CN103385826B - Peel-off type mung bean acne-removing mask and preparation method thereof - Google Patents

Peel-off type mung bean acne-removing mask and preparation method thereof Download PDF

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CN103385826B
CN103385826B CN201310243257.5A CN201310243257A CN103385826B CN 103385826 B CN103385826 B CN 103385826B CN 201310243257 A CN201310243257 A CN 201310243257A CN 103385826 B CN103385826 B CN 103385826B
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skin
semen phaseoli
phaseoli radiati
acne
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CN103385826A (en
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高新龙
高新伟
高新凯
尚柯
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Guangzhou Meizi Biotechnology Co.,Ltd.
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ZHENGZHOU GAOSHANG BIOTECH Co Ltd
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Abstract

The invention discloses a mung bean acne-removing mask and a preparation method thereof. The peel-off type mung bean acne-removing mask is prepared by using a conventional method from the following raw materials by weight: 10 to 14 parts of polyvinyl alcohol, 8 to 12 parts of glycerin, 0.8 to 1.2 parts of hydrolyzed sericin, 4 to 6 parts of ethanol, 6 to 8 parts of C11-15 alcohol polyether-7 sodium carboxylate, 0.8 to 2 parts of a mung bean extract, 0.03 to 0.08 part of a composite antiseptic and 100 parts of deionized water, wherein the composite antiseptic is composed of, by weight, 1 to 3 parts of carnosic acid, 3 to 5 parts of a bamboo leaf antioxidant, 1 to 3 parts of nisin and 1 to 3 parts of 3-iodo-2-propynyl butyl carbamate. The peel-off type mung bean acne-removing mask provided by the invention can purify pores in depth, remove unnecessary grease and promote water-oil balance of the skin, enables the skin to be fresh, comfortable and vital, reduces acne traces, whitens the skin, eliminates dullness of the skin, allows the skin to be uniform, bright and white and is capable of removing acne and clearing heat.

Description

Exfoliated Semen phaseoli radiati Deacne pack and preparation method thereof
Technical field
The present invention relates to facial film and preparation method thereof, be specifically related to a kind of exfoliated Semen phaseoli radiati Deacne pack and preparation method thereof.
Background technology
Facial film is the important content in skin nursing, and for the regular application facial film of all kinds of skin characteristic, can make oily skin defat, thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.Facial film makes skin seem salubrious after using, smooth and pure white delicacy, this is because when facial film is coated on skin, facial film and skin produce affinity, along with the drying gradually of facial film, skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, the sebum of skin secretion and moisture reverse osmosis are in horny layer, epidermis softness is unfolded, pore instinct is opened, effective ingredient in facial film infiltrates skin and is absorbed, facial film is tightly connected with skin simultaneously, when removing facial film, aging cutin on skin, in pore deep layer dirt also by while leukorrhagia, make skin totally pure and fresh.
The principle of facial film, utilize the blink covering face exactly, the air that temporary transient isolation is extraneous and pollution, improve skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, the moisture in facial film infiltrates the horny layer of skin epidermis, skin becomes soft, and skin naturally light is flexible.
Along with the raising of people's quality of the life and people are to the pursuit of U.S., cosmetics kind is more and more various.At present, face mask of traditional Chinese medicine is one of beauty treatment educational circles effective whitening regime, and especially some Chinese medicine extraction liquid have the effect of good toxin expelling, speckle dispelling, reparation, skin care, also by being applied in facial film gradually.
But because facial film is liquid condition, Chinese medicine extraction liquid is easy to mould growth, a lot of face mask of traditional Chinese medicine antiseptic effects are in the market not good, and the shelf-life is short.Therefore all antiseptic can be added in a lot of face mask of traditional Chinese medicine.But a lot of antiseptic, while the microorganism such as kill bacteria, fungus, also can produce zest to skin, even causes erythema and erythra, Long Term Contact antiseptic, organism material sensitization can be increased, cause the danger of anaphylactic reaction.
Iodine propilolic alcohol butyl mephenesin Carbamate (being called for short IPBC) is a kind of novel cosmetic antiseptic, there is good fungistatic effect, and good dissolubility is had in surfactant, emulsifying agent, polar solvent, therefore be widely used in resident class and drip washing class cosmetic formulations, normal and other antiseptic such as diazolidinyl urea, hydantoin with the use of.In China's cosmetics health specification and European Union's regulatory affairs, regulation IPBC limits the use of antiseptic in components of cosmetics, and in cosmetics, maximum permission working concentration is 0.05%, and can not be used for oral hygiene and lip product.But in facial film, antiseptic effect when addition is less than 0.05% is also not obvious.Therefore, there is the little and problem that antiseptic effect is poor, the shelf-life is short of consumption in the antiseptic used in current facial film.Also there are the iodine propilolic alcohol butyl mephenesin Carbamate in partial face mask or other antiseptic large usage quantities, pessimal stimulation can be produced by skin, with rear needs cleaning face, use trouble.
Semen phaseoli radiati (formal name used at school: Vigna radiata) is a kind of pulse family, Papillionoideae Vigna plant, originates in India, Burma area.Present East Asia various countries generally plant, and also there are a small amount of plantation in Africa, Europe, the U.S., and the states such as China, Burma are main Semen phaseoli radiati exported countrys.
Semen phaseoli radiati nature and flavor are sweet cool, have the effect of heat-clearing and toxic substances removing.Summer or the people worked in hot environment perspire many, the loss of water liquid is very large, the loss of potassium is maximum, electrolyte balance in health wrecks, boiling soup to supplement with Semen phaseoli radiati is optimal method, can affix one's name to clearly QI invigorating, diuresis of quenching the thirst, and not only can supplement moisture content, and inorganic salt can be supplemented in time, to maintenance water liquid electrolyte balance important in inhibiting.
1, the Concha Ostreae alkali in Semen phaseoli radiati extract and different Concha Ostreae alkali, have remarkable cleaning, moistening effect, removes sebum function outstanding, effectively can remove the unclean thing of skin, more can thoroughly remove deep skin refuse, make skin clean, transparent.
2, the distinctive moisturizing composition of Semen phaseoli radiati and the sufficient moisture content of mineral supply skin, the moisture content insulating power of efficient hardening skin.Natural polysaccharides forms transparent, strong moisture film at skin surface, skin is moistened, has elastic force.
3, the special composition antioxidation extracted from Semen phaseoli radiati and anti-from/remarkable by base effect, antioxidant effect, higher than vitamin C, vitamin E 50 times, is the powerful mean that opposing is old and feeble, prevent skin splash.
4, extract the extract from Semen phaseoli radiati, still possess the good antipyretic and antidote functions of Semen phaseoli radiati, very good to all kinds of skin problem effect such as eczema, acne.
5, vitality root---the seed constituents that plant is original, can make skin health, dynamic, full of vitality.Comprise AHA composition inside the extract of the seed of Semen phaseoli radiati, non-stimulated removal aging cutin, promote cell regeneration, allow skin taking on a new look.Bean sprout begins to see and be loaded in Shennong's Herbal, and recording as middle product, is made with Semen sojae atricolor, and has the record of nature and flavor, effect, and application for a long time.Semen Phaseoli radiati Germinatus begins to see and be loaded in " record of Menghua, Tokyo ".To late Ming and early Qing, bean sprout and so on is food nationality.Claim according to " the remaining visitor's words of tea ", Semen Phaseoli radiati Germinatus becomes the Imperial Ancestral Temple and recommends new crystalline substance.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention provides a kind of exfoliated Semen phaseoli radiati Deacne pack.
Two of technical problem to be solved by this invention provides the preparation method of above-mentioned exfoliated Semen phaseoli radiati Deacne pack.
The present invention seeks to be achieved through the following technical solutions:
A kind of exfoliated Semen phaseoli radiati Deacne pack, is prepared from according to a conventional method by the raw material of following weight parts:
10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part hydrolyzed-silk glue protein, 4-6 part ethanol, 6-8 part C11-15 alkanol polyethers-7 carboxylic acid sodium, 0.8-2 part Semen phaseoli radiati extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
Wherein, described compound preservative, is made up of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
By carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, described compound preservative can be obtained.
Described exfoliated Semen phaseoli radiati Deacne pack can adopt industry conventional method to be prepared from.
Further, present invention also offers a kind of preparation method of exfoliated Semen phaseoli radiati Deacne pack, be made up of following step:
Polyvinyl alcohol is added in deionized water, be heated to 70-90 DEG C, dissolve, be cooled to 45-55 DEG C, add glycerol, hydrolyzed-silk glue protein, ethanol, the stirring of C11-15 alkanol polyethers-7 carboxylic acid sodium, be cooled to 40 DEG C, add Semen phaseoli radiati extracting solution and compound preservative, stir, described exfoliated Semen phaseoli radiati Deacne pack can be obtained.
Concrete, in the present invention:
Described polyvinyl alcohol can select cosmetics-stage polyvinyl alcohol, specifically can select if the trade mark is the polyvinyl alcohol of PVA1788, PVA1799 or PVA2488.
Glycerol, has another name called: propylene glycol, English name: Glycerin, molecular formula C 3h 8o 3.
Hydrolyzed-silk glue protein, English name: HYDROLYZED SERICIN, CAS accession number: 73049-73-7.The suppression ratio that hydrolyzed-silk glue protein is formed melanin is the highest, and antioxidation is strong.
C11-15 alkanol polyethers-7 carboxylic acid sodium, English name: SODIUM C11-15PARETH-7CARBOXYLATE, CAS accession number: 68603-23-6.There is excellent decontamination, emulsifying, dispersion, solubilising, foaming, surely steep ability.There is good lime soap dispersing power.Enduring high-concentration alkali.Oxidant can be tolerated.Resistance to hard water.High temperature resistant.Compatibility is good, can be composite with cationic surfactant, and is independent of each other.Mild surfactants, and the zest that can reduce other surfactants.Under acid condition, do not affect decontamination, foaming capacity.Can be applicable to infant product.
Semen phaseoli radiati (formal name used at school: Vigna radiata) is a kind of pulse family, Papillionoideae Vigna plant, originates in India, Burma area.Present East Asia various countries generally plant, and also there are a small amount of plantation in Africa, Europe, the U.S., and the states such as China, Burma are main Semen phaseoli radiati exported countrys.Analyze according to nutritionist, the index that prevents disease of Semen phaseoli radiati is 245.93, and biotic energy index is 2.87.Classical TCM is thought: ventilation of can subsiding a swelling, heat-clearing and toxic substances removing.Raw Semen phaseoli radiati grinding is twisted into juice swallow, can cure erysipelas, dysphoria with smothery sensation rubella, YAOSHI is started, steam Pentium, mends the intestines and stomach, tonification vigour, and adjusts the five internal organs, calms the nerves, the current twelve regular channels, except scurf removing, and skin care.
Semen phaseoli radiati extracting solution of the present invention can pass through commercially available and obtain.Also following method can be adopted to prepare and obtain: after Semen phaseoli radiati is pulverized, add the deionized water of 6-10 times of weight, soak 1-3 hour, ultrasonic extraction, 10-15 minute, filter, centrifugal, discard precipitation by supernatant concentration, obtained Semen phaseoli radiati extracting solution.Preferably, after concentrated, controlling Semen phaseoli radiati extracting solution density is 1.02-1.10g/cm 3.
Carnosic acid, molecular formula: C 20h 28o 4, No. CAS: 3650--09-7, source: Labiatae Rosmarinus plant rosemary Rosmarinus officinalis L.
AOB, No. CNS: 04.019, English name: antioxidant of bambooleaves.That AOB extracts from the tender leaf of Phyllostachys (phyllostachys) bamboo, with flavone and phenolic compound to be effective ingredient natural, nutrition, multi-functional food antioxidant.
Nisin, also claims nisin, English name: Nisin, a kind of polypeptide be made up of 34 aminoacid synthesized by streptococcus acidi lactici metabolism, molecular formula C 143h 228o 37n 42s 7molecular weight is 3348, and nisin is made up of water-wet side and hydrophobic side, is typical surfactant, efficient, nontoxic biological antiseptic, be widely used at present milk and milk products, fermented beverage, filling food, vegetable protein food, meat and its products anticorrosion.
Iodine propilolic alcohol butyl mephenesin Carbamate, English name: 3-Iodo-2-propynylbutylcarbamate, is abbreviated as IPBC, No. CAS: 55406-53-6, molecular formula: C 8h 12iNO 2, molecular weight is 281.10.
The present invention uses carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate composite as antiseptic, and antiseptic effect is significantly improved, the long shelf-life of facial film.And, use Compositional antiseptic agent, greatly reduce the consumption of iodine propilolic alcohol butyl mephenesin Carbamate, the consumption of iodine propilolic alcohol butyl mephenesin Carbamate is made to control below 0.03%, meet the IPBC specified in China's cosmetics health specification and European Union's regulatory affairs and limit the use of antiseptic in components of cosmetics, in cosmetics, maximum permission working concentration is 0.05%.Carnosic acid, AOB, nisin are nontoxic biological antiseptic, be widely used in food service industry, be diverted to cosmetic mask in the present invention, ill effect can't be brought to human body or skin, and harmful effect can not be produced to the stability of facial film.
The using method of exfoliated Semen phaseoli radiati Deacne pack of the present invention is: before using facial film, first deeply clean facial, again facial film is coated on face, after 15-25 minute, facial film active substance is absorbed by the skin, and moisture evaporates, thin film is formed gradually at face, this thin film is peeled off from face, the dirt on skin of face, scurf also stick on thin film in company with and be eliminated, face seems clean, smooth.
Exfoliated Semen phaseoli radiati Deacne pack of the present invention, can deep layer cleaning skin of face, and desalination facial lines, makes elasticity of skin compact, and water profit is plentiful.Continue to use, skin water profit is flexible, reproduces youthful vigor.
Exfoliated Semen phaseoli radiati Deacne pack of the present invention, deep layer can purify pore, can clean excess oil, promote skin water oil balance, and provide abundant mineral for skin, make skin clearly comfortable, dynamic, desalinate pox print simultaneously, skin whitening, eliminates obscure, makes skin even, brilliant white, anti-acne is reduced internal heat.
Exfoliated Semen phaseoli radiati Deacne pack of the present invention, adopt the antiseptic that carnosic acid, AOB, nisin, iodine propilolic alcohol butyl mephenesin Carbamate are composite, shelf life of products is long, and can not produce harmful effect to skin.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
Take each raw material according to embodiment 1 data corresponding in table 1, by carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, described compound preservative can be obtained.
Polyvinyl alcohol is added in deionized water, be heated to 70-90 DEG C, dissolve, be cooled to 45-55 DEG C, add glycerol, hydrolyzed-silk glue protein, ethanol, the stirring of C11-15 alkanol polyethers-7 carboxylic acid sodium, be cooled to 40 DEG C, add Semen phaseoli radiati extracting solution and compound preservative, stir, described exfoliated Semen phaseoli radiati Deacne pack can be obtained.
Wherein, the Semen phaseoli radiati extracting solution in embodiment 1 and comparative example 1-5 adopts following method to be prepared from: after Semen phaseoli radiati is pulverized, add the deionized water of 8 times of weight, soak 2 hours, ultrasonic extraction, 12 minutes, filters, centrifugal, discard precipitation by supernatant concentration, after concentrated, obtained density is 1.06g/cm 3semen phaseoli radiati extracting solution.
Table 1: face pack prescription list position: kilogram
Embodiment 1 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4 Comparative example 5
Deionized water 100 100 100 100 100 100
PVA-124 88 12 12 12 12 12 12
Glycerol 10 10 10 10 10 10
Hydrolyzed-silk glue protein 1 1 1 1 1 1
Ethanol 5 5 5 5 5 5
C11-15 alkanol polyethers-7 carboxylic acid sodium 7 7 7 7 7 7
Semen phaseoli radiati extracting solution 1 1 1 1 1 1
Carnosic acid 0.01 / / / / /
AOB 0.02 0.02 0.02 0.03 / /
Nisin 0.01 0.01 0.02 0.01 / /
Iodine propilolic alcohol butyl mephenesin Carbamate 0.01 0.02 0.01 0.01 / /
Methyl parahydroxybenzoate / / / / 0.05 /
Comparative example 1
Each raw material is taken according to comparative example 1 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Semen phaseoli radiati Deacne pack of comparative example 1.
Comparative example 2
Each raw material is taken according to comparative example 2 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Semen phaseoli radiati Deacne pack of comparative example 2.
Comparative example 3
Each raw material is taken according to comparative example 3 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Semen phaseoli radiati Deacne pack of comparative example 3.
Comparative example 4
Each raw material is taken according to comparative example 4 data corresponding in table 1.The method described in embodiment 1 is adopted to prepare the exfoliated Semen phaseoli radiati Deacne pack of comparative example 4.
Comparative example 5
Take each component according to comparative example 5 data corresponding in table 1, adopt method described in embodiment 1, namely obtain the exfoliated Semen phaseoli radiati Deacne pack of comparative example 5.
Test case 1
Respectively by the exfoliated Semen phaseoli radiati Deacne pack that embodiment 1 and comparative example 1-5 obtain, carry out fill with dark brown vial, open wide bottle cap, under being placed in ambient temperature 40 DEG C, relative humidity 85% environment, continuous observation is also tested, and concrete outcome sees the following form.Detect microorganism level, concrete test item, detection method and examination criteria carry out according to QB/T2872-2007.
Observe phenomena
Embodiment 1 No abnormality seen after 60 days, pure in smell
Comparative example 1 After 50 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Comparative example 2 After 40 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Comparative example 3 After 40 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Comparative example 4 After 40 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Comparative example 5 After 5 days, occur mildew, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
The antiseptic methyl parahydroxybenzoate used in comparative example 4 is one of the most frequently used cosmetics preservative in this area.Belong to antiseptic phenols, generally effective to mycete, yeast, antibacterial, there is the effect suppressing growth of microorganism, the shelf-life (under test condition of the present invention 40 days shelf-lifves) of cosmetics is effectively extended after adding, but long-term this antiseptic of excessive use, Diazolidinyl Urea epidermis cell, causes epidermis transition aging.
Can significantly be drawn by test data, the embodiment of the present invention 1 uses carnosic acid, AOB, nisin and the composite Synergistic of iodine propilolic alcohol butyl mephenesin Carbamate, and antiseptic effect (under test condition of the present invention 60 days shelf-lifves) is obviously better than comparative example 1-3 and only adopts AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate three composite (under test condition of the present invention less than 50 days shelf-life).
The accelerated test of facial film under opening is placed in ambient temperature 40 DEG C, relative humidity 85% environment of the embodiment of the present invention 1, can reach 60 days antiseptic effects, the long shelf-life of facial film, and shady and cool dry its shelf-life of place far surpasses 3 years in sealed states in conversion.
Test case 2
With CorneometerCM820 moisture of skin measuring instrument, carry out measurement skin surface moisture at tested position, tested position is respectively the abundant forehead of sebaceous gland.Operating ambient temperature is 22-24 DEG C, and relative humidity is 46%-55%, and the unit of skin moisture content is au (arbitraryunit).Use the female consumer forehead skin of the embodiment of the present invention 1 to test to one, concrete data see the following form.
Before using, au After using, au Use latter 1 hour, au
Embodiment 1 35.0 77.7 72.8
The above; be only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.

Claims (2)

1. an exfoliated Semen phaseoli radiati Deacne pack, it is characterized in that, be prepared from according to a conventional method by the raw material of following weight parts: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part hydrolyzed-silk glue protein, 4-6 part ethanol, 6-8 part C11-15 alkanol polyethers-7 carboxylic acid sodium, 0.8-2 part Semen phaseoli radiati extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters;
Described compound preservative, is made up of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
2. the preparation method of exfoliated Semen phaseoli radiati Deacne pack as claimed in claim 1, it is characterized in that, be made up of following step: polyvinyl alcohol is added in deionized water, be heated to 70-90 DEG C, dissolve, be cooled to 45-55 DEG C, add glycerol, hydrolyzed-silk glue protein, ethanol, the stirring of C11-15 alkanol polyethers-7 carboxylic acid sodium, be cooled to 40 DEG C, add Semen phaseoli radiati extracting solution and compound preservative, stir.
CN201310243257.5A 2013-06-18 2013-06-18 Peel-off type mung bean acne-removing mask and preparation method thereof Active CN103385826B (en)

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CN106265389A (en) * 2016-11-02 2017-01-04 常州创索新材料科技有限公司 A kind of preparation method containing plant enzyme Linesless charcoal/mung bean mud cleaning Deacne pack
CN106727212A (en) * 2016-11-25 2017-05-31 江苏爱西施科技服务咨询股份有限公司 A kind of silk ecchymose removing cosmetics and preparation method thereof
CN108338943B (en) * 2017-01-25 2021-02-26 浏阳河集团股份有限公司 Paste mung bean mask and preparation method and application thereof
CN111939099A (en) * 2020-09-04 2020-11-17 陈广文 Acne-removing moisturizing mask and preparation method thereof

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US7544375B1 (en) * 2006-06-12 2009-06-09 Swiss Skin Repair, Inc. Composition
CN101427991A (en) * 2007-11-07 2009-05-13 熊丽 Acne-removing skin-protection face pack
CN102805720A (en) * 2012-08-01 2012-12-05 青岛文创科技有限公司 Anti-acne mask

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