CN103356469A - Peel-off type pomegranate facial mask and preparation method thereof - Google Patents
Peel-off type pomegranate facial mask and preparation method thereof Download PDFInfo
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- CN103356469A CN103356469A CN2013101971535A CN201310197153A CN103356469A CN 103356469 A CN103356469 A CN 103356469A CN 2013101971535 A CN2013101971535 A CN 2013101971535A CN 201310197153 A CN201310197153 A CN 201310197153A CN 103356469 A CN103356469 A CN 103356469A
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- punica granatum
- facial film
- red punica
- exfoliated
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- QRYRORQUOLYVBU-VBKZILBWSA-N carnosic acid Chemical compound CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 claims abstract description 22
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Abstract
The invention discloses a peel-off type pomegranate facial mask and a preparation method thereof. The peel-off type pomegranate facial mask is prepared from the following raw materials in parts by weight according to a conventional method: 10-14 parts of polyvinyl alcohol, 8-12 parts of glycerin, 0.8-1.2 parts of coco-morpholine oxide, 4-6 parts of ethanol, 6-8 parts of DEA-laureth sulfate, 0.8-2 parts of pomegranate extracting solution, 0.03-0.08 part of compound preservative and 100 parts of deionized water, wherein the compound preservative comprises the following components in parts by weight: 1-3 parts of carnosic acid, 3-5 parts of antioxidant of bamboo leaves, 1-3 parts of nisin and 1-3 parts of iodopropynyl butylcarbamate. The peel-off type pomegranate facial mask disclosed by the invention has the functions of whitening, diminishing inflammation, shrinking pores and making skins delicate and smooth.
Description
Technical field
The present invention relates to facial film and preparation method thereof, be specifically related to a kind of exfoliated red Punica granatum L. facial film and preparation method thereof.
Background technology
Facial film is the important content in the skin nursing, for the regular application facial film of all kinds of skin characteristics, can make the oily skin defat, and thick pore obtains convergence, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.After using, facial film makes skin salubrious, the smooth and pure white delicacy that seems, this is because when facial film is coated on skin, facial film and skin produce affinity, gradually drying along with facial film, the skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, and the sebum of skin secretion and moisture reverse osmosis unfold the epidermis softness in horny layer, the pore instinct is opened, effective ingredient in the facial film infiltrates skin and is absorbed, and facial film tightly links to each other with skin simultaneously, when removing facial film, the deep layer dirt makes skin pure and fresh clean also by the while leukorrhagia in aging cutin on the skin, the pore.
The principle of facial film, utilize exactly the blink that covers face, extraneous air and the pollution of temporary transient isolation improves the skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, the oxygen content of skin is risen, be conducive to the oil substances that skin is got rid of the metabolic product of epidermis cell and accumulation, the moisture in the facial film infiltrates the horny layer of skin epidermis, it is soft that skin becomes, and skin naturally light is flexible.
Along with the raising of people's quality of the life and people to the pursuit of the beauty, the cosmetics kind is more and more various.At present, face mask of traditional Chinese medicine is one of beauty treatment educational circles effective whitening scheme, and especially some Chinese medicine extraction liquid have the preferably effect of toxin expelling, speckle dispelling, reparation, skin care, also by being applied in the facial film gradually.
But because facial film is liquid condition, Chinese medicine extraction liquid is easy to grow mycete, and a lot of face mask of traditional Chinese medicine antiseptic effects in the market are not good, and the shelf-life is short.All can add antiseptic in therefore a lot of face mask of traditional Chinese medicines.Yet a lot of antiseptic also can produce zest to skin, even cause erythema and erythra in the microorganisms such as kill bacteria, fungus, and the Long Term Contact antiseptic can increase organism material sensitization, cause the danger of anaphylactic reaction.
Iodine propilolic alcohol butyl mephenesin Carbamate (being called for short IPBC) is a kind of novel cosmetic antiseptic, has good fungistatic effect, and preferably dissolubility arranged in surfactant, emulsifying agent, polar solvent, therefore be widely used in resident class and the drip washing class cosmetic formulations, other antiseptic such as normal and diazolidinyl urea, hydantoin are used.Regulation IPBC limits the use of antiseptic in the components of cosmetics in China's cosmetics health standard and the European Union's regulatory affairs, and maximum permission working concentration is 0.05% in cosmetics, and can not be used for oral hygiene and lip product.But in facial film, addition is antiseptic effect and not obvious less than 0.05% the time.Therefore, there is little and antiseptic effect is poor, the shelf-life the is short problem of consumption in the antiseptic that uses in the present facial film.Iodine propilolic alcohol butyl mephenesin Carbamate or other antiseptic large usage quantities in the part facial film are also arranged, can be produced pessimal stimulation by skin, with after need to clean facial, use to bother.
Red Punica granatum L. is the kind of Punica granatum L., because peel after the maturation is gained the name for pink.Red Punica granatum L. has: the red Punica granatum L. in Yimeng, beautifully purchase red Punica granatum L..The former be because of the main product of red Punica granatum L. gain the name, the latter uses because of the process technology of red Punica granatum L. and raw material to gain the name.Red Punica granatum L. nature and flavor are sweet, sour and astringent, warm, contain the materials such as abundant vitamin C, Punica granatum L. polyphenol and anthocyanidin in the fruit, and good toxin expelling, anti-oxidation efficacy are arranged.All playing an important role aspect medicinal, beauty treatment, the dietetic therapy.Modern medicine finds that contain a large amount of Punica granatum L. polyphenol and anthocyanidin in the red Punica granatum L., non-oxidizability exceeds 3 times of green tea, and ascorbic 20 times especially, energy efficient neutralization free radical enhances metabolism, discharges toxin.
Summary of the invention
For above shortcomings in the prior art, one of technical problem to be solved by this invention provides a kind of exfoliated red Punica granatum L. facial film.
Two of technical problem to be solved by this invention provides the preparation method of above-mentioned exfoliated red Punica granatum L. facial film.
The present invention seeks to be achieved through the following technical solutions:
A kind of exfoliated red Punica granatum L. facial film is prepared from according to a conventional method by the raw material of following weight parts:
10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part cocoyl morpholine oxide, 4-6 part ethanol, 6-8 part laureth sulfuric ester DEA salt, the red Punica granatum L. extracting solution of 0.8-2 part, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
Wherein, described compound preservative is made of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
With carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Described exfoliated red Punica granatum L. facial film can adopt industry conventional method to be prepared from.
Further, the present invention also provides a kind of preparation method of exfoliated red Punica granatum L. facial film, is comprised of following step:
Polyvinyl alcohol is added in the deionized water, be heated to 70-90 ℃, dissolving, be cooled to 45-55 ℃, add glycerol, cocoyl morpholine oxide, ethanol, the stirring of laureth sulfuric ester DEA salt, be cooled to 40 ℃, add red Punica granatum L. extracting solution and compound preservative, stir, can make described exfoliated red Punica granatum L. facial film.
Concrete, in the present invention:
Described polyvinyl alcohol can be selected the cosmetics-stage polyvinyl alcohol, and specifically can select such as the trade mark is the polyvinyl alcohol of PVA1788, PVA1799 or PVA2488.
Glycerol has another name called: propylene glycol, English name: Glycerin, molecular formula C
3H
8O
3
The cocoyl morpholine oxide, CAS accession number: 68784-65-6.
Laureth sulfuric ester DEA salt, CAS accession number: 58855-36-0.
Red Punica granatum L. extracting solution of the present invention can pass through commercially available getting.Also can adopt the preparation of following method and get: after red Punica granatum L. is pulverized, add the deionized water of 6-10 times of weight, soaked 1-3 hour, ultrasonic extraction, 10-15 minute, filtration, centrifugal, discard and precipitate supernatant concentration, make red Punica granatum L. extracting solution.Preferably, after concentrating, controlling red Punica granatum L. extracting solution density is 1.02-1.10g/cm
3
Carnosic acid, molecular formula: C
20H
28O
4, CAS number: 3650--09-7, source: Labiatae Rosmarinus plant rosemary Rosmarinus officinalis L.
AOB, CNS number: 04.019, English name: antioxidant of bamboo leaves.That AOB extracts from the tender leaf of Phyllostachys (phyllostachys) bamboo, natural, the nutrition take flavone and phenolic compound as effective ingredient, multi-functional food antioxidant.
Nisin also claims nisin, English name: Nisin, and by the synthetic a kind of polypeptide that is formed by 34 aminoacid of streptococcus acidi lactici metabolism, molecular formula C
143H
228O
37N
42S
7Molecular weight is 3348, and nisin is made of water-wet side and hydrophobic side, is typical surfactant, be efficient, nontoxic biological antiseptic, be widely used in the anticorrosion of milk and milk products, fermented beverage, filling food, vegetable protein food, meat and its products at present.
Iodine propilolic alcohol butyl mephenesin Carbamate, English name: 3-Iodo-2-propynyl butylcarbamate, be abbreviated as IPBC, CAS number: 55406-53-6, molecular formula: C
8H
12INO
2, molecular weight is 281.10.
The present invention uses carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate composite as antiseptic, and antiseptic effect is significantly improved, the long shelf-life of facial film.And, use Compositional antiseptic agent, greatly reduce the consumption of iodine propilolic alcohol butyl mephenesin Carbamate, the consumption of iodine propilolic alcohol butyl mephenesin Carbamate is controlled at below 0.03%, meet the IPBC that stipulates in China's cosmetics health standard and the European Union's regulatory affairs and limit the use of antiseptic in the components of cosmetics, maximum permission working concentration is 0.05% in cosmetics.Carnosic acid, AOB, nisin are the nontoxic biological antiseptic, be widely used in food service industry, among the present invention it is diverted to cosmetic mask, can't brings ill effect to human body or skin, and can not produce harmful effect to the stability of facial film.
The using method of exfoliated red Punica granatum L. facial film of the present invention is: before using facial film, deeply cleaning is facial first, again facial film is coated on face, after 15-25 minute, the facial film active substance is absorbed by the skin, the moisture evaporation, form gradually thin film at face, this thin film is peeled off from face, and the dirt on the skin of face, scurf also stick on the thin film in company with and are eliminated, and it is clean, smooth that face seems.
Exfoliated red Punica granatum L. facial film of the present invention can the deep layer cleaning skin of face, desalinates facial microgroove, makes skin elasticity compact, and the water profit is plentiful.Continue to use, skin water profit is flexible, reproduces youthful vigor.
Exfoliated red Punica granatum L. facial film of the present invention has whitening, and the antiinflammatory pore refining makes skin careful smooth.
Exfoliated red Punica granatum L. facial film of the present invention adopts carnosic acid, AOB, nisin, the composite antiseptic of iodine propilolic alcohol butyl mephenesin Carbamate, and shelf life of products is long, and can not produce harmful effect to skin.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1
Take by weighing each raw material according to corresponding embodiment 1 data in the table 1, with carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Polyvinyl alcohol is added in the deionized water, be heated to 70-90 ℃, dissolving, be cooled to 45-55 ℃, add glycerol, cocoyl morpholine oxide, ethanol, the stirring of laureth sulfuric ester DEA salt, be cooled to 40 ℃, add red Punica granatum L. extracting solution and compound preservative, stir, can make described exfoliated red Punica granatum L. facial film.
Wherein, red Punica granatum L. extracting solution among embodiment 1 and the Comparative Examples 1-5 adopts following method to be prepared from: after red Punica granatum L. is pulverized, the deionized water that adds 8 times of weight soaked ultrasonic extraction 2 hours, 12 minutes, filter, centrifugal, discard precipitation with supernatant concentration, after concentrated, making density is 1.06g/cm
3Red Punica granatum L. extracting solution.
Table 1: face pack prescription list position: kilogram
| ? | Embodiment 1 | Comparative Examples 1 | Comparative Examples 2 | Comparative Examples 3 | Comparative Examples 4 | Comparative Examples 5 |
| Deionized water | 100 | 100 | 100 | 100 | 100 | 100 |
| PVA-124 88 | 12 | 12 | 12 | 12 | 12 | 12 |
| Glycerol | 10 | 10 | 10 | 10 | 10 | 10 |
| The cocoyl morpholine oxide | 1 | 1 | 1 | 1 | 1 | 1 |
| Ethanol | 5 | 5 | 5 | 5 | 5 | 5 |
| Laureth sulfuric ester DEA salt | 7 | 7 | 7 | 7 | 7 | 7 |
| Red Punica granatum L. extracting solution | 1 | 1 | 1 | 1 | 1 | 1 |
| Carnosic acid | 0.01 | / | / | / | / | / |
| AOB | 0.02 | 0.02 | 0.02 | 0.03 | / | / |
| Nisin | 0.01 | 0.01 | 0.02 | 0.01 | / | / |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.01 | 0.02 | 0.01 | 0.01 | / | / |
| Methyl parahydroxybenzoate | / | / | / | / | 0.05 | / |
Comparative Examples 1
Take by weighing each raw material according to corresponding Comparative Examples 1 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated red Punica granatum L. facial film of Comparative Examples 1.
Comparative Examples 2
Take by weighing each raw material according to corresponding Comparative Examples 2 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated red Punica granatum L. facial film of Comparative Examples 2.
Comparative Examples 3
Take by weighing each raw material according to corresponding Comparative Examples 3 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated red Punica granatum L. facial film of Comparative Examples 3.
Comparative Examples 4
Take by weighing each raw material according to corresponding Comparative Examples 4 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated red Punica granatum L. facial film of Comparative Examples 4.
Comparative Examples 5
Take by weighing each component according to Comparative Examples 5 data corresponding in the table 1, adopt embodiment 1 described method, namely obtain the exfoliated red Punica granatum L. facial film of Comparative Examples 5.
Test case
The exfoliated red Punica granatum L. facial film that respectively embodiment 1 and Comparative Examples 1-5 is made carries out fill with the dark brown vial, opens wide bottle cap, places under 40 ℃ of ambient temperatures, relative humidity 85% environment, continues to observe also test, and concrete outcome sees the following form.Detect the microorganism level, concrete test item, detection method and examination criteria carry out according to QB/T2872-2007.
| ? | Observe phenomena |
| Embodiment 1 | No abnormality seen after 60 days, abnormal smells from the patient is pure |
| Comparative Examples 1 | After 50 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 2 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 3 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 4 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 5 | After 5 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
The antiseptic methyl parahydroxybenzoate that uses in the Comparative Examples 4 is one of the most frequently used cosmetics preservative in this area.Belong to antiseptic phenols, generally effective to mycete, yeast, antibacterial, the effect that suppresses growth of microorganism is arranged, effectively prolong the shelf-life (40 days lower shelf-lifves of test condition of the present invention) of cosmetics after adding, but long-term this antiseptic of excessive use, the Diazolidinyl Urea epidermis cell causes the epidermis transition aging.
Can significantly be drawn by test data, the embodiment of the invention 1 is used carnosic acid, AOB, nisin and the composite Synergistic of iodine propilolic alcohol butyl mephenesin Carbamate, and antiseptic effect (60 days lower shelf-lifves of test condition of the present invention) obviously is better than Comparative Examples 1-3 and only adopts AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate three composite (in lower shelf-life of test condition of the present invention below 50 days).
The facial film of the embodiment of the invention 1 places accelerated test under 40 ℃ of ambient temperatures, relative humidity 85% environment at opening, can reach 60 days antiseptic effects, the long shelf-life of facial film, and conversion shady and cool dry its shelf-life of place under sealing state far surpasses 3 years.
The above; it only is the specific embodiment of the present invention; but protection scope of the present invention is not limited to this; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; variation or the replacement that can expect without creative work all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (3)
1. exfoliated red Punica granatum L. facial film, it is characterized in that, raw material by following weight parts is prepared from according to a conventional method: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part cocoyl morpholine oxide, 4-6 part ethanol, 6-8 part laureth sulfuric ester DEA salt, 0.8-2 part red Punica granatum L. extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
2. exfoliated red Punica granatum L. facial film as claimed in claim 1, it is characterized in that, described compound preservative is made of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
3. the preparation method of exfoliated red Punica granatum L. facial film as claimed in claim 2, it is characterized in that, formed by following step: polyvinyl alcohol is added in the deionized water, be heated to 70-90 ℃, dissolving is cooled to 45-55 ℃, add glycerol, cocoyl morpholine oxide, ethanol, the stirring of laureth sulfuric ester DEA salt, be cooled to 40 ℃, add red Punica granatum L. extracting solution and compound preservative, stir.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105878102A (en) * | 2015-04-24 | 2016-08-24 | 四川福能源生物科技有限公司 | Facial mask containing punica granatum fruit extract and preparation method of facial mask |
| CN106974843A (en) * | 2016-11-01 | 2017-07-25 | 田鹏新 | A kind of exfoliated apple ferment facial mask and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102198062A (en) * | 2011-05-26 | 2011-09-28 | 成都中医药大学 | Red sage root mask and preparation method thereof |
-
2013
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102198062A (en) * | 2011-05-26 | 2011-09-28 | 成都中医药大学 | Red sage root mask and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| L.V. THOMAS，ET AL: "Nisin synergy with natural antioxidant extracts of the herb rosemary", 《PROC IM IS ON NATURAL PRESERV. IN FOOD SYSTEMS》 * |
| 何琼: "《七彩生活 17 天然滋养美肤面膜：白金升级版》", 30 November 2010, 吉林出版集团有限公司 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105878102A (en) * | 2015-04-24 | 2016-08-24 | 四川福能源生物科技有限公司 | Facial mask containing punica granatum fruit extract and preparation method of facial mask |
| CN105878102B (en) * | 2015-04-24 | 2018-11-02 | 四川福能源生物科技有限公司 | A kind of facial mask and preparation method thereof containing pomegranate berry extract |
| CN106974843A (en) * | 2016-11-01 | 2017-07-25 | 田鹏新 | A kind of exfoliated apple ferment facial mask and preparation method thereof |
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