CN105878102B - A kind of facial mask and preparation method thereof containing pomegranate berry extract - Google Patents
A kind of facial mask and preparation method thereof containing pomegranate berry extract Download PDFInfo
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- CN105878102B CN105878102B CN201510200549.XA CN201510200549A CN105878102B CN 105878102 B CN105878102 B CN 105878102B CN 201510200549 A CN201510200549 A CN 201510200549A CN 105878102 B CN105878102 B CN 105878102B
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Abstract
The present invention relates to a kind of facial mask and preparation method thereof containing pomegranate berry extract, is equipped with functional cosmetic material by water and is made.The raw material group of the facial mask becomes：Deionized water, glycerine, pomegranate（PUNICA GRANATUM）Berry extract, hyaluronic acid, lipoic acid, ginkgo（GINKGO BILOBA）Leaf extract, Cer NP, Abelmoschus esculentus（ABELMOSCHUS ESCLENTUS）Berry extract, carbomer, triethanolamine, Phenoxyethanol；Pomegranate berry extract can effectively neutralize free radical, inhibit the formation of melanin, boost metabolism, toxin is discharged.The facial mask of the present invention can be absorbed nutritional ingredient by skin and reached cosmetic result with whitening, moisturizing, crease-resistant.This facial mask can be used for a long time, without any side effects, securely and reliably.
Description
Technical field
Invention is related to a kind of shielding skin-protecting cosmetic, more particularly to a kind of facial mask.
Background technology
Red pomegranate nature and flavor are sweet, sour and astringent, warm, and the substances such as abundant vitamin C, Punica granatum L. polyphenol and anthocyanidin are contained in fruit,
There are good toxin expelling, anti-oxidation efficacy.It all plays an important role in terms of medicinal, beauty, dietotherapy.Modern medicine discovery, red pomegranate
In contain a large amount of Punica granatum L. polyphenol and anthocyanidin, inoxidizability is higher by 3 times of green tea, 20 times even more ascorbic, can effectively neutralize
Free radical boosts metabolism, toxin is discharged.
Mainly there is following effect delaying skin aging：Punica granatum L. polyphenol, anthocyanidin, ellagic acid are all extremely strong polyphenoils
Matter, grease autoxidation are free chain reactions, can generate a variety of oxygen radicals in reaction process, these oxygen radicals have
Very high reactivity is combined with macromolecular substances such as human body inner lipid, protein and DNA, destroys its structure and function.Cause machine
Body aging, and a variety of diseases such as cause cancer, atherosclerosis and cataract.The National Natural Science base that Sichuan University undertakes
The achievement in research of golden No. 20472058 projects shows the water extract of a concentration of 0.0175 mg/mL of red pomegranate to DPPH freedom
The clearance rate of base is up to 85.2%, is higher than BHT, it is sufficient to prove the inoxidizability of red pomegranate extract.Moisturizing：Hyaluronic acid is people
The most important natural moisture preserving ingredient of body, its decomposition mainly pass through the catalytic action of hyaluronidase.Punica granatum L. polyphenol can inhibit
The activity of bright matter acid enzyme, to slow down the decomposition rate of hyaluronic acid, to achieve the effect that moisturizing.It is crease-resistant：Punica granatum L. polyphenol energy
With hydrogen bond and it is hydrophobic the effects that react with the protein in skin, generate astriction, i.e. convergence.This reaction can make
Skin is tight, reduces wrinkle.
But pomegranate squeezing juice is easier to be aoxidized blackening, influences the effect and long-term preservation of the facial mask made, and
Individual juice of my pomegranate cannot use, and ingredient effect and utilization rate can also be affected.
Invention content
The present invention be solve the problems, such as the utilization rate of active components extracted from pomegranate fruit it is low this, provide one kind for consumer
Facial mask and preparation method thereof of the wrinkle effect preferably containing pomegranate berry extract is removed in whitening, can be convenient for carrying, be attached on the face, very
It is good to absorb, and moisture preserving time is long.
The present invention solves the deficiency of prior art problem, and used technical solution is：One kind is provided and contains pomegranate fruit
The facial mask of Cosmetic Ingredient is by the following weight percent formed：Deionized water：60%~80%, glycerine：5%~10%,
Pomegranate berry extract：3%~10%, hyaluronic acid：0.02%~0.1%, lipoic acid：1%~5%, ginkgo biloba p.e：1%
~5%, Cer NP：2%~5%, Abelmoschus esculentus berry extract：5%~10%, carbomer：0.02%~0.2%, three second
Hydramine：0.01%~0.1%, Phenoxyethanol：0.1%~0.5%.
A kind of being further improved for facial mask containing pomegranate fruit Cosmetic Ingredient of the present invention be：The weight of the facial mask each component is matched
Than for：Deionized water：It is appropriate that facial mask liquid component is made to meet 100%, glycerine：6%~10%, pomegranate berry extract：3%~8%,
Hyaluronic acid：0.01%~0.05%, lipoic acid：1%~3%, ginkgo biloba p.e：1%~4%, Cer NP：3%~
5%, Abelmoschus esculentus berry extract：5%~8%, carbomer：0.02%~0.1%, triethanolamine：0.01%~0.05%, benzene oxygen second
Alcohol：0.2%~0.5%.
The facial mask that the present invention contains pomegranate fruit Cosmetic Ingredient is further preferred that：The weight percent of each component of the facial mask
Than：Deionized water：69.5%, glycerine：8%, pomegranate berry extract：6%, hyaluronic acid：0.05%, lipoic acid：3%, ginkgo leaf extracts
Object：4%, Cer NP：3%, Abelmoschus esculentus berry extract：6%, carbomer：0.1%, triethanolamine：0.05%, Phenoxyethanol：
0.3%。
The present invention provides a kind of preparation method of the facial mask containing pomegranate berry extract Cosmetic Ingredient, which is characterized in that packet
Include following steps：
A. the preparation of pomegranate fruit extracting solution：Select that epidermis is smooth, the tight fresh pomegranate of skin and flesh breaks entire pomegranate fruit
It is broken, make pulp and fruit juice separating, broken raw material is respectively put into round, general tinning amount is the 80% of container capacity,
To reserve discharge of the sufficient space convenient for carbon dioxide gas and heat during fermentation, the tank or quick-fried that overflows caused by air accumulation is prevented
Bottle stands 4 hours, under conditions of 20 DEG C of room temperature, manually adds appropriate yeast, right in 25 DEG C of -28 DEG C of continuing fermentations 4-10 days
Material carries out skin slag separation in tank, collects all liq, lactic acid bacteria is added under conditions of 18 DEG C -20 DEG C of conciliation temperature and pH value 4
It carries out second to ferment, then fermentation process 3-4 days is handled with ultrasonic wave extraction, super in 40 DEG C of -50 DEG C of water temperature F
Sound wave strengthening extraction, atmospheric extraction, intensified by ultrasonic wave extract 20~40 minutes, and extracting solution is then passed through D101 type macroporous absorptions
Resin column, then with pure water rinsing resin column, collect efflux；Efflux collects outflow by NEUTRAL ALUMINUM column with pure water rinsing
Liquid；The efflux of gained is concentrated under reduced pressure, and obtains pomegranate fruit extracting solution；
B. the preparation of hyaluronic acid solution：Deionized water is boiled 20 minutes, after cooling, weighs 1 part of hyaluronic acid in room temperature
It is added in 99 parts of deionized waters, stirs one hour under stirring condition, heating makes water temperature be increased to 70 DEG C -80 DEG C, keeps the temperature half
Hour, constant weight moisturizing is cooled to room temperature and obtains clean and clear transparent liquid；
C. carbomer is dissolved in deionized water, PH to 5.0-7.5 is adjusted with triethanolamine, stone then is added according to proportioning
Pomegranate fruit Essence, hyaluronic acid solution, lipoic acid, ginkgo biloba p.e, Cer NP, Abelmoschus esculentus berry extract, mixing
Phenoxyethanol is added after uniformly, stirs evenly, constant weight moisturizing, adjusts pH value between 5.8-6.5, obtains and carried containing pomegranate fruit
Take the facial mask liquid of object Cosmetic Ingredient.
The preparation method of further preferred facial mask, which is characterized in that include the following steps：
A. the preparation of pomegranate fruit extracting solution：Select that epidermis is smooth, the tight fresh pomegranate of skin and flesh breaks entire pomegranate fruit
It is broken, make pulp and fruit juice separating, broken raw material is respectively put into round, general tinning amount is the 80% of container capacity,
To reserve discharge of the sufficient space convenient for carbon dioxide gas and heat during fermentation, the tank or quick-fried that overflows caused by air accumulation is prevented
Bottle stands 4 hours, under conditions of 20 DEG C of room temperature, manually adds appropriate yeast, in 25 DEG C of -28 DEG C of continuing fermentations 6 days, to tank
Middle material carries out skin slag separation, collects all liq, reconcile be added under conditions of 18 DEG C -20 DEG C of temperature and pH value 4 lactic acid bacteria into
Second of fermentation of row, then fermentation process 4 days is handled with ultrasonic wave extraction, in 40 DEG C of -50 DEG C of water temperature F ultrasonic waves
Strengthening extraction, atmospheric extraction, intensified by ultrasonic wave extract 40 minutes, you can pomegranate berry extract；
B. the preparation of hyaluronic acid solution：Deionized water is boiled 20 minutes, after cooling, weighs 1 part of hyaluronic acid in room temperature
It is added in 99 parts of deionized waters, stirs one hour under stirring condition, heating makes water temperature be increased to 70 DEG C -80 DEG C, keeps the temperature half
Hour, constant weight moisturizing is cooled to room temperature and obtains clean and clear transparent liquid；
C. card wave is dissolved in deionized water, PH to 6.5 is adjusted with triethanolamine, pomegranate fruit essence then is added according to proportioning
Magnificent liquid, hyaluronic acid solution, lipoic acid, ginkgo biloba p.e, Cer NP, Abelmoschus esculentus berry extract, after mixing
Phenoxyethanol is added, stirs evenly, constant weight moisturizing, adjusts pH value between 5.8-6.5, obtains beautiful containing pomegranate berry extract
The facial mask liquid of Rongcheng point.
The beneficial technique effect of the present invention
The superiority of ultrasonic extraction pomegranate fruit is specific physical property based on ultrasound.Mainly pass through piezoelectric energy-conversion
The Quick mechanical vibration wave that device generates is solid to realize to reduce the active force between target extract and sample matrices -- and liquid extracts
Take separation.
（1）Accelerating medium particle movement.Higher than the continuous media of the ultrasonic wave of 20KHz frequency of sound wave（Such as water）Middle propagation
When, according to Huygens's wave principle, the movement of medium particle will be caused in the wave surface of its propagation, medium particle movement is made to obtain
The huge acceleration of row and kinetic energy.The acceleration of particle is computed 2,000 times or more of general reachable acceleration of gravity.Due to being situated between
Ultrasonic energy is acted on pomegranate fruit active ingredient particle and is allowed to obtain huge acceleration and kinetic energy by matter particle, rapidly
It escapes pomegranate fruit matrix and is free in water.
（2）Cavitation.Ultrasonic wave is propagated in liquid medium to be generated special " cavitation effect ", and " cavitation effect " is continuous
The strong impact wave that countless internal pressures reach micro- air pocket of thousands of a atmospheric pressure and constantly " explosion " generates on microcosmic is generated to make
With on pomegranate fruit, making its pomegranate fruit component substances be escaped by " bombardment ", and so that pomegranate fruit matrix is constantly degraded, acceleration stone
The leaching of pomegranate fruit effective ingredient is extracted.
（3）The vibration of ultrasonic wave homogenizes（Sonication）Keep the effect that each point is subject in sample media consistent, makes entire
Sample extraction is evenly.It is obtained in conclusion the active principle in pomegranate fruit serves not only as medium particle under ultrasound field effect
Huge acceleration derived from body and kinetic energy, and powerful external impacts are obtained by " cavitation effect ", so energy high efficiency is simultaneously
It is sufficiently separated out.
Ultrasonic extraction has following outstanding feature：
（1）Without high temperature.It is extracted in 40 DEG C of -50 DEG C of water temperature F intensified by ultrasonic wave, no boiling high temperature does not destroy in pomegranate fruit
Certain effective ingredients with thermally labile, facile hydrolysis or oxidation characteristic.Ultrasonic wave energy with promoting plant cell broken wall improves stone
The effect of pomegranate fruit active ingredient.
（2）Atmospheric extraction, safety is good, and operation is simple, and maintaining is convenient.
（3）Extraction efficiency is high.Intensified by ultrasonic wave, which extracts 20~40 minutes, can obtain optimum extraction rate, and extraction time is only water
It boils, the one third of alcohol deposition method or less.Extraction is abundant, and extraction quantity is two times of conventional method or more.According to statistics, ultrasonic wave exists
65~70oC working efficiencies are very high.And the effective ingredient of temperature pomegranate fruit in 65oC degree is not destroyed substantially.It is added
After ultrasonic wave（Under the conditions of 65 degree）, about 40 minutes active ingredients of plants extraction times.And the digestion time of cooking process often needs
Two to three hours are wanted, is 3 times of the ultrasonic wave extraction time or more times.It is extracted per tank 3 times, substantially extractable effective ingredient
90% or more.
（4）Reduce energy consumption.Since ultrasonic extraction is low without heating or heating temperature, extraction time is short, therefore substantially reduces
Energy consumption.
（5）Extraction process is at low cost, and overall economic efficiency is notable；
（6）Ultrasonic wave has certain bactericidal effect, ensures that extract liquor is unlikely to deteriorate.
Red pomegranate nature and flavor are sweet, sour and astringent, warm, and the substances such as abundant vitamin C, Punica granatum L. polyphenol and anthocyanidin are contained in fruit,
There are good toxin expelling, anti-oxidation efficacy.It all plays an important role in terms of medicinal, beauty, dietotherapy.Modern medicine discovery, red pomegranate
In contain a large amount of Punica granatum L. polyphenol and anthocyanidin, inoxidizability is higher by 3 times of green tea, 20 times even more ascorbic, can effectively neutralize
Free radical boosts metabolism, toxin is discharged.But these active principles can not be extracted completely from pomegranate fruit,
It can not completely be used.In order to avoid in extraction since the traditional extraction techniques such as chemical organic solvent and high temperature are to pomegranate
The destruction of active ingredient in fruit, we select the mode of ultrasonic extraction, while pomegranate fruit, through everfermentation, active ingredient is better
It decomposites and, it is easier to extract, and inventor uses decoloration process.
The present invention selects deionized water, glycerine, pomegranate（PUNICA GRANATUM）Berry extract, hyaluronic acid, sulphur are pungent
Acid, ginkgo（GINKGO BILOBA）Leaf extract, Cer NP, Abelmoschus esculentus（ABELMOSCHUS ESCLENTUS）Fruit carries
Take object, carbomer, triethanolamine, Phenoxyethanol etc. as the raw material of pomegranate fruit facial mask, by the reasonably combined of mentioned component
Later, this facial mask has whitening, delaying skin aging, moisturizing, crease-resistant effect, has to the skin of modern female and repaiies well
Shield acts on, and can provide most sufficient nutrient to skin within the shortest time, skin is made to rejuvenate.
It is compared with the prior art, the remarkable advantage of patent of the present invention：
1, by fermentation, the utilization rate of pomegranate fruit active ingredient is improved using ultrasonic extraction.
2, reasonably combined between different material, promote assimilation effect of the skin to active ingredient.
Description of the drawings
Fig. 1 tyrosinase activity test results.
Specific implementation mode
The present invention is further described below.
One preparation method of the facial mask of 1 present invention of embodiment
It is as follows that a kind of facial mask raw materials weight ratio containing pomegranate fruit Cosmetic Ingredient is made：Deionized water：
69.5%, glycerine：8%, pomegranate berry extract：6%, hyaluronic acid：0.05%, lipoic acid：3%, ginkgo biloba p.e：4%, neural acyl
Amine 3：3%, Abelmoschus esculentus berry extract：6%, carbomer：0.1%, triethanolamine：0.05%, Phenoxyethanol：0.3%.
The preparation method of facial mask containing pomegranate berry extract Cosmetic Ingredient, includes the following steps：
1, the preparation of pomegranate fruit extracting solution：
Select that epidermis is smooth, entire pomegranate fruit is crushed by the tight fresh pomegranate 120kg of skin and flesh, makes pulp and fruit juice point
From.Broken raw material is respectively put into round（General tinning amount is the 80% of container capacity, just with reserved sufficient space
The discharge of carbon dioxide gas and heat during fermentation prevents overflow caused by air accumulation tank or bottle explosion）, 4 hours are stood,
It is artificial to add 300g yeast under conditions of 20 DEG C of room temperature, in 25 DEG C of -28 DEG C of continuing fermentations 8 days.Skin slag point is carried out to material in tank
From collection all liq amounts to 9.48kg, and 30g lactic acid bacterias are added under conditions of 20 DEG C of temperature and pH value 4 and send out for the second time
Ferment, fermentation process 4 days.Then 40 DEG C are heated and carries out processing 40 minutes with ultrasonic wave extraction.After restoring room temperature, centrifuged
Filter；Then by extracting solution by D101 type large pore resin absorption columns, then with pure water rinsing resin column, efflux is collected；Efflux
By NEUTRAL ALUMINUM column efflux is collected with pure water rinsing；70 DEG C of reduced pressures of efflux of gained, obtain pomegranate fruit extracting solution 6.1
Kilogram.
2, the preparation of hyaluronic acid solution：Deionized water is boiled 20 minutes, after cooling, is weighed, 50g hyaluronic acids are in room temperature
It is added in 4950g deionized waters, stirs one hour under stirring condition, heating makes water temperature be increased to 70 DEG C -80 DEG C, keeps the temperature half
Hour, constant weight moisturizing is cooled to room temperature and obtains the liquid of clean and clear clear viscous.
3,0.1kg carbomers are dissolved in 64.55kg in the deionized water of sterilization, stir half an hour, card wave
It is fully dispersed in water；Under agitation, 0.05kg triethanolamines are added in pot, adjust PH to 5.0-7.5, it is practical to survey
It is 6.2 to measure ph values.At room temperature, 8kg glycerine, 6kg pomegranate fruits extracting solution, 5kg hyaluronic acid solutions, 3kg is added according to proportioning
Lipoic acid, 4kg ginkgoes（GINKGO BILOBA）Leaf extract, 3kg Cer NPs, 6kg Abelmoschus esculentus（ABELMOSCHUS
ESCLENTUS）Berry extract is added 0.3kg Phenoxyethanols, stirs evenly, constant weight moisturizing, actually measured ph values after mixing
It is 5.8, obtains the facial mask liquid 100kg containing pomegranate berry extract Cosmetic Ingredient.The facial mask liquid can be used alone, can also
Finished product, every bag of facial mask about 20-40ml containing facial mask liquid is made by production line with facial mask cloth in appropriate facial mask liquid.
2 pomegranate fruit facial mask white-skinned face function of the present invention of embodiment
According to experimental method in the prior art, 5 μ g of vitamin C are selected, 5 μ g of kojic acid, 5 μ g of quinhydrones and the present embodiment 1
The pomegranate mask liquid just prepared（It is equivalent to Punica granatum L. extract content）5 μ g are carried out after inhibiting tyrosinase activity test, and observation is each
Melanin formational situation in test tube, pomegranate mask liquid significantly inhibit effect to the formation of melanin.The pomegranate mask of the present invention
Liquid can inhibit melanin, and 24 hours whens are still effective, and color still maintains shallower, and the change that other samples are all apparent
It is black.（See Fig. 1）
3 clinical trial result of embodiment is assessed
Trier is age-based, and skin quality and profession degree are divided into three groups, and all experimenters are voluntary participation test in 20 years old or more
Healthy women.Wherein 20-30 Sui is one group, and number is 50 people；- 50 years old 30 years old are one group, and number is 50 people.Every trier
The facial mask 30 of the preparation of the present embodiment 1 is distributed respectively, and two days using primary.Usage time 60 days.
20-30 Sui proof test result see the table below：
| Test event | Good results（%） | Effect is general（%） | Effect is bad（%） |
| Applicating property | 96% | 4% | 0 |
| Moisture retention | 98% | 2% | 0 |
| It compacts sense | 80% | 20% | 0 |
| Whitening is dispelled yellow effect | 90% | 10% | 0 |
| Moistness | 86% | 14% | 0 |
30-50 Sui proof test result see the table below：
| Test event | Good results（%） | Effect is general（%） | Effect is bad（%） |
| Applicating property | 96% | 4% | 0 |
| Moisture retention | 100% | 0 | 0 |
| It compacts sense | 94% | 6% | 0 |
| Whitening is dispelled yellow effect | 98% | 2% | 0 |
| Moistness | 96% | 4% | 0 |
The facial mask for preparing of the present invention being found through experiments that no matter in applicating property, moisture retention, sense of compacting, whitening dispels yellow effect,
Moistness can make most consumer satisfactions.
Currently the most important problem of whitening product is:Effect is too slow, it is few then 10-15 days, the at most 2-4 months just have slight
People's using effect othernesses different part effect is larger, deactivate after can rebound, investigate the reason is that:Whitening active is not strong enough,
Whitening composition content is too low;Whitening composition action time is too long;Product poor permeability;Skin is absorbent limited, whitening composition
Poor (being aoxidized before the not being absorbed by the skin) of oxidation resistance to solve the above-mentioned problems, design scheme, using facial mask
Note, dosage is big, and the skin that entire face is equivalent to during use is washed in whitening composition, makes the content of whitening composition, is made
With the time, assimilation effect etc. is guaranteed, generally visible positive effect after forty minutes:Pale, water is tender, fine and smooth, becomes clear, gloss
Effect.Whitening principle, facial mask essence contact skin after with the help of pepper element, ginkegetin rapid osmotic to epidermal hair
Thin blood vessel, vasodilator, improving micro_circulation effect have superoxide dismutase sample effect, remove free radical.Promote skin
Hematology recycles.Required moisture and nutrient are provided for skin.After two hours, lipoic acid and red pomegranate extract and ginkgo leaf carry
It takes object to combine, short-term, mid-term, long-term effect and surface layer, middle level can be reached, deep layer whitening, which synchronizes, to be carried out.Every other day with one
It is secondary, it can significant difference after course for the treatment of use in 10-15 days.In vain, tender, soft, thin, bright five functional is presented, permanence operation
It becomes apparent from.Common facial mask is dried after 15 minutes, and the whitening mask that the present invention designs is especially added with the ingredient for extending moisture preserving time.
Make the whitening of the facial mask, moisturizing, wrinkle-proof effect is more preferable.
Claims (8)
1. a kind of raw material group of the facial mask liquid containing pomegranate berry extract becomes：Deionized water, glycerine, pomegranate berry extract, thoroughly
Bright matter acid, lipoic acid, ginkgo biloba p.e, Cer NP, Abelmoschus esculentus berry extract, carbomer, triethanolamine, benzene oxygen second
Alcohol；
The weight percent respectively formed above is：
Moisturizing ingredient：7.02%~15.1%
Pomegranate berry extract：3%~10%
White-skinned face function raw material：1%~5%
Ginkgo biloba p.e：1%~5%
Abelmoschus esculentus berry extract：5%~10%
Carbomer：0.02%~0.2%
Triethanolamine：0.01%~0.1%
Preservative：0.1%~0.5%
Deionized water：Add in right amount, facial mask liquid recipe ingredient is made to reach 100%；
A kind of preparation method of facial mask liquid containing pomegranate berry extract Cosmetic Ingredient, includes the following steps：
A. the preparation of pomegranate berry extract：Select that epidermis is smooth, entire pomegranate fruit is crushed, makes by the tight fresh pomegranate of skin and flesh
Broken raw material is respectively put into round by pulp and fruit juice separating, and tinning amount is the 80% of container capacity, to stop in advance
Enough spaces prevent overflow caused by air accumulation tank or bottle explosion convenient for the discharge of carbon dioxide gas and heat during fermentation, stand 4
Hour, under conditions of 20 DEG C of room temperature, appropriate yeast is manually added, in 25 DEG C of -28 DEG C of continuing fermentations 4-10 days, to material in tank
Skin slag separation is carried out, all liq is collected, addition lactic acid bacteria carries out second under conditions of adjusting 18 DEG C -20 DEG C of temperature and pH value 4
Secondary fermentation, fermentation process 3-4 days, is then handled with ultrasonic wave extraction, and ultrasonic wave is strong under 40 DEG C of -50 DEG C of water temperatures
Change extraction, atmospheric extraction, intensified by ultrasonic wave extracts 20~40 minutes；Then extracting solution is passed through into D101 type macroporous absorption trees
Fat column, then with pure water rinsing resin column, collect efflux；Efflux collects efflux by NEUTRAL ALUMINUM column with pure water rinsing；
70 DEG C of reduced pressures of efflux of gained, obtain pomegranate fruit extracting solution；
B. the preparation of hyaluronic acid solution：Deionized water is boiled 20 minutes, after cooling, weighed 1 part of hyaluronic acid and is stirred at room temperature
Under the conditions of be added in 99 parts of deionized waters, stir one hour, heating makes water temperature be increased to 70 DEG C -80 DEG C, keeps the temperature half an hour,
Constant weight moisturizing is cooled to room temperature and obtains clean and clear transparent liquid；
C. carbomer is dissolved in deionized water, pH to 5.0-7.5 is adjusted with triethanolamine, pomegranate fruit then is added according to proportioning
Extract, hyaluronic acid solution, lipoic acid, ginkgo biloba p.e, Cer NP, Abelmoschus esculentus berry extract are uniformly mixed
After Phenoxyethanol is added, stir evenly, constant weight moisturizing, adjust pH value between 5.8-6.5, obtain containing pomegranate berry extract
The facial mask liquid of Cosmetic Ingredient.
2. according to a kind of facial mask liquid containing pomegranate berry extract ingredient described in claim 1, it is characterised in that：
The weight percent of each component is：
Glycerine：6%~10%
Pomegranate berry extract：3%~8%
Hyaluronic acid：0.01%~0.05%
Lipoic acid：1%~3%
Ginkgo biloba p.e：1%~4%
Cer NP：3%~5%
Abelmoschus esculentus berry extract：5%~8%
Carbomer：0.02%~0.1%
Triethanolamine：0.01%~0.05%
Phenoxyethanol：0.2%~0.5%
Deionized water：In right amount, facial mask liquid component is made to meet 100%.
3. according to a kind of facial mask liquid containing pomegranate berry extract ingredient described in claim 1, it is characterised in that：
The weight percent of each component is：
Deionized water：69.5%
Glycerine：8%
Pomegranate berry extract：6%
Hyaluronic acid：0.05%
Lipoic acid：3%
Ginkgo biloba p.e：4%
Cer NP：3%
Abelmoschus esculentus berry extract：6%
Carbomer：0.1%
Triethanolamine：0.05%
Phenoxyethanol：0.3%
Deionized water：In right amount, facial mask liquid component is made to meet 100%.
4. according to a kind of facial mask liquid containing pomegranate berry extract Cosmetic Ingredient described in claim 1, it is characterised in that：Institute
It is hyaluronic acid 0.02%~0.1%, Cer NP 2%~5%, glycerine 5 ~ 10% to state moisturizing ingredient.
5. according to a kind of facial mask liquid containing pomegranate berry extract Cosmetic Ingredient described in claim 1, it is characterised in that：Institute
It is lipoic acid to state white-skinned face function raw material.
6. according to a kind of facial mask liquid containing pomegranate berry extract Cosmetic Ingredient described in claim 1, it is characterised in that：Institute
It is Phenoxyethanol to state preservative.
7. a kind of facial mask liquid containing pomegranate berry extract Cosmetic Ingredient according to claim 1 ~ 3 any one, system
Preparation Method includes the following steps：
A. the preparation of pomegranate berry extract：Select that epidermis is smooth, entire pomegranate fruit is crushed, makes by the tight fresh pomegranate of skin and flesh
Broken raw material is respectively put into round by pulp and fruit juice separating, and tinning amount is the 80% of container capacity, to stop in advance
Enough spaces prevent overflow caused by air accumulation tank or bottle explosion convenient for the discharge of carbon dioxide gas and heat during fermentation, stand 4
Hour, under conditions of 20 DEG C of room temperature, manually add appropriate yeast, in 25 DEG C of -28 DEG C of continuing fermentations 6 days, to material in tank into
Row skin slag detaches, and collects all liq, and addition lactic acid bacteria carries out second under conditions of adjusting 18 DEG C -20 DEG C of temperature and pH value 4
Then fermentation, fermentation process 4 days are handled with ultrasonic wave extraction, intensified by ultrasonic wave extracts under 40 DEG C of -50 DEG C of water temperatures
It takes, atmospheric extraction, intensified by ultrasonic wave, which extracts 30 minutes, can obtain pomegranate berry extract；Then extracting solution is passed through into D101 type macropores
Adsorption resin column, then with pure water rinsing resin column, collect efflux；Efflux collects stream by NEUTRAL ALUMINUM column with pure water rinsing
Go out liquid；70 DEG C of reduced pressures of efflux of gained, obtain pomegranate fruit extracting solution；
B. the preparation of hyaluronic acid solution：Deionized water is boiled 20 minutes, after cooling, weighed 1 part of hyaluronic acid and is stirred at room temperature
Under the conditions of be added in 99 parts of deionized waters, stir one hour, heating makes water temperature be increased to 70 DEG C -80 DEG C, keeps the temperature half an hour,
Constant weight moisturizing is cooled to room temperature and obtains clean and clear transparent liquid；
C. carbomer is dissolved in deionized water, pH to 6.5 is adjusted with triethanolamine, the extraction of pomegranate fruit then is added according to proportioning
Object, hyaluronic acid solution, lipoic acid, ginkgo biloba p.e, Cer NP, Abelmoschus esculentus berry extract add after mixing
Enter Phenoxyethanol, stir evenly, constant weight moisturizing adjusts pH value between 5.8-6.5, obtains containing pomegranate berry extract beauty
The facial mask liquid of ingredient.
8. being filled into bottle exclusive use after the facial mask liquid sterilization described in claim 1-6, or it is filled into the face for being placed with facial mask cloth
Facial mask paster is made in film bag.
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| CN106265375A (en) * | 2016-10-12 | 2017-01-04 | 湖南农业大学 | A kind of whitening anti-aging facial film and preparation method thereof |
| CN106619300A (en) * | 2016-12-28 | 2017-05-10 | 广州市聚吉科绿色化学共性技术研究院有限公司 | Moisturizing cosmetic capable of refining pores |
| CN106924073A (en) * | 2017-05-09 | 2017-07-07 | 南通千竹电子科技有限公司 | A kind of replenishing water and preserving moisture facial mask and preparation method thereof |
| CN107982070B (en) * | 2017-12-27 | 2020-12-29 | 上海晓美生物科技有限公司 | Whitening and moisturizing facial mask containing pomegranate essence and preparation method thereof |
| CN108042425B (en) * | 2017-12-27 | 2020-12-22 | 上海晓美生物科技有限公司 | Whitening and moisturizing essence and preparation method thereof |
| CN109125236A (en) * | 2018-08-30 | 2019-01-04 | 谭建新 | A kind of pomegranate ferment facial mask and preparation method thereof and device |
| TWI694843B (en) * | 2019-01-17 | 2020-06-01 | 大江生醫股份有限公司 | Fermentation product of punica granatum and use of the fermentation product of punica granatum for inhibiting melanogenesis and whitening |
| CN110013494A (en) * | 2019-02-12 | 2019-07-16 | 广州小蜜蜂生物科技有限公司 | A kind of pomegranate berry extract and its preparation method and application |
| CN111544355B (en) * | 2020-06-04 | 2021-04-27 | 爱西美(珠海)生物技术有限公司 | Ellagic acid enzyme and preparation method thereof |
| CN114617832A (en) * | 2022-03-31 | 2022-06-14 | 陕西百康实业集团有限公司 | Fruit mask and preparation method thereof |
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| CN103356469A (en) * | 2013-05-23 | 2013-10-23 | 上海珍馨化工科技有限公司 | Peel-off type pomegranate facial mask and preparation method thereof |
| CN103919710A (en) * | 2014-03-31 | 2014-07-16 | 韩雁如 | Facial mask capable of improving sleeping and preparation method thereof |
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| CN103356469A (en) * | 2013-05-23 | 2013-10-23 | 上海珍馨化工科技有限公司 | Peel-off type pomegranate facial mask and preparation method thereof |
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