CN111494290A - Moisturizing mask liquid and preparation method thereof - Google Patents

Moisturizing mask liquid and preparation method thereof Download PDF

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CN111494290A
CN111494290A CN202010343879.5A CN202010343879A CN111494290A CN 111494290 A CN111494290 A CN 111494290A CN 202010343879 A CN202010343879 A CN 202010343879A CN 111494290 A CN111494290 A CN 111494290A
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mask liquid
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王智民
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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    • AHUMAN NECESSITIES
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    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9771Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A61K8/982Reproductive organs; Embryos, Eggs
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A61K8/986Milk; Derivatives thereof, e.g. butter
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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Abstract

The invention provides a moisturizing facial mask liquid and a preparation method thereof, belonging to the technical field of skin care products, and the moisturizing facial mask liquid comprises the following components: 0.5-1 part of traditional Chinese medicine concentrated solution, 8-10 parts of apple extract, 1-3 parts of egg white, 0.1-0.3 part of honey and 1-3 parts of fresh milk; the traditional Chinese medicine concentrated solution is prepared from the following raw materials in parts by weight: 0.5-1 part of ginger and 0.3-0.5 part of ginkgo leaf extract; the apple extract is obtained by carrying out ultrasonic extraction on apple fermentation liquor. The facial mask liquid can improve the skin moisture degree, improve the dry and itching state of the skin, balance skin grease and promote facial blood circulation, thereby improving the skin health condition from inside to outside. The preparation method of the mask liquid is that in the high-speed mixing process, the raw materials can be fully crushed into fine particles, the effective components quickly reach the dissolution balance, and the use is safe and reliable.

Description

Moisturizing mask liquid and preparation method thereof
Technical Field
The invention relates to the technical field of skin care products, and particularly relates to a moisturizing mask liquid and a preparation method thereof.
Background
Due to the reasons of fast pace of life, irregular work and rest, higher pressure and the like, the skin surface of people is easy to produce oil, dry and itchy, redden and even pox, and the occurrence of the symptoms fully explains the phenomenon of water shortage of the skin in the metabolism process. The appearance of these symptoms not only accelerates the aging of the facial skin and the appearance of the stratum corneum, but also causes various losses to the body.
In order to improve the problem of water shortage of skin, people usually adopt a facial mask and drink to moisturize the body and the skin, but the existing moisturizing facial masks are added with various chemical components and additives with the functions of antisepsis and the like, so that the skin and even the body can still be damaged to different degrees in the facial mask applying process. Therefore, research on a moisturizing mask liquid with natural ingredients and without chemical additives becomes the first choice of people, and the mask application can be carried out by soaking the mask paper or the mask in the mask liquid.
Often also contain a large amount of moisturizing compositions in the facial mask that people used daily, like hyaluronic acid facial mask essence of moisturizing, realize three-dimensional moisturizing effect through the hyaluronic acid of different molecular weights, but hyaluronic acid's cost is higher relatively, and can appear on the contrary along with the live time extension anti-moisture suck back and the phenomenon that runs off, influence the effect of moisturizing. Meanwhile, some moisturizing components in the facial mask only have the effect of moisturizing for a short time, are easy to use and have a good moisturizing effect at present, but cannot lock water for a long time, so that the problem of skin water shortage cannot be well improved.
The nutritional ingredients contained in the apples are highly soluble and easy to be absorbed by human bodies, so the apple juice has the name of 'running water', has good moisturizing effect, can dissolve sulfur elements, and can lubricate and soften the skin. The apple also contains abundant microelements such as copper, magnesium, manganese, zinc, potassium, etc., and is helpful for improving symptoms such as skin dryness, dry itching, etc., and making skin fine and glossy. However, the apples are very easy to oxidize after being crushed and are not easy to store, and the moisturizing effect of the individual apple juice after being oxidized is also affected, and long-acting water locking and moisturizing cannot be achieved.
Disclosure of Invention
In order to solve the technical problems, the invention aims to provide the moisturizing mask liquid and the preparation method thereof.
In order to achieve the above object, the technical solution of the present invention is as follows.
The water-replenishing mask liquid is prepared from the following raw materials in parts by weight: 0.5-1 part of traditional Chinese medicine concentrated solution, 8-10 parts of apple extract, 1-3 parts of egg white, 0.1-0.3 part of honey and 1-3 parts of fresh milk;
the traditional Chinese medicine concentrated solution is prepared from the following raw materials in parts by weight: 0.5-1 part of ginger and 0.3-0.5 part of ginkgo leaf extract;
the apple extract is obtained by carrying out ultrasonic extraction on apple fermentation liquor.
Further, the traditional Chinese medicine concentrated solution is prepared by the following method:
a1, weighing ginger and ginkgo leaf extract according to a proportion, grinding the ginkgo leaf extract into fine powder with the particle size of 1-3 mu m, juicing the ginger, and mixing for later use;
a2, mixing the mixture of a1 and 20-30% of ethanol according to the mass ratio of 1: 5-10, uniformly mixing, and carrying out heat preservation leaching at 50-60 ℃ for 30-60 min to obtain a leaching solution;
a3, recovering ethanol from the leaching liquor of a2 under reduced pressure, standing for 6-10 hours at 10-15 ℃, filtering, and concentrating the filtrate to obtain the traditional Chinese medicine concentrated solution.
Further, the apple extract is prepared by the following method:
b1, crushing apples, putting the crushed apples into a fermentation container, adding sugar which is 8-10% of the weight of the raw materials and distilled water which is 10-20% of the weight of the raw materials, mixing and standing for 3-4 hours;
b2, adding yeast into the fermentation tank, fermenting for 5-7 days at 20-30 ℃, and filtering to obtain filtrate;
b3, inoculating lactic acid bacteria into the filtrate b2 for secondary fermentation for 3-4 days to obtain apple fermentation liquor;
b4, carrying out ultrasonic extraction on the apple fermentation liquor obtained in the b3 at 15-20 ℃, wherein the extraction time is 30min, and filtering and concentrating to obtain an apple extracting solution.
Furthermore, in step b3, before the second fermentation, in step b2, the inoculation amount of the yeast is 0.5% -1.0%; in the step b3, the inoculation amount of the lactobacillus is 0.3-0.8%.
Furthermore, in step b3, before the second fermentation, the temperature of the filtrate is adjusted to 15-20 ℃.
Further, in step b3, before the second fermentation, the pH of the filtrate is adjusted to 4-6.
A preparation method of moisturizing facial mask liquid comprises the following steps:
s1, weighing 0.5-1 part of traditional Chinese medicine concentrated solution, 8-10 parts of apple extract, 1-3 parts of egg white, 0.1-0.3 part of honey and 1-3 parts of fresh milk according to the formula ratio, and mixing for later use;
s2, mixing the mixture of S1 at 2 × 104~3×104Mixing at r/min stirring speed, and sterilizing to obtain moisturizing facial mask liquid.
Further, in step S2, the temperature of stirring and mixing is 8-15 ℃.
The invention provides moisturizing mask liquid and a preparation method thereof, and the moisturizing mask liquid has the following beneficial effects:
1. the main raw materials of the moisturizing mask liquid are ginger, ginkgo leaf extract, apple, egg white, honey and fresh milk, which are respectively and briefly described as follows:
the ginger contains gingerol which is a general name of various spicy components, has a certain stimulation effect on cardiovascular systems, can promote blood to reach skin by promoting blood circulation and accelerating blood flow, is helpful for perspiration, promotes the discharge of vivotoxin, has strong oxidation resistance, and is used for removing free radicals in the body, promoting metabolism and discharging toxin.
The folium Ginkgo extract can relieve anxiety symptoms caused by mental stress, and has strong antioxidant and free radical scavenging effects. Meanwhile, the blood circulation can be accelerated, so that capillaries can be expanded and dilated, the absorption of water replenishing components is promoted, the improvement of the blood circulation is beneficial to a nervous system, and the skin aging can be delayed.
The apple extract has the effects of nourishing heart, tonifying qi, promoting production of body fluid and relieving restlessness, and can be used for improving symptoms of dry skin, itching and the like from inside to outside and ensuring that the skin is fine, moist and glossy. The effective components of the fermented product are better separated by ultrasonic extraction after fermentation.
The egg white is rich in protein, vitamins and various trace elements, can effectively reduce the grease secretion of facial skin, has very good astringency effect, is beneficial to astringing pores, and has the effect of enhancing moisture retention; also has very good nursing effect on the acne problem of the skin. The protein and monosaccharide in the egg white also have the effects of removing wrinkles and wrinkles.
The fresh milk is rich in milk fat, vitamins and mineral substances, particularly contains more vitamin B, can moisten skin, protect epidermis and has the effects of preventing cracking and wrinkling. Fresh milk also provides occlusive oil to the skin, forming a film to prevent evaporation of skin moisture.
The honey has strong antioxidation and skin nourishing and moistening effects, and can make skin soft, smooth, tender and keep healthy. Since honey has high hygroscopicity, it can absorb skin secretion and has antibacterial effect, so it can be used as skin bactericide.
The moisturizing mask liquid provided by the invention is mainly used for discharging toxins by utilizing the effect of accelerating blood circulation of the ginger and ginkgo leaf extract concentrated solution; the moisture absorption of the honey is utilized to clean skin secretion, and the function of bacteriostasis is achieved; the strong water replenishing effect of the apple extract is utilized to moisten the skin; the astringency effect of egg white is utilized to astringe pores and strengthen the moisturizing effect; the film is formed by the closed grease of the fresh milk to lock the moisture of the skin.
According to the concept of 'toxin expelling, cleaning, water replenishing, astringing and water locking', the long-acting water replenishing and moisturizing effect of the skin is improved through reasonable matching of different raw materials. Not only can improve the moisture degree of the skin, improve the dry and itching state of the skin, but also can balance the skin grease and promote the facial blood circulation, thereby improving the health condition of the skin from inside to outside.
The preparation method of the moisturizing mask liquid disclosed by the invention has the advantages that in the high-speed mixing process, the raw materials can be fully crushed into fine particles, the absorption of the skin epidermis is facilitated, the effective components are quickly dissolved and balanced, the mixing time is short, and the efficiency is high. Can keep the good state of the facial mask liquid at low temperature, and is safe and reliable to use.
Drawings
FIG. 1 is a graph of the stability of the hydrating mask fluid of example 1 of the present invention with respect to temperature versus time.
FIG. 2 is a bar graph showing the stability at 25 ℃ of example 1 of the present invention and comparative examples 1 to 5.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The water-replenishing mask liquid is prepared from the following raw materials in parts by weight: 0.5 part of traditional Chinese medicine concentrated solution, 8 parts of apple extract, 1 part of egg white, 0.1 part of honey and 1 part of fresh milk;
the traditional Chinese medicine concentrated solution is prepared from the following raw materials in parts by weight: ginger 0.5 parts and ginkgo leaf extract 0.3 parts;
the apple extract is obtained by ultrasonic extraction of apple fermentation liquor.
Preparation of raw materials:
1) preparing a traditional Chinese medicine concentrated solution:
a1, weighing rhizoma Zingiberis recens and folium Ginkgo extract, grinding folium Ginkgo extract into 1 μm fine powder, juicing rhizoma Zingiberis recens, and mixing;
a2, mixing the mixture with 30% ethanol in a mass ratio of 1: 5, mixing uniformly, and carrying out heat preservation and extraction at 50 ℃ for 30 min; obtaining a leaching solution;
a3, recovering ethanol from the leaching liquor of a2 under reduced pressure, standing for 6 hours at 10 ℃, filtering, and concentrating the filtrate to obtain the traditional Chinese medicine concentrated solution.
2) Preparing an apple extracting solution:
b1, crushing the apples, putting the crushed apples into a fermentation container, adding sugar accounting for 8 percent of the weight of the apples and distilled water accounting for 10 percent of the weight of the apples, mixing and standing for 3 hours;
b2, adding yeast into the fermentation tank, wherein the inoculation amount of the yeast is 0.5%, fermenting for 5 days at 20 ℃, and filtering to obtain filtrate;
b3, adjusting the temperature of the filtrate to 15 ℃, adjusting the pH of the filtrate to 4, inoculating lactobacillus into the filtrate b2, wherein the inoculation amount of the lactobacillus is 0.3%, and performing secondary fermentation for 3 days to obtain apple fermentation liquor;
b4, performing ultrasonic extraction on the apple fermentation liquor obtained in the b3 at 15 ℃ for 30min, filtering and concentrating to obtain an apple extracting solution.
The preparation method of the moisturizing facial mask liquid comprises the following steps:
s1, weighing 0.5 part of traditional Chinese medicine concentrated solution, 8 parts of apple extract, 1 part of egg white, 0.1 part of honey and 1 part of fresh milk according to the formula ratio, and mixing for later use;
s2, mixing the mixture of S1 at 2 × 104Mixing at a stirring speed of rpm, and sterilizing to obtain moisturizing mask liquid, wherein the stirring and mixing temperature is 8 ℃.
Example 2
The water-replenishing mask liquid is prepared from the following raw materials in parts by weight: 1 part of traditional Chinese medicine concentrated solution, 10 parts of apple extract, 3 parts of egg white, 0.3 part of honey and 3 parts of fresh milk;
the traditional Chinese medicine concentrated solution is prepared from the following raw materials in parts by weight: 1 part of ginger and 0.5 part of ginkgo leaf extract;
the apple extract is obtained by ultrasonic extraction of apple fermentation liquor.
Preparation of raw materials:
1) preparing a traditional Chinese medicine concentrated solution:
a1, weighing rhizoma Zingiberis recens and folium Ginkgo extract, grinding folium Ginkgo extract into 3 μm fine powder, juicing rhizoma Zingiberis recens, and mixing;
a2, mixing the mixture with 20% ethanol in a mass ratio of 1: 10 mixing uniformly, and carrying out heat preservation and extraction at 60 ℃ for 60 min; obtaining a leaching solution;
a3, recovering ethanol from the leaching liquor of a2 under reduced pressure, standing for 10 hours at 15 ℃, filtering, and concentrating the filtrate to obtain the traditional Chinese medicine concentrated solution.
2) Preparing an apple extracting solution:
b1, crushing the apples, putting the crushed apples into a fermentation container, adding sugar which accounts for 10 percent of the weight of the apples and distilled water which accounts for 20 percent of the weight of the apples, mixing, and standing for 4 hours;
b2, adding yeast into the fermentation tank, wherein the inoculation amount of the yeast is 1.0%, fermenting for 7 days at 28 ℃, and filtering to obtain filtrate;
b3, adjusting the temperature of the filtrate to 20 ℃, adjusting the pH of the filtrate to 6, inoculating lactobacillus into the filtrate b2, wherein the inoculation amount of the lactobacillus is 0.8%, and performing secondary fermentation for 4 days to obtain an apple fermentation liquid;
b4, performing ultrasonic extraction on the apple fermentation liquor obtained in the b3 at the temperature of 20 ℃ for 30min, filtering and concentrating to obtain an apple extracting solution.
The preparation method of the moisturizing facial mask liquid comprises the following steps:
s1, weighing 1 part of traditional Chinese medicine concentrated solution, 10 parts of apple extract, 3 parts of egg white, 0.3 part of honey and 3 parts of fresh milk according to the formula ratio, and mixing for later use;
s2, mixing the mixture of S1 at 3 × 104Mixing at a stirring speed of rpm, and sterilizing to obtain moisturizing mask liquid, wherein the stirring and mixing temperature is 15 ℃.
Example 3
The water-replenishing mask liquid is prepared from the following raw materials in parts by weight: 0.8 part of traditional Chinese medicine concentrated solution, 9 parts of apple extract, 2 parts of egg white, 0.2 part of honey and 2 parts of fresh milk;
the traditional Chinese medicine concentrated solution is prepared from the following raw materials in parts by weight: ginger 0.8 parts and ginkgo leaf extract 0.4 parts;
the apple extract is obtained by ultrasonic extraction of apple fermentation liquor.
Preparation of raw materials:
1) preparing a traditional Chinese medicine concentrated solution:
a1, weighing rhizoma Zingiberis recens and folium Ginkgo extract, grinding folium Ginkgo extract into 2 μm fine powder, juicing rhizoma Zingiberis recens, and mixing;
a2, mixing the mixture with 25% ethanol in a mass ratio of 1: 8, uniformly mixing, and carrying out heat preservation and extraction for 50min at 55 ℃; obtaining a leaching solution;
a3, recovering ethanol from the leaching liquor of a2 under reduced pressure, standing for 8 hours at 12 ℃, filtering, and concentrating the filtrate to obtain the traditional Chinese medicine concentrated solution.
2) Preparing an apple extracting solution:
b1, crushing the apples, putting the crushed apples into a fermentation container, adding sugar which is 9 percent of the weight of the apples and distilled water which is 15 percent of the weight of the apples, mixing, and standing for 4 hours;
b2, adding yeast into the fermentation tank, wherein the inoculation amount of the yeast is 0.8%, fermenting for 6 days at 28 ℃, and filtering to obtain filtrate;
b3, adjusting the temperature of the filtrate to 18 ℃, adjusting the pH of the filtrate to 5, inoculating lactobacillus into the filtrate b2, wherein the inoculation amount of the lactobacillus is 0.5%, and performing secondary fermentation for 4 days to obtain an apple fermentation liquid;
b4, performing ultrasonic extraction on the apple fermentation liquor obtained in the b3 at 18 ℃ for 30min, filtering and concentrating to obtain an apple extracting solution.
The preparation method of the moisturizing facial mask liquid comprises the following steps:
s1, weighing 0.8 part of traditional Chinese medicine concentrated solution, 9 parts of apple extract, 2 parts of egg white, 0.2 part of honey and 2 parts of fresh milk according to the formula ratio, and mixing for later use;
s2, mixing the mixture of S1 at 2.8 × 104Mixing at a stirring speed of rpm, and sterilizing to obtain moisturizing mask liquid, wherein the stirring and mixing temperature is 10 ℃.
Comparative example 1
The raw material composition and the preparation method thereof are the same as those of the embodiment 1, and the differences are that: the moisturizing mask liquid does not comprise 1 part of fresh milk.
Comparative example 2
The raw material composition and the preparation method thereof are the same as those of the embodiment 1, and the differences are that: the moisturizing mask liquid does not comprise 0.1 part of honey and 1 part of fresh milk.
Comparative example 3
The raw material composition and the preparation method thereof are the same as those of the embodiment 1, and the differences are that: the moisturizing mask liquid does not comprise 1 part of traditional Chinese medicine concentrated solution.
Comparative example 4
The raw material composition and the preparation method thereof are the same as those of the embodiment 1, and the differences are that: the apple extracting solution in the moisturizing mask liquid is prepared by the following method:
and c1, crushing the apples, adding 20% ethanol solution which is 5 times of the weight of the raw materials, leaching for 1 hour at room temperature, then extracting for 30min under reflux, and filtering to obtain filtrate to obtain apple extract.
Comparative example 5
The raw material composition and the preparation method thereof are the same as those of the embodiment 1, and the differences are that: in the preparation method of the moisturizing mask liquid, the mixing speed of the raw materials is less than 200 r/min.
The moisturizing facial mask solutions prepared in examples 1-3 have substantially the same effect, and therefore performance tests are performed only by using the moisturizing facial mask solution of example 1 as a test sample.
1. Skin irritation test
In the mouse test, 5 healthy mice with the weight of 16 +/-2 g are respectively cut off hairs with the area of about 3cm × 3cm on two sides of the spinal column of the back of the 5 mice for later use.
Uniformly coating the facial mask solution of the example 1 on the unhairing positions on the left sides of the back spines of 5 mice; meanwhile, clear water is uniformly coated on the unhaired part of the right side of the back spine to serve as a control. The unhaired parts of 5 mice were wound and fixed with gauze, and released to allow the mice to move freely. After 12h, gauze was removed, the unhaired area on both sides was washed with water and the water was blotted off, and the skin condition of the unhaired area of the mouse was observed after 15 min.
The observation results show that the unhairing parts of 5 mice have no phenomena such as red swelling, blisters, erythema and the like, thereby indicating that the moisturizing facial mask liquid prepared in example 1 has no irritation to the skin of the mice.
Human skin testing: based on the above mouse test results, 26 volunteers were collected, of which 21 female volunteers and 5 male volunteers were collected. The arm skin of the volunteer has no scar, no acne mark, and is smooth and healthy. The moisturizing facial mask solution prepared in example 1 was uniformly applied to the arms of the volunteers, and the skin condition of the arms was observed.
The observation results show that the arm skins of 26 volunteers do not have symptoms such as erythema, edema, blisters, pruritus and pain, and therefore the moisturizing mask prepared in the embodiment 1 is high in safety and mild and non-irritant in product.
2. Stability test
2.1 stability test at different temperatures
Taking 6 parts of moisturizing facial mask liquid of example 1 of the invention, wherein each part is 80g, placing the moisturizing facial mask liquid in a thermostat with the temperature of 0 ℃, 5 ℃, 10 ℃, 15 ℃, 20 ℃ and 30 ℃ respectively, standing for 30 days at constant temperature, taking out 2g of samples each day, standing for 30min at room temperature, and observing the stability of the samples respectively. The results are shown in Table 1.
Table 1 stability test results for moisturizing mask solutions of example 1
Figure BDA0002469436440000101
Note: the mask fluid remained stable without color change, precipitation, and odor change, otherwise unstable.
According to the results in the table 1, the moisturizing mask liquid in the embodiment 1 can be stored at 5-15 ℃ and can be kept stable for 30 days; can be stored at 0 ℃ for 25 days and then can precipitate; storage at 20 ℃ is stable for 25 days, after which precipitation occurs with a slight odour; storage at 30 ℃ remains stable for 15 days, after which precipitation occurs with a slight odour. Therefore, the optimal storage temperature of the moisturizing mask liquid in the embodiment 1 of the invention is 5-15 ℃.
2.2 stability test at different storage times
80g of moisturizing mask liquid obtained in the embodiment 1 and the comparative examples 1-5 are respectively placed in a constant temperature box at 25 ℃, kept at constant temperature for 30 days, 2g of samples are taken out every day, kept at room temperature for 30min, and the stability of the moisturizing mask liquid is respectively observed. The results are shown in Table 2.
TABLE 2 stability test results of moisturizing facial mask solutions of example 1 and comparative examples 1-5 at 25 deg.C
Figure BDA0002469436440000111
Note: the mask fluid remained stable without color change, precipitation, and odor change, otherwise unstable.
As can be seen from the results in Table 2, the moisturizing facial mask solutions of example 1 and comparative examples 1-3 of the present invention were stable for 20 days when stored at 25 ℃, and then precipitated with a slight odor; the moisturizing mask solutions of comparative examples 4-5 were stable for 10 days when stored at 25 ℃.
The main reason is that the apple extract of comparative example 4 is prepared by the method of ethanol extraction and reflux extraction, although effective components can be extracted, the effective components are easy to be oxidized and difficult to be stored, and the moisturizing effect of the facial mask liquid is influenced; the preparation process of comparative example 5 adopts low-speed stirring, cannot achieve the dissolution balance of the effective components, and has low stability; this is different from the methods of example 1 and comparative examples 1 to 3.
The apple extract solutions of example 1 and comparative examples 1 to 3 were prepared by the method of "yeast + lactic acid bacteria fermentation + ultrasonic extraction". The method of yeast and lactobacillus fermentation can enhance the biological stability of the apple extract, although alcohol and acidic components are generated in the process of primary fermentation, and the nutritional components in the apple are dissolved in the primary fermentation liquid, the secondary fermentation not only can play a role in biological stability, but also can play a role in reducing acidity, and is beneficial to maintaining the acidity of the apple extract in the application range of the skin. And then the active ingredients are better separated by ultrasonic extraction, a certain sterilization effect is achieved, diseases caused by zymophyte are avoided, and the stability and the safety of the product are further influenced.
3. Water replenishment effect detection
Test subjects: collecting 70 volunteers, wherein 74 female volunteers and 6 male volunteers; on average, the groups were divided into 7 groups of 10.
Test samples: the moisturizing mask solutions of example 1 were used as experimental groups, the moisturizing mask solutions of comparative examples 1-5 were used as control groups, and deionized water was used as blank groups.
The test method comprises the following steps: the face of each volunteer was washed clean with water, the water content of the forehead, cheeks on both sides, and chin of the volunteer was measured with a skin moisture meter, and the average value was calculated.
Uniformly smearing corresponding test samples on the face of the volunteer, patting to help absorption, testing the water content of the forehead, cheeks and chin parts of two sides of the volunteer by using a skin water tester after 10min, and calculating an average value; after 12h the skin moisture tester was used again. The test results are shown in table 3.
Table 3 skin moisture test results
Figure BDA0002469436440000121
Figure BDA0002469436440000131
According to the results in the table 3, the moisturizing mask liquid in the example 1 has good moisturizing effect, and after the moisturizing mask liquid is used for 12 hours, the moisture content of the skin is remarkably improved, the moisture can be locked, the moisture loss is avoided, and the skin can be kept moist for a long time.
Comparing the variation of comparative example 1 with that of example 1, it can be seen that the moisturizing facial mask fluid of comparative example 1 can achieve moisturizing effect only in a short period, and the moisture loss is serious with the time, and the moisture of the skin cannot be locked. This is because the facial mask liquid of comparative example 1 lacks fresh milk having a water-locking function, and is difficult to lock skin water.
Comparing the variation value of comparative example 2 with that of example 1, it can be seen that the moisturizing effect of the moisturizing facial mask liquid of comparative example 2 in a short period is inferior to that of comparative example 1, and the water loss after 12 hours is severe, because the honey with cleaning effect and the fresh milk for locking the skin water function are lacked in comparative example 2, so that the skin can not absorb water well due to the partial blockage of pores caused by the discharged toxin.
Comparing the variation of comparative example 3 with example 1, it can be seen that the short-term moisturizing effect of comparative example 3 is not good, because the facial mask solution of comparative example 3 lacks traditional Chinese medicine components contributing to detoxification, toxins accumulated in pores cannot be discharged, and pores cannot relax, so that it is difficult to effectively absorb water.
Comparing the variation of comparative example 4 with example 1, it was found that the short-term water replenishing effect of comparative example 4 was much worse, because the apple extract was oxidized after crushing, causing partial destruction of the nutrients, and thus the water replenishing effect was significantly worse than that of example 1.
Comparing the variation of comparative example 5 with example 1, it can be seen that the short-term moisturizing effect of the facial mask liquid of comparative example 5 is relatively poor, because the dissolution balance of each active ingredient cannot be achieved due to the low-speed stirring, the stability is not high, flocculation and sedimentation are easily generated, the loss of the active ingredients is caused, and the moisturizing effect is affected.
Based on the detection results, the moisturizing mask liquid prepared in the embodiments 1-3 of the invention discharges toxins by utilizing the effect of accelerating blood circulation of the extracted concentrated solution of ginger and ginkgo leaves according to the concept of 'toxin expelling, cleaning, moisturizing, astringing and water locking'; the moisture absorption of the honey is utilized to clean skin secretion, and the function of bacteriostasis is achieved; the strong water replenishing effect of the apple extract is utilized to moisten the skin; the astringency effect of egg white is utilized to astringe pores and strengthen the moisturizing effect; the film is formed by the closed grease of the fresh milk to lock the moisture of the skin. The long-acting moisturizing effect of the skin is improved by reasonable matching of different raw materials. Not only can improve the moisture degree of the skin, improve the dry and itching state of the skin, but also can balance the skin grease and promote the facial blood circulation, thereby improving the health condition of the skin from inside to outside.
The present invention is not limited to the above preferred embodiments, and any modifications, equivalent substitutions and improvements made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (8)

1. The moisturizing mask liquid is characterized by being prepared from the following raw materials in parts by weight: 0.5-1 part of traditional Chinese medicine concentrated solution, 8-10 parts of apple extract, 1-3 parts of egg white, 0.1-0.3 part of honey and 1-3 parts of fresh milk;
the traditional Chinese medicine concentrated solution is prepared from the following raw materials in parts by weight: 0.5-1 part of ginger and 0.3-0.5 part of ginkgo leaf extract;
the apple extract is obtained by carrying out ultrasonic extraction on apple fermentation liquor.
2. The moisturizing mask liquid according to claim 1, wherein the traditional Chinese medicine concentrated solution is prepared by the following method:
a1, weighing ginger and ginkgo leaf extract according to a proportion, grinding the ginkgo leaf extract into fine powder with the particle size of 1-3 mu m, juicing the ginger, and mixing for later use;
a2, mixing the mixture of a1 and 20-30% of ethanol according to the mass ratio of 1: 5-10, uniformly mixing, and carrying out heat preservation leaching at 50-60 ℃ for 30-60 min to obtain a leaching solution;
a3, recovering ethanol from the leaching liquor of a2 under reduced pressure, standing for 6-10 hours at 10-15 ℃, filtering, and concentrating the filtrate to obtain the traditional Chinese medicine concentrated solution.
3. The moisturizing mask liquid according to claim 1, wherein the apple extract is prepared by the following method:
b1, crushing apples, putting the crushed apples into a fermentation container, adding sugar which is 8-10% of the weight of the raw materials and distilled water which is 10-20% of the weight of the raw materials, mixing and standing for 3-4 hours;
b2, adding yeast into the fermentation tank, fermenting for 5-7 days at 20-30 ℃, and filtering to obtain filtrate;
b3, inoculating lactic acid bacteria into the filtrate b2 for secondary fermentation for 3-4 days to obtain apple fermentation liquor;
b4, carrying out ultrasonic extraction on the apple fermentation liquor obtained in the b3 at 15-20 ℃, wherein the extraction time is 30min, and filtering and concentrating to obtain an apple extracting solution.
4. The moisturizing mask liquid according to claim 3, wherein in step b3, before the second fermentation, in step b2, the inoculation amount of yeast is 0.5% to 1.0%; in the step b3, the inoculation amount of the lactobacillus is 0.3-0.8%.
5. The moisturizing mask liquid according to claim 3, wherein in the step b3, before the second fermentation, the temperature of the filtrate is adjusted to 15-20 ℃.
6. The moisturizing mask liquid according to claim 3, wherein in the step b3, before the second fermentation, the pH of the filtrate is adjusted to 4-6.
7. The preparation method of the moisturizing mask liquid is characterized by comprising the following steps:
s1, weighing 0.5-1 part of traditional Chinese medicine concentrated solution, 8-10 parts of apple extract, 1-3 parts of egg white, 0.1-0.3 part of honey and 1-3 parts of fresh milk according to the formula ratio, and mixing for later use;
s2, mixing the mixture of S1 at 2 × 104~3×104Mixing at r/min stirring speed, and sterilizing to obtain moisturizing facial mask liquid.
8. The method for preparing the moisturizing mask solution according to claim 7, wherein in the step S2, the stirring and mixing temperature is 8-15 ℃.
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Application publication date: 20200807