CN105878102A - Facial mask containing punica granatum fruit extract and preparation method of facial mask - Google Patents
Facial mask containing punica granatum fruit extract and preparation method of facial mask Download PDFInfo
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- CN105878102A CN105878102A CN201510200549.XA CN201510200549A CN105878102A CN 105878102 A CN105878102 A CN 105878102A CN 201510200549 A CN201510200549 A CN 201510200549A CN 105878102 A CN105878102 A CN 105878102A
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Abstract
The invention relates to a facial mask containing a punica granatum fruit extract and a preparation method of the facial mask, wherein the facial mask is prepared by blending functional cosmetic substances with water. The facial mask consists of the following raw materials: de-ionized water, glycerol, the punica granatum fruit extract, hyaluronic acid, lipoic acid, a ginkgo biloba leaf extract, ceramide 3, an abelmoschus esculentus fruit extract, carbomer, triethanolamine and phenoxyethanol; and the punica granatum fruit extract can be used for effectively neutralizing free radicals, inhibiting the formation of melanin, promoting metabolism and eliminating toxins. The facial mask disclosed by the invention is effective on whitening, moisturizing and resisting wrinkles, and nutritional ingredients of the facial mask can be absorbed by skin, so that a beauty effect is achieved. The facial mask can be used for a long time; and the facial mask is free from any toxic and side effects and is safe and reliable.
Description
Technical field
Invention relates to a kind of shielding skin-protecting cosmetic, particularly to a kind of facial film.
Background technology
Red Punica granatum L. nature and flavor are sweet, sour and astringent, warm, containing materials such as abundant vitamin C, Punica granatum L. polyphenol and anthocyanidin in fruit, have good toxin expelling, anti-oxidation efficacy.All play an important role in terms of medicinal, beauty treatment, dietetic therapy.Modern medicine finds, containing substantial amounts of Punica granatum L. polyphenol and anthocyanidin in red Punica granatum L., non-oxidizability exceeds green tea 3 times, the most ascorbic 20 times, can effectively neutralize free radical, enhance metabolism, discharge toxin.
Mainly there is following effect delaying skin aging: Punica granatum L. polyphenol, anthocyanidin, ellagic acid are all extremely strong antioxidant, oils and fats autoxidation is free chain reaction, course of reaction can produce multiple oxygen-derived free radicals, these oxygen-derived free radicals have the highest reactivity, be combined with macromolecular substances such as people's body lipid, protein and DNA, destroy its 26S Proteasome Structure and Function.Cause the multiple diseases such as body aging, and cause cancer, atherosclerosis and cataract.The achievement in research of No. 20472058 projects of state natural sciences fund that Sichuan University undertakes shows, the concentration of red Punica granatum L. is that the water extract of 0.0175 mg/mL is up to 85.2% to the clearance rate of DPPH free radical, higher than BHT, it is sufficient to prove the non-oxidizability of red Punica granatum L. extract.Moisturizing: hyaluronic acid is human body topmost natural moisture preserving composition, decomposing of it is main by the catalytic action of hyaluronidase.Punica granatum L. polyphenol can suppress the activity of hyaluronidase, thus slows down the decomposition rate of hyaluronic acid, thus reaches the effect of moisturizing.Crease-resistant: Punica granatum L. polyphenol can act on hydrogen bond and hydrophobic etc. and reacting with the protein in skin, produces astriction, i.e. convergence.This reaction can make skin tight, reduces wrinkle.
But Punica granatum L. squeezing juice is easier oxidized blackening, the effect of the facial film that impact is made and long-term preservation, and individually Sucus Granati can not use, and composition effect and utilization rate also can be affected.
Summary of the invention
The present invention solves utilization rate of active components this problem low extracted from Punica granatum L., there is provided a kind of whitening wrinkle removing effect facial film preferably containing Punica granatum L. extract and preparation method thereof for consumer, can be convenient for carrying, be attached on the face, good absorption, and moisture preserving time is long.
The present invention solves the deficiency of prior art problem, a kind of facial film containing Punica granatum L. Cosmetic Ingredient of offer is provided, by the following percentage by weight formed it is: deionized water: 60%～80%, glycerol: 5%～10%, Punica granatum L. extract: 3%～10%, hyaluronic acid: 0.02%～0.1%, thioctic acid: 1%～5%, Folium Ginkgo extract: 1%～5%, ceramide 3: 2%～5%, Abelmoschus esculentus berry extract: 5%～10%, carbomer: 0.02%～0.2%, triethanolamine: 0.01%～0.1%, phenoxyethanol: 0.1%～0.5%.
Improving further of a kind of facial film containing Punica granatum L. Cosmetic Ingredient of the present invention is: the weight proportion of this facial film each component is: deionized water: make facial mask liquid component meet 100% in right amount, glycerol: 6%～10%, Punica granatum L. extract: 3%～8%, hyaluronic acid: 0.01%～0.05%, thioctic acid: 1%～3%, Folium Ginkgo extract: 1%～4%, ceramide 3: 3%～5%, Abelmoschus esculentus berry extract: 5%～8%, carbomer: 0.02%～0.1%, triethanolamine: 0.01%～0.05%, phenoxyethanol: 0.2%～0.5%.
Being further preferred that of the facial film that the present invention contains Punica granatum L. Cosmetic Ingredient: the percentage by weight of each component of this facial film: deionized water: 69.5%, glycerol: 8%, Punica granatum L. extract: 6%, hyaluronic acid: 0.05%, thioctic acid: 3%, Folium Ginkgo extract: 4%, ceramide 3: 3%, Abelmoschus esculentus berry extract: 6%, carbomer: 0.1%, triethanolamine: 0.05%, phenoxyethanol: 0.3%.
The present invention provides the preparation method of a kind of facial film containing Punica granatum L. extract Cosmetic Ingredient, it is characterised in that comprise the steps:
nullA. the preparation of Punica granatum L. extracting solution: select epidermis smooth，The fresh Punica granatum L. that skin and flesh is tight，Whole Punica granatum L. is crushed，Make sarcocarp and fruit juice separating，Broken raw material is respectively put in round，General tinning amount is the 80% of container capacity，Carbon dioxide gas and the discharge of heat during being easy to ferment with reserved sufficient space，Prevent excessive tank or bottle explosion that air accumulation causes，Stand 4 hours，Under conditions of room temperature 20 DEG C，The appropriate yeast of artificial interpolation，25 DEG C of-28 DEG C of continuing fermentations 4-10 days，Material in tank is carried out skin slag separation，Collect all liq，Add lactic acid bacteria under conditions of reconciling temperature 18 DEG C-20 DEG C and pH value 4 to carry out fermenting for the second time，Sweat 3-4 days，Then process with ultrasonic wave extraction，Extract at 40 DEG C-50 DEG C water temperature F intensified by ultrasonic wave，Atmospheric extraction，Intensified by ultrasonic wave extracts 20～40 minutes，Then by extracting solution by D101 type macroporous adsorptive resins，Use pure water rinsing resin column again，Collect effluent；Effluent passes through NEUTRAL ALUMINUM post, by pure water rinsing, collects effluent；The effluent concentrating under reduced pressure of gained, obtains Punica granatum L. extracting solution；
B. the preparation of hyaluronic acid solution: deionized water boils 20 minutes, after cooling, weighing joins in 99 parts of deionized waters under the conditions of 1 part of hyaluronic acid is stirred at room temperature, stir one hour, heating makes water temperature be increased to 70 DEG C-80 DEG C, insulation half an hour, constant weight moisturizing, it is cooled to room temperature and obtains clean and clear transparent liquid；
C. carbomer is dissolved in deionized water, PH to 5.0-7.5 is regulated with triethanolamine, then according to proportioning adds Punica granatum L. essence, hyaluronic acid solution, thioctic acid, Folium Ginkgo extract, ceramide 3, Abelmoschus esculentus berry extract, phenoxyethanol is added after mix homogeneously, stir, constant weight moisturizing, regulation pH value, between 5.8-6.5, i.e. prepares the facial mask liquid containing Punica granatum L. extract Cosmetic Ingredient.
The preparation method of further preferred facial film, it is characterised in that comprise the steps:
nullA. the preparation of Punica granatum L. extracting solution: select epidermis smooth，The fresh Punica granatum L. that skin and flesh is tight，Whole Punica granatum L. is crushed，Make sarcocarp and fruit juice separating，Broken raw material is respectively put in round，General tinning amount is the 80% of container capacity，Carbon dioxide gas and the discharge of heat during being easy to ferment with reserved sufficient space，Prevent excessive tank or bottle explosion that air accumulation causes，Stand 4 hours，Under conditions of room temperature 20 DEG C，The appropriate yeast of artificial interpolation，25 DEG C of-28 DEG C of continuing fermentations 6 days，Material in tank is carried out skin slag separation，Collect all liq，Add lactic acid bacteria under conditions of reconciling temperature 18 DEG C-20 DEG C and pH value 4 to carry out fermenting for the second time，Sweat 4 days，Then process with ultrasonic wave extraction，Extract at 40 DEG C-50 DEG C water temperature F intensified by ultrasonic wave，Atmospheric extraction，Intensified by ultrasonic wave extracts 40 minutes，Can Punica granatum L. extract；
B. the preparation of hyaluronic acid solution: deionized water boils 20 minutes, after cooling, weighing joins in 99 parts of deionized waters under the conditions of 1 part of hyaluronic acid is stirred at room temperature, stir one hour, heating makes water temperature be increased to 70 DEG C-80 DEG C, insulation half an hour, constant weight moisturizing, it is cooled to room temperature and obtains clean and clear transparent liquid；
C. card ripple is dissolved in deionized water, PH to 6.5 is regulated with triethanolamine, then according to proportioning adds Punica granatum L. essence, hyaluronic acid solution, thioctic acid, Folium Ginkgo extract, ceramide 3, Abelmoschus esculentus berry extract, phenoxyethanol is added after mix homogeneously, stir, constant weight moisturizing, regulation pH value, between 5.8-6.5, i.e. prepares the facial mask liquid containing Punica granatum L. extract Cosmetic Ingredient.
The useful technique effect of the present invention
The superiority of ultrasonic extraction Punica granatum L., is specific physical character based on ultrasound wave.The Quick mechanical vibration wave mainly produced by piezoelectric transducer is reduced the active force between target extract and sample matrices thus realizes solid--liquid extract and separate.
(1) accelerating medium particle movement.Higher than when the continuous media (such as water) of the ultrasound wave of 20KHz frequency of sound wave is propagated, according to Huygens's wave principle, its wave surface propagated will cause the motion of medium particle, make medium particle movement obtain the huge acceleration of row and kinetic energy.The acceleration of particle is computed typically up to more than 2,000 times of acceleration of gravity.Be allowed to obtain huge acceleration and kinetic energy owing to ultrasonic energy is acted on by medium particle on Punica granatum L. effective ingredient particle, rapidly effusion Punica granatum L. matrix and be free in water.
(2) cavitation.Ultrasound wave is propagated in liquid medium and is produced special " cavitation effect ", " cavitation effect " constantly produces countless internal pressures and reaches the powerful shock wave on micro-air pocket the most constantly " explosion " generation microcosmic of thousands of atmospheric pressure on Punica granatum L., its Punica granatum L. component substances is made " to be bombarded " effusion, and Punica granatum L. matrix is constantly degraded, the leaching accelerating Punica granatum L. active ingredient is extracted.
(3) to homogenize the effect that (Sonication) make each point in sample media be subject to consistent in the vibration of ultrasound wave, makes whole sample extraction evenly.In sum, the active substance in Punica granatum L. serves not only as medium particle under ultrasound field effect and obtains self huge acceleration and kinetic energy, and obtains powerful external impacts by " cavitation effect ", so can high efficiency be sufficiently separated out.
Ultrasonic extraction has a following outstanding feature:
(1) without high temperature.Extract at 40 DEG C-50 DEG C water temperature F intensified by ultrasonic wave, without decocting in water high temperature, do not destroy in Punica granatum L. some active ingredient with thermally labile, facile hydrolysis or oxidation characteristic.Ultrasonic wave energy promotes plant cell ground breaking cellular wall, improves the effect of Punica granatum L. effective ingredient.
(2) atmospheric extraction, safety is good, and operation is simple, and maintaining is convenient.
(3) extraction efficiency is high.Intensified by ultrasonic wave extraction can obtain optimum extraction rate in 20～40 minutes, extraction time be only decocting in water, 1/3rd of alcohol deposition method or less.Fully, extraction quantity is more than two times of traditional method in extraction.According to statistics, ultrasound wave is the highest in 65～70 C work efficiencies.And temperature active ingredient of Punica granatum L. in 65 C degree is not the most destroyed.Add after ultrasound wave (under the conditions of 65 degree), about 40 minutes active ingredients of plants extraction times.And the digestion time of cooking process generally requires two to three hours, it it is more than the 3 times times of ultrasonic extraction time.Every tank extracts 3 times, substantially can extract more than the 90% of active ingredient.
(4) energy consumption is reduced.Owing to ultrasonic extraction is low without heating or heating-up temperature, extraction time is short, is therefore substantially reduced energy consumption.
(5) extraction process low cost, overall economic efficiency is notable；
(6) ultrasound wave has certain bactericidal action, it is ensured that extract is unlikely to deteriorate.
Red Punica granatum L. nature and flavor are sweet, sour and astringent, warm, containing materials such as abundant vitamin C, Punica granatum L. polyphenol and anthocyanidin in fruit, have good toxin expelling, anti-oxidation efficacy.All play an important role in terms of medicinal, beauty treatment, dietetic therapy.Modern medicine finds, containing substantial amounts of Punica granatum L. polyphenol and anthocyanidin in red Punica granatum L., non-oxidizability exceeds green tea 3 times, the most ascorbic 20 times, can effectively neutralize free radical, enhance metabolism, discharge toxin.But these active substance can not extract completely from Punica granatum L., can not be used completely.In order to avoid extract in owing to the traditional extraction technique such as chemical organic solvent and high temperature is to the destruction of effective ingredient in Punica granatum L., we select the mode of supersound extraction, and Punica granatum L. is by fermentation simultaneously, and effective ingredient preferably is decomposed out, it is easier to extract, and inventor have employed decoloration process.
The present invention selects deionized water, glycerol, Punica granatum L. (PUNICA GRANATUM) berry extract, hyaluronic acid, thioctic acid, Semen Ginkgo (GINKGO BILOBA) leaf extract, ceramide 3, Abelmoschus esculentus (ABELMOSCHUS
ESCLENTUS) berry extract, carbomer, triethanolamine, phenoxyethanol etc. are as the raw material of Punica granatum L. facial film, by after reasonably combined to mentioned component, this facial film has whitening, delaying skin aging, moisturizing, crease-resistant effect, the skin of modern female there is good maintenance effect, within the shortest time, the most sufficient nutrient can be provided to skin, make skin rejuvenate.
It is compared with the prior art, the remarkable advantage of patent of the present invention:
1, by fermentation, supersound extraction is utilized to improve the utilization rate of Punica granatum L. effective ingredient.
2, reasonably combined between different material, promotes the skin assimilation effect to effective ingredient.
Accompanying drawing explanation
Fig. 1Tyrosinase activity test result.
Detailed description of the invention
The present invention is further described below.
Embodiment
1
One preparation method of the facial film of the present invention
Make a kind of facial film raw materials part by weight containing Punica granatum L. Cosmetic Ingredient as follows: deionized water: 69.5%, glycerol: 8%, Punica granatum L. extract: 6%, hyaluronic acid: 0.05%, thioctic acid: 3%, Folium Ginkgo extract: 4%, ceramide 3: 3%, Abelmoschus esculentus berry extract: 6%, carbomer: 0.1%, triethanolamine: 0.05%, phenoxyethanol: 0.3%.
The preparation method of the facial film containing Punica granatum L. extract Cosmetic Ingredient, comprises the steps:
1, the preparation of Punica granatum L. extracting solution:
Select epidermis smooth, the fresh Punica granatum L. 120kg that skin and flesh is tight, whole Punica granatum L. is crushed, makes sarcocarp and fruit juice separating.Broken raw material is respectively put in round that (general tinning amount is the 80% of container capacity, carbon dioxide gas and the discharge of heat during being easy to ferment with reserved sufficient space, prevent excessive tank or bottle explosion that air accumulation causes), stand 4 hours, under conditions of room temperature 20 DEG C, artificial add 300g yeast, 25 DEG C of-28 DEG C of continuing fermentations 8 days.Material in tank is carried out skin slag separation, collects all liq and amount to 9.48kg, under conditions of temperature 20 DEG C and pH value 4, add 30g lactic acid bacteria carry out fermenting for the second time, sweat 4 days.Then heating 40 DEG C carries out processing 40 minutes with ultrasonic wave extraction.After recovering room temperature, centrifugal filtration；Then by extracting solution by D101 type macroporous adsorptive resins, then use pure water rinsing resin column, collect effluent；Effluent passes through NEUTRAL ALUMINUM post, by pure water rinsing, collects effluent；70 DEG C of concentrating under reduced pressure of the effluent of gained, obtain Punica granatum L. extracting solution 6.1 kilograms.
2, the preparation of hyaluronic acid solution: deionized water boils 20 minutes, after cooling, weigh, 50g hyaluronic acid joins under the conditions of being stirred at room temperature in 4950g deionized water, stirring one hour, heating makes water temperature be increased to 70 DEG C-80 DEG C, is incubated half an hour, constant weight moisturizing, is cooled to room temperature and obtains the liquid of clean and clear clear viscous.
3, being dissolved in by 0.1kg carbomer in the deionized water of 64.55kg sterilization, stir half an hour, card ripple is fully dispersed in water；Under agitation, joining in pot by 0.05kg triethanolamine, regulate PH to 5.0-7.5, actual ph value of measuring is 6.2.At room temperature, 8kg glycerol, 6kg Punica granatum L. extracting solution, 5kg hyaluronic acid solution, 3kg thioctic acid, 4kg Semen Ginkgo (GINKGO BILOBA) leaf extract, 3kg ceramide 3,6kg Abelmoschus esculentus (ABELMOSCHUS are added according to proportioning
ESCLENTUS) berry extract, adds 0.3kg phenoxyethanol, stirs after mix homogeneously, constant weight moisturizing, and actually measured ph value is 5.8, i.e. prepares facial mask liquid 100kg containing Punica granatum L. extract Cosmetic Ingredient.This facial mask liquid can be used alone, it is also possible to appropriate facial mask liquid makes finished product, every bag of facial film about 20-40ml Han facial mask liquid with facial mask cloth by production line.
Embodiment
2
Punica granatum L. facial film white-skinned face function of the present invention
According to experimental technique of the prior art, select vitamin C 5 μ g, kojic acid 5 μ g, after pomegranate mask liquid (being equivalent to Punica granatum L. extract content) 5 μ g prepared by the side of hydroquinone 5 μ g and the present embodiment 1 carries out suppressing tyrosinase activity test, observing melanin formational situation in each test tube, pomegranate mask liquid is formed with, to melanic, the effect of significantly inhibiting.The pomegranate mask liquid of the present invention can suppress melanin, and still effective when of 24 hours, color remains in that shallower, and the blackening that other samples are the most clearly.(see figure 1)
Embodiment
3
Clinical trial result is assessed
Trier is age-based, and skin quality and specialty degree are divided into three groups, and all experimenters are the healthy women of voluntary participation test in more than 20 years old.Wherein 20-30 year is one group, and number is 50 people；Within 30 years old-50 years old, being one group, number is 50 people.Every trier distributes the facial film 30 of the present embodiment 1 preparation respectively, within two days, uses once.60 days use time.
20-30 year proof test result see table:
| Test event | Good results (%) | Effect is general (%) | Effect bad (%) |
| Applicating property | 96% | 4% | 0 |
| Moisture retention | 98% | 2% | 0 |
| Compact sense | 80% | 20% | 0 |
| Whitening is dispelled yellow effect | 90% | 10% | 0 |
| Moistness | 86% | 14% | 0 |
30-50 year proof test result see table:
| Test event | Good results (%) | Effect is general (%) | Effect bad (%) |
| Applicating property | 96% | 4% | 0 |
| Moisture retention | 100% | 0 | 0 |
| Compact sense | 94% | 6% | 0 |
| Whitening is dispelled yellow effect | 98% | 2% | 0 |
| Moistness | 96% | 4% | 0 |
Prepared by present invention facial film being found through experiments no matter at applicating property, moisture retention, sense of compacting, whitening dispels yellow effect, and moistness can make most consumer satisfaction.
The current topmost problem of whitening product is: effect is the slowest, 10-15 days at least, just having slight part effect at most the 2-4 month. different people's using effect diversityes is relatively big, can rebound after disabling, chasing after traces it to its cause is: whitening active is strong not, and whitening composition content is the lowest;Whitening composition is oversize for action time;Product poor permeability;Skin is absorbent limited, whitening composition oxidation resistance poor (the most oxidized before not being absorbed by the skin). in order to solve the problems referred to above, and design, using facial film note, consumption is big, and the skin being equivalent to whole face during use is washed in whitening composition, make the content of whitening composition, action time, assimilation effect etc. is the most guaranteed, visible positive effect after general 40 minutes: pale, water is tender, exquisiteness, bright, the effect of gloss.Whitening principle, after facial mask essence contact skin with the help of piperonyl alcohol, ginkegetin rapid osmotic to superficial cutaneous capillaries, vasodilator, improving micro_circulation effect, there is superoxide dismutase sample effect, remove free radical.Promote hematology's circulation of skin.Moisture needed for providing for skin and nutrient.After two hours, thioctic acid and red Punica granatum L. extract and Folium Ginkgo extract combination, short-term, mid-term, long-term effect, and top layer, middle level can be reached, deep layer whitening synchronizes to carry out.Every other day with once, can be clearly distinguished from after using 10-15 days courses for the treatment of.In vain, five functional tender, soft, thin, bright present, permanence operation becomes apparent from.Common facial film became dry after 15 minutes, and the cleawhite pack of present invention design is especially added with extending the composition of moisture preserving time.Making the whitening of this facial film, moisturizing, wrinkle-proof effect is more preferable.
Claims (10)
1. the raw material of the facial film containing Punica granatum L. extract consists of: deionized water, glycerol, Punica granatum L. extract, hyaluronic acid, thioctic acid, Folium Ginkgo extract, ceramide 3, Abelmoschus esculentus berry extract, carbomer, triethanolamine, phenoxyethanol；
The percentage by weight of each composition is above:
Moisturizing ingredient: 7.02%～15.1%
Punica granatum L. extract: 3%～10%
White-skinned face function raw material: 1%～5%
Folium Ginkgo extract: 1%～5%
Abelmoschus esculentus berry extract: 5%～10%
Carbomer: 0.02%～0.2%
Triethanolamine: 0.01%～0.1%
Preservative: 0.1%～0.5%
Deionized water: add appropriate, make face pack prescription component reach 100%.
2. according to a kind of facial film containing Punica granatum L. extract component described in claim 1, it is characterised in that:
The percentage by weight of described each component is:
Deionized water: 69.5%
Glycerol: 8%
Punica granatum L. extract: 6%
Hyaluronic acid: 0.05%
Thioctic acid: 3%
Folium Ginkgo extract: 4%
Ceramide 3: 3%
Abelmoschus esculentus berry extract: 6%
Carbomer: 0.1%
Triethanolamine: 0.05%
Phenoxyethanol: 0.3%.
3. according to a kind of facial film containing Punica granatum L. extract Cosmetic Ingredient described in claim 1 or 2, it is characterised in that: described Punica granatum L. extract raw material extracts from Punica granatum L. fermentation liquid.
4. according to a kind of facial film containing Punica granatum L. extract Cosmetic Ingredient described in claim 1, it is characterised in that: described moisture-keeping efficacy raw material is hyaluronic acid 0.02%～0.1%, ceramide 3 2%～5%, glycerol 5-10%.
5. according to a kind of facial film containing Punica granatum L. extract Cosmetic Ingredient described in claim 1, it is characterised in that: described white-skinned face function raw material is thioctic acid.
6. according to a kind of facial film containing Punica granatum L. extract Cosmetic Ingredient described in claim 1, it is characterised in that: described preservative is phenoxyethanol.
7. according to a kind of facial film containing Punica granatum L. extract Cosmetic Ingredient described in claim 1 or 2, it is characterised in that: described pH value is 5.8-6.5.
8. the preparation method of the facial film containing Punica granatum L. extract Cosmetic Ingredient, it is characterised in that comprise the steps:
nullA. the preparation of Punica granatum L. extracting solution: select epidermis smooth，The fresh Punica granatum L. that skin and flesh is tight，Whole Punica granatum L. is crushed，Make sarcocarp and fruit juice separating，Broken raw material is respectively put in round，General tinning amount is the 80% of container capacity，Carbon dioxide gas and the discharge of heat during being easy to ferment with reserved sufficient space，Prevent excessive tank or bottle explosion that air accumulation causes，Stand 4 hours，Under conditions of room temperature 20 DEG C，The appropriate yeast of artificial interpolation，25 DEG C of-28 DEG C of continuing fermentations 4-10 days，Material in tank is carried out skin slag separation，Collect all liq，Add lactic acid bacteria under conditions of reconciling temperature 18 DEG C-20 DEG C and pH value 4 to carry out fermenting for the second time，Sweat 3-4 days，Then process with ultrasonic wave extraction，Extract at 40 DEG C-50 DEG C water temperature F intensified by ultrasonic wave，Atmospheric extraction，Intensified by ultrasonic wave extracts 20～40 minutes；Then by extracting solution by D101 type macroporous adsorptive resins, then use pure water rinsing resin column, collect effluent；Effluent passes through NEUTRAL ALUMINUM post, by pure water rinsing, collects effluent；70 DEG C of concentrating under reduced pressure of the effluent of gained, obtain Punica granatum L. extracting solution；
B. the preparation of hyaluronic acid solution: deionized water boils 20 minutes, after cooling, weighing joins in 99 parts of deionized waters under the conditions of 1 part of hyaluronic acid is stirred at room temperature, stir one hour, heating makes water temperature be increased to 70 DEG C-80 DEG C, insulation half an hour, constant weight moisturizing, it is cooled to room temperature and obtains clean and clear transparent liquid；
C. carbomer is dissolved in deionized water, PH to 5.0-7.5 is regulated with triethanolamine, then according to proportioning adds Punica granatum L. essence, hyaluronic acid solution, thioctic acid, Folium Ginkgo extract, ceramide 3, Abelmoschus esculentus berry extract, phenoxyethanol is added after mix homogeneously, stir, constant weight moisturizing, regulation pH value, between 5.8-6.5, i.e. prepares the facial mask liquid containing Punica granatum L. extract Cosmetic Ingredient.
9. the preparation method of the facial film containing Punica granatum L. extract Cosmetic Ingredient, it is characterised in that comprise the steps:
nullA. the preparation of Punica granatum L. extracting solution: select epidermis smooth，The fresh Punica granatum L. that skin and flesh is tight，Whole Punica granatum L. is crushed，Make sarcocarp and fruit juice separating，Broken raw material is respectively put in round，General tinning amount is the 80% of container capacity，Carbon dioxide gas and the discharge of heat during being easy to ferment with reserved sufficient space，Prevent excessive tank or bottle explosion that air accumulation causes，Stand 4 hours，Under conditions of room temperature 20 DEG C，The appropriate yeast of artificial interpolation，25 DEG C of-28 DEG C of continuing fermentations 6 days，Material in tank is carried out skin slag separation，Collect all liq，Add lactic acid bacteria under conditions of reconciling temperature 18 DEG C-20 DEG C and pH value 4 to carry out fermenting for the second time，Sweat 4 days，Then process with ultrasonic wave extraction，Extract at 40 DEG C-50 DEG C water temperature F intensified by ultrasonic wave，Atmospheric extraction，Intensified by ultrasonic wave extracts 30 minutes to obtain Punica granatum L. extract；Then by extracting solution by D101 type macroporous adsorptive resins, then use pure water rinsing resin column, collect effluent；Effluent passes through NEUTRAL ALUMINUM post, by pure water rinsing, collects effluent；70 DEG C of concentrating under reduced pressure of the effluent of gained, obtain Punica granatum L. extracting solution；
B. the preparation of hyaluronic acid solution: deionized water boils 20 minutes, after cooling, weighing joins in 99 parts of deionized waters under the conditions of 1 part of hyaluronic acid is stirred at room temperature, stir one hour, heating makes water temperature be increased to 70 DEG C-80 DEG C, insulation half an hour, constant weight moisturizing, it is cooled to room temperature and obtains clean and clear transparent liquid；
C. carbomer is dissolved in deionized water, PH to 6.5 is regulated with triethanolamine, then according to proportioning adds Punica granatum L. essence, hyaluronic acid solution, thioctic acid, Folium Ginkgo extract, ceramide 3, Abelmoschus esculentus berry extract, phenoxyethanol is added after mix homogeneously, stir, constant weight moisturizing, regulation pH value, between 5.8-6.5, i.e. prepares the facial mask liquid containing Punica granatum L. extract Cosmetic Ingredient.
10. it is filled into bottle after the facial film liquid sterilization described in claim 1-7 to be used alone, or is filled into be placed with in the facial film bag of facial mask cloth and makes facial mask paster.
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| CN106265375A (en) * | 2016-10-12 | 2017-01-04 | 湖南农业大学 | A kind of whitening anti-aging facial film and preparation method thereof |
| CN106619300A (en) * | 2016-12-28 | 2017-05-10 | 广州市聚吉科绿色化学共性技术研究院有限公司 | Moisturizing cosmetic capable of refining pores |
| CN106924073A (en) * | 2017-05-09 | 2017-07-07 | 南通千竹电子科技有限公司 | A kind of replenishing water and preserving moisture facial mask and preparation method thereof |
| CN107982070A (en) * | 2017-12-27 | 2018-05-04 | 上海晓美生物科技有限公司 | A kind of whitening moisturizing face masque of elite containing pomegranate and preparation method thereof |
| CN108042425A (en) * | 2017-12-27 | 2018-05-18 | 上海晓美生物科技有限公司 | Super infiltration skin whitening, moisturizing Essence of one kind and preparation method thereof |
| CN109125236A (en) * | 2018-08-30 | 2019-01-04 | 谭建新 | A kind of pomegranate ferment facial mask and preparation method thereof and device |
| CN110013494A (en) * | 2019-02-12 | 2019-07-16 | 广州小蜜蜂生物科技有限公司 | A kind of pomegranate berry extract and its preparation method and application |
| CN111437273A (en) * | 2019-01-17 | 2020-07-24 | 大江生医股份有限公司 | Pomegranate fermentation product and application thereof in inhibiting melanin generation and whitening skin |
| CN111544355A (en) * | 2020-06-04 | 2020-08-18 | 爱西美(珠海)生物技术有限公司 | Ellagic acid enzyme and preparation method thereof |
| CN114617832A (en) * | 2022-03-31 | 2022-06-14 | 陕西百康实业集团有限公司 | Fruit mask and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106265375A (en) * | 2016-10-12 | 2017-01-04 | 湖南农业大学 | A kind of whitening anti-aging facial film and preparation method thereof |
| CN106619300A (en) * | 2016-12-28 | 2017-05-10 | 广州市聚吉科绿色化学共性技术研究院有限公司 | Moisturizing cosmetic capable of refining pores |
| CN106924073A (en) * | 2017-05-09 | 2017-07-07 | 南通千竹电子科技有限公司 | A kind of replenishing water and preserving moisture facial mask and preparation method thereof |
| CN108042425B (en) * | 2017-12-27 | 2020-12-22 | 上海晓美生物科技有限公司 | Whitening and moisturizing essence and preparation method thereof |
| CN108042425A (en) * | 2017-12-27 | 2018-05-18 | 上海晓美生物科技有限公司 | Super infiltration skin whitening, moisturizing Essence of one kind and preparation method thereof |
| CN107982070A (en) * | 2017-12-27 | 2018-05-04 | 上海晓美生物科技有限公司 | A kind of whitening moisturizing face masque of elite containing pomegranate and preparation method thereof |
| CN107982070B (en) * | 2017-12-27 | 2020-12-29 | 上海晓美生物科技有限公司 | Whitening and moisturizing facial mask containing pomegranate essence and preparation method thereof |
| CN109125236A (en) * | 2018-08-30 | 2019-01-04 | 谭建新 | A kind of pomegranate ferment facial mask and preparation method thereof and device |
| CN111437273A (en) * | 2019-01-17 | 2020-07-24 | 大江生医股份有限公司 | Pomegranate fermentation product and application thereof in inhibiting melanin generation and whitening skin |
| CN110013494A (en) * | 2019-02-12 | 2019-07-16 | 广州小蜜蜂生物科技有限公司 | A kind of pomegranate berry extract and its preparation method and application |
| CN111544355A (en) * | 2020-06-04 | 2020-08-18 | 爱西美(珠海)生物技术有限公司 | Ellagic acid enzyme and preparation method thereof |
| CN111544355B (en) * | 2020-06-04 | 2021-04-27 | 爱西美(珠海)生物技术有限公司 | Ellagic acid enzyme and preparation method thereof |
| CN114617832A (en) * | 2022-03-31 | 2022-06-14 | 陕西百康实业集团有限公司 | Fruit mask and preparation method thereof |
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