CN110613664A

CN110613664A - Soothing massage cream and preparation method thereof

Info

Publication number: CN110613664A
Application number: CN201911029495.XA
Authority: CN
Inventors: 张惠生; 黄飞
Original assignee: Hunan Woman Spring Cosmetology Co Ltd
Current assignee: Hunan Woman Spring Cosmetology Co Ltd
Priority date: 2019-10-28
Filing date: 2019-10-28
Publication date: 2019-12-27

Abstract

The invention provides a soothing massage cream and a preparation method thereof, wherein the soothing massage cream comprises the following raw materials in parts by weight: the wheat germ and hydrogenated sweet almond skin care product comprises, by weight, 3-8 parts of glycerin, 2-4 parts of xanthan gum, 5-12 parts of wheat germ fermentation liquid, 3-8 parts of ginseng, 2-6 parts of seaweed, 3.8-9 parts of pseudo-ginseng, 1-6 parts of angelica, 2-7 parts of hydrogenated sweet almond and 20-64 parts of water.

Description

Soothing massage cream and preparation method thereof

Technical Field

The invention relates to the field of skin care products, and particularly relates to a soothing massage cream and a preparation method thereof.

Background

At present, women pay more and more attention to skin maintenance, in order to keep young and beautiful, the skin maintenance is paid more attention to in daily life, the massage cream is also one of common skin care products, mainly the skin blood circulation and metabolism are promoted, the skin is prevented from being loose, the massage cream is matched with massage, the skin can be deeply cleaned, the blood circulation can be promoted, nutrition permeation and absorption are helped, the skin is moistened, subcutaneous fat is dissolved, the fat reducing effect is achieved, the massage cream is directly applied to the skin, the massage cream on the market at present is various in types and mostly prepared from chemical raw materials, the massage cream is mainly prepared from natural raw materials, certain side effects are realized on the skin, and the pursuit of natural skin care and health preservation of consumers is not met.

Disclosure of Invention

In view of the above, the present invention provides a soothing massage cream and a preparation method thereof, which solve the above problems.

The technical scheme of the invention is realized as follows: a soothing massage cream comprises: the feed comprises the following raw materials in parts by weight: 3-8 parts of glycerol, 2-4 parts of xanthan gum, 5-12 parts of wheat germ fermentation liquor, 3-8 parts of ginseng, 2-6 parts of seaweed, 3.8-9 parts of pseudo-ginseng, 1-6 parts of angelica, 2-7 parts of hydrogenated sweet almond and 20-64 parts of water.

Further, the feed comprises the following raw materials in parts by weight: 4-6 parts of glycerol, 2.5-3.4 parts of xanthan gum, 8-10 parts of wheat germ fermentation liquor, 4-6 parts of ginseng, 3-5 parts of seaweed, 4-6 parts of pseudo-ginseng, 3-5 parts of angelica, 3-5 parts of hydrogenated sweet almond and 30-54 parts of water.

Further, the feed comprises the following raw materials in parts by weight: 5 parts of glycerol, 3 parts of xanthan gum, 9 parts of wheat germ fermentation liquor, 5 parts of ginseng, 4 parts of seaweed, 5 parts of pseudo-ginseng, 4 parts of angelica, 4 parts of hydrogenated sweet almond and 39 parts of water.

The invention also provides a preparation method of the soothing massage cream, which comprises the following steps:

s1: pretreating herba Hylotelephii Erythrosticti, Ginseng radix, Notoginseng radix, radix Angelicae sinensis and water, mixing, grinding, and performing supercritical carbon dioxide extraction at 30-50 deg.C under 32-60MPa with carbon dioxide flow rate of 10-25kg/h for 60-150min to obtain mixed extractive solution;

s2: after being treated, wheat germs are added with trehalose and vitamin E and then are frozen for 4-8 hours at the temperature of-3 to-20 ℃, wherein the weight ratio of the wheat germs to the trehalose to the vitamin E is 1: 0.01-0.25: 0.001-0.013, crushing the wheat germs after freezing, adding a buffer solution for homogenization, wherein the buffer solution is any one of an acetic acid-sodium acetate buffer solution, a potassium phosphate buffer solution and a sodium citrate buffer solution, and the weight ratio of the wheat germs to the buffer solution is 1: 2-5; the concentration of the buffer solution is 0.1-0.6 mol/L, pH value 5-7.6; adding the bacterial liquid into the wheat germ homogenate, and fermenting at the temperature of 20-35 ℃ for 5-13 h to obtain wheat germ fermentation liquid, wherein the bacterial liquid is prepared from the following components in a mass ratio of 1-3: 1.4-2: 2.1-3 of lactic acid double-bud bacteria, Streptomyces rochei and saccharomyces cerevisiae.

S3: and putting the wheat germ fermentation liquor and the mixed extracting solution into a stirring pot, heating to 60-100 ℃, stirring for 1-3 h, uniformly dissolving, cooling to 50-58 ℃, slowly adding glycerol, hydrogenated sweet almonds and xanthan gum, uniformly stirring, cooling to 38-45 ℃, vacuumizing, defoaming, cooling to 30-35 ℃, uniformly stirring, sieving by a 100-300-mesh sieve, and discharging to obtain the massage cream.

Compared with the prior art, the invention has the beneficial effects that:

the invention extracts pure natural seaweed, ginseng, pseudo-ginseng and angelica to obtain mixed extract, combines the mixed extract with wheat germ fermentation liquor and hydrogenated sweet almond, has scientific proportioning, fully releases the beneficial effects of the traditional Chinese medicine by utilizing the compounding effect of the wheat germ fermentation liquor and the hydrogenated sweet almond, and is added with glycerin and xanthan gum as an adhesive to be fused and locked with water, thereby being a safe and available product with the functions of relieving and moistening, reducing fat and losing weight, tightening skin;

(1) the sea grass in the formula of the invention contains components such as sea grass acid, sodium glycerate, mannitol and the like, and is fully combined with pure natural elements such as saponin, flavone compounds, ferulic acid, nicotinic acid and the like in the extracting solution of ginseng, pseudo-ginseng and Chinese angelica to serve as a natural plant moisturizing softener, so that the activity of epidermal cells is enhanced, skin aging is prevented, and skin is moistened; the wheat germ fermentation solution can enhance the activity of the mixed extracting solution, eliminate free radicals, promote blood circulation, keep water and oil balance, enable cells to absorb nutrients more easily and enable the skin to be ruddy and compact;

(2) the mixed extracting solution is extracted by adopting carbon dioxide supercritical, the temperature, the time, the pressure and the flow of the carbon dioxide are controlled, the components in the mixed extracting solution can be completely extracted, the extraction content reaches the peak value under proper temperature and pressure, other impurities are reduced, and the purity is improved during mixing;

(3) the wheat germ protein contains a large amount of amino acids, and is fermented by bacteria liquid after freezing treatment to generate an active yeast extract, wherein rich components such as vitamins, amino acids, mineral substances, organic acids and the like which are very similar to skin are combined with the mixed extracting solution, so that the metabolism of the skin can be effectively regulated, the skin regeneration is promoted, the skin stability is maintained, the skin quality is improved, the skin is more delicate, the pH value of the skin is adjusted, and pores are converged.

Detailed Description

In order to better understand the technical content of the invention, specific examples are provided below to further illustrate the invention.

The experimental methods used in the examples of the present invention are all conventional methods unless otherwise specified.

The materials, reagents and the like used in the examples of the present invention can be obtained commercially without specific description.

Example 1

A soothing massage cream comprises: the feed comprises the following raw materials in parts by weight: 3 parts of glycerin, 2 parts of xanthan gum, 5 parts of wheat germ fermentation liquor, 3 parts of ginseng, 2 parts of seaweed, 3.8 parts of pseudo-ginseng, 1 part of angelica, 2 parts of hydrogenated sweet almond and 20 parts of water.

Example 2

A soothing massage cream comprises: the feed comprises the following raw materials in parts by weight: 8 parts of glycerol, 4 parts of xanthan gum, 12 parts of wheat germ fermentation liquor, 8 parts of ginseng, 6 parts of seaweed, 9 parts of pseudo-ginseng, 6 parts of angelica, 7 parts of hydrogenated sweet almond and 64 parts of water.

Example 3

A soothing massage cream comprises: the feed comprises the following raw materials in parts by weight: 4 parts of glycerin, 2.5 parts of xanthan gum, 8 parts of wheat germ fermentation liquor, 4 parts of ginseng, 3 parts of seaweed, 4 parts of pseudo-ginseng, 3 parts of angelica, 3 parts of hydrogenated sweet almond and 30-parts of water.

Example 4

A soothing massage cream comprises: the feed comprises the following raw materials in parts by weight: 6 parts of glycerol, 3.4 parts of xanthan gum, 10 parts of wheat germ fermentation liquor, 6 parts of ginseng, 5 parts of seaweed, 6 parts of pseudo-ginseng, 5 parts of angelica, 5 parts of hydrogenated sweet almond and 54 parts of water.

Example 5

A soothing massage cream comprises: the feed comprises the following raw materials in parts by weight: 5 parts of glycerol, 3 parts of xanthan gum, 9 parts of wheat germ fermentation liquor, 5 parts of ginseng, 4 parts of seaweed, 5 parts of pseudo-ginseng, 4 parts of angelica, 4 parts of hydrogenated sweet almond and 39 parts of water;

the preparation method of the soothing massage cream in the embodiment 1-5 comprises the following steps:

s1: pretreating the above sea weed, ginseng, pseudo-ginseng, angelica and water in parts by weight, mixing, grinding, and performing carbon dioxide supercritical extraction at 40 ℃, 40MPa, 15kg/h of carbon dioxide flow and 105min of extraction time to obtain a mixed extract;

s2: processing wheat germs, adding trehalose and vitamin E, and freezing at-15 deg.C for 6h, wherein the weight ratio of wheat germs to trehalose to vitamin E is 1: 0.15: 0.08, crushing the wheat germs after freezing treatment, adding a buffer solution for homogenization treatment, wherein the buffer solution is an acetic acid-sodium acetate buffer solution, and the weight ratio of the wheat germs to the buffer solution is 1: 3; the concentration of the buffer is 0.3mol/L, pH value 6; adding a bacterial liquid into the wheat germ homogenate, and fermenting at the temperature of 28 ℃ for 8 hours to obtain a wheat germ fermentation liquid, wherein the bacterial liquid is prepared from the following components in a mass ratio of 2: 1.7: 2.5 lactic acid double-bud bacteria, Streptomyces rochei and Saccharomyces cerevisiae.

S3: and putting the wheat germ fermentation liquor and the mixed extracting solution into a stirring pot, heating to 80 ℃, stirring for 2h, dissolving uniformly, cooling to 54 ℃, slowly adding glycerol, hydrogenated sweet almond and xanthan gum, stirring uniformly, cooling to 42 ℃, vacuumizing, defoaming, cooling to 32 ℃, stirring uniformly, sieving with a 200-mesh sieve, and discharging to obtain the massage cream.

Example 6

A soothing massage cream comprises: the feed comprises the following raw materials in parts by weight: 5 parts of glycerin, 3 parts of xanthan gum, 9 parts of wheat germ fermentation liquor, 5 parts of ginseng extract, 4 parts of seaweed extract, 5 parts of pseudo-ginseng extract, 4 parts of Chinese angelica extract, 4 parts of hydrogenated sweet almond and 39 parts of water;

s1: pretreating herba Hylotelephii Erythrosticti, Ginseng radix, Notoginseng radix, radix Angelicae sinensis and water, mixing, grinding, performing carbon dioxide supercritical extraction at 30 deg.C under 32MPa with carbon dioxide flow rate of 10kg/h for 60min to obtain mixed extractive solution;

s2: processing wheat germs, adding trehalose and vitamin E, and freezing at-3 ℃ for 4h, wherein the weight ratio of the wheat germs to the trehalose to the vitamin E is 1: 0.01: 0.001, crushing the wheat germs after freezing treatment, adding a buffer solution for homogenization treatment, wherein the buffer solution is potassium phosphate buffer solution, and the weight ratio of the wheat germs to the buffer solution is 1: 2; the concentration of the buffer is 0.1mol/L, pH value 5; adding a bacterial liquid into the wheat germ homogenate, and fermenting at the temperature of 20 ℃ for 5 hours to obtain a wheat germ fermentation liquid, wherein the bacterial liquid is prepared from the following components in a mass ratio of 1: 1.4: 2.1 lactic acid double-bud bacteria, Streptomyces rochei and saccharomyces cerevisiae.

S3: and putting the wheat germ fermentation liquor and the mixed extracting solution into a stirring pot, heating to 60 ℃, stirring for 1h, dissolving uniformly, cooling to 50 ℃, slowly adding glycerol, hydrogenated sweet almond and xanthan gum, stirring uniformly, cooling to 38 ℃, vacuumizing, defoaming, cooling to 30 ℃, stirring uniformly, sieving by a 100-mesh sieve, and discharging to obtain the massage cream.

Example 7

s1: pretreating herba Hylotelephii Erythrosticti, Ginseng radix, Notoginseng radix, radix Angelicae sinensis and water, mixing, grinding, performing carbon dioxide supercritical extraction at 50 deg.C under 60MPa for 150min to obtain mixed extractive solution;

s2: processing wheat germs, adding trehalose and vitamin E, and freezing at-20 deg.C for 8h, wherein the weight ratio of wheat germs to trehalose to vitamin E is 1: 0.25: 0.013, crushing the wheat germs after freezing treatment, adding a buffer solution for homogenization treatment, wherein the buffer solution is a sodium citrate buffer solution, and the weight ratio of the wheat germs to the buffer solution is 1: 5; the concentration of the buffer is 0.6mol/L, pH value 7.6; adding a bacterial liquid into the wheat germ homogenate, and fermenting at the temperature of 35 ℃ for 13 hours to obtain a wheat germ fermentation liquid, wherein the bacterial liquid is prepared from the following components in a mass ratio of 3: 2: 3 lactic acid double-bud bacterium, Streptomyces rochei and saccharomyces cerevisiae.

S3: and putting the wheat germ fermentation liquor and the mixed extracting solution into a stirring pot, heating to 100 ℃, stirring for 3h, dissolving uniformly, cooling to 58 ℃, slowly adding glycerol, hydrogenated sweet almond and xanthan gum, stirring uniformly, cooling to 45 ℃, vacuumizing, defoaming, cooling to 35 ℃, stirring uniformly, sieving by a 300-mesh sieve, and discharging to obtain the massage cream.

Example 8

The difference between this example and example 5 is that the preparation method of the soothing massage cream is as follows: in the step S2, the bacterial liquid is mixed by mass ratio of 1: 1: 2 lactic acid double-bud bacteria, Streptomyces rochei and saccharomyces cerevisiae.

Example 9

The difference between this example and example 5 is that the preparation method of the soothing massage cream is as follows: in the step S2, the bacterial liquid does not contain Streptomyces rochei.

Comparative example 1

The difference between the comparative example and the example 5 is that the soothing massage cream comprises the following raw materials in parts by weight: 2 parts of glycerol, 5 parts of xanthan gum, 3 parts of wheat germ fermentation liquor, 2 parts of ginseng, 7 parts of seaweed, 3 parts of pseudo-ginseng, 7 parts of angelica, 1 part of hydrogenated sweet almond and 15 parts of water.

Comparative example 2

The comparison example differs from example 5 in that the soothing massage cream does not contain wheat germ fermentation broth or seaweed extract.

First, experimental analysis

(one) measurement of skin moisture

Selecting 120 healthy volunteers aged 18-40 years, wherein 28 men and 92 women are randomly divided into 12 groups (male is not controlled to be divided into the same group); after each subject takes a bath at night, the product is used, the same method is adopted, the massage is carried out for 15 minutes, and the test period is 15 days.

According to a standardized detection method for measuring skin moisture and oil, a standard operation procedure is established, a standard instrument is adopted to detect the skin of a subject, each subject is measured for three times, an average value is obtained, and the measurement results of each index of each group of subjects are averaged.

The test results are given in the following table:

(II) slimming Performance test

The massage creams prepared in examples 1 to 9 were used as test samples 1 to 9, and the massage creams prepared in comparative examples 1 to 2 were used as control samples 1 to 2.

The test method comprises the following steps: randomly selecting 120 healthy people of 18-40 years old in the same area as volunteers, taking 60 men and women respectively, measuring and recording the waistline of each volunteer by using a waistline measuring tape before the test, measuring the waistline of each volunteer for three times and averaging the values, smearing the product on the abdomen for 60 days continuously, measuring the waistline of each volunteer for 20 days, 40 days and 60 days respectively, and taking the average value of each group.

As can be seen from the above table, in the massage cream prepared by using the raw material formula of examples 1 to 5, the moisturizing and moisturizing effect is significant and the slimming effect is significant in example 5, whereas in examples 5 to 9, the process parameters for preparing the massage cream are selected, the traditional Chinese medicine components are extracted, the beneficial components are fully extracted, the fermentation temperature and time of wheat germs are limited, and the bacteria liquid is selected, so that the massage cream prepared by using the process parameters selected in example 5 has the best effect; in comparative examples 1-2, it can be seen that the massage cream prepared by adopting the raw materials with scientific and reasonable proportion in the embodiment 5 has the effects of moisturizing, slimming, reducing fat and firming skin.

The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims

1. The soothing massage cream is characterized in that: the feed comprises the following raw materials in parts by weight: 3-8 parts of glycerol, 2-4 parts of xanthan gum, 5-12 parts of wheat germ fermentation liquor, 3-8 parts of ginseng, 2-6 parts of seaweed, 3.8-9 parts of pseudo-ginseng, 1-6 parts of angelica, 2-7 parts of hydrogenated sweet almond and 20-64 parts of water.

2. A soothing massage cream as claimed in claim 1, wherein: 4-6 parts of glycerol, 2.5-3.4 parts of xanthan gum, 8-10 parts of wheat germ fermentation liquor, 4-6 parts of ginseng, 3-5 parts of seaweed, 4-6 parts of pseudo-ginseng, 3-5 parts of angelica, 3-5 parts of hydrogenated sweet almond and 30-54 parts of water.

3. A soothing massage cream as claimed in claim 1, wherein: 5 parts of glycerol, 3 parts of xanthan gum, 9 parts of wheat germ fermentation liquor, 5 parts of ginseng, 4 parts of seaweed, 5 parts of pseudo-ginseng, 4 parts of angelica, 4 parts of hydrogenated sweet almond and 39 parts of water.

4. A method of preparing a soothing massage cream as claimed in claim 1, characterized in that: the method comprises the following steps:

s2: processing wheat germs, adding trehalose and vitamin E, and freezing at the temperature of between-3 and-20 ℃, wherein the weight ratio of the wheat germs to the trehalose to the vitamin E is 1: 0.01-0.25: 0.001-0.013, crushing the wheat germs after freezing, adding a buffer solution for homogenizing, wherein the weight ratio of the wheat germs to the buffer solution is 1: 2-5; the concentration of the buffer solution is 0.1-0.6 mol/L, pH value 5-7.6; adding the bacterial liquid into the wheat germ homogenate, and fermenting at the temperature of 20-35 ℃ to obtain wheat germ fermentation liquid;

s3: and putting the wheat germ fermentation liquor and the mixed extracting solution into a stirring pot, heating to 60-100 ℃, stirring for 1-3 h, uniformly dissolving, cooling to 50-58 ℃, slowly adding glycerol, hydrogenated sweet almonds and xanthan gum, uniformly stirring, cooling to 38-45 ℃, vacuumizing, defoaming, cooling to 30-35 ℃, uniformly stirring, filtering and discharging to obtain the massage cream.

5. A method for preparing a soothing massage cream as claimed in claim 4, wherein in step S2, wheat germ is frozen for 4-8 h.

6. The method of claim 4, wherein in step S2, the buffer is any one of acetic acid-sodium acetate buffer, potassium phosphate buffer, and sodium citrate buffer.

7. The preparation method of the soothing massage cream as claimed in claim 4, wherein in the step S2, the bacteria liquid is prepared from the following raw materials in a mass ratio of 1-3: 1.4-2: 2.1-3 of lactic acid double-bud bacteria, Streptomyces rochei and saccharomyces cerevisiae.

8. The method for preparing a soothing massage cream as claimed in claim 4, wherein in step S2, the fermentation time is 5-13 h.

9. A method for preparing a soothing massage cream as claimed in claim 4, wherein in step S3, the filtering mesh is 100-300 mesh.