CN106929231A - A kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay and preparation method thereof - Google Patents
A kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay and preparation method thereof Download PDFInfo
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- CN106929231A CN106929231A CN201710134550.6A CN201710134550A CN106929231A CN 106929231 A CN106929231 A CN 106929231A CN 201710134550 A CN201710134550 A CN 201710134550A CN 106929231 A CN106929231 A CN 106929231A
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- acid
- amino acid
- royal jelly
- cinnamomum kanahirai
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The present invention discloses transparent amino acid crystal soap of a kind of Cinnamomum kanahirai hay and preparation method thereof, is mainly made up of the component of following weight percentage：Antrodia camphorata extract 0.05 5%, royal jelly acid 0.01 2%, Chinese wistaria flower extract 0.1 1%, amino acid surfactant 10 20%, aliphatic acid 8 15%, polyalcohol 20 30%, NaOH 2 3.6%, edible alcohol 3 12%, NMF 3 10%, deionized water is surplus.Crystal soap of the invention has that transparency is high, hardness is moderate, foaming power and also have excellent anti-wrinkle effect while stronger cleaning force, and avoids and reduces the situation that perspire under wet environment, is allowed to more robust.
Description
Technical field
The present invention relates to field of daily chemicals, a kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay and its preparation side are specifically related to
Method.
Background technology
Amino acid transparent soap is a kind of hand with amino acid type surfactant as primary surfactant for rising in recent years
Work soap, with faintly acid, transparency skin-friendly high, good and security, it is low to skin irritatin the characteristics of, increasingly consumed
Person is received.However, the production technology of amino acid transparent soap is ripe not enough at present, main cause is amino acid pattern surface-active
The foaming power and cleaning force of agent are weak, cause soap body to be difficult to meet the demand of consumer's deep layer cleaning；Additionally there are amino acid pattern
Surfactant into the partially soft problem of soap body, be easily caused deformation of products, in-convenience in use.
Chinese patent application CN201410470096.8 discloses a kind of transparent solid of amino acid surfactant matrix
Soap, its composition includes each component of following weight portion：Amino acid surfactant 55-75 parts, pure water 3-13 parts, castor oil polyoxy
3-10 parts of vinethene (15-40EO), glycerine 3-8 parts, glucose 3-10 parts, ethanol 2-8 parts, 0.1-3 parts of PH poising agents, essence
0.2-0.5 parts.The invention employs castor oil polyoxyethylene ether (15-40EO) as auxiliary surfactant to lift soap body
Cleaning force, but the cosurfactant is a kind of solubilizer of high hlb, and foaming power itself is weak, to soap body foaming power
Castering action is little.
The content of the invention
Regarding to the issue above, it is an object of the invention to provide a kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay and its preparation side
Method.Crystal soap of the invention has that transparency is high, hardness is moderate, foaming power and also have excellent dispelling while stronger cleaning force
Wrinkle effect, and avoid and reduces the situation that perspire under wet environment, it is allowed to more robust.
The concrete technical scheme for solving above-mentioned technical problem is as follows：
A kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay, it is mainly made up of the component of following weight percentage：Antrodia camphorata extract
0.05-5%, royal jelly acid 0.01-2%, Chinese wistaria flower extract 0.1-1%, amino acid surfactant 10-20%, aliphatic acid 8-15%,
Polyalcohol 20-30%, NaOH 2-3.6%, edible alcohol 3-12%, NMF 3-10%, deionized water is surplus, wherein, ox
Antrodia extract, royal jelly acid, Chinese wistaria flower extract are under mutual cooperation, and anti-wrinkle effect is more preferable.
A kind of transparent amino acid crystal soap of described Cinnamomum kanahirai hay, it is mainly made up of the component of following weight percentage：Cinnamomum kanahirai hay
Sesame extract 0.05-1.5%, royal jelly acid 0.2-0.4%, Chinese wistaria flower extract 0.1-0.5%, amino acid surfactant 10-15%,
Aliphatic acid 10-15%, polyalcohol 20-25%, NaOH 2-3.2%, edible alcohol 5-10%, NMF 5-10%, deionized water is
Surplus.
The Antrodia camphorata extract is prepared by conventional extraction technique, and Antrodia camphorata is the distinctive fungi in Taiwan, is only grow on
In the distinctive cinnamomum kanehirai in Taiwan.Antrodia camphorata has the physiologically active ingredient of many, such as polysaccharide body, triterpene compound, super oxygen disproportionation
Enzyme, adenosine, protein（Containing immune protein）, vitamin, trace element, nucleic acid, agglutinin, amino acid, solid liquor-saturated tired, cellulose,
Blood pressure stabilization material etc..Antrodia camphorata has extensive physiologically active, its have treating cancer, enhance immunity, anti-oxidant, anti-inflammatory and
The functions such as antibacterial.By the rational proportion of crystal soap body system, the particularly addition of Antrodia camphorata extract, the polysaccharide physical efficiency that it contains
Superoxide radical and DPPH free radicals are effectively removed, the extent of damage of skin photoage can be effectively improved；And Antrodia camphorata is extracted
The triterpene compound that thing contains has the effect for improving skin quality, increases the moisture feeling after washing one's face；Additionally, Antrodia camphorata extract is also
Can be used as in spices addition crystal soap body system, its distinctive fragrance promotes the pleasant feeling after washing one's face, and makes one happy.
It is prepared by the preferably following preparation method of the royal jelly acid：Step is as follows：
1）Royal jelly extracting residue, in adding the ethanol solution of 85-95%, by ethanol solution heating water bath to 45 degrees Celsius, then
Vibration, extracts 50-70 minutes, suction filtration.
2）By gained filtrate under 46 degrees Celsius of environmental condition, according to 1:5-1:5.5 volume is added in deionized water
It is stripped, is inserted 6 hours in the refrigerator that temperature is 4 degrees Celsius, taken out and filter, is obtained royal jelly acid crystalline solid.
3）The royal jelly acid crystalline solid for being obtained is dissolved again, and king is carried out using boric acid complexometry with D201 resins
Slurry acid solution carries out desugar treatment.
4）Solubilization liquid is inserted 6 hours in the refrigerator that temperature is 4 degrees Celsius again again after desugar, is taken out and is filtered, and is taken off
Royal jelly acid crystalline solid after sugar.
5）Royal jelly acid crystalline solid is air-dried 24 hours, and acquisition finished product is vacuum dried to it with vacuum drier.
Royal jelly has nutritive value very high, is always very precious nutriment.The royal jelly of high nutritive value its
It is also in fact the excellent materials of beauty and skin care.Royal jelly can be promoted and enhancing table by the epidermal absorption of human body, nutrition epidermal cell
The vitality of chrotoplast, improves the metabolism of cell, accelerates the exclusion of metabolite, reduces pigment deposition, prevents elastic force
Fibre modification, is skin high resilience, gloss, exquisiteness, can also smooth away wrinkles and postpone the appearance of wrinkle.Royal jelly contains 20
Various free fatties, including linoleic acid, arachidic acid, n-nonanoic acid, octanoic acid, decylenic acid etc., wherein 10- hydroxyls -2- decylenic acids
(10- HDA) is distinctive in royal jelly in the middle of nature, is the mark of royal jelly, referred to as royal jelly acid.In queen bee
In the quality standard of slurry, the special provision content requirement of royal jelly acid.Royal jelly acid is royal jelly antibacterial, anticancer, strengthen immunity
Main component.Royal jelly contains the abundant nutritional ingredient such as protein, amino acid, vitamin, and in honeycomb temperature, (35 take the photograph
Family name's degree or so) under be adapted to the growth of bacterium and mould, royal jelly acid shields to fresh royal jelly.A series of researchs show, honeybee
Royal jelly to staphylococcus aureus, streptococcus, proteus, Escherichia coli, typhoid bacillus, hay bacillus, tubercle bacillus and
Starlike trichophyte and Epidermophyton etc. have antibacterial action, and them can be suppressed during low concentration, there is bactericidal action during high concentration.Queen bee
The antibacterial action of slurry is relevant with aliphatic acid contained therein, such as royal jelly acid.
The preparation method of royal jelly acid generally has extraction method and chemical synthesis in the prior art.Chemical synthesis purity compared with
Height, but the impurity of more other complicated ingredients is lost, lose the natural sex of extract.And prepared in existing extraction method
In royal jelly acid, using royal jelly as raw material, cost is very high, and extraction efficiency is not high, and the product for being obtained contains one
Quantitative fructose and glucose, is unfavorable for directly being applied in cosmetics.Inventor in view of the shortcomings of the prior art, first takes
The method of ethanol extraction, extracts royal jelly acid from royal jelly residue, the concentration for controlling ethanol solution appropriate, and in proper temperature condition
Under carry out, substantially increase the efficiency for having extracted, saved resource.Entered using boric acid complexometry to just carrying product afterwards
One step desugar is processed.The royal jelly acid that the present invention will be extracted is applied in crystal soap body system so that consumer is carrying out face clearly
Bacterium while cleaning and nursing to face generates inhibitory action, serves good beauty, crease-resistant, degerming effect；Except this
Outside, royal jelly acid also further enhances the transparency and hardness of soap body.
Wistaria flower is the inflorescence of legume Chinese wistaria, is a kind of common edibility flower, with Li Shui disappear lump in the abdomen the effect of, it is purple
The flavone compound contained in rattan flower extract, the effect with anti-inflammatory, resisting oxidation free radical compounds Antrodia camphorata extract,
Accelerate to remove superoxide radical and DPPH free radicals.
In a preferred embodiment of the invention, the amino acid surfactant is cocounut oil acyl glutamic acid, myristoyl
Glutamic acid, stearoyl-glutamic acid, lauroyl glutamate, lauroyl glutamate potassium, sodium lauroyl glutamate, cocoyl
Glutamic acid, cocoyl potassium glutamate, sodium cocoyl glutamate, myristoyl potassium glutamate, myristoyl glutamic acid
One or more mixture in sodium.
Further preferred ammonia cocounut oil acyl glutamic acid, the mixing of myristoyl sodium glutamate.
More preferably cocounut oil acyl glutamic acid, sodium lauroyl glutamate, the weight of myristoyl sodium glutamate are
（1-3）：（1-3）：（1-3）.By the reasonable compounding use of three, increase the foaming power and stability of soap body, be allowed to milder,
It is not tight after washing one's face.
In a preferred embodiment of the invention, the aliphatic acid is octanoic acid, capric acid, laurate, myristic acid, palm
In acid, stearic acid, oleic acid, linoleic acid, leukotrienes, erucic acid, arachidic acid, behenic acid, lignin acid, cerinic acid, montanic acid, beeswax acid
One or more mixture.
Further preferred laurate, stearic acid, the mixing of behenic acid.
More preferably laurate, stearic acid, the weight of behenic acid are（1-2）：（1-4）：（1-2）.The aliphatic acid is mixed
The combination of compound, hardness, outward appearance, cleaning force and skin sense needed for assigning crystal soap of the present invention, it is preferably matched, and is ensureing good
The degreasing power of crystal soap is reduced while the cleaning force got well, helps to reduce the tight feeling after washing one's face.
In a preferred embodiment of the invention, the polyalcohol be glycerine, propane diols, butanediol, pentanediol, oneself two
It is alcohol, sorbierite, erythrite, ethanol, PEG-8, polyethylene glycol -32, dipropylene glycol, diglycerol, glycerin polyether -26, poly- sweet
One or more mixture in oil -10, polyglycereol -8.
Further preferred butanediol, the mixing of sorbierite.
More preferably butanediol, the weight of sorbierite are（1-2）：（1-3）.
In a preferred embodiment of the invention, the NMF is glucose, reed fragrant plant oil, glycerine, reed fragrant plant glue, oligomeric fruit
One or more mixture in sugar, trehalose.
It is preferred that reed fragrant plant is oily, the mixing of glycerine.
More preferably reed fragrant plant oil, the weight of glycerine are 1：（5-10）.The excellent moisture-keeping functions compounding glycerine of reed fragrant plant oil,
Xi Hou faces are moist, with good moisturizing efficiency.
A kind of preparation method of the transparent amino acid crystal soap of Cinnamomum kanahirai hay, comprises the following steps：
（1）Amino acid surfactant, polyalcohol, NMF are sequentially added into agitated kettle, intensification is heated to 80-85 DEG C, constant temperature
Stirring is to being completely dissolved；
（2）Aliphatic acid is added into agitated kettle, stirring and dissolving；
（3）NaOH is dissolved in deionized water, then is slowly added into agitated kettle, insulated and stirred 30-50 minutes；
（4）Edible alcohol is added into agitated kettle, insulated and stirred；
（5）Antrodia camphorata extract, royal jelly acid, olive fruit oil are added into agitated kettle, insulated and stirred 5-10 minutes；
（6）Temperature is down to 50-60 DEG C, transparent then in turn through froth breaking, injection molding, cooling, the demoulding, air-dried, packaging acquisition Cinnamomum kanahirai hay
Amino acid crystal soap.
Relative to prior art, technical scheme has the advantages that：
（1）Transparency is high, hardness is moderate, by the addition of the rational proportion of crystal soap body system, especially royal jelly acid, greatly increases
The transparency of soap body；The compounding of aliphatic acid and royal jelly acid, assigns soap body moderate hardness, it is to avoid and reduce perspiration under wet environment
Situation, is allowed to more robust.
（2）Foaming power is good, cleaning capacity is strong, by cocounut oil acyl glutamic acid, sodium lauroyl glutamate, nutmeg in system
The rational proportion of acyl glutamic acid sodium, increases the foaming power and stability of soap body, is allowed to milder, and cleaning capacity is stronger, washes one's face
It is not tight afterwards.
（3）Antrodia camphorata extract is added in crystal soap body system as spices, substitutes chemically composite perfume, and reducing soap body stimulates
Property, it is allowed to milder.
（4）The distinctive bactericidal action of royal jelly acid, replaces preservative, reduces soap body side effect.
（5）Antrodia camphorata extract of the present invention, royal jelly acid and Chinese wistaria flower extract have fine by rationally compounding to skin
Anti-wrinkle effect, mutually promoted between each composition, Synergistic so that the transparent amino acid crystal soap of Cinnamomum kanahirai hay of the invention can promote
Enter cytothesis, effectively smooth skin microgroove, repair impaired skin, recover skin elasticity, make skin smooth tender.
（6）The process is simple that the present invention is used, simple equipments are easy to large-scale production.
Brief description of the drawings
Accompanying drawing of the invention is form；
Fig. 1 is table 1, the transparent amino acid crystal soap formula of embodiment 1-7 Cinnamomum kanahirai hays；
Fig. 2 is table 2, embodiment and comparative example application sense evaluation result；
Fig. 3 is table 3, transparent amino acid crystal soap bacteriostatic experiment result (inhibition zone diameter mm)；
Fig. 4 is table 4, result on trial.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.
The transparent amino acid crystal soap formula of embodiment of the present invention 1-7 Cinnamomum kanahirai hays is shown in Table 1；
The preparation method of above-mentioned royal jelly acid：Comprise the following steps：
1）Royal jelly extracting residue, in adding 85% ethanol solution, by ethanol solution heating water bath to 45 degrees Celsius, Ran Houzhen
Swing, extract 60 minutes, suction filtration.
2）By gained filtrate under 46 degrees Celsius of environmental condition, according to 1:5 volume is carried out instead in adding deionized water
Extraction, inserts 6 hours in the refrigerator that temperature is 4 degrees Celsius, takes out and filters, and obtains royal jelly acid crystalline solid.
3）The royal jelly acid crystalline solid for being obtained is dissolved again, and king is carried out using boric acid complexometry with D201 resins
Slurry acid solution carries out desugar treatment.
4）Solubilization liquid is inserted 6 hours in the refrigerator that temperature is 4 degrees Celsius again again after desugar, is taken out and is filtered, and is taken off
Royal jelly acid crystalline solid after sugar.
5）Royal jelly acid crystalline solid is air-dried 24 hours, and acquisition finished product is vacuum dried to it with vacuum drier.
Above-described embodiment preparation method is comprised the following steps：
（1）Amino acid surfactant, polyalcohol, NMF are sequentially added into agitated kettle, intensification is heated to 80-85 DEG C, constant temperature
Stirring is to being completely dissolved；
（2）Aliphatic acid is added into agitated kettle, stirring and dissolving；
（3）NaOH is dissolved in deionized water, then is slowly added into agitated kettle, insulated and stirred 30-50 minutes；
（4）Edible alcohol is added into agitated kettle, insulated and stirred；
（5）Antrodia camphorata extract, royal jelly acid, Chinese wistaria flower extract are added into agitated kettle, insulated and stirred 5-10 minutes；
（6）Temperature is down to 50-60 DEG C, transparent then in turn through froth breaking, injection molding, cooling, the demoulding, air-dried, packaging acquisition Cinnamomum kanahirai hay
Amino acid crystal soap.
Comparative example 1
It is not add Antrodia camphorata extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 2
It is not add royal jelly acid with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 3
It is not add Chinese wistaria flower extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 4
Not add Antrodia camphorata extract, royal jelly acid and olive fruit oil with the difference of embodiment 1, other preparation conditions and method with
Embodiment 1 is identical.
Applicating evaluating
Applicating evaluating includes ocular estimate and use feeling evaluation.
30 testers (each 15 people of men and women, age bracket -55 years old 15 years old) of selection, are carried out to embodiment 1-7 and comparative example 1-4
Blind Test.Each embodiment and comparative example parallel determination 3 times.Tester feels to be scored according to the application of oneself, assessment item
It is related to foaming abundancy degree, cleaning force washes rear skin sense (gentle, moist, moist not tight etc.) and transparency.Standards of grading are used
5 points of systems, 1 point worst, and 5 points best.Evaluation result is the average mark of all tester's fractions, and average mark more high effect is better.
The method of the ocular estimate is：When No. 14 (4mm) black matrixes can be seen clearly by the thick soap blank of (1/4 inch) of 6.35mm
The transparency of word is qualified；Conversely, can not see clearly but have certain transparency for unqualified；It is fully opaque, transparency
It is nothing；It is medium when No. 12 soap transparencies of boldface type can be seen clearly by (1/4 inch) thick soap blank of 6.35mm；When passing through
(1/4 inch) of 6.35mm thick soap blank can see No. 10 soap transparencies of boldface type clearly preferably.
Described use appraisal method is：Face and both hands are soaked with water；Take pebble soap and wipe 10 on hand
Secondary, drop 2.0g water in the palm of the hand, rub to a large amount of foams of generation by both hands；Both hands with a large amount of foams are gently washed by rubbing with the hands simultaneously on the face
Massage；Finally foam on the face is rinsed well with clear water.
The application sense evaluation result of embodiment and comparative example is listed in table 2.
As seen from Table 2, the PH of the transparent amino acid crystal soap of Cinnamomum kanahirai hay prepared by embodiment 1-7 is respectively less than 7, in faintly acid；
The hardness balance of embodiment 1-7 and comparative example 1-4 understands that the transparent amino acid crystal soap hardness of Cinnamomum kanahirai hay prepared by the present invention is obtained
Lifting；Embodiment 1-7 understands that the addition of royal jelly acid can further increase the hardness of product with the hardness balance of comparative example 2；It is real
Foaming power and the cleaning force contrast for applying a 1-7 and comparative example 1-4 understands, the transparent amino acid crystal soap prepared by the present invention it is clear
Clean power and foaming power are more preferably；Embodiment 1-7 and comparative example 1-4's washes knowable to rear skin sense contrast, the transparent ammonia prepared by the present invention
Base acid crystal soap washes rear skin sense more preferably.
Carry out bacteriostatic experiment
(1) it is grouped according to embodiment and comparative example, every group there are 30 culture dishes；
(2) prepared by bacteriostatic agent：Weigh transparent amino acid crystal soap product 5g obtained in each embodiment and comparative example and be put into conical flask
In, and add sterile distilled water 25mL to be vibrated to sample in 30 DEG C of water-baths and be completely dissolved, it is made the antibacterial agent solution of different product；
(3) cultured staphylococcus aureus, Escherichia coli and white chain pearl bacterium are inoculated in above-mentioned each group culture respectively
On base, every kind of bacterium is inoculated with 10 culture dishes；
(4) finished culture dish is positioned in 37 degree of insulating box and is cultivated 24 hours.
(5) hole of formed objects, and implantation step (2) in hole are beaten in the center of above-mentioned every group of culture dish using card punch
Obtained bacteriostatic agent, and be placed in 37 degree of insulating box and cultivate 36 hours.
(6) diameter of antibacterial circle in culture dish is finally measured respectively, obtains average value.
(7) antibacterial effect is bigger according to antibacterial loop diameter, and the better principle of antibacterial effect show that antibacterial experiment result is shown in
Table 3.
Anti-wrinkle efficacy validation
Detection results on probation are carried out to product prepared by embodiment 1-7 and comparative example 1-4, while commercially available declaring have with a
The Transparent handmade soap of good anti-wrinkle effect is control group.Test object：Each experimental group is 20 women（25-50 Sui）；Test
Region：Face；Use：Twice daily, persistently use 4 weeks；Test event：Skin elasticity, skin water are tender, wrinkle depth（Fish tail
Line region）.Result on trial see the table below 4.
By the visible embodiment 1-7 skin elasticities of table 4, water is tender and wrinkle depth improves obvious number and is significantly more than comparative example
1-4 and control group, illustrate the transparent amino acid crystal soap of Cinnamomum kanahirai hay of the present invention be significantly improved skin elasticity, skin water it is tender and wrinkle
The effect of line depth；The skin elasticity of comparative example 4 is obviously improved 4 people, and skin water is tender to be obviously improved 5 people, and wrinkle depth is obviously improved 5
People, hence it is evident that less than other embodiment and comparative example, principle active component is in illustrating the transparent amino acid crystal soap of Cinnamomum kanahirai hay of the present invention
Antrodia camphorata extract, royal jelly acid, Chinese wistaria flower extract；The delay skin aging facial mask of comparative example 1 does not add Antrodia camphorata extract,
Its skin elasticity, water are tender and wrinkle depth improves obvious number and is respectively 8 people, 7 people, 7 people far below the skin bullet of embodiment 1
Property, water is tender and wrinkle depth improves obvious number；Comparative example 2 and comparative example 3 are respectively not added with royal jelly acid and wistaria flower is carried
Thing is taken, its skin elasticity, water are tender and wrinkle depth improves obvious number and is significantly lower than embodiment 1, comparative example 1-3 and implementation
Example 1 is contrasted, it is seen that in the transparent amino acid crystal soap of Cinnamomum kanahirai hay of the present invention, Antrodia camphorata extract, royal jelly acid, Chinese wistaria flower extract tool
There is Synergistic.
Above example only illustrates embodiment of the present invention, does not there is any formal limitation to the present invention；Appoint
What is engaged in professional and technical personnel, all has the ability to make some changes using the technology contents for disclosing or modifies, as equivalent
The Equivalent embodiments of change, according to the technology of the present invention essence, simply modification, equivalent variations and modification are carried out to the present invention, are belonged to
In the range of technical solution of the present invention.
Claims (8)
1. the transparent amino acid crystal soap of a kind of Cinnamomum kanahirai hay, it is characterised in that be mainly made up of the component of following weight percentage：Cinnamomum kanahirai hay
Sesame extract 0.05-5%, royal jelly acid 0.01-2%, Chinese wistaria flower extract 0.1-1%, amino acid surfactant 10-20%, fat
Sour 8-15%, polyalcohol 20-30%, NaOH 2-3.6%, edible alcohol 3-12%, NMF 3-10%, deionized water is surplus.
2. the transparent amino acid crystal soap of a kind of Cinnamomum kanahirai hay according to claim 1, it is characterised in that main by following weight hundred
Divide the component composition of ratio：Antrodia camphorata extract 0.05-1.5%, royal jelly acid 0.2-0.4%, Chinese wistaria flower extract 0.1-0.5%, amino
Acid surfaces activating agent 10-15%, aliphatic acid 10-15%, polyalcohol 20-25%, NaOH 2-3.2%, edible alcohol 5-10%, protect
Humectant 5-10%, deionized water is surplus.
3. a kind of transparent amino acid crystal soap of Cinnamomum kanahirai hay according to claim 1, it is characterised in that the preparation of the royal jelly acid
Method is comprised the following steps：
1）Royal jelly extracting residue, in adding the ethanol solution of 85-95%, by ethanol solution heating water bath to 45 degrees Celsius, then
Vibration, extracts 50-70 minutes, suction filtration；
2）By gained filtrate under 46 degrees Celsius of environmental condition, according to 1:5-1:5.5 volume is carried out in adding deionized water
Back extraction, inserts 6 hours in the refrigerator that temperature is 4 degrees Celsius, takes out and filters, and obtains royal jelly acid crystalline solid；
3）The royal jelly acid crystalline solid for being obtained is dissolved again, and royal jelly acid is carried out using boric acid complexometry with D201 resins
Solution carries out desugar treatment；
4）Solubilization liquid is inserted 6 hours in the refrigerator that temperature is 4 degrees Celsius again again after desugar, is taken out and is filtered, after obtaining desugar
Royal jelly acid crystalline solid；
5）Royal jelly acid crystalline solid is air-dried 24 hours, and acquisition finished product is vacuum dried to it with vacuum drier.
4. the transparent amino acid crystal soap of a kind of Cinnamomum kanahirai hay according to claim 1, it is characterised in that the amino acid surface is lived
Property agent be cocounut oil acyl glutamic acid, myristoyl glutamate, stearoyl-glutamic acid, lauroyl glutamate, lauroyl glutamate
Potassium, sodium lauroyl glutamate, cocoyl glutamic acid, cocoyl potassium glutamate, sodium cocoyl glutamate, myristoyl
One or more mixture in base potassium glutamate, myristoyl sodium glutamate；It is preferred that ammonia cocounut oil acyl glutamic acid, meat
The mixing of cardamom acyl group sodium glutamate；More preferably cocounut oil acyl glutamic acid, sodium lauroyl glutamate, myristoyl sodium glutamate
Weight be（1-3）：（1-3）：（1-3）.
5. the transparent amino acid crystal soap of a kind of Cinnamomum kanahirai hay according to claim 1, it is characterised in that the aliphatic acid is pungent
Acid, capric acid, laurate, myristic acid, palmitic acid, stearic acid, oleic acid, linoleic acid, leukotrienes, erucic acid, arachidic acid, behenic acid,
One or more mixture in lignin acid, cerinic acid, montanic acid, beeswax acid；It is preferred that laurate, stearic acid, behenyl
The mixing of acid；More preferably laurate, stearic acid, the weight of behenic acid are（1-2）：（1-4）：（1-2）.
6. the transparent amino acid crystal soap of a kind of Cinnamomum kanahirai hay according to claim 1, it is characterised in that the polyalcohol is sweet
Oil, propane diols, butanediol, pentanediol, hexylene glycol, sorbierite, erythrite, ethanol, PEG-8, polyethylene glycol -32, double third
One or more mixing in glycol, diglycerol, glycerin polyether -26, Natrulon H-10, polyglycereol -8；More preferably fourth two
The mixture of alcohol, sorbierite；It is preferred that the weight of butanediol, sorbierite is（1-2）：（1-3）.
7. the transparent amino acid crystal soap of a kind of Cinnamomum kanahirai hay according to claim 1, it is characterised in that the NMF is grape
One or more mixture in sugar, reed fragrant plant oil, glycerine, reed fragrant plant glue, FOS, trehalose；It is preferred that reed fragrant plant is oily, sweet
The mixing of oil；More preferably reed fragrant plant oil, the weight of glycerine are 1：（5-10）.
8. a kind of method of the transparent amino acid crystal soap of the Cinnamomum kanahirai hay prepared as described in claim any one of 1-7, it is characterised in that
Comprise the following steps：（1）Amino acid surfactant, polyalcohol, NMF are sequentially added into agitated kettle, intensification is heated to 80-
85 DEG C, constant temperature is stirred to being completely dissolved；（2）Aliphatic acid is added into agitated kettle, stirring and dissolving；（3）NaOH is dissolved in
In ionized water, then agitated kettle is slowly added into, insulated and stirred 30-50 minutes；（4）Edible alcohol is added into agitated kettle, insulated and stirred；
（5）Antrodia camphorata extract, royal jelly acid, Chinese wistaria flower extract are added into agitated kettle, insulated and stirred 5-10 minutes；（6）Temperature is down to
50-60 DEG C, the transparent amino acid crystal soap of Cinnamomum kanahirai hay is obtained then in turn through froth breaking, injection molding, cooling, the demoulding, air-dried, packaging.
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Application publication date: 20170707 |