder is high, and cherry juice commonly used is embrocated face and wrinkle place, can make skin of face ruddy tender white, and makes the skin consolidation, recovers elasticity.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention provides a kind of exfoliated Fructus Pruni pseudocerasi extra firming facial mask.
Two of technical problem to be solved by this invention provides the preparation method of above-mentioned exfoliated Fructus Pruni pseudocerasi extra firming facial mask.
The present invention seeks to be achieved through the following technical solutions:
A kind of exfoliated Fructus Pruni pseudocerasi extra firming facial mask is prepared from according to a conventional method by the raw material of following weight parts:
10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part hydrolysis extensin, 4-6 part ethanol, 6-8 part cetyl betaine, 0.8-2 part cherry extract, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
Wherein, described compound preservative consists of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
By carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Described exfoliated Fructus Pruni pseudocerasi extra firming facial mask can adopt industry conventional method to be prepared from.
Further, the present invention also provides a kind of preparation method of exfoliated Fructus Pruni pseudocerasi extra firming facial mask, is comprised of following step:
Polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, hydrolysis extensin, ethanol, cetyl betaine to stir, be cooled to 40 ℃, add cherry extract and compound preservative, stir, can make described exfoliated Fructus Pruni pseudocerasi extra firming facial mask.
Concrete, in the present invention:
Described polyvinyl alcohol can be selected the cosmetics-stage polyvinyl alcohol, and specifically can select as the trade mark is the polyvinyl alcohol of PVA1788, PVA1799 or PVA2488.
Glycerol has another name called: propylene glycol, English name: Glycerin, molecular formula C
3H
8O
3.
The hydrolysis extensin, English name: HYDROLYZED EXTENSIN, CAS accession number: 73049-73-7.The hydrolysis extensin can improve the natural moist function of skin, prevents the evaporation of skin internal moisture, makes dry skin moist, fine and smooth.
Cetyl betaine, English name: CETYL BETAINE, CAS accession number: 693-33-4.Have good decontamination, emulsifying, foaming, steady bubble, antistatic, thickening capabilities.Gentle surfactant.Can reduce the zest of other surfactants.Anti-hard water.Compatibility is good.
Cherry extract of the present invention can pass through commercially available obtaining.Also can adopt following method preparation and obtain: after Fructus Pruni pseudocerasi is pulverized, add the deionized water of 6-10 times of weight, soak 1-3 hour, ultrasonic extraction, 10-15 minute, filter, centrifugal, discards precipitation by supernatant concentration, makes cherry extract.Preferably, after concentrating, controlling cherry extract density is 1.02-1.10g/cm
3.
Carnosic acid, molecular formula: C
20H
28O
4, No. CAS: 3650--09-7, source: Labiatae Rosmarinus plant rosemary Rosmarinus officinalis L.
AOB, No. CNS: 04.019, English name: antioxidant of bamboo leaves.AOB from the tender leaf of Phyllostachys (phyllostachys) bamboo, extract, take flavone and phenolic compound and be natural, the nutrition of effective ingredient, multi-functional food antioxidant.
Nisin also claims nisin, English name: Nisin, and by the synthetic a kind of polypeptide formed by 34 aminoacid of streptococcus acidi lactici metabolism, molecular formula C
143H
228O
37N
42S
7Molecular weight is 3348, and nisin consists of water-wet side and hydrophobic side, is typical surfactant, be efficient, nontoxic biological antiseptic, be widely used in the anticorrosion of milk and milk products, fermented beverage, filling food, vegetable protein food, meat and its products at present.
Iodine propilolic alcohol butyl mephenesin Carbamate, English name: 3-Iodo-2-propynyl butylcarbamate, be abbreviated as IPBC, No. CAS: 55406-53-6, molecular formula: C
8H
12INO
2, molecular weight is 281.10.
The present invention uses carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate composite as antiseptic, and antiseptic effect is significantly improved, the long shelf-life of facial film.And, use Compositional antiseptic agent, greatly reduce the consumption of iodine propilolic alcohol butyl mephenesin Carbamate, the consumption of iodine propilolic alcohol butyl mephenesin Carbamate is controlled at below 0.03%, meet the IPBC stipulated in China's cosmetics health standard and European Union's regulatory affairs and limit the use of antiseptic in components of cosmetics, maximum permission working concentration is 0.05% in cosmetics.Carnosic acid, AOB, nisin are the nontoxic biological antiseptic, be widely used in food service industry, in the present invention, it is diverted to cosmetic mask, can't brings ill effect to human body or skin, and can not produce harmful effect to the stability of facial film.
The using method of exfoliated Fructus Pruni pseudocerasi extra firming facial mask of the present invention is: before using facial film, first deeply clean facial, again facial film is coated on to face, after 15-25 minute, the facial film active substance is absorbed by the skin, the moisture evaporation, at face, form gradually thin film, this thin film is peeled off from face, and the dirt on skin of face, scurf also stick on thin film in company with and are eliminated, and it is clean, smooth that face seems.
Exfoliated Fructus Pruni pseudocerasi extra firming facial mask of the present invention, can the deep layer cleaning skin of face, desalinates facial microgroove, makes skin elasticity compact, and the water profit is plentiful.Continue to use, skin water profit is flexible, reproduces youthful vigor.
Exfoliated Fructus Pruni pseudocerasi extra firming facial mask of the present invention, can supplement the nutritional labelings such as vitamin C that skin day by day lacks, pore refining, contain the various active compositions such as vitamin, arginine, prevent the dark yellow tarnish of skin, wherein contained organic acid can also be eliminated the fatigue of facial muscle, wake the skin vigor up, salubrious moistening, prevent the dark yellow tarnish of skin, and make skin consolidation, recovery elasticity.
Exfoliated Fructus Pruni pseudocerasi extra firming facial mask of the present invention, adopt carnosic acid, AOB, nisin, the composite antiseptic of iodine propilolic alcohol butyl mephenesin Carbamate, and shelf life of products is long, and can not produce harmful effect to skin.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1
According to corresponding embodiment 1 data in table 1, take each raw material, by carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, hydrolysis extensin, ethanol, cetyl betaine to stir, be cooled to 40 ℃, add cherry extract and compound preservative, stir, can make described exfoliated Fructus Pruni pseudocerasi extra firming facial mask.
Wherein, the cherry extract in embodiment 1 and Comparative Examples 1-5 adopts following method to be prepared from: after Fructus Pruni pseudocerasi is pulverized, add the deionized water of 8 times of weight, soaked 2 hours, ultrasonic extraction, 12 minutes, filter, centrifugal, discard precipitation by supernatant concentration, after concentrating, making density is 1.06g/cm
3Cherry extract.
Table 1: face pack prescription list position: kilogram
| ? | Embodiment 1 | Comparative Examples 1 | Comparative Examples 2 | Comparative Examples 3 | Comparative Examples 4 | Comparative Examples 5 |
| Deionized water | 100 | 100 | 100 | 100 | 100 | 100 |
| PVA-124 88 | 12 | 12 | 12 | 12 | 12 | 12 |
| Glycerol | 10 | 10 | 10 | 10 | 10 | 10 |
| The hydrolysis extensin | 1 | 1 | 1 | 1 | 1 | 1 |
| Ethanol | 5 | 5 | 5 | 5 | 5 | 5 |
| Cetyl betaine | 7 | 7 | 7 | 7 | 7 | 7 |
| Cherry extract | 1 | 1 | 1 | 1 | 1 | 1 |
| Carnosic acid | 0.01 | / | / | / | / | / |
| AOB | 0.02 | 0.02 | 0.02 | 0.03 | / | / |
| Nisin | 0.01 | 0.01 | 0.02 | 0.01 | / | / |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.01 | 0.02 | 0.01 | 0.01 | / | / |
| Methyl parahydroxybenzoate | / | / | / | / | 0.05 | / |
Comparative Examples 1
According to corresponding Comparative Examples 1 data in table 1, take each raw material.Adopt the described method of embodiment 1 to prepare the exfoliated Fructus Pruni pseudocerasi extra firming facial mask of Comparative Examples 1.
Comparative Examples 2
According to corresponding Comparative Examples 2 data in table 1, take each raw material.Adopt the described method of embodiment 1 to prepare the exfoliated Fructus Pruni pseudocerasi extra firming facial mask of Comparative Examples 2.
Comparative Examples 3
According to corresponding Comparative Examples 3 data in table 1, take each raw material.Adopt the described method of embodiment 1 to prepare the exfoliated Fructus Pruni pseudocerasi extra firming facial mask of Comparative Examples 3.
Comparative Examples 4
According to corresponding Comparative Examples 4 data in table 1, take each raw material.Adopt the described method of embodiment 1 to prepare the exfoliated Fructus Pruni pseudocerasi extra firming facial mask of Comparative Examples 4.
Comparative Examples 5
According to Comparative Examples 5 data corresponding in table 1, take each component, adopt the described method of embodiment 1, namely obtain the exfoliated Fructus Pruni pseudocerasi extra firming facial mask of Comparative Examples 5.
Test case 1
The exfoliated Fructus Pruni pseudocerasi extra firming facial mask respectively embodiment 1 and Comparative Examples 1-5 made, carry out fill with the dark brown vial, opens wide bottle cap, is placed under 40 ℃ of ambient temperatures, relative humidity 85% environment, continues to observe and test, and concrete outcome sees the following form.Detect the microorganism level, concrete test item, detection method and examination criteria carry out according to QB/T2872-2007.
| ? | Observe phenomena |
| Embodiment 1 | No abnormality seen after 60 days, abnormal smells from the patient is pure |
| Comparative Examples 1 | After 50 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 2 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 3 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 4 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 5 | After 5 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
The antiseptic methyl parahydroxybenzoate used in Comparative Examples 4 is one of the most frequently used cosmetics preservative in this area.Belong to antiseptic phenols, generally effective to mycete, yeast, antibacterial, the effect that suppresses growth of microorganism is arranged, after adding, effectively extend the shelf-life (40 days shelf-lifves under test condition of the present invention) of cosmetics, but long-term this antiseptic of excessive use, the Diazolidinyl Urea epidermis cell, cause the epidermis transition aging.
By test data, can significantly be drawn, the embodiment of the present invention 1 is used carnosic acid, AOB, nisin and the composite Synergistic of iodine propilolic alcohol butyl mephenesin Carbamate, and antiseptic effect (60 days shelf-lifves under test condition of the present invention) obviously is better than Comparative Examples 1-3 and only adopts AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate three composite (in the shelf-life under test condition of the present invention below 50 days).
The facial film of the embodiment of the present invention 1 is placed in the accelerated test under 40 ℃ of ambient temperatures, relative humidity 85% environment at opening, can reach 60 days antiseptic effects, the long shelf-life of facial film, and conversion shady and cool dry its shelf-life of place under sealing state far surpasses 3 years.
Fructus Pruni pseudocerasi is rich in vitamin C, fruit acid and vitamin A.Vitamin C can moisten tender white muscle skin, effectively resists melanic formation, and vitamin C is important antioxidant in addition.Fruit acid: promote cuticular formation.Vitamin A: the balance sebum secretion, alleviate agingly, make skin younger.In addition, adhere to using the present invention, can make skin of face tender ruddy in vain, the clear speckle of wrinkle removing.
Test case 2
With CorneometerCM820 moisture of skin measuring instrument, at tested position, measure the skin surface moisture, tested position is respectively the forehead that sebaceous gland is abundant.Operating ambient temperature is 22-24 ℃, and relative humidity is 46%-55%, and the unit of skin moisture content is au (arbitraryunit).Female consumer forehead skin to a use embodiment of the present invention 1 is tested, and concrete data see the following form.
| ? | Before use, au | After use, au | Used au latter 1 hour |
| Embodiment 1 | 35.8 | 79.2 | 76.2 |
The above; it is only the specific embodiment of the present invention; but protection scope of the present invention is not limited to this; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; variation or the replacement that can expect without creative work, within all should being encompassed in protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (3)
1. exfoliated Fructus Pruni pseudocerasi extra firming facial mask, it is characterized in that, raw material by following weight parts is prepared from according to a conventional method: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part hydrolysis extensin, 4-6 part ethanol, 6-8 part cetyl betaine, 0.8-2 part cherry extract, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
2. exfoliated Fructus Pruni pseudocerasi extra firming facial mask as claimed in claim 1, it is characterized in that, described compound preservative consists of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
3. the preparation method of exfoliated Fructus Pruni pseudocerasi extra firming facial mask as claimed in claim 2, it is characterized in that, by following step, formed: polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, hydrolysis extensin, ethanol, cetyl betaine to stir, be cooled to 40 ℃, add cherry extract and compound preservative, stir.
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| CN104306201A (en) * | 2014-09-25 | 2015-01-28 | 广州莎蔓生物科技有限公司 | Mask fluid for tightening facial contour |
| CN106974843A (en) * | 2016-11-01 | 2017-07-25 | 田鹏新 | A kind of exfoliated apple ferment facial mask and preparation method thereof |
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| CN104207947A (en) * | 2014-08-18 | 2014-12-17 | 贵州捷欣合金技术开发有限公司 | Preparation method for film-forming liquid |
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| CN106974843A (en) * | 2016-11-01 | 2017-07-25 | 田鹏新 | A kind of exfoliated apple ferment facial mask and preparation method thereof |
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