CN107307245A - A kind of beverage with antioxidation function and preparation method thereof - Google Patents

A kind of beverage with antioxidation function and preparation method thereof Download PDF

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CN107307245A
CN107307245A CN201710470351.2A CN201710470351A CN107307245A CN 107307245 A CN107307245 A CN 107307245A CN 201710470351 A CN201710470351 A CN 201710470351A CN 107307245 A CN107307245 A CN 107307245A
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juice
black garlic
beverage
preparation
collybia albuminosa
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李湘利
刘静
吴淑华
周生稳
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Jining University
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Jining University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/84Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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Abstract

Present invention belongs to food processing technology field, specifically related to a kind of beverage with antioxidation function and preparation method thereof, the present invention is with collybia albuminosa juice, black garlic juice is primary raw material, to collybia albuminosa juice, the composite juice of black garlic juice is using ultrasonic assistant and complex enzyme Enzymatic Extraction, oxidation-resistant active ingredient and nutritional ingredient in using pure water as solvent extraction collybia albuminosa juice and black garlic juice, it is formulated again, degassing, homogeneous, a kind of light/dark balance that the processes such as sterilization are prepared from, have the composite beverage of collybia albuminosa and the peculiar taste of black garlic concurrently, sour and sweet palatability, mouthfeel is soft, it is nutritious, rich in polysaccharide, polyphenol, protein and polypeptide, saponin(e, allicin, superoxide dismutase, melanoidin, the oxidation-resistant active ingredients such as dietary fiber, radicals scavenging effect is good, with very strong anti-oxidation efficacy, anti-aging, production cost is low, market prospects are considerable.

Description

A kind of beverage with antioxidation function and preparation method thereof
Technical field
Present invention belongs to food processing technology field, and in particular to a kind of beverage with antioxidation function and its preparation side Method.
Background technology
Collybia albuminosa also known as ant fir, shredded chicken mushroom, often and symbiosis of termite, containing protein needed by human, fat, amino acid, The mineral element such as various vitamins and calcium, potassium, phosphorus and polysaccharide, polyphenol isoreactivity composition, with nourishing generate fluid, anti-aging, resist and swell The multiple pharmacological effect such as knurl, antifatigue and antioxidation activity, have unique effects in terms of cancer-resisting, hypoglycemic.
Black garlic is using fresh garlic as raw material, under the conditions of hot and humid, through enzyme catalysis and Maillard reaction, belt leather Ferment a kind of food being prepared from, nutritious, and mouthfeel is unique.Act on by fermentation, the composition of former garlic changes, greatly Garlic odour taste is removed, and strengthens original physiologically active.The main functional component content of black garlic is obviously higher than Common garlic, its super oxygen Compound dismutase activity is higher by more than 10 times than fresh garlic, and polyphenol content is higher by more than 5 times.Black garlic have it is anti-oxidant, prolong Slow aging, raising immunity of organisms, bactericidal antiphlogistic, suppression tumour isoreactivity.But black garlic product level is single, and sugar content compared with Height, it is easily putrid and deteriorated.In recent years, black garlic head, black garlic piece, black garlic preserved fruit, black garlic mud, black garlic sauce, A black garlic vinegar and a method for preparing the same, black garlic capsule etc. Product is listed successively.Various black garlic deep processed products enrich black garlic market, promote garlic industry development.Black garlic juice The appearance of beverage enriches the kind of beverage, but (Li Xin, Zhang Min, Zhang Liming wait black garlics to existing black garlic beverage bitter taste The determination of drink sterilization condition and its influence research [J] food security quality testing journals to physicochemical property, 2014, (11): 3711-3717), bad taste experience is brought when drinking, the existing preparation technology to black garlic juice is generally flooding, used This method is that recovery rate is relatively low to black garlic juice extraction defect, it is impossible to the nutrition in black garlic and functional component is effectively leached, institute Obtain the unstable easy layering and precipitating of black garlic juice.
Drinks are one of conventional foods in people's life, and with natural in color, mouthfeel is smooth, local flavor is salubrious, shape The uniform drinks of state will possess broader market prospects.Collybia albuminosa, black garlic are prepared to a kind of function drink of antioxidation Material integrates the Nutrition and health function of raw material, and its production Technology meets current food industries development trend.
The content of the invention
Present invention aims at provide a kind of beverage with antioxidation function, using collybia albuminosa juice, black garlic juice as primary raw material, antioxygen The property changed is strong, anti-aging, while having unique flavor, the features such as nutritious, color and luster is good, product stability is high;The present invention is also The preparation method of the beverage with antioxidation function is provided.
Beverage with antioxidation function of the present invention, includes the raw material of following parts by weight:It is 60~80 parts of collybia albuminosa juice, black 20~40 parts of garlic juice, 0.5~2.0 part of complex enzyme, 3~6 parts of white granulated sugar, 0.1 part of citric acid, 0.1 part of ascorbic acid, salt 0.3 ~0.4 part, 0.1~0.2 part of compound stabilizer, 1 part of cycloheptaamylose, 0.04 part of potassium sorbate.
The complex enzyme is cellulase and pectase by weight 1:1 mixes.
The compound stabilizer is xanthans and CMC by weight 1:1 mixes.
The preparation method of beverage with antioxidation function of the present invention, comprises the following steps:
1) preparation of collybia albuminosa juice:Select it is fleshy hypertrophy, without rotting to go mouldy, fresh collybia albuminosa, cleaned, blanching, beat Gained after slurry, filtering;
2) preparation of black garlic juice:
21) black garlic pre-treatment:Select it is fresh, without rotting to go mouldy, fleshy hypertrophy black garlic, exocuticle is peeled, gone simultaneously Except the debris for being attached to black garlic surface, then black garlic is cleaned up with 0.9% saline solution;
22) slurrying:Pre-treatment black garlic is pressed into material-water ratio 1:Precrushing is carried out after 1~2 addition pure water, black garlic slurries are obtained;
23) hot dipping is carried:Black garlic slurries are extracted in two times using 0.5% citric acid solution, it is 1 that material-water ratio is extracted first:3 ~5, second of extraction material-water ratio is 1:1~3, each extraction temperature is 60-65 DEG C, 10~20min of extraction time, merges extraction Liquid;
24) gained leaching liquor is produced into black garlic juice using the filter-cloth filtering of 200 mesh;
3) composite juice is ultrasonically treated:By step 1) gained collybia albuminosa juice and step 2) gained black garlic juice is by weight being 1.5 ~4:1 mixes to obtain composite juice, and composite juice is extracted using ultrasonic assistant, and ultrasonic power is 300~1000W, and ultrasonic temperature 35~ 60 DEG C, 10~40min of ultrasonic time;
4) composite juice complex enzyme zymohydrolysis:Ultrasonically treated composite juice pH=4.5~5.5 are adjusted, complex enzyme is added, complex enzyme is Cellulase is with pectase by weight 1:1 is mixed, and 30~90min is digested at 35~50 DEG C, promotes the work in raw material The leaching of property material;
5) post-process:By step 4) composite juice after enzymolysis through filtering, allotment, vacuum outgas, homogeneous, sterile filling, kill Drinks are produced after bacterium, cooling;
Wherein:
Step 5) in allotment operation be:White granulated sugar, the lemon for calculating parts by weight are added at 90~95 DEG C to filtrate Acid, ascorbic acid, salt, fully dissolving are mixed, and add the compound stabilizer for calculating parts by weight, cycloheptaamylose and mountain Potassium sorbate, glue grinds 3~5min and completes mixing preparation in colloid mill.
Step 1) in clean after collybia albuminosa by material water quality ratio be 1:5 add 90~95 DEG C of pure water, blanching 5min.
Step 5) in filtering operation be:Composite juice uses 300 mesh filter cloth pre-filterings first, then uses plate and frame filter press mistake Filter.
Step 5) in the process conditions of vacuum outgas be:Taken off under conditions of 80~85 DEG C of vacuum 0.01MPa and temperature Gas.
Step 5) in the operation of homogeneous be:The mixeding liquid temperature of vacuum outgas is adjusted to 70~80 DEG C, in 15~35MPa 5~30min of homogeneous.
Step 5) in sterilization process conditions be:90~100 DEG C of sterilization temperature, 20~25min of sterilizing time or uses 121 DEG C sterilization 10~20min.
Step 22) black garlic carries out precrushing using high-speed tissue mashing machine or beater or slurry-residue separation refining machine.
Beverage with antioxidation function of the present invention, using collybia albuminosa juice, black garlic juice as primary raw material, to collybia albuminosa juice, black The composite juice of garlic juice is using ultrasonic assistant and complex enzyme Enzymatic Extraction, using pure water as solvent extraction collybia albuminosa juice and black garlic juice In oxidation-resistant active ingredient and nutritional ingredient, a kind of then somber that the process such as formulated, degassing, homogeneous, sterilization is prepared from Color, has the composite beverage of collybia albuminosa and the peculiar taste of black garlic concurrently, and drinks is had higher anti-oxidation efficacy, prolongs Slow aging.
The present invention compared with prior art, has the advantages that.
(1) present invention is mixed with the wind in drinks, collybia albuminosa juice using black garlic juice and collybia albuminosa juice as activated feedstock Taste material can suppress the bitter taste of black garlic juice, and gained drinks outward appearance is in light/dark balance, and taste is unique, and mouthfeel and taste are substantially excellent In black garlic juice, itself local flavor of collybia albuminosa juice, but still retain certain collybia albuminosa and the flavour of black garlic, finished acid is comfortable Mouth, mouthfeel are soft, and its physical and chemical index and microbiological indicator meet relevant national standard;
(2) present invention passes through the protein and polypeptide in collybia albuminosa, polysaccharide, dietary fiber, saponin(e etc. and the class in black garlic The composition complementation of the effects such as black essence, amino acid, superoxide dismutase, polyphenol, for essential amino acid, the group ammonia in collybia albuminosa Acid, threonine, lysine and black garlic methionine, isoleucine can complementary surplus and deficiency, the required amino that can be enriched to human body offer Acid, often drunk it is aid digestion, improve a poor appetite, fatigue-relieving, strengthen immunity, preventing cold, softening blood vessel and blood fat-reducing blood pressure-decreasing The effects such as;
(3) present invention uses ultrasonic assistant and complex enzyme Enzymatic Extraction to the composite juice of collybia albuminosa juice, black garlic juice, passes through Efficient cavitation effect and mechanism destruction cell membrane are produced, promotes the substance decompositions such as pectin, cellulose, is made in raw material effectively Composition separate out within the relatively short time, effectively prevent active component and is oxidized, while crushing juice rate is significantly improved, and Finished product is stable without layering, and process conditions are gentle, workable;
(4) present invention combines the oxidation-resistant active ingredient of collybia albuminosa and black garlic together, and experiment measures the drinks pair DPPH free radical scavenging activities are up to 75%~90%, to ultra-oxygen anion free radical clearance rate up to 22%~35%, to hydroxyl Free radical scavenging activity is up to 55%~80%, to hydrogen peroxide clearance rate up to 50%~75%, to ABTS free radical scavenging activities Up to 75%~100%, illustrate that this product has very strong anti-oxidation efficacy, there is anti-aging.
Embodiment
With reference to embodiment, the present invention will be further described.
Embodiment 1
Beverage with antioxidation function described in the present embodiment, includes the raw material of following parts by weight:60 parts of collybia albuminosa juice, black garlic (cellulase and pectase are by weight 1 for 40 parts of juice, complex enzyme:1 mixes) 1.0 parts, 5 parts of white granulated sugar, citric acid 0.1 (xanthans and CMC are by weight 1 for part, 0.1 part of ascorbic acid, 0.3 part of salt, compound stabilizer:1 mixes) 0.1 part, β- 1.0 parts of cyclodextrine, 0.04 part of potassium sorbate.
The preparation method of beverage with antioxidation function described in the present embodiment, comprises the following steps:
(1) preparation of collybia albuminosa juice:1. select:Selection is fleshy hypertrophy, nothing is rotted goes mouldy, fresh collybia albuminosa;2. clean: Collybia albuminosa after selecting first is soaked after 5min in cold water, cleans surface dirt and debris;3. blanching:By the collybia albuminosa after cleaning Compare 1 by material water quality:5 add 90 DEG C of pure water, blanching 5min;4. it is beaten:Milled while hot with slurry-residue separation refining machine, repeatedly Mill 3 times, gained slurries grind 5min with colloid mill again;5. filter:Slurry after milling is obtained into chicken fir with 200 mesh filter-cloth filterings Bacterium juice;
(2) preparation of black garlic juice:1. select:Selection is fresh, nothing is rotted goes mouldy, fleshy hypertrophy black garlic;2. remove the peel:Will be black Garlic exocuticle is peeled, while removing the debris for being attached to black garlic surface;3. clean:Black garlic is cleaned dry with 0.9% saline solution Only;4. slurrying:Raw material black garlic presses material-water ratio 1:1 addition pure water, precrushing is carried out using high-speed tissue mashing machine, obtains black garlic slurry Liquid;5. hot dipping is carried:Extracted in two times with 0.5% citric acid solution, it is 1 that material-water ratio is extracted first:3, the 2nd time extraction material-water ratio is 1:3, each extraction temperature is 60 DEG C, extraction time 20min, merges leaching liquor;6. filter:Mixed leaching liquor is used The filter-cloth filtering of 200 mesh produces black garlic juice;
(3) preparation of composite juice with it is ultrasonically treated:Gained collybia albuminosa juice and black garlic juice are mixed by weight, using super Sound wave assisted extraction, ultrasonic power is 300W, 35 DEG C of ultrasonic temperature, ultrasonic time 40min;
(4) complex enzyme zymohydrolysis:Adjust pH=5.0, the complex enzyme assisted extraction for plus 1.0%, complex enzyme be cellulase with Pectase presses 1:1 mixing, digests 30min at 50 DEG C, promotes the leaching of the active material in raw material;
(5) filter:Filtered using 300 mesh filter cloth pre-filterings, then with plate and frame filter press, obtain filtrate;
(6) allocate:Under the conditions of 95 DEG C, white granulated sugar, the lemon for calculating parts by weight are added to filtrate obtained by step (5) Acid, ascorbic acid, salt, fully dissolving are mixed, and add the compound stabilizer for calculating parts by weight, cycloheptaamylose and mountain Potassium sorbate, glue mill 3min completes mixing preparation in colloid mill;
(7) vacuum outgas:The good bland of mixing preparation is taken off under conditions of 80 DEG C of vacuum 0.01MPa and temperature Gas;
(8) homogeneous:Bland temperature is adjusted to 75 DEG C, in 25MPa homogeneous 25min;
(9) sterile filling:Beverage filling after homogeneous is in the bottle for cleaning, disinfecting;
(10) sterilization and cooling:Sterilize, cover, 90 DEG C of sterilization temperature, sterilizing time 25min while hot after filling, cooling is Obtain drinks.
Embodiment 2
Beverage with antioxidation function described in the present embodiment, includes the raw material of following parts by weight:75 parts of collybia albuminosa juice, black garlic (cellulase and pectase are by weight 1 for 25 parts of juice, complex enzyme:1 mixes) 2 parts, 3 parts of white granulated sugar, 0.1 part of citric acid, (xanthans and CMC are by weight 1 for 0.1 part of ascorbic acid, 0.4 part of salt, compound stabilizer:1 mixes) 0.2 part, β-ring 1.0 parts of shape dextrin, 0.04 part of potassium sorbate.
The preparation method of beverage with antioxidation function described in the present embodiment, comprises the following steps:
(1) preparation of collybia albuminosa juice:1. select:Selection is fleshy hypertrophy, nothing is rotted goes mouldy, fresh collybia albuminosa;2. clean: Collybia albuminosa after selecting first is soaked after 5min in cold water, cleans surface dirt and debris;3. blanching:By the collybia albuminosa after cleaning Compare 1 by material water quality:5 add boiled pure water, in 92 DEG C of blanching 5min;4. it is beaten:Ground while hot with slurry-residue separation refining machine Mill, mills 3 times repeatedly, and gained slurries grind 3min with colloid mill again;5. filter:By the slurry after milling with 200 mesh filter cloth mistakes Filter to obtain collybia albuminosa juice;
(2) preparation of black garlic juice:1. select:Selection is fresh, nothing is rotted goes mouldy, fleshy hypertrophy black garlic;2. remove the peel:Will be black Garlic exocuticle is peeled, while removing the debris for being attached to black garlic surface;3. clean:Black garlic is cleaned dry with 0.9% saline solution Only;4. slurrying:Raw material black garlic presses material-water ratio 1:1.5 addition pure water, carry out precrushing using beater, obtain black garlic slurries;⑤ Hot dipping is carried:Extracted in two times with 0.5% citric acid solution, it is 1 that material-water ratio is extracted first:5, the 2nd time extraction material-water ratio is 1:1, Each extraction temperature is 65 DEG C, extraction time 10min, merges leaching liquor;6. filter:Mixed leaching liquor is used into 200 mesh Filter-cloth filtering produce black garlic juice;
(3) preparation of composite juice with it is ultrasonically treated:Gained collybia albuminosa juice and black garlic juice are mixed by weight, using super Sound wave assisted extraction, ultrasonic power is 800W, 50 DEG C of ultrasonic temperature, ultrasonic time 20min;
(4) complex enzyme zymohydrolysis:PH=4.5, plus complex enzyme assisted extraction are adjusted, complex enzyme is that cellulase is pressed with pectase 1:1 mixing, digests 60min at 45 DEG C, promotes the leaching of the active material in raw material;
(5) filter:Filtered using 300 mesh filter cloth pre-filterings, then with plate and frame filter press, obtain filtrate;
(6) allocate:Under the conditions of 92 DEG C, white granulated sugar, the lemon for calculating parts by weight are added into filtrate obtained by step (5) Lemon acid, ascorbic acid, salt, fully dissolving mix, add the compound stabilizer for calculating parts by weight, cycloheptaamylose and Potassium sorbate, glue mill 4min completes mixing preparation in colloid mill;
(7) vacuum outgas:The good bland of mixing preparation is taken off under conditions of 85 DEG C of vacuum 0.01MPa and temperature Gas;
(8) homogeneous:Bland temperature is adjusted to 70 DEG C, in 35MPa homogeneous 5min;
(9) sterile filling:Beverage filling after homogeneous is in the bottle for cleaning, disinfecting;
(10) sterilization and cooling:Sterilize, cover, 100 DEG C of sterilization temperature, sterilizing time 20min while hot after filling, cooling is Obtain drinks.
Embodiment 3
Beverage with antioxidation function described in the present embodiment, includes the raw material of following parts by weight:80 parts of collybia albuminosa juice, black garlic (cellulase and pectase are by weight 1 for 20 parts of juice, complex enzyme:1 mixes) 0.5 part, 6 parts of white granulated sugar, citric acid 0.1 (xanthans and CMC are by weight 1 for part, 0.1 part of ascorbic acid, 0.35 part of salt, compound stabilizer:1 mixes) 0.15 part, 1.0 parts of cycloheptaamylose, 0.04 part of potassium sorbate.
The preparation method of beverage with antioxidation function described in the present embodiment, comprises the following steps:
(1) preparation of collybia albuminosa juice:1. select:Selection is fleshy hypertrophy, nothing is rotted goes mouldy, fresh collybia albuminosa;2. clean: Collybia albuminosa after selecting first is soaked after 5min in cold water, cleans surface dirt and debris;3. blanching:By the collybia albuminosa after cleaning Compare 1 by material water quality:5 add boiled pure water, in 95 DEG C of blanching 5min;4. it is beaten:Ground while hot with slurry-residue separation refining machine Mill, mills 3 times repeatedly, and gained slurries grind 4min with colloid mill again;5. filter:By the slurry after milling with 200 mesh filter cloth mistakes Filter to obtain collybia albuminosa juice;
(2) preparation of black garlic juice:1. select:Selection is fresh, nothing is rotted goes mouldy, fleshy hypertrophy black garlic;2. remove the peel:Will be black Garlic exocuticle is peeled, while removing the debris for being attached to black garlic surface;3. clean:Black garlic is cleaned dry with 0.9% saline solution Only;4. slurrying:Raw material black garlic presses material-water ratio 1:2 addition pure water, precrushing is carried out using slurry-residue separation refining machine, obtains black garlic slurry Liquid;5. hot dipping is carried:Extracted in two times with 0.5% citric acid solution, it is 1 that material-water ratio is extracted first:4, the 2nd time extraction material-water ratio is 1:2, each extraction temperature is 62 DEG C, extraction time 15min, merges leaching liquor;6. filter:Mixed leaching liquor is used The filter-cloth filtering of 200 mesh produces black garlic juice;
(3) preparation of composite juice with it is ultrasonically treated:Gained collybia albuminosa juice and black garlic juice are mixed by weight, using super Sound wave assisted extraction, ultrasonic power is 1000W, 60 DEG C of ultrasonic temperature, ultrasonic time 15min;
(4) complex enzyme zymohydrolysis:PH=5.5, plus complex enzyme assisted extraction are adjusted, complex enzyme is that cellulase is pressed with pectase 1:1 mixing, digests 90min at 30 DEG C, promotes the leaching of the active material in raw material;
(5) filter:Filtered using 300 mesh filter cloth pre-filterings, then with plate and frame filter press;
(6) allocate:White granulated sugar, citric acid, ascorbic acid, the salt for calculating parts by weight are added under the conditions of 90 DEG C, Fully dissolving is mixed, and the compound stabilizer for calculating parts by weight, cycloheptaamylose and potassium sorbate is added, in colloid mill Glue mill 5min completes mixing preparation;
(6) vacuum outgas:The good bland of mixing preparation is taken off under conditions of 85 DEG C of vacuum 0.01MPa and temperature Gas;
(7) homogeneous:Beverage temperature is adjusted to 80 DEG C, in 15MPa homogeneous 30min;
(8) sterile filling:Beverage filling after homogeneous is in the bottle for cleaning, disinfecting;
(9) sterilization and cooling:Sterilize, cover while hot after filling, using 121 DEG C of sterilization 10min, cooling produces function drink Material.

Claims (10)

1. a kind of beverage with antioxidation function, it is characterised in that:Include the raw material of following parts by weight:60~80 parts of collybia albuminosa juice, 20~40 parts of black garlic juice, 0.5~2.0 part of complex enzyme, 3~6 parts of white granulated sugar, 0.1 part of citric acid, 0.1 part of ascorbic acid, salt 0.3~0.4 part, 0.1~0.2 part of compound stabilizer, 1 part of cycloheptaamylose, 0.04 part of potassium sorbate.
2. beverage with antioxidation function according to claim 1, it is characterised in that:Complex enzyme is that cellulase and pectase are pressed Weight compares 1:1 mixes.
3. beverage with antioxidation function according to claim 1, it is characterised in that:Compound stabilizer is that xanthans is pressed with CMC Weight compares 1:1 mixes.
4. a kind of preparation method of beverage with antioxidation function, it is characterised in that:Comprise the following steps:
1) preparation of collybia albuminosa juice:Select it is fleshy hypertrophy, without rotting to go mouldy, fresh collybia albuminosa, cleaned, blanching, mashing, mistake Gained after filter;
2) preparation of black garlic juice:
21) black garlic pre-treatment:Select it is fresh, without rotting to go mouldy, fleshy hypertrophy black garlic, exocuticle is peeled, while removing attached In the debris on black garlic surface, then cleaned up black garlic with 0.9% saline solution;
22) slurrying:Pre-treatment black garlic is pressed into material-water ratio 1:Precrushing is carried out after 1~2 addition pure water, black garlic slurries are obtained;
23) hot dipping is carried:Black garlic slurries are extracted in two times using 0.5% citric acid solution, it is 1 that material-water ratio is extracted first:3~5, Second of extraction material-water ratio is 1:1~3, each extraction temperature is 60~65 DEG C, 10~20min of extraction time, merges leaching liquor;
24) gained leaching liquor is produced into black garlic juice using the filter-cloth filtering of 200 mesh;
3) composite juice is ultrasonically treated:By step 1) gained collybia albuminosa juice and step 2) gained black garlic juice is 1.5~4 in mass ratio:1 Mix to obtain composite juice, composite juice is extracted using ultrasonic assistant, ultrasonic power is 300~1000W, 35~60 DEG C of ultrasonic temperature, 10~40min of ultrasonic time;
4) composite juice complex enzyme zymohydrolysis:Ultrasonically treated composite juice pH=4.5~5.5 are adjusted, complex enzyme are added, complex enzyme is fiber Plain enzyme is with pectase by weight 1:1 is mixed, and 30~90min is digested at 35~50 DEG C, promotes the active matter in raw material The leaching of matter;
5) post-process:By step 4) composite juice after enzymolysis is through filtering, allotment, vacuum outgas, homogeneous, sterile filling, sterilization, cold But drinks are produced afterwards;
Wherein:Step 5) in allotment operation be:White granulated sugar, the lemon for calculating parts by weight are added at 90~95 DEG C to filtrate Acid, ascorbic acid, salt, fully dissolving are mixed, and add the compound stabilizer for calculating parts by weight, cycloheptaamylose and mountain Potassium sorbate, glue grinds 3~5min and completes mixing preparation in colloid mill.
5. the preparation method of beverage with antioxidation function according to claim 4, it is characterised in that:Step 1) in clean after Collybia albuminosa is 1 by material water quality ratio:5 add 90~95 DEG C of pure water, blanching 5min.
6. the preparation method of beverage with antioxidation function according to claim 4, it is characterised in that:Step 5) the middle behaviour filtered As:Composite juice uses 300 mesh filter cloth pre-filterings first, then is filtered with plate and frame filter press.
7. the preparation method of beverage with antioxidation function according to claim 4, it is characterised in that:Step 5) in vacuum outgas Process conditions be:Deaerated under conditions of 80~85 DEG C of vacuum 0.01MPa and temperature.
8. the preparation method of beverage with antioxidation function according to claim 4, it is characterised in that:Step 5) in homogeneous behaviour As:The mixeding liquid temperature of vacuum outgas is adjusted to 70~80 DEG C, in 15~35MPa homogeneous, 5~30min.
9. the preparation method of beverage with antioxidation function according to claim 4, it is characterised in that:Step 5) the middle work sterilized Skill condition is:90~100 DEG C of sterilization temperature, 121 DEG C of 10~20min of sterilization of 20~25min of sterilizing time or use.
10. the preparation method of beverage with antioxidation function according to claim 4, it is characterised in that:Step 22) black garlic use High-speed tissue mashing machine or beater or slurry-residue separation refining machine carry out precrushing.
CN201710470351.2A 2017-06-20 2017-06-20 A kind of beverage with antioxidation function and preparation method thereof Pending CN107307245A (en)

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CN108783304A (en) * 2018-06-29 2018-11-13 河北科技大学 Grape skin powder and Termitomyces albuminosus with black skin composite dietary oral solution and preparation method thereof
CN110367419A (en) * 2019-08-21 2019-10-25 上海交通大学云南(大理)研究院 A kind of black garlic composite beverage and preparation method thereof

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CN108783304A (en) * 2018-06-29 2018-11-13 河北科技大学 Grape skin powder and Termitomyces albuminosus with black skin composite dietary oral solution and preparation method thereof
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