CN110037968A - A kind of wrinkle resistant patch and preparation method thereof containing dendrobium extract - Google Patents
A kind of wrinkle resistant patch and preparation method thereof containing dendrobium extract Download PDFInfo
- Publication number
- CN110037968A CN110037968A CN201910332274.3A CN201910332274A CN110037968A CN 110037968 A CN110037968 A CN 110037968A CN 201910332274 A CN201910332274 A CN 201910332274A CN 110037968 A CN110037968 A CN 110037968A
- Authority
- CN
- China
- Prior art keywords
- dendrobium
- wrinkle resistant
- resistant patch
- liquid containing
- dendrobium extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Biophysics (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of wrinkle resistant patch and preparation method thereof containing dendrobium extract, consist of the following components in percentage by weight: dendrobium extract 5~25%, grape pip essential oil 5~10%, vitamin 5~10%, moisturizer 10~20%, carbomer 0.02~0.2%, triethanolamine 0.01~0.1%, preservative 0.1%~0.5%, surplus are water；By reasonably combined between different material, skin damaged cell can be repaired, moisturizing, nourish, lighten the stain, eliminate microgroove, improve cell activity, promote collagen synthesis, restore elasticity of skin, delaying skin aging；Simultaneously by broken wall crusher machine, enzymatic hydrolysis and then the sporoderm-broken rate for improving using ultrasonic extraction dendrobium nobile medicinal material, facilitate the dissolution and utilization rate of effective active composition in dendrobium nobile, assimilation effect of the enhancement skin to effective component.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of wrinkle resistant patch containing dendrobium extract and its preparation
Method.
Background technique
Modern society's life rhythm is fast, and especially in big city, working strength is very big, is not conducive to good health；People exist
After overworking, the colour of skin is often poor, and intensive work year in year out, frequently can lead to cutis laxa, wrinkle increases；
In view of this, there is dazzling skin care item on the market, a degree of moisturizing, whitening, moisturizing, oil-control, taste can be played
Moisten skin, pore refining and other effects；However, these skin care item usually only have the function of preventing skin aging, once and skin
Phenomena such as skin quality has deteriorated, such as wrinkle increases, commercially available major part cosmetics are all of no avail, for wrinkle removal beauty treatment, perhaps
More Mries middle age often select facial rhytidectomy, although significant effect, quick, presence very big risk and side effect, and
It is costly.
Therefore it provides a kind of significant skin care item of wrinkle improvement effect, are one of the emphasis of cosmetic field research staff research；
Facial mask is a kind of common skin care item, and the high-quality facial mask in part is capable of providing dual anti-aging effect, can stimulate cell neogenesis energy,
The texture and the colour of skin uniformity for improving skin surface, keep skin finer and smoother, therefore be favored by people；However, commercially available facial mask
Equal cosmetics tend not to efficiently remove the wrinkle generated.
Dendrobium nobile is a kind of rare traditional Chinese medicine, is measured through modern science and technology, dendrobium nobile active polysaccharide rich in dendrobium nobile,
Its content 25% or more, dendrobium nobile active polysaccharide have antitumor, anti-inflammatory, blood pressure lowering, hypoglycemic, anti-lipid peroxidation,
Anti-aging accelerates constitution and restores, improve human leukocytes quantity, assistant treating cancer, improve the immunity of the human body and other effects；Iron sheet
Also contain dendrobine in dendrobium nobile, shows that dendrobine there is certain inhibition to grow and kill tumour cell according to modern pharmacology experiment
The effect of going out has apparent anti-tumor activity, and chemicotherapy is reduced by improving the immunity of the human body to the toxic side effect of human body, also
It can reduce blood glucose, anti-aging；In dendrobium nobile contain 18 kinds of amino acid, be able to satisfy demand of the human body to amino acid, have it is anti-oxidant,
The health-care efficacies such as anti-aging, hypoglycemic, liver protection moistening lung, softening blood vessel, nourishing the stomach and protecting stomach；Contain lot of trace member in dendrobium nobile simultaneously
Element can promote human metabolism, restore cell activity, play the role of anti-aging.
Summary of the invention
In response to the problems existing in the prior art, the purpose of the present invention is to provide a kind of wrinkle resistant patch containing dendrobium extract
And preparation method thereof, collagen can either effectively be increased by reaching, and can effectively eliminate the purpose of facial wrinkles, and the present invention closes
Reason utilizes the active constituent of Herba Dendrobii extract, and selected other skin conditioning agents carry out compatibilities, while using suitable moisturizing
Agent, thickener, emulsifier and preservative, to prepare the effective wrinkle resistant patch of anti-wrinkle by specific proportion.
To achieve the above object, the technical solution adopted by the present invention is that:
A kind of wrinkle resistant patch liquid containing dendrobium extract, consists of the following components in percentage by weight: dendrobium extract 5
~25%, grape pip essential oil 5~10%, vitamin 5~10%, moisturizer 10~20%, carbomer 0.02~0.2%, three second
Hydramine 0.01~0.1%, preservative 0.1%~0.5%, surplus are water.
The present invention also provides the dendrobium extracts the preparation method comprises the following steps: the clean, dissection by dendrobium fresh strips, is put into wall-breaking machine
In, water homogenate is added, adds the enzyme of the destruction plant cell wall of dendrobium nobile weight 0.5~1%, and sonic oscillation extracts, and collects
Fresh dendrobium nobile slurries filter up to fresh dendrobium extract.
It is as above-mentioned technical proposal to further limit, the dendrobium nobile dissection to 2~3cm size.
It is as above-mentioned technical proposal to further limit, it is that water homogenate is added in 1:10~20 by the solid-to-liquid ratio of dendrobium nobile and water.
It is as above-mentioned technical proposal to further limit, the sonic oscillation extraction conditions are as follows: control temperature is 25~30
DEG C, in 35000r/min ultrasonic extraction 10min.
As above-mentioned technical proposal to further limit, the enzyme for destroying plant cell wall is that cellulase or β-Portugal are poly-
One of carbohydrase or a variety of combinations.
It is as above-mentioned technical proposal to further limit, it is filtered using 200 mesh gauzes.
As above-mentioned technical proposal to further limit, the moisturizer is hyaluronic acid, Cer NP, glycerol by weight
Amount is than the mixture for 1:1~3:3~5.
As above-mentioned technical proposal to further limit, the preservative is sorb potassium alcoholate.
The present invention provides a kind of preparation method of wrinkle resistant patch containing dendrobium extract, includes the following steps:
S1, dendrobium fresh strips are cleaned, dissection, is put into wall-breaking machine, water homogenate is added, and sonic oscillation extracts, collect fresh
Dendrobium nobile slurries filter up to fresh dendrobium extract；
S2, carbomer is dissolved in deionized water, pH to 6.0-7.5 is adjusted with triethanolamine, is then added according to the proportion
Dendrobium extract, grape pip essential oil, vitamin and moisturizer, preservative is added after mixing, stirs evenly, and adjusts pH value and exists
Between 5.8-6.5, the facial mask liquid containing dendrobium extract is obtained；
S3, above-mentioned facial mask liquid is filled into the facial mask bag for be placed with facial mask cloth wrinkle resistant patch is made.
Compared with prior art, the beneficial effects of the present invention are:
(1) a kind of wrinkle resistant patch containing dendrobium extract of the invention when in use can repair skin damaged cell
It mends, moisturizing, nourishes, lighten the stain, eliminate microgroove, improve cell activity, promote collagen synthesis, restore elasticity of skin, prolong
Slow skin aging.
(2) present invention selects deionized water, glycerol, dendrobium extract, grape pip essential oil, hyaluronic acid, vitamin, nerve
The raw material as the wrinkle resistant patch of dendrobium nobile such as amide 3, carbomer, triethanolamine, sorb potassium alcoholate passes through rationally taking to mentioned component
With later, this facial mask has whitening, delaying skin aging, moisturizing, crease-resistant effect, has well to the skin of modern female
Maintenance effect can provide most sufficient nutrient to skin within the shortest time, skin is made to rejuvenate, and promote cytotoxin row
Out, skin problem caused by repairing because of extraneous factor and the intracorporal variation of people.
(3) by broken wall crusher machine, enzymatic hydrolysis, then improve using ultrasonic extraction the sporoderm-broken rate of dendrobium nobile cell, facilitate
The dissolution and utilization rate of effective active composition in dendrobium nobile.
Detailed description of the invention
Fig. 1 is the oxidation resistance comparison result of wrinkle resistant patch liquid made from Examples 1 to 3 and comparative example 1.
Fig. 2 is that the oxidation resistance of wrinkle resistant patch liquid made from embodiment 1, embodiment 4~5 and comparative example 2~3 compares knot
Fruit.
Fig. 3 is the oxidation resistance comparison result of embodiment 1, wrinkle resistant patch liquid made from embodiment 6~7.
Fig. 4 is that the oxidation resistance of wrinkle resistant patch liquid made from embodiment 1, embodiment 8~10 and comparative example 4~5 compares
As a result.
Fig. 5 is that the oxidation resistance of wrinkle resistant patch liquid made from embodiment 1, embodiment 11~12 and comparative example 6 compares knot
Fruit.
Fig. 6 is the oxidation resistance comparison result of embodiment 1, wrinkle resistant patch liquid made from embodiment 13~14.
Fig. 7 is the oxidation resistance comparison result of wrinkle resistant patch liquid made from embodiment 1 and comparative example 7~8.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated；It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention；Unless stated otherwise, the present invention uses reagent, method and apparatus is the art conventional reagents, method
And equipment.
Embodiment 1
A kind of wrinkle resistant patch liquid containing dendrobium extract, consists of the following components in percentage by weight: dendrobium extract
15%, grape pip essential oil 8%, vitamin 8%, moisturizer 15%, carbomer 0.1%, triethanolamine 0.05%, sorb potassium alcoholate
0.3%, surplus is water.
The moisturizer is the mixture that hyaluronic acid, Cer NP, glycerol are 1:2:4 by weight.
The dendrobium extract the preparation method comprises the following steps: by dendrobium fresh strips clean, dissection to 2~3cm size, be put into wall-breaking machine
In, the water that 15 times of volumes of dendrobium nobile weight are added is homogenized, the cellulase of dendrobium nobile weight 0.8% is added, and at 27 DEG C,
With 35000r/min ultrasonic extraction 10min, fresh dendrobium nobile slurries are collected, are filtered with 200 mesh gauzes up to fresh dendrobium extract.
A kind of preparation method of wrinkle resistant patch containing dendrobium extract, includes the following steps:
S1, dendrobium fresh strips are cleaned, dissection to 2~3cm size, is put into wall-breaking machine, 15 times of volumes of dendrobium nobile weight are added
Water be homogenized, the cellulase of dendrobium nobile weight 0.8% is added, and at 27 DEG C, with 35000r/min ultrasonic extraction
10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract；
S2, the carbomer of the weight percent is dissolved in deionized water, pH to 7.0 is adjusted with triethanolamine, then
Dendrobium extract, grape pip essential oil, vitamin and moisturizer are added according to the proportion, sorb potassium alcoholate, stirring are added after mixing
Uniformly, pH value is adjusted to 6.0, obtains the facial mask liquid containing dendrobium extract；
S3, above-mentioned facial mask liquid is filled into the facial mask bag for be placed with facial mask cloth wrinkle resistant patch is made.
Embodiment 2
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In consisting of the following components in percentage by weight: dendrobium extract 5%, grape pip essential oil 10%, vitamin 10%, moisturizer
10%, carbomer 0.2%, triethanolamine 0.01%, sorb potassium alcoholate 0.1%, surplus are water.
Embodiment 3
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In consisting of the following components in percentage by weight: dendrobium extract 25%, grape pip essential oil 5%, vitamin 5%, moisturizer
5%, carbomer 0.02%, triethanolamine 0.1%, sorb potassium alcoholate 0.5%, surplus are water.
Embodiment 4
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 10 times of volumes of dendrobium nobile weight is homogenized, and adds the cellulase of dendrobium nobile weight 0.8%, and at 27 DEG C, with
35000r/min ultrasonic extraction 10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Embodiment 5
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 20 times of volumes of dendrobium nobile weight is homogenized, and adds the cellulase of dendrobium nobile weight 0.8%, and at 27 DEG C, with
35000r/min ultrasonic extraction 10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Embodiment 6
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 15 times of volumes of dendrobium nobile weight is homogenized, and adds the cellulase of dendrobium nobile weight 0.8%, and at 25 DEG C, with
35000r/min ultrasonic extraction 10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Embodiment 7
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 15 times of volumes of dendrobium nobile weight is homogenized, and adds the cellulase of dendrobium nobile weight 0.8%, and at 30 DEG C, with
35000r/min ultrasonic extraction 10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Embodiment 8
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 15 times of volumes of dendrobium nobile weight is homogenized, and adds the cellulase of dendrobium nobile weight 0.5%, and at 27 DEG C, with
35000r/min ultrasonic extraction 10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Embodiment 9
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 15 times of volumes of dendrobium nobile weight is homogenized, and adds the cellulase of dendrobium nobile weight 1%, and at 27 DEG C, with
35000r/min ultrasonic extraction 10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Embodiment 10
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 15 times of volumes of dendrobium nobile weight is homogenized, and adds the 1,4 beta-glucanase of dendrobium nobile weight 0.8%, and at 27 DEG C, with
35000r/min ultrasonic extraction 10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Embodiment 11
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In the moisturizer is the mixture that hyaluronic acid, Cer NP, glycerol are 1:1:5 by weight.
Embodiment 12
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In the moisturizer is the mixture that hyaluronic acid, Cer NP, glycerol are 1:3:3 by weight.
Embodiment 13
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In a kind of preparation method of wrinkle resistant patch containing dendrobium extract includes the following steps:
S1, dendrobium fresh strips are cleaned, dissection to 2~3cm size, is put into wall-breaking machine, 15 times of volumes of dendrobium nobile weight are added
Water be homogenized, the cellulase of dendrobium nobile weight 0.8% is added, and at 27 DEG C, with 35000r/min ultrasonic extraction
10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract；
S2, the carbomer of the weight percent is dissolved in deionized water, pH to 6.0 is adjusted with triethanolamine, then
Dendrobium extract, grape pip essential oil, vitamin and moisturizer are added according to the proportion, sorb potassium alcoholate, stirring are added after mixing
Uniformly, pH value is adjusted to 5.8, obtains the facial mask liquid containing dendrobium extract；
S3, above-mentioned facial mask liquid is filled into the facial mask bag for be placed with facial mask cloth wrinkle resistant patch is made.
Embodiment 14
The present embodiment provides a kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, difference exists
In a kind of preparation method of wrinkle resistant patch containing dendrobium extract includes the following steps:
S1, dendrobium fresh strips are cleaned, dissection to 2~3cm size, is put into wall-breaking machine, 15 times of volumes of dendrobium nobile weight are added
Water be homogenized, the cellulase of dendrobium nobile weight 0.8% is added, and at 27 DEG C, with 35000r/min ultrasonic extraction
10min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract；
S2, the carbomer of the weight percent is dissolved in deionized water, pH to 7.5 is adjusted with triethanolamine, then
Dendrobium extract, grape pip essential oil, vitamin and moisturizer are added according to the proportion, sorb potassium alcoholate, stirring are added after mixing
Uniformly, pH value is adjusted to 6.5, obtains the facial mask liquid containing dendrobium extract；
S3, above-mentioned facial mask liquid is filled into the facial mask bag for be placed with facial mask cloth wrinkle resistant patch is made.
Comparative example 1
A kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, the difference is that, by following weight
The group of percentage is grouped as: dendrobium extract 2%, grape pip essential oil 12%, vitamin 12 %, moisturizer 15%, carbomer
0.1%, triethanolamine 0.05%, preservative 0.3%, surplus are water.
Comparative example 2
A kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, the difference is that, the dendrobium nobile mentions
Take liquid the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, are put into wall-breaking machine, are added 8 times of dendrobium nobile weight
The water of volume is homogenized, and the cellulase of dendrobium nobile weight 0.8% is added, and at 27 DEG C, is mentioned with 35000r/min ultrasound
10min is taken, fresh dendrobium nobile slurries are collected, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Comparative example 3
A kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, the difference is that, the dendrobium nobile mentions
Take liquid the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, are put into wall-breaking machine, dendrobium nobile weight 25 is added
The water of times volume is homogenized, and adds the cellulase of dendrobium nobile weight 0.8%, and at 27 DEG C, with 35000r/min ultrasound
10min is extracted, fresh dendrobium nobile slurries are collected, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Comparative example 4
A kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, the difference is that, the dendrobium nobile mentions
Take liquid the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, are put into wall-breaking machine, dendrobium nobile weight 15 is added
The water of times volume is homogenized, and adds the cellulase of dendrobium nobile weight 0.3%, and at 27 DEG C, with 35000r/min ultrasound
10min is extracted, fresh dendrobium nobile slurries are collected, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Comparative example 5
A kind of wrinkle resistant patch liquid containing dendrobium extract, compared with Example 1, the difference is that, the dendrobium nobile mentions
Take liquid the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, are put into wall-breaking machine, dendrobium nobile weight 25 is added
The water of times volume is homogenized, and adds the cellulase of dendrobium nobile weight 1.2%, and at 27 DEG C, with 35000r/min ultrasound
10min is extracted, fresh dendrobium nobile slurries are collected, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Comparative example 6
This comparative example provides a kind of wrinkle resistant patch liquid containing dendrobium extract, and compared with Example 1, difference exists
In the moisturizer is the mixture that hyaluronic acid, Cer NP, glycerol are 1:4:2 by weight.
Comparative example 7
This comparative example provides a kind of wrinkle resistant patch liquid containing dendrobium extract, and compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 15 times of volumes of dendrobium nobile weight is homogenized, and adds the cellulase of dendrobium nobile weight 0.8%, and extract at 27 DEG C
30min collects fresh dendrobium nobile slurries, is filtered with 200 mesh gauzes up to fresh dendrobium extract.
Comparative example 8
This comparative example provides a kind of wrinkle resistant patch liquid containing dendrobium extract, and compared with Example 1, difference exists
In, the dendrobium extract the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection to 2~3cm size, it is put into wall-breaking machine, adds
The water for entering 15 times of volumes of dendrobium nobile weight is homogenized, and at 27 DEG C, with 35000r/min ultrasonic extraction 10min, collects fresh stone
Dry measure used in former times slurries are filtered with 200 mesh gauzes up to fresh dendrobium extract.
Test example
It is removed by comparing the wrinkle resistant patch liquid made from different embodiments of the invention and comparative example containing dendrobium extract
DPPH free radical ability, superoxide anion resisitance ability and scavenging hydroxyl ability, it is prepared by the present invention containing dendrobium nobile to illustrate
The wrinkle resistant oxidation resistant ability of patch liquid of extracting solution.
Test method: specific test method uses spectrophotometric standard method according to DPPH free radical scavenging ability, and hydroxyl is certainly
α-deoxy-D-ribose standard method is used by base Scavenging activity, the measurement of ultra-oxygen anion free radical Scavenging activity is using adjacent benzene
Triphenol standard method carries out.
Fig. 1 is the oxidation resistance comparison result of wrinkle resistant patch liquid made from Examples 1 to 3 and comparative example 1, can by Fig. 1
To find out, the oxidation resistance of embodiment 1 is best, and illustrating each component compatibility rationally mentions facial mask liquid Scavenging ability significantly
Height can reach higher to reach better antioxidant and anti-aging purpose, and within the scope of the weight proportion that the present invention limits
Oxidation resistance.
Fig. 2 is that the oxidation resistance of wrinkle resistant patch liquid made from embodiment 1, embodiment 4~5 and comparative example 2~3 compares knot
Fruit, as seen from Figure 2, with the increase of solid-to-liquid ratio in dendrobium extract preparation method, the oxidation resistance of wrinkle resistant patch liquid
The oxidation resistance of first increases and then decreases, 1 solid-to-liquid ratio of embodiment wrinkle resistant patch liquid when being 1:15 is best.
Fig. 3 is the oxidation resistance comparison result of embodiment 1, wrinkle resistant patch liquid made from embodiment 6~7, can be with by Fig. 3
Find out, with the increase of ultrasonic extraction temperature in dendrobium extract preparation method, the oxidation resistance of wrinkle resistant patch liquid first increases
After reduce, the oxidation resistance of wrinkle resistant patch is most strong when 1 temperature of embodiment is 27 DEG C, illustrate at this temperature, and dendrobium nobile, which extracts, imitates
Rate highest and the active constituent in dendrobium nobile can be made to play optimal drug effect.
Fig. 4 is that the oxidation resistance of wrinkle resistant patch liquid made from embodiment 1, embodiment 8~10 and comparative example 4~5 compares
As a result, as seen from Figure 4, changing the enzyme dosage or type for destroying plant cell wall in dendrobium extract preparation method,
The oxidation resistance of wrinkle resistant patch can be impacted, with the increase for not having dosage, the oxidation resistance of wrinkle resistant patch first increases
After reduce, when enzyme dosage is dendrobium nobile weight 0.8%, the oxidation resistance of wrinkle resistant patch reaches maximum.
Fig. 5 is that the oxidation resistance of wrinkle resistant patch liquid made from embodiment 1, embodiment 11~12 and comparative example 6 compares knot
Fruit, as seen from Figure 5, change hyaluronic acid in moisturizer, Cer NP, glycerol weight proportion will affect it is obtained anti-
The oxidation resistance of wrinkle patch liquid, when hyaluronic acid, Cer NP, glycerol are 1:2:4 proportion by weight, that produces is anti-
The oxidation resistance of wrinkle patch is best, and finds by many experiments, in the range of weight ratio 1:1~3:3~5 of the present invention,
Preferable antioxidant effect can be reached.
Fig. 6 is the oxidation resistance comparison result of embodiment 1, wrinkle resistant patch liquid made from embodiment 13~14, can by Fig. 6
To find out, the oxidation resistance of wrinkle resistant patch influenced by preparation method it is smaller, so that the large-scale production for wrinkle resistant patch provides
Advantageous condition.
Fig. 7 is the oxidation resistance comparison result of wrinkle resistant patch liquid made from embodiment 1 and comparative example 7~8, can by Fig. 7
To find out, compared with individually preparing dendrobium extract using enzymatic isolation method or ultrasonic extraction, the present invention passes through enzymatic isolation method and ultrasound
Synergistic effect is extracted, the extraction efficiency of dendrobium nobile active constituent is improved, helps to improve the oxidation resistance of wrinkle resistant patch liquid.
The above, only of the invention illustrates embodiment, not to the present invention in any form with substantial limitation,
It should be pointed out that for those skilled in the art, under the premise of not departing from the method for the present invention, that makes several changes
It also should be regarded as protection scope of the present invention into supplement；All those skilled in the art, do not depart from spirit of that invention and
In the case where range, using the equivalent variations of a little change, modification and differentiation that disclosed above technology contents are made, it is
Equivalent embodiment of the invention；Meanwhile any equivalent variations that all substantial technologicals according to the present invention do above-described embodiment
Change, modification and differentiation, still fall within protection scope of the present invention.
Claims (10)
1. a kind of wrinkle resistant patch liquid containing dendrobium extract, which is characterized in that consist of the following components in percentage by weight: stone
Dry measure used in former times extracting solution 5~25%, grape pip essential oil 5~10%, vitamin 5~10%, moisturizer 10~20%, carbomer 0.02~
0.2%, triethanolamine 0.01~0.1%, preservative 0.1%~0.5%, surplus are water.
2. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 1, which is characterized in that the dendrobium nobile mentions
Take liquid the preparation method comprises the following steps: dendrobium fresh strips are cleaned, dissection, are put into wall-breaking machine, water homogenate is added, adds dendrobium nobile weight
The enzyme of 0.5~1% destruction plant cell wall, and sonic oscillation extracts, and collects fresh dendrobium nobile slurries, filters and extracts up to fresh dendrobium nobile
Liquid.
3. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 2, which is characterized in that the dendrobium nobile is cut
Section is to 2~3cm size.
4. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 2, which is characterized in that press dendrobium nobile and water
Solid-to-liquid ratio be 1:10~20 be added water homogenate.
5. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 2, which is characterized in that the ultrasound vibration
Swing extraction conditions are as follows: control temperature is at 25~30 DEG C in 35000r/min ultrasonic extraction 10min.
6. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 2, which is characterized in that the destruction is planted
The enzyme of object cell wall is one of cellulase or 1,4 beta-glucanase or a variety of combinations.
7. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 2, which is characterized in that use 200 mesh
Gauze filtering.
8. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 1 or 2, which is characterized in that the guarantor
The mixture that humectant is hyaluronic acid, Cer NP, glycerol are 1:1~3:3~5 by weight.
9. a kind of wrinkle resistant patch liquid containing dendrobium extract according to claim 1 or 2, which is characterized in that described anti-
Rotten agent is sorb potassium alcoholate.
10. a kind of preparation method of wrinkle resistant patch containing dendrobium extract described in claim 1, which is characterized in that including
Following steps:
S1, dendrobium fresh strips are cleaned, dissection, is put into wall-breaking machine, water homogenate is added, and sonic oscillation extracts, and collects fresh dendrobium nobile
Slurries filter up to fresh dendrobium extract；
S2, carbomer is dissolved in deionized water, pH to 6.0-7.5 is adjusted with triethanolamine, dendrobium nobile is then added according to the proportion
Extracting solution, grape pip essential oil, vitamin and moisturizer, preservative is added after mixing, stirs evenly, and adjusts pH value in 5.8-
Between 6.5, the facial mask liquid containing dendrobium extract is obtained；
S3, above-mentioned facial mask liquid is filled into the facial mask bag for be placed with facial mask cloth wrinkle resistant patch is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910332274.3A CN110037968B (en) | 2019-04-24 | 2019-04-24 | Anti-wrinkle patch containing dendrobium extract and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910332274.3A CN110037968B (en) | 2019-04-24 | 2019-04-24 | Anti-wrinkle patch containing dendrobium extract and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110037968A true CN110037968A (en) | 2019-07-23 |
| CN110037968B CN110037968B (en) | 2022-05-24 |
Family
ID=67278966
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910332274.3A Active CN110037968B (en) | 2019-04-24 | 2019-04-24 | Anti-wrinkle patch containing dendrobium extract and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110037968B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112972288A (en) * | 2021-03-31 | 2021-06-18 | 烟台泊奥俪泉商贸有限公司 | Anti-aging collagen skin cream and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20160009752A (en) * | 2014-07-16 | 2016-01-27 | 재단법인 전남생물산업진흥원 | Composition comprising Dendrobium moniliforme Extract for skin whitening and anti-wrinkle Effects, Functional food and Korean herb cosmetic manufactured by using them |
| CN108904429A (en) * | 2018-09-28 | 2018-11-30 | 安徽霍山黑石渡生物科技有限公司 | A kind of dendrobium candidum anti-ageing face mask and preparation method thereof |
| CN109232759A (en) * | 2018-09-19 | 2019-01-18 | 北京明弘科贸有限责任公司 | A kind of preparation process and its application of dendrobium nobile micromolecular polysaccharide extracting solution |
-
2019
- 2019-04-24 CN CN201910332274.3A patent/CN110037968B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20160009752A (en) * | 2014-07-16 | 2016-01-27 | 재단법인 전남생물산업진흥원 | Composition comprising Dendrobium moniliforme Extract for skin whitening and anti-wrinkle Effects, Functional food and Korean herb cosmetic manufactured by using them |
| CN109232759A (en) * | 2018-09-19 | 2019-01-18 | 北京明弘科贸有限责任公司 | A kind of preparation process and its application of dendrobium nobile micromolecular polysaccharide extracting solution |
| CN108904429A (en) * | 2018-09-28 | 2018-11-30 | 安徽霍山黑石渡生物科技有限公司 | A kind of dendrobium candidum anti-ageing face mask and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112972288A (en) * | 2021-03-31 | 2021-06-18 | 烟台泊奥俪泉商贸有限公司 | Anti-aging collagen skin cream and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110037968B (en) | 2022-05-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105997735B (en) | A kind of natural hair-washing hair-care articles and its preparation method and application | |
| CN106309280B (en) | A kind of Ginger P.E and its preparation method and application | |
| CN105476939B (en) | A kind of facial mask essence of Transdermal absorption metabolism promoting | |
| CN105878102A (en) | Facial mask containing punica granatum fruit extract and preparation method of facial mask | |
| CN105287292A (en) | Whitening moisture-retention face cream and preparation method thereof | |
| CN107898686B (en) | Agar extract, preparation method and application thereof in cosmetics | |
| CN111419760A (en) | Fresh black tiger leaf extracting solution and preparation method and application thereof | |
| CN108175741A (en) | A kind of anti-aging beauty-care frost and preparation method thereof | |
| CN105125429A (en) | Anti-aging and moisturizing facial mask | |
| CN110037968A (en) | A kind of wrinkle resistant patch and preparation method thereof containing dendrobium extract | |
| CN107224418B (en) | Natural sleep-aiding beauty mask and preparation method thereof | |
| CN108309851A (en) | A kind of face cream with anti-senescence function | |
| CN108379218A (en) | A kind of anti-aging beauty-care frost and preparation method thereof | |
| CN107320357A (en) | A kind of cosmetics containing polysaccharide | |
| CN111494290A (en) | Moisturizing mask liquid and preparation method thereof | |
| CN108888554B (en) | Stem cell beauty emulsion with skin tendering and spot lightening functions and preparation method thereof | |
| CN110101616A (en) | A kind of pregnant woman releives facial mask and preparation method thereof | |
| CN106333883A (en) | Chayote stock solution, extraction method thereof, composition containing chayote stock solution and application of chayote stock solution | |
| CN108096177A (en) | A kind of compound stem cell factor cosmetic composition and its application | |
| CN107536780A (en) | A kind of removing acne and eliminating mark shin moisturizer and preparation method thereof | |
| CN107375154A (en) | A kind of nti-freckle white composition and preparation method thereof only | |
| CN105878152A (en) | Pasty bath salt containing punica granatum fruit extract | |
| CN108042425B (en) | Whitening and moisturizing essence and preparation method thereof | |
| CN108451811A (en) | A kind of delay aging drug facial mask | |
| CN108338960A (en) | A kind of tender skin face mask of traditional Chinese medicine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |