CN108143648B - Preparation method of mask containing peony essential oil - Google Patents
Preparation method of mask containing peony essential oil Download PDFInfo
- Publication number
- CN108143648B CN108143648B CN201810187627.0A CN201810187627A CN108143648B CN 108143648 B CN108143648 B CN 108143648B CN 201810187627 A CN201810187627 A CN 201810187627A CN 108143648 B CN108143648 B CN 108143648B
- Authority
- CN
- China
- Prior art keywords
- essential oil
- peony
- parts
- minutes
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a preparation method of a mask containing peony essential oil, which comprises the following steps: preparing peony essential oil; mixing glycerol, hyaluronic acid and water, and stirring at 70-80 deg.C to obtain water phase liquid; mixing vitamin E, fructus Citri Tangerinae essential oil, radix Rhodiolae essential oil, grape seed essential oil, and peony essential oil, and stirring at 70-80 deg.C to obtain oil phase liquid; adding the oil phase liquid into the water phase liquid, homogenizing for 15-20 minutes to obtain a mask base liquid, immersing the silk mask cloth into the mask base liquid for 20-30 minutes, and taking out to obtain the mask containing the peony essential oil. The effective components in the facial mask prepared by the method can quickly permeate into the skin of a human body, and have the effects of tendering and whitening, resisting wrinkles, preventing aging, fading color spots, enhancing skin elasticity and the like.
Description
Technical Field
The invention relates to the field of mask preparation, and particularly relates to a preparation method of a mask containing peony essential oil.
Background
With the progress of society, the development of economy and the continuous improvement of the living standard of people, the requirements of people on beauty and skin care cosmetics are higher and higher, and the beauty and skin care cosmetics are developed in the direction of naturalization, nutrition and curative effect. However, most of the various cosmetic products on the market contain harmful chemical substances to human body, such as toxic and harmful substances containing lead, mercury and the like, and these cosmetic products are easy to cause skin allergy and damage to human organs and functions. From the 80 s of the last century, skin experts find that various natural raw materials added into skin care products have good nourishing effect on skin, have no toxic or side effect, and particularly have remarkable effect when effective components are extracted from plants and added into the skin care products.
The facial mask has multiple effects of repairing, resisting aging, resisting wrinkle, whitening, moisturizing, removing freckles and the like, and is suitable for various skin problems caused by aging, improper nursing and the like. There are many kinds of facial masks, such as moisturizing facial masks, anti-aging/firming facial masks, spot-removing facial masks, whitening facial masks, and the like. Plant essential oil components are added into a plurality of facial masks in the market, the peony essential oil is volatile oily liquid extracted and separated from peony, is rich in various amino acids and trace elements, has the effects of resisting sensitivity, improving blood circulation, maintaining beauty and keeping young, promoting cell regeneration, relieving skin aging, regulating skin problems and the like, and is a raw material of cosmetics. However, the essential oil added in the mask at present has many impurities and low purity, and contains a large amount of chemical compositions.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method of a mask containing peony essential oil, and the effective components in the mask prepared by the method can rapidly permeate into the skin of a human body, and have the effects of whitening, resisting wrinkles, preventing aging, fading color spots, enhancing the skin elasticity and the like.
The invention provides a preparation method of a mask containing peony essential oil, which comprises the following steps:
s1, mixing fresh peony petals with water, crushing, performing ultrasonic treatment, and performing centrifugal separation to obtain peony juice;
s2, adding super absorbent resin into the peony flower juice obtained in S1, stirring for 10-20 minutes, and standing for 20-30 minutes to obtain a gel-like peony extract;
s3, performing supercritical carbon dioxide extraction on the gel-like peony extract obtained in the S2 to obtain peony essential oil;
s4, weighing 10-15 parts of glycerol, 8-12 parts of hyaluronic acid, 1-2 parts of vitamin E, 5-8 parts of orange essential oil, 2-4 parts of rhodiola rosea essential oil, 6-9 parts of grape seed essential oil, 20-25 parts of water and 7-10 parts of peony essential oil prepared in S3 for later use;
s5, mixing the glycerol, the hyaluronic acid and the water weighed in the S4, and uniformly stirring at 70-80 ℃ to obtain an aqueous phase liquid;
s6, mixing the vitamin E, the orange essential oil, the rhodiola essential oil, the grape seed essential oil and the peony essential oil weighed in the S4, and stirring uniformly at 70-80 ℃ to obtain an oil phase liquid;
s7, adding the oil phase liquid obtained in the S6 into the water phase liquid obtained in the S5, homogenizing for 15-20 minutes to obtain a mask base liquid, immersing the silk mask cloth into the mask base liquid for 20-30 minutes, and taking out to obtain the mask containing the peony essential oil.
Preferably, the raw materials of the super absorbent resin in S2 comprise, by weight: 12-15 parts of corn starch, 65-70 parts of acrylic acid, 5-8 parts of corn straw powder, 0.5-0.7 part of potassium persulfate, 0.06-0.08 part of N, N' -methylene bisacrylamide, 85-95 parts of 26-29% sodium hydroxide solution and 15-17 parts of water.
Preferably, in the raw material of the super absorbent resin, the water content of the corn straw powder is 5-8%, and the granularity is 60-80 meshes
Preferably, the preparation method of the super absorbent resin in S2 comprises the following steps:
step one, adding corn starch into water with the temperature of 70-80 ℃, and stirring for 40-50 minutes at constant temperature to obtain gelatinized starch solution A;
adding acrylic acid into a sodium hydroxide solution, stirring for 20-30 minutes, adding corn straw powder, potassium persulfate and N, N' -methylene-bisacrylamide, and uniformly stirring to obtain a mixed solution B;
step three, uniformly mixing the starch solution A obtained in the step one and the mixed solution B obtained in the step two, placing the mixture into a microwave reactor for microwave treatment for 3-5 minutes, wherein the microwave power is 250-300W, and drying and crushing the mixture to obtain the super absorbent resin for preparing the peony essential oil.
Preferably, the drying temperature in the third step is 70-80 ℃ and the drying time is 15-20 hours.
Preferably, the particle size of the super absorbent resin for preparing the peony essential oil obtained after the crushing in the third step is 70-80 meshes.
Preferably, the weight ratio of the fresh peony petals to the water in S1 is 1: 1-1.3.
Preferably, the amount of the super absorbent resin added in S2 is 0.02-0.04 times of the weight of the peony juice.
Preferably, in the S3 super-near carbon dioxide extraction, the extraction pressure is 23-35Mpa, the extraction temperature is 35-45 ℃, the extraction time is 50-90 minutes, and the carbon dioxide flow is 15-18L/h.
Preferably, in the supercritical carbon dioxide extraction of S3, the supercritical carbon dioxide extractor has two separation kettles, the pressure of the first separation kettle is 8-10Mpa, the temperature is 40-45 ℃, the pressure of the second separation kettle is 3-5Mpa, and the temperature is 30-35 ℃.
Preferably, the super-adjacent carbon dioxide extraction in S3 uses cyclohexane as entrainer.
Preferably, the flow rate of the entrainer cyclohexane in the S3 super-adjacent carbon dioxide extraction is 6-8% of the flow rate of the carbon dioxide.
Preferably, the ultrasonic power of the ultrasonic treatment in S1 is 200-300w, the frequency is 28-32Hz, and the ultrasonic time is 15-20 min.
Preferably, the stirring rotation number for homogenization in S7 is 2800-3200 rpm.
The facial mask prepared by the method contains natural components such as peony essential oil, orange essential oil, rhodiola rosea essential oil, grape seed essential oil and the like, has no stimulation to human skin, can quickly permeate into the human skin by being matched with glycerin, hyaluronic acid and the like, and has the effects of tendering and whitening, resisting wrinkles, preventing aging, fading color spots, enhancing skin elasticity and the like.
The peony essential oil has the effects of resisting oxidation, delaying skin aging, inhibiting color spots, preventing acne, improving skin condition, and the like; the orange essential oil has the functions of resisting bacteria, expelling toxin, fading color spots, balancing the pH value of the skin, helping the formation of collagen and helping the growth and repair of skin tissues, and the fragrance of the orange essential oil can drive off the nervous mood and pressure, improve the insomnia caused by anxiety, make people have a good mood and restore the vitality; the rhodiola essential oil can clear away heat and toxic materials, regulate qi and activate blood, can resist darkness and uneven skin caused by oxidation by only a small amount of rhodiola essential oil, improves the dry and water-deficient conditions, enhances the elasticity and vitality of skin, and can make the skin tender and white; the grape seed oil has two very important elements, namely linoleic acid and proanthocyanidin, the linoleic acid can resist free radicals, is anti-aging, helps to absorb vitamin C and vitamin E, strengthens the elasticity of a circulatory system, reduces the damage of ultraviolet rays, protects collagen in skin, improves venous swelling and edema, prevents melanin from being precipitated, and the original anthocyanin has the effects of protecting blood vessel elasticity, protecting the skin from the toxic action of the ultraviolet rays, preventing the damage of collagen fibers and elastic fibers, keeping the skin with due elasticity and tension and avoiding the generation of skin sagging and wrinkles.
The peony essential oil used in the method takes fresh peony petals as raw materials, and the fresh peony petals are firstly crushed and subjected to ultrasonic wall breaking, so that essential oil components in the peony flowers are released from cells. The high water absorption resin is used for absorbing peony flower juice and then is subjected to supercritical carbon dioxide extraction, and the high water absorption resin has strong absorptivity and water retention property, and hardly loses water under external pressure. The high water absorption resin has different binding capacities to water molecules and essential oil components, volatile oily components in the high water absorption resin are taken away when carbon dioxide passes through the high water absorption resin absorbing peony flower juice, water and impurities are left in the high water absorption resin to realize oil-water separation, and pure essential oil can be directly recovered from a separation kettle. The super absorbent resin can absorb water repeatedly and be recycled, and the production cost is reduced. When supercritical carbon dioxide extraction is carried out, the cyclohexane is used as an entrainer, so that the extraction efficiency can be improved. The method for extracting the peony essential oil can extract essential oil components in peony to the maximum extent, has high essential oil purity, no impurities, no extractant residue and easy absorption, and is an efficient and rapid method for extracting peony essential oil from peony.
Detailed Description
The technical solution of the present invention will be described in detail below with reference to specific examples.
Example 1
The invention provides a preparation method of a mask containing peony essential oil, which comprises the following steps:
s1, mixing fresh peony petals and water in a weight ratio of 1:1.2, crushing the mixture to 20 meshes, carrying out ultrasonic treatment for 17min with ultrasonic power of 240w and frequency of 30Hz, and carrying out centrifugal separation to obtain peony juice;
s2, adding super absorbent resin into the peony flower juice obtained in S1, wherein the addition amount of the super absorbent resin is 0.028 times of the weight of the peony flower juice, stirring for 13 minutes, and standing for 26 minutes to obtain a gel-like peony extract;
s3, performing supercritical carbon dioxide extraction on the gel-like peony extract obtained in the step S2, wherein in the supercritical carbon dioxide extraction, the extraction pressure is 27Mpa, the extraction temperature is 42 ℃, the extraction time is 71 minutes, and the carbon dioxide flow is 16.8L/h; the supercritical carbon dioxide extraction apparatus comprises two separation kettles, wherein the pressure of the first separation kettle is 8.9Mpa, the temperature is 42 ℃, the pressure of the second separation kettle is 3.6Mpa, and the temperature is 33 ℃; in the S3, adopting cyclohexane as an entrainer for super-near carbon dioxide extraction, wherein the flow rate of the cyclohexane is 1.13L/h, and combining the extracts of the first separation kettle and the second separation kettle to obtain peony essential oil;
s4, weighing 12 parts of glycerol, 10 parts of hyaluronic acid, 1.4 parts of vitamin E, 6.2 parts of orange essential oil, 2.2 parts of rhodiola rosea essential oil, 6.9 parts of grape seed essential oil, 23 parts of water and 8.1 parts of peony essential oil prepared in S3 for later use;
s5, mixing the glycerol, the hyaluronic acid and the water weighed in the S4, and uniformly stirring at 76 ℃ to obtain an aqueous phase liquid;
s6, mixing the vitamin E, the orange essential oil, the rhodiola essential oil, the grape seed essential oil and the peony essential oil weighed in the S4, and stirring uniformly at 76 ℃ to obtain an oil phase liquid;
s7, adding the oil phase liquid obtained in the S6 into the water phase liquid obtained in the S5, homogenizing for 17 minutes under the stirring revolution of 3000rpm to obtain a mask base liquid, immersing the silk mask cloth into the mask base liquid for 25 minutes, and taking out to obtain the mask containing the peony essential oil.
Wherein the raw materials of the super absorbent resin in S2 comprise the following components in parts by weight: 13 parts of corn starch, 67 parts of acrylic acid, 6.8 parts of corn straw powder, 0.62 part of potassium persulfate, 0.074 part of N, N' -methylene-bisacrylamide, 86 parts of sodium hydroxide solution with the mass fraction of 27% and 15.8 parts of water. The water content of the corn straw powder is 5.4 percent, and the granularity is 70 meshes.
The preparation method of the super absorbent resin comprises the following steps:
step one, adding corn starch into 76 ℃ water, and stirring for 43 minutes at constant temperature to obtain a gelatinized starch solution A;
adding acrylic acid into a sodium hydroxide solution, stirring for 27 minutes, adding corn straw powder, potassium sulfate and N, N' -methylene bisacrylamide, and uniformly stirring to obtain a mixed solution B;
step three, uniformly mixing the starch solution A obtained in the step one and the mixed solution B obtained in the step two, placing the mixture into a microwave reactor for microwave treatment for 4.3 minutes, wherein the microwave power is 280W, drying the mixture for 18 hours at 76 ℃, crushing the dried mixture, and sieving the dried mixture through a 70-mesh sieve to obtain the super absorbent resin.
Example 2
The invention provides a preparation method of a mask containing peony essential oil, which comprises the following steps:
s1, mixing the components in a weight ratio of 1: 1.1, mixing fresh peony petals with water, crushing the mixture to 20 meshes, carrying out ultrasonic treatment for 16min by using ultrasonic waves with the ultrasonic power of 280w and the frequency of 29Hz, and carrying out centrifugal separation to obtain peony flower juice;
s2, adding super absorbent resin into the peony flower juice obtained in S1, wherein the addition amount of the super absorbent resin is 0.033 times of the weight of the peony flower juice, stirring for 15 minutes, and standing for 22 minutes to obtain a gel-like peony extract;
s3, performing supercritical carbon dioxide extraction on the gel-like peony extract obtained in the step S2, wherein in the supercritical carbon dioxide extraction, the extraction pressure is 33Mpa, the extraction temperature is 37 ℃, the extraction time is 86 minutes, and the carbon dioxide flow is 15.4L/h; the supercritical carbon dioxide extraction apparatus comprises two separation kettles, wherein the pressure of the first separation kettle is 8.3Mpa, the temperature is 43 ℃, the pressure of the second separation kettle is 4.2Mpa, and the temperature is 31 ℃; in the S3, adopting cyclohexane as an entrainer for super-near carbon dioxide extraction, wherein the flow rate of the cyclohexane is 1.20L/h, and combining the extracts of the first separation kettle and the second separation kettle to obtain peony essential oil;
s4, weighing 13 parts of glycerol, 9 parts of hyaluronic acid, 1.6 parts of vitamin E, 7.8 parts of orange essential oil, 3.3 parts of rhodiola rosea essential oil, 7.6 parts of grape seed essential oil, 21 parts of water and 8.9 parts of peony essential oil prepared in S3 for later use;
s5, mixing the glycerol, the hyaluronic acid and the water weighed in the S4, and uniformly stirring at 72 ℃ to obtain an aqueous phase liquid;
s6, mixing the vitamin E, the orange essential oil, the rhodiola essential oil, the grape seed essential oil and the peony essential oil weighed in the S4, and stirring uniformly at 78 ℃ to obtain an oil phase liquid;
s7, adding the oil phase liquid obtained in the S6 into the water phase liquid obtained in the S5, homogenizing for 18 minutes under the stirring rotation number of 2900rpm to obtain a mask base liquid, immersing the silk mask cloth into the mask base liquid for 23 minutes, and taking out to obtain the mask containing the peony essential oil.
Wherein the raw materials of the super absorbent resin in S2 comprise the following components in parts by weight: 12 parts of corn starch, 68 parts of acrylic acid, 7.7 parts of corn straw powder, 0.53 part of potassium persulfate, 0.066 part of N, N' -methylene bisacrylamide, 91 parts of sodium hydroxide solution with the mass fraction of 26% and 16.2 parts of water. The water content of the corn straw powder is 5.8 percent, and the granularity is 65 meshes.
The preparation method of the super absorbent resin comprises the following steps:
step one, adding corn starch into water with the temperature of 73 ℃, and stirring for 48 minutes at constant temperature to obtain gelatinized starch solution A;
adding acrylic acid into a sodium hydroxide solution, stirring for 24 minutes, adding corn straw powder, potassium persulfate and N, N' -methylene-bisacrylamide, and uniformly stirring to obtain a mixed solution B;
step three, uniformly mixing the starch solution A obtained in the step one and the mixed solution B obtained in the step two, placing the mixture into a microwave reactor for microwave treatment for 3.4 minutes, wherein the microwave power is 260W, drying the mixture for 19.4 hours at 73 ℃, crushing the dried mixture, and sieving the dried mixture through a 75-mesh sieve to obtain the super absorbent resin.
Example 3
The invention provides a preparation method of a mask containing peony essential oil, which comprises the following steps:
s1, mixing the components in a weight ratio of 1:1, mixing fresh peony petals with water, crushing, sieving by a 20-mesh sieve, treating for 19min by using ultrasonic waves with the ultrasonic power of 210w and the frequency of 31Hz, and performing centrifugal separation to obtain peony flower juice;
s2, adding super absorbent resin into the peony flower juice obtained in S1, wherein the addition amount of the super absorbent resin is 0.023 times of the weight of the peony flower juice, stirring for 19 minutes, and standing for 29 minutes to obtain a gel-like peony extract;
s3, performing supercritical carbon dioxide extraction on the gel-like peony extract obtained in the step S2, wherein in the supercritical carbon dioxide extraction, the extraction pressure is 24Mpa, the extraction temperature is 44 ℃, the extraction time is 54 minutes, and the carbon dioxide flow is 16.1L/h; the supercritical carbon dioxide extraction apparatus comprises two separation kettles, wherein the pressure of the first separation kettle is 9.7Mpa, the temperature is 41 ℃, the pressure of the second separation kettle is 4.8Mpa, and the temperature is 34 ℃; in the S3, adopting cyclohexane as an entrainer for super-near carbon dioxide extraction, wherein the flow rate of the cyclohexane is 1.01L/h, and combining the extracts of the first separation kettle and the second separation kettle to obtain peony essential oil;
s4, weighing 11 parts of glycerol, 11 parts of hyaluronic acid, 1.2 parts of vitamin E, 5.4 parts of orange essential oil, 2.7 parts of rhodiola rosea essential oil, 8.8 parts of grape seed essential oil, 22 parts of water and 7.3 parts of peony essential oil prepared in S3 for later use;
s5, mixing the glycerol, the hyaluronic acid and the water weighed in the S4, and uniformly stirring at 78 ℃ to obtain an aqueous phase liquid;
s6, mixing the vitamin E, the orange essential oil, the rhodiola essential oil, the grape seed essential oil and the peony essential oil weighed in the S4, and stirring uniformly at 74 ℃ to obtain an oil phase liquid;
s7, adding the oil phase liquid obtained in the S6 into the water phase liquid obtained in the S5, homogenizing at the stirring speed of 3100rpm for 19 minutes to obtain a mask base liquid, immersing the silk mask cloth into the mask base liquid for 27 minutes, and taking out to obtain the mask containing the peony essential oil.
Example 4
The invention provides a preparation method of a mask containing peony essential oil, which comprises the following steps:
s1, mixing the components in a weight ratio of 1: 1.3, mixing fresh peony petals with water, crushing the mixture to pass through a 20-mesh sieve, carrying out ultrasonic treatment for 18min at the ultrasonic power of 260w and the frequency of 28Hz, and carrying out centrifugal separation to obtain peony flower juice;
s2, adding super absorbent resin into the peony flower juice obtained in S1, wherein the addition amount of the super absorbent resin is 0.037 times of the weight of the peony flower juice, stirring for 17 minutes, and standing for 24 minutes to obtain a gel-like peony extract;
s3, performing supercritical carbon dioxide extraction on the gel-like peony extract obtained in the step S2, wherein in the supercritical carbon dioxide extraction, the extraction pressure is 31Mpa, the extraction temperature is 39 ℃, the extraction time is 62 minutes, and the carbon dioxide flow is 17.7L/h; the supercritical carbon dioxide extraction apparatus comprises two separation kettles, wherein the pressure of the first separation kettle is 9.4Mpa, the temperature is 44 ℃, the pressure of the second separation kettle is 3.2Mpa, the temperature is 32 ℃, and the extracts of the first separation kettle and the second separation kettle are combined to obtain the peony essential oil;
s4, weighing 14 parts of glycerol, 8 parts of hyaluronic acid, 1.8 parts of vitamin E, 7.1 parts of orange essential oil, 3.6 parts of rhodiola rosea essential oil, 6.3 parts of grape seed essential oil, 24 parts of water and 9.7 parts of peony essential oil prepared in S3 for later use;
s5, mixing the glycerol, the hyaluronic acid and the water weighed in the S4, and uniformly stirring at 74 ℃ to obtain an aqueous phase liquid;
s6, mixing the vitamin E, the orange essential oil, the rhodiola essential oil, the grape seed essential oil and the peony essential oil weighed in the S4, and stirring uniformly at 72 ℃ to obtain an oil phase liquid;
s7, adding the oil phase liquid obtained in the S6 into the water phase liquid obtained in the S5, homogenizing for 16 minutes under the stirring revolution of 3200rpm to obtain a mask base liquid, immersing the silk mask cloth into the mask base liquid for 29 minutes, and taking out to obtain the mask containing the peony essential oil.
Example 5
The method for preparing a mask containing peony essential oil of example 1, wherein the flow rate of the entrainer cyclohexane extracted with super-adjacent carbon dioxide in S3 may be 1.21L/h.
Example 6
The preparation method of the mask containing peony essential oil in example 1, wherein the raw materials of the super absorbent resin in S2 may further include, in parts by weight: 14 parts of corn starch, 66 parts of acrylic acid, 5.2 parts of corn straw powder, 0.57 part of potassium persulfate, 0.078 part of N, N' -methylene-bisacrylamide, 88 parts of 29% sodium hydroxide solution by mass fraction and 15.3 parts of water. The water content of the corn straw powder is 6.9 percent, and the granularity is 75 meshes.
Example 7
The preparation method of the mask containing peony essential oil in example 1, wherein the raw materials of the super absorbent resin in S2 may further include, in parts by weight: 15 parts of corn starch, 69 parts of acrylic acid, 6.1 parts of corn straw powder, 0.68 part of potassium persulfate, 0.062 part of N, N' -methylene-bisacrylamide, 93 parts of 28% sodium hydroxide solution and 16.7 parts of water. The water content of the corn straw powder is 7.8 percent, and the granularity is 80 meshes.
Example 8
The method for preparing the mask containing peony essential oil in example 1, wherein the method for preparing the super absorbent resin may further include the following steps:
step one, adding corn starch into water of 78 ℃, and stirring for 46 minutes at constant temperature to obtain gelatinized starch solution A;
adding acrylic acid into a sodium hydroxide solution, stirring for 22 minutes, adding corn straw powder, potassium persulfate and N, N' -methylene-bisacrylamide, and uniformly stirring to obtain a mixed solution B;
step three, uniformly mixing the starch solution A obtained in the step one and the mixed solution B obtained in the step two, placing the mixture into a microwave reactor for microwave treatment for 4.8 minutes at the microwave power of 270W, drying the mixture for 16.4 hours at the temperature of 79 ℃, crushing the dried mixture, and sieving the dried mixture with a 80-mesh sieve to obtain the super absorbent resin.
The microwave reactor related to the invention can be selected from the existing equipment on the market as long as the required functions of the invention can be realized, and is preferably the LWMC-201 type microwave reactor of Nanjing optical rotation technology Limited company.
The methods of mixing, stirring, centrifuging, homogenizing and the like involved in the invention are all common knowledge in the field, and are not described herein again.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (8)
1. A preparation method of a mask containing peony essential oil is characterized by comprising the following steps:
s1, mixing fresh peony petals with water, crushing, performing ultrasonic treatment, and performing centrifugal separation to obtain peony juice;
s2, adding super absorbent resin into the peony flower juice obtained in S1, stirring for 10-20 minutes, and standing for 20-30 minutes to obtain a gel-like peony extract;
s3, performing supercritical carbon dioxide extraction on the gel-like peony extract obtained in the S2 to obtain peony essential oil;
s4, weighing 10-15 parts of glycerol, 8-12 parts of hyaluronic acid, 1-2 parts of vitamin E, 5-8 parts of orange essential oil, 2-4 parts of rhodiola rosea essential oil, 6-9 parts of grape seed essential oil, 20-25 parts of water and 7-10 parts of peony essential oil prepared in S3 for later use;
s5, mixing the glycerol, the hyaluronic acid and the water weighed in the S4, and uniformly stirring at 70-80 ℃ to obtain an aqueous phase liquid;
s6, mixing the vitamin E, the orange essential oil, the rhodiola essential oil, the grape seed essential oil and the peony essential oil weighed in the S4, and stirring uniformly at 70-80 ℃ to obtain an oil phase liquid;
s7, adding the oil phase liquid obtained in the S6 into the water phase liquid obtained in the S5, homogenizing for 15-20 minutes to obtain a mask base liquid, immersing the silk mask cloth into the mask base liquid for 20-30 minutes, and taking out to obtain a mask containing peony essential oil;
the raw materials of the super absorbent resin in the S2 comprise the following components in parts by weight: 12-15 parts of corn starch, 65-70 parts of acrylic acid, 5-8 parts of corn straw powder, 0.5-0.7 part of potassium persulfate, 0.06-0.08 part of N, N' -methylene bisacrylamide, 85-95 parts of 26-29% sodium hydroxide solution and 15-17 parts of water;
the preparation method of the super absorbent resin in S2 comprises the following steps:
step one, adding corn starch into water with the temperature of 70-80 ℃, and stirring for 40-50 minutes at constant temperature to obtain gelatinized starch solution A;
adding acrylic acid into a sodium hydroxide solution, stirring for 20-30 minutes, adding corn straw powder, potassium persulfate and N, N' -methylene-bisacrylamide, and uniformly stirring to obtain a mixed solution B;
step three, uniformly mixing the starch solution A obtained in the step one and the mixed solution B obtained in the step two, placing the mixture into a microwave reactor for microwave treatment for 3-5 minutes, wherein the microwave power is 250-300W, and drying and crushing the mixture to obtain the super absorbent resin.
2. The method for preparing a mask containing peony essential oil according to claim 1, wherein the weight ratio of the fresh peony petals to the water in S1 is 1: 1-1.3.
3. The method for preparing a mask containing peony essential oil according to claim 1, wherein the amount of the super absorbent resin added in S2 is 0.02-0.04 times of the weight of the peony juice.
4. The preparation method of the mask containing peony essential oil according to claim 1, wherein in the S3 supercritical carbon dioxide extraction, the extraction pressure is 23-35Mpa, the extraction temperature is 35-45 ℃, the extraction time is 50-90 minutes, and the carbon dioxide flow rate is 15-18L/h.
5. The method for preparing a mask containing peony essential oil according to claim 1, wherein the supercritical carbon dioxide extractor used in the S3 supercritical carbon dioxide extraction comprises two separation vessels, the first separation vessel has a pressure of 8-10Mpa and a temperature of 40-45 ℃, and the second separation vessel has a pressure of 3-5Mpa and a temperature of 30-35 ℃.
6. The method for preparing a mask containing peony essential oil according to claim 1, wherein in the step S3, ethylene is used as an entrainer for supercritical carbon dioxide extraction, and the flow rate of ethylene is 6% -8% of the flow rate of carbon dioxide.
7. The preparation method of the mask containing peony essential oil as claimed in claim 6, wherein the ultrasonic power of the ultrasonic treatment in S1 is 200-300w, the frequency is 28-32Hz, and the ultrasonic time is 15-20 min.
8. The method as claimed in claim 1, wherein the stirring rotation speed for homogenization in S7 is 2800 and 3200 rpm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810187627.0A CN108143648B (en) | 2018-03-07 | 2018-03-07 | Preparation method of mask containing peony essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810187627.0A CN108143648B (en) | 2018-03-07 | 2018-03-07 | Preparation method of mask containing peony essential oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108143648A CN108143648A (en) | 2018-06-12 |
| CN108143648B true CN108143648B (en) | 2021-07-23 |
Family
ID=62456102
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810187627.0A Active CN108143648B (en) | 2018-03-07 | 2018-03-07 | Preparation method of mask containing peony essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108143648B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111939108A (en) * | 2020-08-18 | 2020-11-17 | 江西中医药大学 | Kumquat essential oil hydrolat mask and preparation method thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102363641A (en) * | 2011-10-09 | 2012-02-29 | 常熟市威腾进出口有限公司 | Preparation method of starch maize modified sodium polyacrylate composite material |
| CN103937609A (en) * | 2014-03-26 | 2014-07-23 | 顾丽霞 | Preparation technology for citrus peel essential oil |
| CN104224633B (en) * | 2014-09-30 | 2017-07-21 | 河南科技大学 | A kind of pure tree peony heal-care essential oil and preparation method thereof |
| CN105769683B (en) * | 2016-04-13 | 2018-04-24 | 武汉市农业科学技术研究院林业果树科学研究所 | A kind of anti-oxidant moisturizing sleep mask containing peony seed oil and preparation method thereof |
| CN107320359A (en) * | 2017-06-23 | 2017-11-07 | 芜湖凌梦电子商务有限公司 | A kind of preparation method of the fibroin facial mask containing peony essential oil |
| CN107496325A (en) * | 2017-08-17 | 2017-12-22 | 河南科技大学 | Facial mask containing peony essential oil, green cucumber extract solution and snail stoste and preparation method thereof |
-
2018
- 2018-03-07 CN CN201810187627.0A patent/CN108143648B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN108143648A (en) | 2018-06-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104173251B (en) | A kind of bone glue of yak former peptide cleawhite pack and preparation method thereof | |
| CN103494760B (en) | Moistening and whitening facial mask and preparation method thereof | |
| CN105078875B (en) | A kind of cosmetics and preparation method thereof containing peony extract | |
| CN105832622A (en) | Tremella fuciformis extract and preparation method and application thereof | |
| CN103599063A (en) | Anti-aging face cream | |
| CN106798722A (en) | A kind of anti-ageing moisturizing maintenance creams of not silicate-containing oil and preparation method thereof | |
| CN107789206A (en) | A kind of plant collagen eye patch | |
| CN108635291B (en) | Beautifying liquid based on plant small molecular peptide and preparation method thereof | |
| CN104940064A (en) | Brasenia schreberi emulsion | |
| CN109381407A (en) | One kind is releived anti-ageing Aloe Vera Gel of moisturizing and preparation method thereof | |
| CN108158885A (en) | Repair composition of striae of pregnancy and its preparation method and application | |
| CN107496307A (en) | A kind of whitening and moisturizing facial mask | |
| CN107011993B (en) | Compound essential oil and preparation method thereof | |
| CN108143648B (en) | Preparation method of mask containing peony essential oil | |
| CN108158861B (en) | Preparation method of essence containing peony essential oil | |
| CN103462855B (en) | Cosmetic containing American ginseng and longan and preparation method thereof | |
| CN104958205A (en) | Water shield essential lotion | |
| CN108888554B (en) | Stem cell beauty emulsion with skin tendering and spot lightening functions and preparation method thereof | |
| CN107260634A (en) | A kind of green Chinese nti-freckle suncream and preparation method thereof | |
| CN106852838A (en) | A kind of compound method of moisture saver mask | |
| CN104958203A (en) | Water shield mask lotion | |
| CN108143674A (en) | A kind of lotion containing peony seed oil and preparation method thereof | |
| CN109364014A (en) | A kind of anti-aging Essence | |
| CN108498358A (en) | A kind of machine ingredient skin care item living | |
| CN108514531A (en) | A kind of moisturizing anti-wrinkle cosmetic and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20210406 Address after: 233000 Room 1402, Ziyang Building, Pearl Plaza, Huaishang District, Bengbu City, Anhui Province Applicant after: Anhui Hanbang Technology Consulting Co., Ltd Address before: 233000 building C1, Oracle science and Technology Innovation Park, south section of Yan'an Road, Bengbu City, Anhui Province Applicant before: ANHUI XINYUANKANG BIOTECHNOLOGY Co.,Ltd. |
|
| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20210907 Address after: 201502 Building 1, No. 35, Xingta Jiangong Road, Fengjing town, Jinshan District, Shanghai Patentee after: Shanghai meisi'ao Biotechnology Co.,Ltd. Address before: 233000 Room 1402, Ziyang Building, Pearl Plaza, Huaishang District, Bengbu City, Anhui Province Patentee before: Anhui Hanbang Technology Consulting Co., Ltd |
|
| TR01 | Transfer of patent right | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 201502 Building 1, No. 35, Xingta Jiangong Road, Fengjing town, Jinshan District, Shanghai Patentee after: Fuxi Pharmaceutical (Shanghai) Co.,Ltd. Address before: 201502 Building 1, No. 35, Xingta Jiangong Road, Fengjing town, Jinshan District, Shanghai Patentee before: Shanghai meisi'ao Biotechnology Co.,Ltd. |
|
| CP01 | Change in the name or title of a patent holder |