CN114404328A - SOD repair essence and preparation method thereof - Google Patents
SOD repair essence and preparation method thereof Download PDFInfo
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- CN114404328A CN114404328A CN202111401362.8A CN202111401362A CN114404328A CN 114404328 A CN114404328 A CN 114404328A CN 202111401362 A CN202111401362 A CN 202111401362A CN 114404328 A CN114404328 A CN 114404328A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N55/00—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur
- A01N55/02—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur containing metal atoms
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/50—Surfactants; Emulsifiers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Organic Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Biotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
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- Birds (AREA)
- Epidemiology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Inorganic Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
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Abstract
The invention discloses SOD repair essence which comprises the following components in parts by mass: the SOD repair essence comprises 100-120 parts by mass of a prefabricated material, 5-10 parts by mass of pomegranate seed extract and 20-25 parts by mass of an additive, and also discloses a preparation method of the SOD repair essence; the method changes the traditional mode of adding SOD extracts, adopts sufficient pomegranate raw materials with high SOD content and has no special requirement on preparation temperature, is beneficial to realizing large-scale mass production, and further reduces the production cost.
Description
Technical Field
The invention belongs to the technical field of cosmetic preparation, and particularly relates to SOD repair essence and a preparation method thereof.
Background
Superoxide dismutase (SOD) is a type of oxidoreductase which is widely present in various organisms, is a metalloenzyme capable of clearing Superoxide radical anions in vivo, can effectively prevent the toxic action of the Superoxide radical anions on organisms, and is a medicinal enzyme with wide curative effect.
The traditional cosmetics can be added with the SOD extract to resist the damage of free radicals to cells, repair the damaged cells in time, recover the damage of the free radicals to the cells and play a role in resisting aging, but the SOD extract has low activity and needs to be stored at low temperature, and a series of additives are required to be added during production to ensure the activity of the SOD, so that the production cost is high and the scale production cannot be achieved.
Disclosure of Invention
Aiming at the situation, in order to overcome the defects of the prior art, the invention provides the SOD repair essence and the preparation method thereof, not only the repair essence with the functions of delaying skin aging, preserving moisture and resisting wrinkles is provided, but also the original ecological pomegranate with high SOD content and prepared by a specific method is used for preparing the essence.
The technical scheme adopted by the invention is as follows: the invention relates to SOD repair essence which is characterized by comprising the following components in parts by mass: the method comprises 100-120 parts by mass of a prefabricated material, 5-10 parts by mass of a pomegranate seed extract and 20-25 parts by mass of an additive, wherein the prefabricated material comprises a concentrated solution rich in SOD pomegranate ripe fruit, pink ripe fruit and immature green fruit, and the mass ratio of ripe fruit, pink ripe fruit and immature green fruit in the concentrated solution is 10:2: 1; tests prove that the active contents of SOD in the growth process of pomegranate fruits are respectively from high to low: mature fruit, pink ripe fruit, green fruit, choose the red ripe fruit and pink ripe fruit with better maturity as the raw materials of the preformed material can guarantee the juice of pomegranate in the preformed material contains SOD activity of higher concentration, but because the soluble protein amount of the part of aging in the plant cell can be obviously reduced, therefore add the soluble protein content in the preformed material of green fruit of certain proportion in the preformed material, and the soluble protein can play the water retention role to the skin, adopt preformed material and pomegranate seed extract to mix, can have further improved anti-aging, antioxidation and moisturizing effect.
Furthermore, the pomegranate rich in SOD is pomegranate fruit which is sprayed with foliar fertilizer for a plurality of times in the growing period, and the active content of SOD in the fresh pomegranate fruit rich in SOD is 70000-80000 unit/ml.
Furthermore, the active content of SOD in mature fruit is 65000-80000 unit/ml, the active content of SOD in green immature fruit is 50000-70000 unit/ml, and the active content of SOD in pink mature fruit is 60000-75000 unit/ml.
Further, the foliar fertilizer comprises EDTA complex zinc, EDTA complex manganese, EDTA complex selenium, EDTA complex nickel, EDTA complex titanium, EDTA complex cobalt, a surfactant and a synergist.
Further, the additive comprises the following components in parts by mass: 5-8 parts of glycerol, 1-3 parts of lactic acid, 2-5 parts of allantoin, 1-4 parts of sodium hyaluronate, 2-8 parts of sclerotinia sclerotiorum gum and 1-2 parts of GPL preservative.
The preparation method of the SOD repairing essence is characterized by comprising the following steps:
firstly, spraying foliar fertilizer aqueous solution for multiple times in the branching period, the flowering period, the fruit setting period and the fruit development period of the pomegranate respectively, wherein the foliar fertilizer aqueous solution comprises EDTA complex zinc, EDTA complex manganese, EDTA complex selenium, EDTA complex nickel, EDTA complex titanium, EDTA complex cobalt, a surfactant and a synergist; harvesting mature fruits, pink mature fruits and immature green fruits of the pomegranates in a ratio of 10:2:1 in the fruit development period of the pomegranates; squeezing and filtering the harvested pomegranate within 12 hours, taking clear liquid, evaporating the clear liquid to 1/3-1/4 of the original volume at 85 ℃, and homogenizing for 20-30 min to obtain a pomegranate mixed liquid rich in SOD; heating the pomegranate mixed solution rich in SOD to 85 ℃, keeping the temperature at constant temperature, adding glycerol, lactic acid, sodium hyaluronate, pomegranate seed extract and allantoin, stirring until the glycerol, the lactic acid, the sodium hyaluronate, the pomegranate seed extract and the allantoin are completely dissolved, homogenizing for 10 minutes, cooling to 50 ℃, adding sclerotium rolfsii gum and GPL preservative, stirring uniformly, and discharging; before general discharging, the essence is sterilized by 60 deg.C for 30min to ensure cleanness, no additional water is added during the preparation process, and all liquid components are extracted from Sucus Punicae Granati to increase SOD concentration.
Further, in the step of spraying the foliar fertilizer aqueous solution for a plurality of times in the branching period, the flowering period and the fruit setting period of the pomegranate respectively, the method for spraying the foliar fertilizer aqueous solution comprises the following steps: the pomegranate branches 1-2 times per year, the fertilizer is sprayed at least once in each branching period and each flowering period of the pomegranate, the fertilizer is applied at least once in the fruit setting period of the pomegranate, and the fertilizer is applied at least 3 times in the fruit development period of the pomegranate.
Further, the method for extracting the clear liquid after squeezing and filtering the mature fruit, the pink mature fruit and the immature green fruit of the pomegranate comprises the following steps: crushing ripe fruits, pink ripe fruits and immature green fruits of pomegranate, squeezing, leaching and centrifuging to obtain mixed juice, and screening the mixed juice through a 40-60-mesh sieve to obtain clear liquid.
Further, in the step of adding and stirring the glycerol, the lactic acid, the sodium hyaluronate and the allantoin until the glycerol, the lactic acid, the sodium hyaluronate and the allantoin are completely dissolved, the stirring speed is 15-40 r/min, and the stirring time is 20-30 minutes.
Further, before the discharging step, a 200-mesh sieve is selected for filtering the essence.
The beneficial effects obtained by adopting the scheme are as follows: according to the scheme, the SOD repair essence and the preparation method thereof, not only is the repair essence with the effects of delaying skin aging, preserving moisture and resisting wrinkles provided, but also the original ecological pomegranate with high SOD content obtained by planting through a specific method is used for preparing the essence, the method changes the traditional mode of adding the SOD extract, adopts sufficient pomegranate raw materials with high SOD content and has no special requirement on the preparation temperature, large-scale mass production is favorably realized, and the production cost is further reduced.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments; all other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows: SOD repair essence comprises the following components in parts by mass: the fruit juice beverage comprises 100 parts by mass of a prefabricated material, 5 parts by mass of a pomegranate seed extract and 20 parts by mass of an additive, wherein the prefabricated material comprises a concentrated solution of ripe fruits, pink ripe fruits and immature green fruits rich in SOD pomegranate, and the mass ratio of the ripe fruits, the pink ripe fruits and the immature green fruits is 2: 1; the additive comprises the following components in parts by mass: 5 parts of glycerin, 1 part of lactic acid, 2 parts of allantoin, 1 part of sodium hyaluronate, 2 parts of sclerotinia sclerotiorum gel and 1 part of GPL preservative.
Example two: SOD repair essence comprises the following components in parts by mass: the fruit juice beverage comprises 120 parts by mass of a prefabricated material, 10 parts by mass of a pomegranate seed extract and 25 parts by mass of an additive, wherein the prefabricated material comprises a concentrated solution of ripe fruits, pink ripe fruits and immature green fruits rich in SOD pomegranate, and the mass ratio of the ripe fruits, the pink ripe fruits and the immature green fruits is 2: 1; the additive comprises the following components in parts by mass: 8 parts of glycerol, 3 parts of lactic acid, 5 parts of allantoin, 4 parts of sodium hyaluronate, 8 parts of sclerotinia sclerotiorum gel and 2 parts of GPL preservative.
Example three: SOD repair essence comprises the following components in parts by mass: the fruit juice beverage comprises 110 parts by mass of a prefabricated material, 8 parts by mass of a pomegranate seed extract and 23.5 parts by mass of an additive, wherein the prefabricated material comprises a concentrated solution of ripe fruits, pink ripe fruits and immature green fruits rich in SOD pomegranate, and the mass ratio of the ripe fruits, the pink ripe fruits and the immature green fruits is 2: 1; the additive comprises the following components in parts by mass: 6.8 parts of glycerin, 1.9 parts of lactic acid, 4 parts of allantoin, 2 parts of sodium hyaluronate, 5.5 parts of sclerotinia sclerotiorum gel and 2 parts of GPL preservative.
In some embodiments, the pomegranate rich in SOD is pomegranate fruit which is sprayed with foliar fertilizer for multiple times in a growth period, and the active content of SOD in the fresh pomegranate fruit rich in SOD is 70000-80000 unit/ml;
in some embodiments, the active content of SOD in ripe fruit is 65000-80000 units/ml, the active content of SOD in unripe green fruit is 50000-70000 units/ml, and the active content of SOD in pink ripe fruit is 60000-75000 units/ml;
in some embodiments, the foliar feed comprises zinc EDTA complex, manganese EDTA complex, selenium EDTA complex, nickel EDTA complex, titanium EDTA complex, and cobalt EDTA complex, a surfactant, and a synergist.
The preparation method of the SOD repairing essence comprises the following steps:
firstly, spraying foliar fertilizer aqueous solution for multiple times in the branching period, the flowering period, the fruit setting period and the fruit development period of the pomegranate respectively, wherein the foliar fertilizer aqueous solution comprises EDTA complex zinc, EDTA complex manganese, EDTA complex selenium, EDTA complex nickel, EDTA complex titanium, EDTA complex cobalt, a surfactant and a synergist; the weight ratio of the pomegranate fruit in the development period is 10:2:1, harvesting mature fruits, pink mature fruits and immature green fruits of the pomegranate; juicing and filtering mature fruits, pink mature fruits and immature green fruits of pomegranate, taking clear liquid, evaporating at low temperature of 85 ℃ to 1/3-1/4 of the original volume, and homogenizing for 20-30 min to obtain pomegranate mixed liquid rich in SOD; heating the pomegranate mixed solution rich in SOD to 85 ℃, keeping the temperature at constant temperature, adding glycerol, lactic acid, sodium hyaluronate, pomegranate seed extract and allantoin, stirring until the glycerol, the lactic acid, the sodium hyaluronate, the pomegranate seed extract and the allantoin are completely dissolved, homogenizing for 10 minutes, cooling to 50 ℃, adding sclerotium rolfsii gum and GPL preservative, stirring uniformly, and discharging; no additional water is added in the preparation process of the essence, and all liquid components are taken from pomegranate juice, so that the SOD concentration is higher.
In some embodiments, in the step of spraying the aqueous solution of the foliar fertilizer for a plurality of times in the branching stage, the flowering stage and the fruit setting stage of the pomegranate respectively, the method for spraying the aqueous solution of the foliar fertilizer is as follows: the pomegranate branches 1-2 times per year, the fertilizer is sprayed at least once in each branching period and each flowering period of the pomegranate, the fertilizer is applied at least once in the fruit setting period of the pomegranate, and the fertilizer is applied at least 3 times in the fruit development period of the pomegranate.
In some embodiments, the method of juicing and filtering mature fruit, pink mature fruit and green immature fruit of pomegranate and collecting the supernatant comprises: crushing immature green fruits and pink ripe fruits of pomegranate, squeezing, leaching and centrifuging to obtain mixed juice, and screening the mixed juice through a 40-60-mesh sieve to obtain clear liquid.
In some embodiments, in the step of adding and stirring the glycerol, the lactic acid, the sodium hyaluronate and the allantoin to be completely dissolved, the stirring speed is 15-40 r/min, and the stirring time is 20-30 minutes.
In some embodiments, a 200 mesh screen is selected to filter the serum prior to the discharge step.
It is to be noted that the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
The invention and its embodiments have been described above, without this being limitative. In conclusion, those skilled in the art should appreciate that they can readily use the disclosed conception and specific embodiments as a basis for designing or modifying other structures for carrying out the same purposes of the present invention without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (10)
1. The SOD repair essence is characterized by comprising the following components in parts by mass: the method comprises 100-120 parts by mass of a prefabricated material, 5-10 parts by mass of a pomegranate seed extract and 20-25 parts by mass of an additive, wherein the prefabricated material comprises a concentrated solution rich in mature fruits, pink mature fruits and immature green fruits of SOD pomegranates, and the mass ratio of the mature fruits, the pink mature fruits and the immature green fruits in the concentrated solution is 10:2: 1.
2. the SOD repairing essence according to claim 1, wherein: the pomegranate rich in SOD is pomegranate fruits which are sprayed with foliar fertilizer for many times in the growing period, and the active content of SOD in the fresh pomegranate fruits rich in SOD is 50000-80000 unit/ml.
3. The SOD repairing essence according to claim 1, wherein: the active content of SOD in the ripe fruit is 65000-80000 units/ml, the active content of SOD in the unripe green fruit is 50000-70000 units/ml, and the active content of SOD in the pink ripe fruit is 60000-75000 units/ml.
4. The SOD repairing essence according to claim 1, wherein: the foliar fertilizer comprises EDTA complex zinc, EDTA complex manganese, EDTA complex selenium, EDTA complex nickel, EDTA complex titanium, EDTA complex cobalt, a surfactant and a synergist.
5. The SOD repairing essence according to claim 1, wherein: the additive comprises the following components in parts by mass: 5-8 parts of glycerol, 1-3 parts of lactic acid, 2-5 parts of allantoin, 1-4 parts of sodium hyaluronate, 2-8 parts of sclerotinia sclerotiorum gum and 1-2 parts of GPL preservative.
6. The method for preparing the SOD repairing essence according to claim 1, which comprises the following steps:
firstly, spraying a foliar fertilizer aqueous solution for multiple times in the branching period, the flowering period, the fruit setting period and the fruit development period of the pomegranate respectively, wherein the foliar fertilizer aqueous solution comprises EDTA complex zinc, EDTA complex manganese, EDTA complex selenium, EDTA complex nickel, EDTA complex titanium, EDTA complex cobalt, a surfactant and a synergist;
the weight ratio of the pomegranate fruit in the development period is 10:2:1, harvesting mature fruits, pink mature fruits and immature green fruits of the pomegranate;
juicing and filtering mature fruits, pink mature fruits and immature green fruits of pomegranate, evaporating clear liquid to 1/3-1/4 of the original volume at 85 ℃, and homogenizing for 20-30 min to obtain a pomegranate mixed liquid rich in SOD;
heating the pomegranate mixed solution rich in SOD to 85 ℃, keeping the temperature at constant temperature, adding glycerol, lactic acid, sodium hyaluronate, pomegranate seed extract and allantoin, stirring until the glycerol, the lactic acid, the sodium hyaluronate, the pomegranate seed extract and the allantoin are completely dissolved, homogenizing for 10 minutes, cooling to 50 ℃, adding sclerotium rolfsii gum and GPL preservative, stirring uniformly, and discharging.
7. The method for preparing the SOD repairing essence according to claim 6, wherein in the step of spraying the foliar fertilizer aqueous solution for a plurality of times in the branching stage, the flowering stage and the fruit setting stage of the pomegranate respectively, the method for spraying the foliar fertilizer aqueous solution comprises the following steps: the pomegranate branches 1-2 times per year, the fertilizer is sprayed at least once in each branching period and each flowering period of the pomegranate, the fertilizer is applied at least once in the fruit setting period of the pomegranate, and the fertilizer is applied at least 3 times in the fruit development period of the pomegranate.
8. The method for preparing SOD repairing essence according to claim 6, wherein the step of extracting the supernatant after juicing and filtering mature fruits, pink ripe fruits and green unripe fruits of pomegranate comprises: crushing ripe fruits, pink ripe fruits and immature green fruits of pomegranate, squeezing, leaching and centrifuging to obtain mixed juice, and screening the mixed juice through a 40-60-mesh sieve to obtain clear liquid.
9. The method for preparing SOD repairing essence according to claim 6, wherein the SOD repairing essence comprises the following steps: in the step of adding and stirring the glycerol, the lactic acid, the sodium hyaluronate and the allantoin until the glycerol, the lactic acid, the sodium hyaluronate and the allantoin are completely dissolved, the stirring speed is 15-40 r/min, and the stirring time is 20-30 minutes.
10. The method for preparing SOD repairing essence according to claim 6, wherein a 200-mesh sieve is selected for filtering the essence before the discharging step.
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106748230A (en) * | 2016-12-30 | 2017-05-31 | 深圳市芭田生态工程股份有限公司 | Winter resistance foliar fertilizer and preparation method thereof |
CN107982070A (en) * | 2017-12-27 | 2018-05-04 | 上海晓美生物科技有限公司 | A kind of whitening moisturizing face masque of elite containing pomegranate and preparation method thereof |
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2021
- 2021-11-24 CN CN202111401362.8A patent/CN114404328A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106748230A (en) * | 2016-12-30 | 2017-05-31 | 深圳市芭田生态工程股份有限公司 | Winter resistance foliar fertilizer and preparation method thereof |
CN107982070A (en) * | 2017-12-27 | 2018-05-04 | 上海晓美生物科技有限公司 | A kind of whitening moisturizing face masque of elite containing pomegranate and preparation method thereof |
Non-Patent Citations (1)
Title |
---|
REBOGILE RMPHAHLELEWEMI 等: ""Effects of different maturity stages and growing locations on changes in chemical biochemical and aroma volatile composition of Wonderful\' pomegranate juice"", 《J SCI FOOD AGRIC》, vol. 96, pages 1002 - 1009 * |
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