CN107982070B - Whitening and moisturizing facial mask containing pomegranate essence and preparation method thereof - Google Patents
Whitening and moisturizing facial mask containing pomegranate essence and preparation method thereof Download PDFInfo
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- CN107982070B CN107982070B CN201711439770.6A CN201711439770A CN107982070B CN 107982070 B CN107982070 B CN 107982070B CN 201711439770 A CN201711439770 A CN 201711439770A CN 107982070 B CN107982070 B CN 107982070B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The invention discloses a pomegranate essence-containing whitening and moisturizing mask which is prepared from raw materials including a biological fiber mask base material, a pearlized film and essence. The essence is prepared from deionized water, jojoba oil, nicotinamide, potassium salt of azelaic acid amino acid, betaine, chlorphenesin, octyl methicone, glycerol, 2-methyl-1, 3-propanediol, water-soluble ceramide, sodium hyaluronate, phenoxyethanol, triethanolamine, bisabolol, carbomer, and natural plant essence extract. The invention also discloses a preparation method of the pomegranate essence-containing whitening and moisturizing mask.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a pomegranate essence-containing whitening and moisturizing facial mask and a preparation method thereof.
Background
The mask is a key product in a skin care procedure, and the most basic and important purpose of the mask is to compensate the insufficient cleaning work of makeup removal and face washing, and to realize the maintenance functions such as water replenishing, moisture preserving, whitening, anti-aging, grease balancing and the like by matching with other essential nutrients on the basis. The facial mask is a 'tonic' for the skin, and can provide energy which cannot be provided by basic skin care products for the skin and stimulate the maximum vitality of the skin in a short time.
The maintenance principle of the facial mask is that the facial mask is covered on the face for a short time, external air and pollution are temporarily isolated, the skin temperature is increased, pores of the skin are expanded, sweat gland secretion and metabolism are promoted, the oxygen content of the skin is increased, products of epidermal cell metabolism and accumulated grease substances are favorably removed from the skin, water in the facial mask permeates into the cuticle of the epidermis, the skin becomes soft, the skin is naturally bright and elastic, and therefore, the selection of a facial mask base material and carried essence and the adjustment of the facial mask base material play an important role in playing the effects of the facial mask. The biological fiber facial mask base material texture that is made by the natural fermentation of acetobacter xylinum is soft to be elastic toughness strong, it is amazing free from extraneous odour, difficult growth bacterium, and have superstrong close skin nature and can paste the cladding ability of wrinkle and skin dune depths, therefore weave the facial mask more than general cloth and promote the effect of applying face, and can hug closely the skin, the phenomenon that general facial mask drops can not appear, if the absorption that the natural efficient facial mask essence of collocation superstrong osmotic ability and composition can improve the facial mask greatly, reach best result of use.
Disclosure of Invention
In order to solve the above problems, one aspect of the present invention provides a pomegranate essence-containing whitening and moisturizing mask, which is prepared from the following raw materials: a biological fiber mask base material, a pearlized film and essence.
The essence comprises the following raw materials in parts by weight:
80-90 parts of deionized water
2-9 parts of jojoba oil
0.5-1 part of nicotinamide
3-6 parts of potassium azelaic acid amino acid salt
1.5-2 parts of betaine
0.1 to 0.3 portion of chlorphenesin
3-10 parts of octyl polymethylsiloxane
3-10 parts of glycerol
5-9 parts of 2-methyl-1, 3-propanediol
2-5 parts of water-soluble ceramide
0.1-0.3 part of sodium hyaluronate
0.1 to 0.3 portion of phenoxyethanol
0.05 to 0.1 portion of triethanolamine
0.05-0.1 part of bisabolol
0.05-0.1 part of carbomer
8-12 parts of natural plant essence extract.
Preferably, the essence comprises the following raw materials in parts by weight:
83-88 parts of deionized water
4-8 parts of jojoba oil
0.7-1 part of nicotinamide
4-6 parts of potassium azelaic acid amino acid salt
1.7-2 parts of betaine
0.1 to 0.2 portion of chlorphenesin
5-9 parts of octyl polymethylsiloxane
6-9 parts of glycerol
6-9 parts of 2-methyl-1, 3-propanediol
3-5 parts of water-soluble ceramide
0.2-0.3 part of sodium hyaluronate
0.1-0.2 part of phenoxyethanol
0.05 to 0.08 portion of triethanolamine
0.07-0.1 part of bisabolol
0.07-0.09 part of carbomer
9-12 parts of natural plant essence extract.
More preferably, the essence comprises the following raw materials in parts by weight:
87 parts of deionized water
Jojoba oil 7 parts
0.9 portion of nicotinamide
6 parts of potassium salt of azelaic acid amino acid
1.9 portions of betaine
Chlorphenesin 0.1 part
Octyl polymethylsiloxane 8 parts
7 parts of glycerol
9 parts of 2-methyl-1, 3-propanediol
Water soluble ceramide 3 portions
0.3 portion of sodium hyaluronate
0.15 part of phenoxyethanol
Triethanolamine 0.06 parts
0.1 part of bisabolol
Carbomer 0.07 part
11 parts of natural plant essence extract.
In one embodiment, the biological fiber facial mask base material is selected from materials with 12-position veneering cutting design.
In one embodiment, the pearlized film is made of a material with 12-position overlaid cutting design.
In one embodiment, the glycerol is a bio-refined glycerol.
In one embodiment, the natural plant essence extract is pomegranate essence extract.
In one embodiment, the pomegranate essence extract is prepared by the following steps:
(1) screening and shelling: selecting fully mature and plump pomegranate fruits, removing rotten, deteriorated, damaged and other bad fruits, washing with clear water with the volume more than 3 times, drying in the shade, and shelling and peeling by using a pomegranate peeler.
(2) Crushing: crushing pomegranate pulp and pomegranate seeds by using a crusher, setting the rotation speed of the crusher to be 100-150 rpm, selecting a filter screen with the diameter of 1-3 mm, fully crushing the pulp, and separately collecting pomegranate pulp residues and pomegranate juice for later use.
(3) Ultrasonic: drying the pomegranate rind at the temperature of 30-40 ℃, crushing the pomegranate rind by using a crusher, mixing the pomegranate rind with the pulp residues, adding distilled water according to the mass ratio of 1:10, uniformly mixing and stirring the mixture for 20 minutes, putting the mixture into an ultrasonic cell crusher, performing ultrasonic treatment at the ultrasonic frequency of 22KHz for 40-60 minutes at the temperature of 0-10 ℃, filtering an ultrasonic product by using a 10-micron pore size filter, collecting filtrate, fully mixing the filtrate with the pomegranate juice obtained in the step 2, adding trisodium ethylenediamine tetraacetic acid according to the mass ratio of 1: 0.01-0.05, performing 40 revolutions per minute, and stirring the mixture for 20-30 minutes to obtain a mixed solution.
(4) Preparing fermentation liquor: adding glutamine into the mixed liquid obtained in the step 3 according to the mass ratio of 1: 0.01-0.03, adding glucose to adjust the sugar content to 16-20%, and adding sodium citrate according to the mass ratio of 1:0.2 to adjust the pH value to 5.0-5.5.
(5) Fermentation: pouring the fermentation liquor into a thoroughly sterilized fermentation tank, adding yeast according to the mass ratio of 1:0.01, and fermenting at a constant temperature of 26-28 ℃ at a stirring speed of 100-150 r/min for 8 days.
(6) Clarification: and filtering the fermentation liquor by using a 100-mesh filter screen to remove impurities, and then centrifuging by using a low-speed centrifuge at 500-800 rpm to remove precipitates.
(7) Concentration: concentrating the clear liquid by using a freeze concentrator, wherein the concentration cycle is as follows: firstly, reducing the temperature to 0-4 ℃ for 20-30 hours, removing ice crystals at-4-10 ℃ for 10-20 hours, and removing the ice crystals to obtain concentrated solution.
(8) And (3) ultrafiltration sterilization: and (4) sterilizing and filtering the concentrated solution obtained in the step (7) by using a 0.45 mu m sterilizing and filtering membrane to obtain the pomegranate essence extract.
The invention also provides a preparation method of the pomegranate essence-containing whitening and moisturizing mask, which comprises the following steps:
1. putting deionized water, jojoba oil, nicotinamide, potassium salt of azelaic acid amino acid, betaine, chlorphenesin and octyl polymethylsiloxane into a stirrer, and stirring for 20-30 minutes at the temperature of 60-80 ℃ at 800-1500 rpm to obtain a mixture A.
2. Putting glycerol, 2-methyl-1, 3-propylene glycol, water-soluble ceramide, sodium hyaluronate, phenoxyethanol, triethanolamine and bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 rpm to obtain a mixture B.
3. And adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding carbomer and natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
5. After sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
Compared with the prior art, the invention has the beneficial effects that:
1. the whitening and moisturizing essence contains various safe and effective whitening and moisturizing nutritional ingredients, and is particularly added with specially-made natural plant pomegranate essence, so that the whitening and moisturizing essence is richer and more natural in nutritional ingredients, easy to absorb and free of side effects. The facial mask essence is subjected to sufficient emulsification and nano treatment, so that essence molecules reach a nano level, a super-permeation effect is generated, the absorption rate of the skin surface can be greatly improved, the skin problem caused by accumulation of a large amount of nutrient components is avoided, and the using effect of the essence facial mask is remarkably improved.
2. The biological fiber prepared by natural fermentation of acetobacter xylinum is used as the mask base material, and compared with a common cloth-woven mask, the biological fiber mask has the advantages that the mask base material has super-strong skin-friendly property and the covering capability of being stuck into wrinkles and deep in skin dunes, the mask effect can be improved, the biological fiber mask can be tightly stuck to the skin and cannot fall off, the absorption rate of the mask is greatly improved, and the optimal using effect is achieved.
Detailed Description
Example 1
1. Putting 87 parts of deionized water, 7 parts of jojoba oil, 0.9 part of nicotinamide, 6 parts of potassium salt of azelaic acid amino acid, 1.9 parts of betaine, 0.1 part of chlorphenesin and 8 parts of octyl polymethylsiloxane into a stirrer, and stirring for 20-30 minutes at the temperature of 60-80 ℃ at 800-1500 rpm to obtain a mixture A.
2. Putting 7 parts of glycerol, 9 parts of 2-methyl-1, 3-propylene glycol, 3 parts of water-soluble ceramide, 0.3 part of sodium hyaluronate, 0.15 part of phenoxyethanol, 0.06 part of triethanolamine and 0.1 part of bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. And adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding 0.07 part of carbomer and 11 parts of natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
5. After sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
Example 2
1. 90 parts of deionized water, 5 parts of jojoba oil, 1 part of nicotinamide, 4 parts of potassium salt of azelaic acid amino acid, 1.5 parts of betaine, 0.2 part of chlorphenesin and 6 parts of octyl polymethylsiloxane are placed into a stirrer and stirred for 20-30 minutes at the temperature of 60-80 ℃ at 800-1500 revolutions per minute to obtain a mixture A.
2. Putting 10 parts of glycerol, 8 parts of 2-methyl-1, 3-propylene glycol, 4 parts of water-soluble ceramide, 0.2 part of sodium hyaluronate, 0.1 part of phenoxyethanol, 0.07 part of triethanolamine and 0.08 part of bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. And adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding 0.1 part of carbomer and 12 parts of natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
5. After sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
Example 3
1. Putting 83 parts of deionized water, 8 parts of jojoba oil, 0.6 part of nicotinamide, 5 parts of potassium salt of azelaic acid amino acid, 1.98 parts of betaine, 0.1 part of chlorphenesin and 4 parts of octyl polymethylsiloxane into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 rpm to obtain a mixture A.
2. Putting 5 parts of glycerol, 7 parts of 2-methyl-1, 3-propylene glycol, 5 parts of water-soluble ceramide, 0.2 part of sodium hyaluronate, 0.2 part of phenoxyethanol, 0.1 part of triethanolamine and 0.05 part of bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. And adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding 0.05 part of carbomer and 10 parts of natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
5. After sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
Example 4
1. Putting 90 parts of deionized water, 4 parts of jojoba oil, 0.8 part of nicotinamide, 3 parts of azelaic acid amino acid potassium salt, 2 parts of betaine, 0.3 part of chlorphenesin and 5 parts of octyl polymethylsiloxane into a stirrer, and stirring for 20-30 minutes at the temperature of 60-80 ℃ at 800-1500 rpm to obtain a mixture A.
2. Putting 7 parts of glycerol, 5 parts of 2-methyl-1, 3-propylene glycol, 4 parts of water-soluble ceramide, 0.3 part of sodium hyaluronate, 0.3 part of phenoxyethanol, 0.05 part of triethanolamine and 0.07 part of bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. And adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding 0.07 part of carbomer and 9 parts of natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
5. After sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
Example 5
1. Putting 88 parts of deionized water, 7 parts of jojoba oil, 0.5 part of nicotinamide, 5 parts of potassium salt of azelaic acid amino acid, 1.5 parts of betaine, 0.2 part of chlorphenesin and 10 parts of octyl polymethylsiloxane into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 rpm to obtain a mixture A.
2. Putting 6 parts of glycerol, 8 parts of 2-methyl-1, 3-propylene glycol, 3 parts of water-soluble ceramide, 0.15 part of sodium hyaluronate, 0.1 part of phenoxyethanol, 0.07 part of triethanolamine and 0.08 part of bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. And adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding 0.06 part of carbomer and 10 parts of natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
5. After sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
Example 6
1. Putting 85 parts of deionized water, 6 parts of jojoba oil, 1 part of nicotinamide, 6 parts of azelaic acid amino acid potassium salt, 1.7 parts of betaine, 0.3 part of chlorphenesin and 4 parts of octyl polymethylsiloxane into a stirrer, and stirring for 20-30 minutes at the temperature of 60-80 ℃ at 800-1500 rpm to obtain a mixture A.
2. Putting 9 parts of glycerol, 8 parts of 2-methyl-1, 3-propylene glycol, 34 parts of water-soluble ceramide, 0.1 part of sodium hyaluronate, 0.15 part of phenoxyethanol, 0.05 part of triethanolamine and 0.05 part of bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. And adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding 0.1 part of carbomer and 12 parts of natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
5. After sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
Mask moisturizing Performance test
18 test subjects with no obvious difference between skin types and skin moisture contents were selected, the skin was cleaned for 10 minutes, and then the skin was applied for 25 minutes in a group of 3 test subjects using examples 1 to 6 under the conditions of room temperature and relative humidity of 80 to 90%, and the skin moisture value was measured with a skin moisture tester before the skin was used as a product, immediately after the use, and 1 hour after the use.
| Time of day | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 |
| Before use | 34～38 | 36～40 | 35～41 | 33～39 | 37～40 | 36～39 |
| Immediately after use | 81～83 | 79～81 | 76～78 | 77～81 | 77～80 | 78～80 |
| After 1 hour of use | 71～75 | 69～72 | 67～70 | 68～71 | 67～71 | 69～71 |
Skin improvement assay
18 test persons with no obvious difference between skin types and skin moisture content are selected, the test persons are applied for 25 minutes by using the test examples 1-6 in every 3 test persons after the skin is cleaned for 10 minutes under the conditions of room temperature and relative humidity of 80-90%, and the skin types of the test persons before and after the test persons use the product are detected by using a skin type tester to compare the change of the skin types.
| Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | |
| Pigment value before use | 1.8～3 | 2～2.9 | 2～3 | 1.9～3 | 2.1～2.9 | 2.1～3 |
| Pigment value after use | 0.4～1.1 | 0.7～1 | 0.6～1.2 | 0.6～1 | 0.8～1.2 | 0.7～1.1 |
| Pre-use skin color value | 5.7～7 | 5.9～7 | 6～7.2 | 6.1～7 | 5.7～7.1 | 5.9～7.1 |
| After use skin color value | 8.5～9.4 | 8.4～9 | 8.5～9.1 | 8～8.7 | 7.9～8.9 | 8.4～9.2 |
| Degree of improvement of skin texture before and after use | 12%～16% | 10%～13% | 10%～14% | 11%～13% | 10%～14% | 10%～12% |
The data show that after the product disclosed by the invention is used, the moisture content data of the skin is very high, the moisturizing effect is very good, the indexes of the pigment value, the skin color value and the texture improvement rate are all remarkably improved, and the absorption effect of the mask is good, so that the beneficial technical achievements of the invention are improved.
The foregoing examples are merely illustrative of preferred embodiments of the present invention, and the scope of the present invention is not limited thereto, and the appended claims are intended to claim as broad a scope as can be conceived and the embodiments presented herein are merely illustrative of selected embodiments in accordance with all possible combinations of embodiments. Accordingly, it is applicants' intention that the appended claims are not to be limited by the choice of examples illustrating features of the invention. The technical solution and the inventive concept thereof according to the present invention should be equally replaced or changed within the protection scope of the present invention.
Claims (6)
1. The pomegranate essence-containing whitening and moisturizing mask comprises the following preparation raw materials: a biological fiber mask base material, a pearlized film and essence;
the essence is prepared from the following raw materials:
80-90 parts of deionized water
2-9 parts of jojoba oil
0.5-1 part of nicotinamide
3-6 parts of potassium azelaic acid amino acid salt
1.5-2 parts of betaine
0.1 to 0.3 portion of chlorphenesin
3-10 parts of octyl polymethylsiloxane
3-10 parts of glycerol
5-9 parts of 2-methyl-1, 3-propanediol
2-5 parts of water-soluble ceramide
0.1-0.3 part of sodium hyaluronate
0.1 to 0.3 portion of phenoxyethanol
0.05 to 0.1 portion of triethanolamine
0.05-0.1 part of bisabolol
0.05-0.1 part of carbomer
8-12 parts of natural plant essence extract;
the glycerol is biological refined glycerol; the natural plant essence extract is a pomegranate essence extract;
the preparation method of the pomegranate essence extract comprises the following steps:
(1) screening and shelling: selecting fully mature and plump pomegranate fruits, removing rotten, deteriorated and damaged bad fruits, washing with clear water with the volume more than 3 times, drying in the shade, and shelling and peeling by using a pomegranate peeler;
(2) crushing: crushing pomegranate pulp and pomegranate seeds by using a crusher, setting the rotation speed of the crusher to be 100-150 rpm, selecting a filter screen with the diameter of 1-3 mm, fully crushing the pulp, and separately collecting pomegranate pulp residues and pomegranate juice for later use;
(3) ultrasonic: drying the pomegranate rind at the temperature of 30-40 ℃, crushing the pomegranate rind by using a crusher, mixing the pomegranate rind with the pulp residues, adding distilled water according to the mass ratio of 1:10, uniformly mixing and stirring the mixture for 20 minutes, putting the mixture into an ultrasonic cell crusher, performing ultrasonic treatment at the ultrasonic frequency of 22KHz for 40-60 minutes at the temperature of 0-10 ℃, filtering an ultrasonic product by using a 10-micron pore size filter, collecting filtrate, fully mixing the filtrate with the pomegranate juice obtained in the step 2, adding trisodium ethylenediamine tetraacetic acid according to the mass ratio of 1: 0.01-0.05, performing 40 revolutions per minute, and stirring the mixture for 20-30 minutes to obtain a mixed solution;
(4) preparing fermentation liquor: adding glutamine into the mixed liquid obtained in the step 3 according to the mass ratio of 1: 0.01-0.03, adding glucose to adjust the sugar content to 16-20%, and adding sodium citrate according to the mass ratio of 1:0.2 to adjust the pH value to 5.0-5.5;
(5) fermentation: pouring the fermentation liquor into a thoroughly sterilized fermentation tank, adding saccharomycetes according to the mass ratio of 1:0.01, and fermenting at a constant temperature of 26-28 ℃ at a stirring speed of 100-150 rpm for 8 days;
(6) clarification: filtering the fermentation liquor by using a 100-mesh filter screen to remove impurities, and then centrifuging by using a low-speed centrifuge at 500-800 rpm to remove precipitates;
(7) concentration: concentrating the clear liquid by using a freeze concentrator, wherein the concentration cycle is as follows: firstly, reducing the temperature to 0-4 ℃, 20-30 hours, removing ice crystals, and removing the ice crystals at-4-10 ℃ for 10-20 hours to obtain concentrated solution;
(8) and (3) ultrafiltration sterilization: and (4) sterilizing and filtering the concentrated solution obtained in the step (7) by using a 0.45 mu m sterilizing and filtering membrane to obtain the pomegranate essence extract.
2. The pomegranate essence-containing whitening and moisturizing mask as claimed in claim 1, wherein the essence is prepared from the following raw materials in parts by weight:
83-88 parts of deionized water
4-8 parts of jojoba oil
0.7-1 part of nicotinamide
4-6 parts of potassium azelaic acid amino acid salt
1.7-2 parts of betaine
0.1 to 0.2 portion of chlorphenesin
5-9 parts of octyl polymethylsiloxane
6-9 parts of glycerol
6-9 parts of 2-methyl-1, 3-propanediol
3-5 parts of water-soluble ceramide
0.2-0.3 part of sodium hyaluronate
0.1-0.2 part of phenoxyethanol
0.05 to 0.08 portion of triethanolamine
0.07-0.1 part of bisabolol
0.07-0.09 part of carbomer
9-12 parts of natural plant essence extract.
3. The pomegranate essence-containing whitening and moisturizing mask as claimed in claim 1, wherein the essence is prepared from the following raw materials in parts by weight:
87 parts of deionized water
Jojoba oil 7 parts
0.9 portion of nicotinamide
6 parts of potassium salt of azelaic acid amino acid
1.9 portions of betaine
Chlorphenesin 0.1 part
Octyl polymethylsiloxane 8 parts
7 parts of glycerol
9 parts of 2-methyl-1, 3-propanediol
Water soluble ceramide 3 portions
0.3 portion of sodium hyaluronate
0.15 part of phenoxyethanol
Triethanolamine 0.06 parts
0.1 part of bisabolol
Carbomer 0.07 part
11 parts of natural plant essence extract.
4. The preparation method of the pomegranate essence-containing whitening and moisturizing mask as claimed in claim 1, comprising the following steps:
(1) putting deionized water, jojoba oil, nicotinamide, potassium salt of azelaic acid amino acid, betaine, chlorphenesin and octyl polymethylsiloxane into a stirrer, and stirring for 20-30 minutes at the temperature of 60-80 ℃ at 800-1500 rpm to obtain a mixture A;
(2) putting glycerol, 2-methyl-1, 3-propylene glycol, water-soluble ceramide, sodium hyaluronate, phenoxyethanol, triethanolamine and bisabolol into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 rpm to obtain a mixture B;
(3) adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding carbomer and natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain an emulsion C;
(4) carrying out nanocrystallization on the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure to be 150-200 Mpa, and homogenizing for 3 times to finally obtain essence;
(5) after sterilizing and irradiating the biological fiber mask base material and the matched pearlized film, attaching, folding, filling into an aluminum foil bag, conveying to a packaging production line, injecting essence into a filling machine, sterilizing and irradiating again, and sealing by a sealing machine.
5. The pomegranate essence-containing whitening and moisturizing mask as claimed in claim 1, wherein the bio-fiber mask base material is a material with 12-position cut design; the pearlized film is made of a material with 12-position veneering cutting design.
6. The preparation method of the pomegranate essence-containing whitening and moisturizing mask as claimed in claim 4, wherein the stirring speed in the step 1 and the step 2 is 800-1500 rpm, the stirring temperature is 60-80 ℃, and the stirring time is 20-30 minutes; step 3, homogenizing at 2000-3000 r/min for 10-20 s; step 3, mixing speed is 200-300 r/min, mixing temperature is normal temperature, and mixing time is 10-20 minutes; and step 4, setting the pressure to be 150-200 Mpa, and homogenizing for 3 times.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711439770.6A CN107982070B (en) | 2017-12-27 | 2017-12-27 | Whitening and moisturizing facial mask containing pomegranate essence and preparation method thereof |
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| CN201711439770.6A CN107982070B (en) | 2017-12-27 | 2017-12-27 | Whitening and moisturizing facial mask containing pomegranate essence and preparation method thereof |
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| CN107982070B true CN107982070B (en) | 2020-12-29 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102274146A (en) * | 2011-08-10 | 2011-12-14 | 唯美度科技（北京）有限公司 | Whitening and moisturizing toner |
| CN104473812A (en) * | 2014-11-28 | 2015-04-01 | 海南海之润生物工程有限公司 | Biological fiber facial mask |
| CN105878102A (en) * | 2015-04-24 | 2016-08-24 | 四川福能源生物科技有限公司 | Facial mask containing punica granatum fruit extract and preparation method of facial mask |
| CN106343563A (en) * | 2016-08-29 | 2017-01-25 | 赵彦军 | Preparing method of pomegranate enzyme |
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2017
- 2017-12-27 CN CN201711439770.6A patent/CN107982070B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102274146A (en) * | 2011-08-10 | 2011-12-14 | 唯美度科技（北京）有限公司 | Whitening and moisturizing toner |
| CN104473812A (en) * | 2014-11-28 | 2015-04-01 | 海南海之润生物工程有限公司 | Biological fiber facial mask |
| CN105878102A (en) * | 2015-04-24 | 2016-08-24 | 四川福能源生物科技有限公司 | Facial mask containing punica granatum fruit extract and preparation method of facial mask |
| CN106343563A (en) * | 2016-08-29 | 2017-01-25 | 赵彦军 | Preparing method of pomegranate enzyme |
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