CN108042425B - Whitening and moisturizing essence and preparation method thereof - Google Patents
Whitening and moisturizing essence and preparation method thereof Download PDFInfo
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- CN108042425B CN108042425B CN201711439383.2A CN201711439383A CN108042425B CN 108042425 B CN108042425 B CN 108042425B CN 201711439383 A CN201711439383 A CN 201711439383A CN 108042425 B CN108042425 B CN 108042425B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses hyper-osmotic whitening moisturizing essence which is prepared from raw materials including deionized water, jojoba oil, arbutin, potassium azelaic acid salt, methylparaben, octyl-polymethylsiloxane, glycerol, propylene glycol, water-soluble ceramide, sodium hyaluronate, phenoxyethanol, triethanolamine, carbomer and natural plant essence extracts. The invention also discloses a preparation method of the hyper-osmotic whitening and moisturizing essence.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to hyper-osmotic whitening and moisturizing essence and a preparation method thereof.
Background
The essence is one of the skin care products with the highest and most delicate nutrient components, the smallest molecular particles, the most powerful efficacy and the most obvious effect, and is prepared by extracting natural effective components of animals, plants or minerals and the like by high-tech hyperlink and preparing a concentrated product. When the skin is rough, dry, tired, dim and dark due to factors such as alternate seasons, endocrine imbalance, hormone change, long-time sunburn or age increase, and the like, the essence, which is a high-concentration high-functionality care product, is used, so that an excellent beautifying effect can be achieved. The essence is extracted from low temperature, the active and effective components of the essence can be well preserved, and the essence is easier to enter a basal layer from the surface of skin than common skin care products, supplements nutrients and water required by the skin, and has good health care effects on skin moisture retention, wrinkle resistance, skin firming, nutrition and the like.
The essence contains a large amount of nutrient components, but when the nutrient components are concentrated on the face and absorbed by the skin, the essence is evaporated to influence the efficacy or bacteria are accumulated on the face to cause the problems of pore blockage, inflammation and the like due to insufficient absorption capacity of the skin. Therefore, the problem that how to improve the permeability of the essence and enable the skin to absorb the nutrient components of the essence to the maximum extent is needed to be solved by a good essence product.
Disclosure of Invention
In order to solve the above problems, one aspect of the present invention provides a hyper-osmotic whitening and moisturizing essence, which comprises the following raw materials, by weight:
80-90 parts of deionized water
2-9 parts of jojoba oil
1-3 parts of arbutin
3-6 parts of potassium azelaic acid amino acid salt
0.1 to 0.3 part of methylparaben
3-10 parts of octyl polymethylsiloxane
3-10 parts of glycerol
5-9 parts of propylene glycol
2-5 parts of water-soluble ceramide
0.1-0.3 part of sodium hyaluronate
0.1 to 0.3 portion of phenoxyethanol
0.05 to 0.1 portion of triethanolamine
0.05-0.1 part of carbomer
8-12 parts of natural plant essence extract
Preferably, the hyper-osmotic whitening and moisturizing essence comprises the following raw materials in parts by weight:
83-90 parts of deionized water
4-7 parts of jojoba oil
1.5-2 parts of arbutin
4-6 parts of potassium azelaic acid amino acid salt
0.1 to 0.2 part of methylparaben
5-8 parts of octyl polymethylsiloxane
5-9 parts of glycerol
7-9 parts of propylene glycol
2-4 parts of water-soluble ceramide
0.2-0.3 part of sodium hyaluronate
0.1-0.2 part of phenoxyethanol
0.07 to 0.1 portion of triethanolamine
0.05-0.08 part of carbomer
9-11 parts of natural plant essence extract
More preferably, the hyper-osmotic whitening and moisturizing essence comprises the following components in parts by weight:
88 parts of deionized water
Jojoba oil 7 parts
Arbutin 2 parts
4 parts of potassium azelaic acid amino acid
0.1 part of methylparaben
Octyl polymethylsiloxane 7 parts
8 portions of glycerol
9 portions of propylene glycol
Water soluble ceramide 3 portions
0.3 portion of sodium hyaluronate
0.2 part of phenoxyethanol
0.1 portion of triethanolamine
Carbomer 0.07 part
10 parts of natural plant essence extract
In one embodiment, the glycerol is a bio-refined glycerol.
In one embodiment, the arbutin is beta-arbutin.
In one embodiment, the natural plant essence extract is pomegranate essence extract.
In one embodiment, the pomegranate essence extract is prepared by the following steps:
(1) screening and shelling: selecting fully mature and plump pomegranate fruits, removing rotten, deteriorated, damaged and other bad fruits, washing with clear water with the volume more than 3 times, and drying in the shade. And (4) shelling and peeling by using a pomegranate peeler.
(2) Crushing: crushing pomegranate pulp and pomegranate seeds by using a crusher, setting the rotating speed of the crusher to be 100-150 rpm, and selecting a filter screen with the diameter of 1-3 mm. And after the pulp is fully crushed, separately collecting the pomegranate pulp residue and pomegranate juice for later use.
(3) Ultrasonic: and drying the pomegranate rind at the temperature of 30-40 ℃, and crushing the pomegranate rind by using a crusher. Mixing pericarpium Granati and the above pulp residue, adding distilled water at a mass ratio of 1:10, mixing and stirring for 20 min. And putting the mixture into an ultrasonic cell disruptor, and performing ultrasonic treatment at the temperature of 0-10 ℃ and the ultrasonic frequency of 22KHz for 40-60 minutes. The sonicated product was filtered through a 10 micron pore size filter and the filtrate was collected. And (3) fully mixing the filtrate with the pomegranate juice obtained in the step (2), adding trisodium ethylenediamine tetraacetate into the mixture according to the mass ratio of 1: 0.01-0.05, rotating the mixture at a speed of 40 revolutions per minute, and stirring the mixture for 20-30 minutes to obtain a mixed solution.
(4) Preparing fermentation liquor: adding glutamine into the mixed liquid obtained in the step 3 according to the mass ratio of 1: 0.01-0.03, adding glucose to adjust the sugar content to 16-20%, and adding sodium citrate according to the mass ratio of 1:0.2 to adjust the pH value to 5.0-5.5.
(5) Fermentation: pouring the fermentation liquor into a thoroughly sterilized fermentation tank, adding yeast according to the mass ratio of 1:0.01, and fermenting at a constant temperature of 26-28 ℃ at a stirring speed of 100-150 r/min for 8 days.
(6) Clarification: filtering the fermentation liquor with a 100-mesh filter screen to remove impurities. And then centrifuging at 500-800 rpm by using a low-speed centrifuge to remove the precipitate.
(7) Concentration: concentrating the clear liquid by using a freeze concentrator, wherein the concentration cycle is as follows: firstly, reducing the temperature to 0-4 ℃ for 20-30 hours, removing ice crystals at-4-10 ℃ for 10-20 hours, and removing the ice crystals to obtain concentrated solution.
(8) And (3) ultrafiltration sterilization: and (4) sterilizing and filtering the concentrated solution obtained in the step (7) by using a 0.45 mu m sterilizing and filtering membrane to obtain the pomegranate essence extract.
In another aspect of the present invention, a preparation method of the hyper-osmotic whitening and moisturizing essence is provided, which comprises the following steps:
1. putting deionized water, jojoba oil, arbutin, potassium azelaic acid amide, methyl hydroxybenzoate and octyl polymethylsiloxane into a stirrer, and stirring at 800-1500 rpm and 60-80 ℃ for 20-30 minutes to obtain a mixture A.
2. Putting glycerol, propylene glycol, water-soluble ceramide, sodium hyaluronate, phenoxyethanol and triethanolamine into a stirrer, and stirring at the speed of 800-1500 rpm and the temperature of 60-80 ℃ for 20-30 minutes to obtain a mixture B.
3. Adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, and homogenizing for 10-20 seconds at a speed of 2000-3000 r/min. And cooling, adding carbomer and the natural plant essence extract, and mixing at the normal temperature for 10-20 minutes at the speed of 200-300 revolutions per minute to obtain the emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
Compared with the prior art, the invention has the beneficial effects that:
1. the whitening and moisturizing essence contains various safe and effective whitening and moisturizing nutritional ingredients, and is particularly added with specially-made natural plant pomegranate essence, so that the whitening and moisturizing essence is richer and more natural in nutritional ingredients, easy to absorb and free of side effects.
2. The essence is subjected to sufficient emulsification and nano treatment, so that the essence molecules reach the nano level, the hyper-osmotic effect is generated, the absorption rate of the skin surface can be greatly improved, the skin problem caused by accumulation of a large amount of nutrient components is avoided, and the using effect of the essence is remarkably improved.
Detailed Description
Example 1
1. Putting 88 parts of deionized water, 7 parts of jojoba oil, 2 parts of arbutin, 4 parts of potassium salt of azelaic acid amino acid, 0.1 part of methylparaben and 7 parts of octyl polymethylsiloxane into a stirrer, and stirring at 800-1500 rpm and 60-80 ℃ for 20-30 minutes to obtain a mixture A.
2. Putting 8 parts of glycerol, 9 parts of propylene glycol, 3 parts of water-soluble ceramide, 0.3 part of sodium hyaluronate, 0.2 part of phenoxyethanol and 0.1 part of triethanolamine into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. Adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, and homogenizing for 10-20 seconds at a speed of 2000-3000 r/min. After cooling, 0.07 part of carbomer and 10 parts of natural plant essence extract are added, and the mixture is mixed for 10 to 20 minutes at normal temperature at the speed of 200 to 300 revolutions per minute to obtain emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
Example 2
1. Putting 90 parts of deionized water, 5 parts of jojoba oil, 2 parts of arbutin, 3 parts of azelaic acid amino acid potassium salt, 0.1 part of methylparaben and 5 parts of octyl polymethylsiloxane into a stirrer, and stirring at the speed of 800-1500 rpm and the temperature of 60-80 ℃ for 20-30 minutes to obtain a mixture A.
2. Putting 8 parts of glycerol, 8 parts of propylene glycol, 4 parts of water-soluble ceramide, 0.2 part of sodium hyaluronate, 0.3 part of phenoxyethanol and 0.07 part of triethanolamine into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. Adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, and homogenizing for 10-20 seconds at a speed of 2000-3000 r/min. After cooling, adding 0.1 part of carbomer and 10 parts of natural plant essence extract, and mixing at the normal temperature for 10-20 minutes at the speed of 200-300 revolutions per minute to obtain emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
Example 3
1. Putting 85 parts of deionized water, 7 parts of jojoba oil, 1 part of arbutin, 4 parts of potassium amino acid azelate, 0.3 part of methylparaben and 4 parts of octyl polymethylsiloxane into a stirrer, and stirring at the speed of 800-1500 rpm and the temperature of 60-80 ℃ for 20-30 minutes to obtain a mixture A.
2. Putting 5 parts of glycerol, 6 parts of propylene glycol, 5 parts of water-soluble ceramide, 0.1 part of sodium hyaluronate, 0.3 part of phenoxyethanol and 0.05 part of triethanolamine into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. Adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, and homogenizing for 10-20 seconds at a speed of 2000-3000 r/min. And cooling, adding 0.05 part of carbomer and 9 parts of natural plant essence extract, and mixing at the normal temperature for 10-20 minutes at the speed of 200-300 revolutions per minute to obtain emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
Example 4
1. Putting 88 parts of deionized water, 9 parts of jojoba oil, 3 parts of arbutin, 6 parts of potassium azelate, 0.2 part of methylparaben and 10 parts of octyl methicone into a stirrer, and stirring at 800-1500 rpm and 60-80 ℃ for 20-30 minutes to obtain a mixture A.
2. Putting 7 parts of glycerol, 8 parts of propylene glycol, 4 parts of water-soluble ceramide, 0.3 part of sodium hyaluronate, 0.2 part of phenoxyethanol and 0.05 part of triethanolamine into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. Adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, and homogenizing for 10-20 seconds at a speed of 2000-3000 r/min. After cooling, 0.06 part of carbomer and 12 parts of natural plant essence extract are added, and the mixture is mixed for 10 to 20 minutes at normal temperature at the speed of 200 to 300 revolutions per minute to obtain emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
Example 5
1. Putting 87 parts of deionized water, 8 parts of jojoba oil, 3 parts of arbutin, 4 parts of azelaic acid amino acid potassium salt, 0.3 part of methylparaben and 8 parts of octyl polymethylsiloxane into a stirrer, and stirring at 800-1500 rpm and 60-80 ℃ for 20-30 minutes to obtain a mixture A.
2. Putting 9 parts of glycerol, 7 parts of propylene glycol, 3 parts of water-soluble ceramide, 0.2 part of sodium hyaluronate, 0.2 part of phenoxyethanol and 0.08 part of triethanolamine into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. Adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, and homogenizing for 10-20 seconds at a speed of 2000-3000 r/min. After cooling, adding 0.1 part of carbomer and 10 parts of natural plant essence extract, and mixing at the normal temperature for 10-20 minutes at the speed of 200-300 revolutions per minute to obtain emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
Example 6
1. Putting 90 parts of deionized water, 9 parts of jojoba oil, 1 part of arbutin, 5 parts of potassium salt of azelaic acid amino acid, 0.3 part of methylparaben and 9 parts of octyl polymethylsiloxane into a stirrer, and stirring at 800-1500 rpm and 60-80 ℃ for 20-30 minutes to obtain a mixture A.
2. Putting 7 parts of glycerol, 9 parts of propylene glycol, 2 parts of water-soluble ceramide, 0.2 part of sodium hyaluronate, 0.1 part of phenoxyethanol and 0.1 part of triethanolamine into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 revolutions per minute to obtain a mixture B.
3. Adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, and homogenizing for 10-20 seconds at a speed of 2000-3000 r/min. After cooling, adding 0.07 part of carbomer and 11 parts of natural plant essence extract, and mixing at the normal temperature for 10-20 minutes at the speed of 200-300 revolutions per minute to obtain emulsion C.
4. And (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
In vitro method for detecting moisture retention property
Controlling humidity in a desiccator using saturated ammonium sulfate and potassium acetate solutions at RH81% and RH60%, and applying 3M adhesive tape to a glass plate of appropriate size, wherein the sample amount is about 2mg/cm26 parts of each of the examples was applied to a glass plate to which a 3M adhesive tape was attached, weighed, put in a desiccator for about one hour, taken out, weighed again, and a moisture retention rate was calculated.
Calculating the formula: moisture retention rate (%) = weight of moisture after leaving/weight of moisture before leaving × 100
| Sample (I) | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 |
| RH81% | 66.3 | 61.5 | 58.7 | 62.4 | 55.8 | 59.5 |
| RH60% | 44.3 | 40.2 | 38.4 | 41.5 | 36.7 | 38.9 |
DPPH free radical scavenging assay
DPPH is also called 1, 1-diphenyl-2-trinitrophenylhydrazine, is a stable free radical, and the absolute ethanol solution of DPPH is purple, has maximum absorption at the wavelength of 517nm, and the absorbance and the concentration are in a linear relationship. When a radical scavenger is added thereto, DPPH may be combined with or substituted for the radical scavenger, whereby the radical scavenging ability can be evaluated by decreasing the number of radicals, decreasing the absorbance, and decreasing the color of the solution. Namely, the DPPH removing effect of the sample is detected at the wavelength of 517nm to calculate the antioxidant capacity, and the larger the removing rate is, the stronger the antioxidant capacity is.
| Sample (I) | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 |
| Clearance rate | 92% | 95% | 94% | 97% | 93% | 95% |
The data show that the moisture retention rate measured by the in vitro method is very high, the moisture retention effect is good, the clearance rate of all the examples in DPPH free radical clearance measurement is more than 90%, and the method has very good free radical clearance and oxidation resistance, so that the beneficial technical achievement of the method is improved.
The foregoing examples are merely illustrative of preferred embodiments of the present invention, and the scope of the present invention is not limited thereto, and the appended claims are intended to claim as broad a scope as can be conceived and the embodiments presented herein are merely illustrative of selected embodiments in accordance with all possible combinations of embodiments. Accordingly, it is applicants' intention that the appended claims are not to be limited by the choice of examples illustrating features of the invention. The technical solution and the inventive concept thereof according to the present invention should be equally replaced or changed within the protection scope of the present invention.
Claims (4)
1. The whitening and moisturizing essence comprises the following raw materials in parts by weight:
80-90 parts of deionized water
2-9 parts of jojoba oil
1-3 parts of arbutin
3-6 parts of potassium azelaic acid amino acid salt
0.1 to 0.3 part of methylparaben
3-10 parts of octyl polymethylsiloxane
3-10 parts of glycerol
5-9 parts of propylene glycol
2-5 parts of water-soluble ceramide
0.1-0.3 part of sodium hyaluronate
0.1 to 0.3 portion of phenoxyethanol
0.05 to 0.1 portion of triethanolamine
0.05-0.1 part of carbomer
8-12 parts of natural plant essence extract;
the glycerol is biological refined glycerol; the arbutin is beta-arbutin; the natural plant essence extract is a pomegranate essence extract, and the preparation method of the pomegranate essence extract comprises the following steps:
(1) screening and shelling: selecting fully mature and plump pomegranate fruits, removing rotten, deteriorated and damaged bad fruits, washing with clear water with the volume more than 3 times, drying in the shade, and shelling and peeling by using a pomegranate peeler;
(2) crushing: crushing pomegranate pulp and pomegranate seeds by using a crusher, setting the rotation speed of the crusher to be 100-150 rpm, selecting a filter screen with the diameter of 1-3 mm, fully crushing the pulp, and separately collecting pomegranate pulp residues and pomegranate juice for later use;
(3) ultrasonic: drying the pomegranate rind at the temperature of 30-40 ℃, crushing the pomegranate rind by using a crusher, mixing the pomegranate rind with the pulp residues, adding distilled water according to the mass ratio of 1:10, uniformly mixing and stirring the mixture for 20 minutes, putting the mixture into an ultrasonic cell crusher, performing ultrasonic treatment at the ultrasonic frequency of 22KHz for 40-60 minutes at the temperature of 0-10 ℃, filtering an ultrasonic product by using a 10-micron pore size filter, collecting filtrate, fully mixing the filtrate with the pomegranate juice obtained in the step 2, adding trisodium ethylenediamine tetraacetic acid according to the mass ratio of 1: 0.01-0.05, performing 40 revolutions per minute, and stirring the mixture for 20-30 minutes to obtain a mixed solution;
(4) preparing fermentation liquor: adding glutamine into the mixed liquid obtained in the step 3 according to the mass ratio of 1: 0.01-0.03, adding glucose to adjust the sugar content to 16-20%, and adding sodium citrate according to the mass ratio of 1:0.2 to adjust the pH value to 5.0-5.5;
(5) fermentation: pouring the fermentation liquor into a thoroughly sterilized fermentation tank, adding saccharomycetes according to the mass ratio of 1:0.01, and fermenting at a constant temperature of 26-28 ℃ at a stirring speed of 100-150 rpm for 8 days;
(6) clarification: filtering the fermentation liquor by using a 100-mesh filter screen to remove impurities, and then centrifuging by using a low-speed centrifuge at 500-800 rpm to remove precipitates;
(7) concentration: concentrating the clear liquid by using a freeze concentrator, wherein the concentration cycle is as follows: firstly, reducing the temperature to 0-4 ℃, 20-30 hours, removing ice crystals, and removing the ice crystals at-4-10 ℃ for 10-20 hours to obtain concentrated solution;
(8) and (3) ultrafiltration sterilization: and (4) sterilizing and filtering the concentrated solution obtained in the step (7) by using a 0.45 mu m sterilizing and filtering membrane to obtain the pomegranate essence extract.
2. The whitening and moisturizing essence according to claim 1, which is prepared from the following raw materials in parts by weight:
83-90 parts of deionized water
4-7 parts of jojoba oil
1.5-2 parts of arbutin
4-6 parts of potassium azelaic acid amino acid salt
0.1 to 0.2 part of methylparaben
5-8 parts of octyl polymethylsiloxane
5-9 parts of glycerol
7-9 parts of propylene glycol
2-4 parts of water-soluble ceramide
0.2-0.3 part of sodium hyaluronate
0.1-0.2 part of phenoxyethanol
0.07 to 0.1 portion of triethanolamine
0.05-0.08 part of carbomer
9-11 parts of natural plant essence extract.
3. The whitening and moisturizing essence according to claim 1, which is prepared from the following raw materials in parts by weight:
88 parts of deionized water
Jojoba oil 7 parts
Arbutin 2 parts
4 parts of potassium azelaic acid amino acid
0.1 part of methylparaben
Octyl polymethylsiloxane 7 parts
8 portions of glycerol
9 portions of propylene glycol
Water soluble ceramide 3 portions
0.3 portion of sodium hyaluronate
0.2 part of phenoxyethanol
0.1 portion of triethanolamine
Carbomer 0.07 part
10 parts of natural plant essence extract.
4. A preparation method of the whitening and moisturizing essence as claimed in any one of claims 1 to 3, comprising the following steps:
(1) putting deionized water, jojoba oil, arbutin, potassium azelaic acid amide, methyl hydroxybenzoate and octyl polymethylsiloxane into a stirrer, and stirring at the speed of 800-1500 rpm and the temperature of 60-80 ℃ for 20-30 minutes to obtain a mixture A;
(2) putting glycerol, propylene glycol, water-soluble ceramide, sodium hyaluronate, phenoxyethanol and triethanolamine into a stirrer, and stirring at the temperature of 60-80 ℃ for 20-30 minutes at 800-1500 rpm to obtain a mixture B;
(3) adding the mixture B into an emulsifying and homogenizing device, slowly adding the mixture A, homogenizing for 10-20 seconds at the speed of 2000-3000 r/min, cooling, adding carbomer and natural plant essence extract, and mixing for 10-20 minutes at normal temperature at the speed of 200-300 r/min to obtain an emulsion C;
(4) and (3) nanocrystallizing the emulsion C by using a nanoscale ultrahigh-pressure homogenizer, controlling the pressure at 150-200 Mpa, and homogenizing for 3 times to finally obtain the essence.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105125476A (en) * | 2015-10-19 | 2015-12-09 | 广州科玛生物科技有限公司 | Anti-wrinkle essence and preparing method thereof |
| CN105878102A (en) * | 2015-04-24 | 2016-08-24 | 四川福能源生物科技有限公司 | Facial mask containing punica granatum fruit extract and preparation method of facial mask |
| KR101666783B1 (en) * | 2015-09-21 | 2016-10-19 | 주식회사 더가든오브내추럴솔루션 | Cosmetic composition comprising fermentates of herbal medicine fruits improving whitening and antioxidation |
-
2017
- 2017-12-27 CN CN201711439383.2A patent/CN108042425B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105878102A (en) * | 2015-04-24 | 2016-08-24 | 四川福能源生物科技有限公司 | Facial mask containing punica granatum fruit extract and preparation method of facial mask |
| KR101666783B1 (en) * | 2015-09-21 | 2016-10-19 | 주식회사 더가든오브내추럴솔루션 | Cosmetic composition comprising fermentates of herbal medicine fruits improving whitening and antioxidation |
| CN105125476A (en) * | 2015-10-19 | 2015-12-09 | 广州科玛生物科技有限公司 | Anti-wrinkle essence and preparing method thereof |
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