CN110037968B - Anti-wrinkle patch containing dendrobium extract and preparation method thereof - Google Patents
Anti-wrinkle patch containing dendrobium extract and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a crease-resistant paster containing dendrobium extract and a preparation method thereof, wherein the crease-resistant paster comprises the following components in percentage by weight: 5-25% of a dendrobium extract, 5-10% of grape seed essential oil, 5-10% of vitamins, 10-20% of a humectant, 0.02-0.2% of carbomer, 0.01-0.1% of triethanolamine, 0.1-0.5% of a preservative and the balance of water; through reasonable matching of different raw materials, the skin-care product can repair damaged cells of the skin, preserve moisture, nourish, fade color spots, eliminate fine wrinkles, improve the activity of cells, promote the synthesis of collagen, recover the elasticity of the skin and delay the aging of the skin; meanwhile, the wall breaking rate of the dendrobium medicinal material is improved by breaking through a wall breaking machine, performing enzymolysis and then utilizing ultrasonic extraction, the dissolution and utilization rate of effective active ingredients in the dendrobium are facilitated, and the absorption effect of skin on the effective ingredients is improved.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a crease-resistant paster containing a dendrobium extract and a preparation method of the crease-resistant paster.
Background
The modern society has fast pace of life, especially in large cities, the working intensity is high, and the health is not facilitated; after people are tired excessively, the skin color is poor, and the loose skin and the increase of wrinkles are caused by the high-intensity work for a long time; aiming at the problem, the skin care product full of Linglan exists in the market, and has the effects of moisturizing, whitening, moisturizing, controlling oil, moisturizing skin, shrinking pores and the like to a certain degree; however, these skin care products generally only have the effect of preventing skin aging, and once the skin quality has deteriorated, such as increased wrinkles, most of the cosmetics on the market are useless, and many middle-aged women often choose wrinkle-removing operation for wrinkle-removing beauty, although the effect is remarkable and quick, there are great risks and side effects, and the cost is not high.
Therefore, providing a skin care product with remarkable wrinkle removing effect is one of the key points of research and development of researchers in the field of cosmetics; the facial mask is a common skin care product, and part of high-quality facial masks can provide double anti-aging effects, stimulate cell neogenesis energy, improve the texture and the skin color uniformity of the surface layer of the skin, and enable the skin to be more delicate, so the facial mask is deeply loved by people; however, cosmetics such as commercially available facial masks often fail to remove wrinkles that have already been generated efficiently.
The dendrobium is a famous and precious traditional Chinese medicinal material, and is determined by modern scientific technology, the dendrobium contains abundant dendrobium active polysaccharide, the content of the dendrobium active polysaccharide is 25% or more, and the dendrobium active polysaccharide has the effects of resisting tumors, diminishing inflammation, reducing blood pressure and blood sugar, inhibiting lipid peroxidation, resisting aging, accelerating the recovery of physique, improving the number of human white blood cells, assisting in the treatment of cancers, improving the immunity of human bodies and the like; the dendrobium officinale also contains dendrobine, and the modern pharmacological experiments show that the dendrobine has certain effects of inhibiting growth and killing tumor cells, has obvious anti-tumor activity, reduces the toxic and side effects of radiotherapy and chemotherapy on a human body by improving the immunity of the human body, and can also reduce blood sugar and resist aging; the dendrobium contains 18 kinds of amino acids, can meet the requirements of human bodies for the amino acids, and has the health-care effects of resisting oxidation, resisting aging, reducing blood sugar, protecting liver, moistening lung, softening blood vessels, nourishing stomach, protecting stomach and the like; meanwhile, the dendrobium contains various trace elements, can promote metabolism of a human body, recover cell activity and play a role in delaying senescence.
Disclosure of Invention
The invention aims to solve the problems in the prior art, and provides a crease-resistant paster containing a dendrobium extract and a preparation method thereof, which can effectively increase collagen and effectively eliminate facial wrinkles.
In order to achieve the purpose, the invention adopts the technical scheme that:
a wrinkle-resistant paster liquid containing a dendrobe extracting solution comprises the following components in percentage by weight: 5-25% of dendrobe extracting solution, 5-10% of grape seed essential oil, 5-10% of vitamins, 10-20% of humectant, 0.02-0.2% of carbomer, 0.01-0.1% of triethanolamine, 0.1-0.5% of preservative and the balance of water.
The invention also provides a preparation method of the dendrobium extract, which comprises the following steps: cleaning and cutting fresh dendrobium strips, placing the fresh dendrobium strips into a wall breaking machine, adding water to homogenate, adding 0.5-1% of enzyme for breaking plant cell walls, extracting the dendrobium by ultrasonic oscillation, collecting fresh dendrobium pulp, and filtering to obtain the fresh dendrobium extract.
As a further limitation of the technical scheme, the dendrobium nobile is cut into segments with the size of 2-3 cm.
As a further limitation of the technical scheme, adding water into the dendrobium according to the solid-liquid ratio of 1: 10-20 of dendrobium to water for homogenizing.
As a further limitation of the above technical solution, the ultrasonic oscillation extraction conditions are: controlling the temperature at 25-30 ℃, and performing ultrasonic extraction at 35000r/min for 10 min.
As a further limitation of the above technical solution, the enzyme for destroying plant cell walls is one or a combination of cellulase and beta-glucanase.
As a further limitation of the technical proposal, 200-mesh gauze filtration is adopted.
As a further limitation of the technical scheme, the humectant is a mixture of hyaluronic acid, ceramide 3 and glycerol in a weight ratio of 1: 1-3: 3-5.
As a further limitation of the above technical solution, the preservative is potassium sorbate.
The invention provides a preparation method of a crease-resistant paster containing a dendrobium extract, which comprises the following steps:
s1, cleaning fresh dendrobium strips, cutting into sections, putting the sections into a wall breaking machine, adding water for homogenate, performing ultrasonic oscillation extraction, collecting fresh dendrobium pulp, and filtering to obtain fresh dendrobium extract;
s2, dissolving carbomer in deionized water, adjusting the pH to 6.0-7.5 by using triethanolamine, adding the dendrobium extract, grape seed essential oil, vitamins and a humectant according to the proportion, uniformly mixing, adding a preservative, uniformly stirring, and adjusting the pH value to 5.8-6.5 to obtain the mask liquid containing the dendrobium extract;
s3, filling the mask liquid into a mask bag with mask cloth to make into wrinkle-proof patch.
Compared with the prior art, the invention has the beneficial effects that:
(1) when the anti-wrinkle patch containing the dendrobium extract is used, damaged cells of the skin can be repaired, moisture is preserved, the skin is nourished, color spots are lightened, fine wrinkles are eliminated, cell activity is improved, collagen synthesis is promoted, skin elasticity is restored, and skin aging is delayed.
(2) The dendrobium wrinkle-resistant facial mask selects deionized water, glycerin, a dendrobium extract, grape seed essential oil, hyaluronic acid, vitamins, ceramide 3, carbomer, triethanolamine, potassium sorbate and the like as raw materials of the dendrobium wrinkle-resistant patch, has the effects of whitening, delaying skin aging, moisturizing and resisting wrinkles by reasonably matching the components, has a good repairing effect on the skin of modern women, can provide the most sufficient nutrients for the skin in the shortest time, enables the skin to recover the vitality, promotes the discharge of cytotoxins, and repairs skin problems caused by external factors and changes in the human body.
(3) The wall breaking rate of the dendrobium cells is improved by breaking through a wall breaking machine, performing enzymolysis and then utilizing ultrasonic extraction, and the dissolution and utilization rate of effective active ingredients in the dendrobium are facilitated.
Drawings
FIG. 1 shows the results of comparing the antioxidant ability of the wrinkle-preventing patch liquids obtained in examples 1 to 3 and comparative example 1.
FIG. 2 is a graph showing the results of comparing the antioxidant ability of the wrinkle-preventing patch liquids obtained in examples 1, 4 to 5, and 2 to 3.
FIG. 3 is a graph showing the results of comparing the antioxidant ability of the wrinkle-preventing patch liquids obtained in examples 1 and 6 to 7.
FIG. 4 is a graph showing the results of comparing the antioxidant ability of the wrinkle-preventing patch liquids obtained in examples 1, 8 to 10, and 4 to 5.
FIG. 5 shows the results of comparing the antioxidant ability of the wrinkle-preventing patch liquids obtained in examples 1, 11 to 12 and comparative example 6.
FIG. 6 is a graph showing the results of comparing the antioxidant ability of the wrinkle-preventing patch liquids obtained in examples 1 and 13 to 14.
FIG. 7 shows the results of comparing the antioxidant ability of the wrinkle-preventing patch liquids obtained in example 1 and comparative examples 7 to 8.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more clearly apparent, the present invention is further described in detail with reference to the following embodiments; it should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention; reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.
Example 1
A wrinkle-resistant patch liquid containing a dendrobium extract is composed of the following components in percentage by weight: the dendrobium nobile lindl essence oil moisturizer comprises 15% of dendrobium nobile lindl extract, 8% of grape seed essential oil, 8% of vitamin, 15% of moisturizer, 0.1% of carbomer, 0.05% of triethanolamine, 0.3% of potassium sorbate and the balance of water.
The humectant is a mixture of hyaluronic acid, ceramide 3 and glycerol in a weight ratio of 1:2: 4.
The preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
The preparation method of the anti-wrinkle patch containing the dendrobium extract comprises the following steps:
s1, cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, putting the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain a fresh dendrobium extracting solution;
s2, dissolving carbomer in percentage by weight in deionized water, adjusting the pH to 7.0 by using triethanolamine, then adding the dendrobium extract, the grape seed essential oil, the vitamins and the humectant according to the proportion, uniformly mixing, adding potassium sorbate, uniformly stirring, and adjusting the pH value to 6.0 to obtain the mask liquid containing the dendrobium extract;
s3, filling the facial mask liquid into a facial mask bag with facial mask cloth to prepare the anti-wrinkle patch.
Example 2
The embodiment provides a wrinkle-resistant patch liquid containing dendrobium extract, which is different from the wrinkle-resistant patch liquid in embodiment 1 in that the wrinkle-resistant patch liquid comprises the following components in percentage by weight: 5% of dendrobium extract, 10% of grape seed essential oil, 10% of vitamin, 10% of humectant, 0.2% of carbomer, 0.01% of triethanolamine, 0.1% of potassium sorbate and the balance of water.
Example 3
The embodiment provides a wrinkle-resistant patch liquid containing dendrobium extract, which is different from the wrinkle-resistant patch liquid in embodiment 1 in that the wrinkle-resistant patch liquid comprises the following components in percentage by weight: 25% of dendrobium extract, 5% of grape seed essential oil, 5% of vitamin, 5% of humectant, 0.02% of carbomer, 0.1% of triethanolamine, 0.5% of potassium sorbate and the balance of water.
Example 4
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the dendrobium extract in embodiment 1 in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 10 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Example 5
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the dendrobium extract in embodiment 1 in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 20 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Example 6
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the dendrobium extract in embodiment 1 in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 25 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Example 7
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the dendrobium extract in embodiment 1 in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 30 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Example 8
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the dendrobium extract in embodiment 1 in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.5% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Example 9
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the dendrobium extract in embodiment 1 in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 1% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Example 10
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the dendrobium extract in embodiment 1 in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding beta-glucanase with the weight of 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Example 11
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the wrinkle-resistant patch liquid in embodiment 1 in that the humectant is a mixture of hyaluronic acid, ceramide 3 and glycerol in a weight ratio of 1:1: 5.
Example 12
The embodiment provides a wrinkle-resistant patch liquid containing a dendrobium extract, which is different from the wrinkle-resistant patch liquid in embodiment 1 in that the humectant is a mixture of hyaluronic acid, ceramide 3 and glycerol in a weight ratio of 1:3: 3.
Example 13
The embodiment provides a wrinkle-resistant paster liquid containing dendrobium extract, which is different from the embodiment 1 in that the preparation method of the wrinkle-resistant paster containing dendrobium extract comprises the following steps:
s1, cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, putting the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain a fresh dendrobium extracting solution;
s2, dissolving carbomer in percentage by weight in deionized water, adjusting the pH to 6.0 by using triethanolamine, then adding the dendrobium extract, the grape seed essential oil, the vitamins and the humectant according to the proportion, uniformly mixing, adding potassium sorbate, uniformly stirring, and adjusting the pH value to 5.8 to obtain the mask liquid containing the dendrobium extract;
s3, filling the facial mask liquid into a facial mask bag with facial mask cloth to prepare the anti-wrinkle patch.
Example 14
The embodiment provides a wrinkle-resistant paster liquid containing dendrobium extract, which is different from the embodiment 1 in that the preparation method of the wrinkle-resistant paster containing dendrobium extract comprises the following steps:
s1, cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, putting the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain a fresh dendrobium extracting solution;
s2, dissolving carbomer in percentage by weight in deionized water, adjusting the pH to 7.5 by using triethanolamine, adding a dendrobium extract, grape seed essential oil, vitamins and a humectant according to a ratio, uniformly mixing, adding potassium sorbate, uniformly stirring, and adjusting the pH value to 6.5 to obtain a mask liquid containing the dendrobium extract;
s3, filling the facial mask liquid into a facial mask bag with facial mask cloth to prepare the anti-wrinkle patch.
Comparative example 1
Compared with the embodiment 1, the wrinkle-resistant patch liquid containing the dendrobium extract is characterized by comprising the following components in percentage by weight: 2% of dendrobium extract, 12% of grape seed essential oil, 12% of vitamin, 15% of humectant, 0.1% of carbomer, 0.05% of triethanolamine, 0.3% of preservative and the balance of water.
Comparative example 2
Compared with example 1, the wrinkle-resistant paster liquid containing the dendrobium extract is characterized in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting the fresh dendrobium strips into 2-3 cm, putting the dendrobium strips into a wall breaking machine, adding water with the volume 8 times that of the dendrobium, homogenizing the dendrobium strips, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering the pulp by using a 200-mesh gauze to obtain the fresh dendrobium extract.
Comparative example 3
Compared with example 1, the wrinkle-resistant paster liquid containing the dendrobium extract is characterized in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 25 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Comparative example 4
Compared with example 1, the wrinkle-resistant paster liquid containing the dendrobium extract is characterized in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.3% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Comparative example 5
Compared with example 1, the wrinkle-resistant paster liquid containing the dendrobium extract is characterized in that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 25 times that of the dendrobium to homogenate, adding cellulase with the weight 1.2% of the dendrobium, performing ultrasonic extraction at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Comparative example 6
The comparison example provides a wrinkle-resistant patch liquid containing a dendrobium extract, and compared with example 1, the wrinkle-resistant patch liquid is different in that the humectant is a mixture of hyaluronic acid, ceramide 3 and glycerol in a weight ratio of 1:4: 2.
Comparative example 7
The comparative example provides a wrinkle-resistant paster liquid containing a dendrobium extract, and compared with example 1, the difference is that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times that of the dendrobium to homogenate, adding cellulase with the weight 0.8% of the dendrobium, leaching for 30min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Comparative example 8
The comparative example provides a wrinkle-resistant paster liquid containing a dendrobium extract, and compared with example 1, the difference is that the preparation method of the dendrobium extract comprises the following steps: cleaning fresh dendrobium strips, cutting into segments of 2-3 cm, placing the segments into a wall breaking machine, adding water with the volume 15 times of the weight of dendrobium, homogenizing, ultrasonically extracting at 35000r/min for 10min at 27 ℃, collecting fresh dendrobium pulp, and filtering with a 200-mesh gauze to obtain the fresh dendrobium extract.
Test examples
The anti-wrinkle patch liquid containing the dendrobium extract prepared by the invention is shown by comparing the DPPH free radical removing capacity, the superoxide anion resisting capacity and the hydroxyl free radical removing capacity of the anti-wrinkle patch liquid containing the dendrobium extract prepared by different embodiments of the invention and comparative examples.
The test method comprises the following steps: the specific test method adopts a spectrophotometric standard method according to DPPH free radical scavenging capacity, adopts an alpha-deoxy-D-ribose standard method according to hydroxyl free radical scavenging capacity, and adopts a pyrogallol standard method to measure superoxide anion free radical scavenging capacity.
Fig. 1 shows the results of comparing the antioxidant capacity of the wrinkle-resistant patch liquid prepared in examples 1 to 3 and comparative example 1, and it can be seen from fig. 1 that the antioxidant capacity of example 1 is the best, which shows that the reasonable compatibility of the components greatly improves the ability of the facial mask liquid to scavenge free radicals, so as to achieve better antioxidant and anti-aging purposes, and within the weight ratio range defined by the present invention, higher antioxidant capacity can be achieved.
Fig. 2 is a comparison result of the antioxidant capacity of the wrinkle-resistant patch liquid prepared in example 1, examples 4 to 5 and comparative examples 2 to 3, and it can be seen from fig. 2 that the antioxidant capacity of the wrinkle-resistant patch liquid increases and then decreases with the increase of the solid-to-liquid ratio in the preparation method of the dendrobium extract, and the antioxidant capacity of the wrinkle-resistant patch liquid is the best when the solid-to-liquid ratio of example 1 is 1: 15.
Fig. 3 is a comparison result of the antioxidant capacity of the wrinkle-resistant patch liquid prepared in examples 1 and 6 to 7, and it can be seen from fig. 3 that the antioxidant capacity of the wrinkle-resistant patch liquid increases first and then decreases as the ultrasonic extraction temperature in the preparation method of the dendrobium extract solution increases, and the antioxidant capacity of the wrinkle-resistant patch is strongest when the temperature of example 1 is 27 ℃, which indicates that the dendrobium extraction efficiency is highest and the active ingredients in dendrobium can exert the best efficacy at the temperature.
Fig. 4 is a comparison result of the antioxidant capacity of the wrinkle-resistant patch liquids prepared in examples 1, 8 to 10 and 4 to 5, and it can be seen from fig. 4 that changing the amount or kind of enzymes that destroy plant cell walls in the preparation method of the dendrobium extract liquid affects the antioxidant capacity of the wrinkle-resistant patch, the antioxidant capacity of the wrinkle-resistant patch increases and then decreases with the increase of the unused amount, and the antioxidant capacity of the wrinkle-resistant patch reaches the maximum when the amount of the enzymes is 0.8% of the weight of dendrobium.
Fig. 5 is a comparison result of the antioxidant capacity of the wrinkle-resistant patch liquid prepared in example 1, examples 11 to 12 and comparative example 6, and it can be seen from fig. 5 that changing the weight ratio of hyaluronic acid, ceramide 3 and glycerin in the humectant affects the antioxidant capacity of the prepared wrinkle-resistant patch liquid, when the weight ratio of hyaluronic acid, ceramide 3 and glycerin is 1:2:4, the antioxidant capacity of the prepared wrinkle-resistant patch is optimal, and a large number of experiments show that a better antioxidant effect can be achieved within the weight ratio of 1: 1-3: 3-5 of the invention.
Fig. 6 is a comparison result of the antioxidant capacity of the wrinkle resistant patch liquids prepared in examples 1 and 13 to 14, and it can be seen from fig. 6 that the antioxidant capacity of the wrinkle resistant patch is less affected by the preparation method, thereby providing favorable conditions for mass production of the wrinkle resistant patch.
Fig. 7 is a comparison result of the antioxidant capacity of the wrinkle-resistant patch liquid prepared in example 1 and comparative examples 7 to 8, and it can be seen from fig. 7 that, compared with a method for preparing a dendrobium extract by using an enzymolysis method or an ultrasonic extraction method alone, the extraction efficiency of the active ingredients of dendrobium is improved by the synergistic effect of the enzymolysis method and the ultrasonic extraction, which is beneficial to improving the antioxidant capacity of the wrinkle-resistant patch liquid.
While the invention has been described with respect to specific embodiments thereof, it will be understood by those skilled in the art that the foregoing and other changes, omissions and deviations in the form and detail thereof may be made without departing from the scope of this invention; those skilled in the art should appreciate that they can readily use the disclosed conception and specific embodiments as a basis for designing or modifying other structures for carrying out the same purposes of the present invention without departing from the spirit and scope of the invention; meanwhile, any equivalent changes, modifications and alterations of the above embodiments according to the spirit and techniques of the present invention are also within the scope of the present invention.
Claims (5)
1. The anti-wrinkle paster liquid containing the dendrobium extract is characterized by comprising the following components in percentage by weight: 5-25% of a dendrobium extract, 5-10% of grape seed essential oil, 5-10% of vitamins, 10-20% of a humectant, 0.02-0.2% of carbomer, 0.01-0.1% of triethanolamine, 0.1-0.5% of a preservative, and the balance of water;
the preparation method of the dendrobium extract comprises the following steps: cleaning and cutting fresh dendrobium strips, putting the fresh dendrobium strips into a wall breaking machine, adding water into the dendrobium strips according to the weight-volume ratio of 1: 10-20 of the dendrobium to water for homogenate, adding an enzyme for breaking plant cell walls, the weight of the enzyme is 0.5-1% of that of the dendrobium, performing ultrasonic oscillation extraction, collecting fresh dendrobium pulp, and filtering to obtain a dendrobium extracting solution;
the enzyme for destroying the plant cell wall is one or more of cellulase or beta-glucanase;
the ultrasonic oscillation extraction conditions are as follows: controlling the temperature at 25-30 ℃, and carrying out ultrasonic extraction at 35000r/min for 10 min;
the humectant is a mixture of hyaluronic acid, ceramide 3 and glycerol in a weight ratio of 1: 1-3: 3-5.
2. The anti-wrinkle patch liquid containing dendrobium nobile lindl extract as claimed in claim 1, wherein the dendrobium nobile lindl is cut into segments with the size of 2-3 cm.
3. The anti-wrinkle patch liquid containing dendrobium nobile lindl extract as claimed in claim 1, wherein 200 mesh gauze is adopted for filtration.
4. The wrinkle-resistant patch liquid containing dendrobium nobile lindl extract as claimed in claim 1, wherein the preservative is potassium sorbate.
5. A method for preparing a wrinkle resistant patch containing the wrinkle resistant patch fluid of claim 1, comprising the steps of:
s1, preparing a dendrobe extracting solution;
s2, dissolving carbomer in deionized water, adjusting the pH to 6.0-7.5 by using triethanolamine, adding a dendrobium extract, grape seed essential oil, vitamins and a humectant according to the proportion, uniformly mixing, adding a preservative, uniformly stirring, and adjusting the pH value to be 5.8-6.5 to obtain a crease-resistant paster liquid containing the dendrobium extract;
and S3, filling the anti-wrinkle patch liquid into a mask bag with mask cloth to prepare the anti-wrinkle patch.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20160009752A (en) * | 2014-07-16 | 2016-01-27 | 재단법인 전남생물산업진흥원 | Composition comprising Dendrobium moniliforme Extract for skin whitening and anti-wrinkle Effects, Functional food and Korean herb cosmetic manufactured by using them |
| CN108904429A (en) * | 2018-09-28 | 2018-11-30 | 安徽霍山黑石渡生物科技有限公司 | A kind of dendrobium candidum anti-ageing face mask and preparation method thereof |
| CN109232759A (en) * | 2018-09-19 | 2019-01-18 | 北京明弘科贸有限责任公司 | A kind of preparation process and its application of dendrobium nobile micromolecular polysaccharide extracting solution |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20160009752A (en) * | 2014-07-16 | 2016-01-27 | 재단법인 전남생물산업진흥원 | Composition comprising Dendrobium moniliforme Extract for skin whitening and anti-wrinkle Effects, Functional food and Korean herb cosmetic manufactured by using them |
| CN109232759A (en) * | 2018-09-19 | 2019-01-18 | 北京明弘科贸有限责任公司 | A kind of preparation process and its application of dendrobium nobile micromolecular polysaccharide extracting solution |
| CN108904429A (en) * | 2018-09-28 | 2018-11-30 | 安徽霍山黑石渡生物科技有限公司 | A kind of dendrobium candidum anti-ageing face mask and preparation method thereof |
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