CN108823013A - amino acid camellia handmade soap and preparation method thereof - Google Patents
amino acid camellia handmade soap and preparation method thereof Download PDFInfo
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- CN108823013A CN108823013A CN201810984848.0A CN201810984848A CN108823013A CN 108823013 A CN108823013 A CN 108823013A CN 201810984848 A CN201810984848 A CN 201810984848A CN 108823013 A CN108823013 A CN 108823013A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
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Abstract
The present invention relates to a kind of amino acid camellia handmade soaps and preparation method thereof, according to mass fraction meter, are prepared from the following raw materials：20-30 parts of lauroyl glutamate, 20-30 parts of cocounut oil acyl glutamic acid, 10-18 parts of moisturizer, 28-35 parts of triethanolamine ethanol solution, 5-10 parts of sodium hydrate aqueous solution, plant extraction liquid 20-30 parts antibacterial, 3-8 parts of camellia oil, 0.1-0.3 parts of essence.Preparation method is：Amino acid starting material and antibacterial plant extraction liquid and moisturizer are dissolved by heating, triethanolamine ethanol solution, sodium hydrate aqueous solution progress saponification is then added, is eventually adding camellia oil, essence, stands after mixing evenly, is filling.The amino acid camellia oil handmade soap carries out saponification using triethanolamine ethanol solution and sodium hydrate aqueous solution, and soap body hardness after cooling increases, and is unlikely to deform addition plant extraction liquid, still has bacteriostasis under neutrallty condition.
Description
Technical field
The present invention relates to a kind of handmade soap, especially a kind of amino acid camellia handmade soap and preparation method thereof.
Background technique
Amino acid soap is that a kind of pH value is weakly acidic handmade soap, washes temperature-sensitive and comfortable, does not stimulate eyes, but it is inclined at soap
Soft, mutability, soap body surface is sticky, limits manner of packing, beautiful using catching up with bubble mode that could present by hand after coating
The technique of appearance, nontraditional amino acid soap has the reaction time long, and manufacturing procedure is more, and feeding soap is of long duration, and man efficiency is low, and soap body is easy
The problems such as denaturation, and because its pH is faintly acid, the bacteriostasis of cold handmade soap script processed is lost, needs to add preservative ability
Guarantee the stability of product.
Summary of the invention
An object of the present invention be overcome the above-mentioned insufficient of the prior art and provide a kind of amino acid camellia handmade soap and
Preparation method, this method processing step is simple, and man efficiency is high, and process time is short, stable product quality, without adding chemistry
Preservative.Resulting amino acid camellia oil handmade soap is that a kind of molding is fast, hardness is high, is unlikely to deform, when more saving packaging production
Between, mildly moist stabilized formulations, are rich in a variety of natural bacteriostatic ingredients, and the long-acting inhibition bacterium of energy increases, and protect family health.
The second object of the present invention is to provide the preparation method of the amino acid camellia handmade soap.
The technical scheme is that：A kind of amino acid camellia handmade soap is made in terms of mass fraction of following component：
20-30 parts of lauroyl glutamate, 20-30 parts of cocounut oil acyl glutamic acid, 10-18 parts of moisturizer, triethanolamine ethanol solution 28-
35 parts, 5-10 parts of sodium hydrate aqueous solution, plant extraction liquid 20-30 parts antibacterial, 3-8 parts of camellia oil, 0.1-0.3 parts of essence.
Preferably, the antibacterial plant extraction liquid is by 20-30 parts of camellia seed powder, 20-30 parts of lemon peel, flos caryophylli
10-20 parts, 10-20 parts of crushing and water-addings of dandelion extract, dosage is too low, does not have inhibition antibacterial effect；Dosage is excessively high,
Cost will increase, and fungistatic effect will not enhance.
Preferably, the moisturizer is mixed by 40-50 parts of glycerol, 20-30 parts of sorbierite, 20-30 parts of propylene glycol.
Preferably, the triethanolamine ethanol solution is by 60-80 parts of triethanolamine, 20-40 parts of dehydrated alcohol mixing
It forms.
Preferably, the sodium hydrate aqueous solution be by 20-25 parts of sodium hydroxide, 75-80 parts of deionized water mixing and
At.
The preparation process of the antibacterial plant extraction liquid is：
（1）Selection：Select color, the normal camellia seed shell of smell, lemon peel, flos caryophylli, dandelion；
（2）It crushes：By step（1）Middle raw material is put in proportion into pulverizer, and is sieved（50-100 mesh）；
（3）It extracts：By step（2）Gained plant material powder is according to 1:The ratio of 5-10 is mixed with water, is heated to 70-90 DEG C, is held
Cold filtration after continuous stirring 1-3 hours, obtains antibacterial plant extraction liquid.
The preparation method of the amino acid camellia oil handmade soap, in turn includes the following steps：
（1）It is prewired：Antibacterial plant extraction liquid will be weighed up and lauroyl amino acid, cocoamido acid and moisturizer raw material investment are anti-
It answers in kettle and slowly dissolves by heating, temperature sets 70-90 DEG C, and mixing speed is 10-30 revs/min；
（2）Saponification：The triethanolamine ethanol solution, the sodium hydrate aqueous solution that weigh up are slowly added into reaction kettle, stirring turns
Speed is set as 25-35 revs/min, reacts 30-50 minutes；
（3）Compounding：The camellia oil weighed up, essence are added in reaction kettle, stirring is closed after continuing stirring 5-10 minutes, after continuation of insurance
Warm 70-90 DEG C；
（4）Stand defoaming：70-90 DEG C of heat preservation stands 1-2 hours；
（5）It is filling：Material is squeezed into the bottle placer of heat preservation and carries out filling, cooling and shaping after being quantitatively circulated into mold；
（6）Demoulding：It is demoulded after 30-40 minutes filling, obtains amino acid camellia oil handmade soap.
In saponification process, triethanolamine ethanol solution and sodium hydrate aqueous solution is added, is avoided that in the process of feeding intake former
Expect agglomerating, reaction efficiency can be accelerated, while making to show that soap hardness is high, if only sodium hydrate aqueous solution saponification, pH value is added
For alkalinity, be easy stimulation skin, be not easy moisturizing, raw material be easy it is agglomerating, it is unstable.
The beneficial effects of the present invention are：
（1）This method processing step is simple, and process time is short, and yield is high, and high production efficiency, after demoulding, soap body hardness is good, appearance
More attractive, manner of packing is simpler.
（2）Gained amino acid camellia oil handmade soap is a kind of transparent soap, possesses a variety of natural plants antipathogenic compositions, can guarantee
Product stability and long-acting bacteriostatic can more protect our skin while mild clean skin.
Primary raw material used in the present invention is described as follows：
Camellia seed：It is the fruit of tea oil tree.Tea oil tree is the main woody oleiferous plants tree in China, is known as " east tree ", and camellia is belonged to
Section's Camellia evergreen dungarunga is the distinctive woody vegetable oil resource in China.Set 3-6 meters high, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe.Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be mature, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon.Fruit is capsule, mostly ellipse, have fine, soft fur.Seed
Mostly yellowish-brown, glossy, triangular shape.Tea oil tree is grown in remote mountains, to the greatest extent suction natural nutrient, and evergreen longevity, the age of tree was up to 200 years
More than.Camellia seed powder used in the present invention is powder made of camellia seed shell.
Lemon peel, is dry lemon pericarp, and the primary efficacy of lemon peel is diuresis, anti-inflammatory, antihistaminicum, promotes food
It is intended to, stimulation.Lemon peel bubble in water for bathing, water can not only be made to issue the fragrance of fragrance, but also oil contained by lemon peel
Rouge and nutrient can moisturize the skin.The coarse skin that hand, foot or other positions are such as wiped through common lemon peel, can be such that skin becomes gradually
Delicate, lubrication.
Flos caryophylli：Flos caryophylli is conventional Chinese medicine, is one of China's tradition import " southern medicine ", first recorded in《Haigoushen》.It is modern
Studies have shown that cloves contains volatile oil, mainly oleic acid containing cloves, acetyl cloves oleic acid and cloves alkene, Methylpentanone, methyl in oil
The ingredients such as positive heptanone, vanillin.Have antibacterial and anthelmintic action, be used as fragrance, antispastic carminative treats stomach trouble, and abdominal pain is vomitted
It spits, neuralgia, the diseases such as toothache.Cloves is not only the rare spice berry of Medicinal plants and the world.
Dandelion：Contain a variety of health such as taraxol, taraxacin, choline, organic acid, synanthrin in dandelion plant
Nutritional ingredient.Nature and flavor are sweet, slight bitter, tremble with fear.Return liver, stomach meridian.There are diuresis, laxative, removing jaundice subcutaneous ulcer, cholagogue and other effects.Control heat toxin, carbuncle swells,
Sore, internal carbuncle, red eye, swell pain, damp and hot, jaundice, the puckery pain of dribbling urination, furuncle swelling toxin, acute mastitis, scrofula, toothache, hot eyes, pharyngalgia,
Pulmonary abscess, acute appendicitis, jaundice with damp-heat pathogen, puckery pain of heat gonorrhea.Control acute mastitis, adenolymphitis, scrofula, boil poisonous soreness, acute conjunctivitis, sense
Emit fever, acute tonsillitis, acute bronchitis, gastritis, hepatitis, cholecystitis, urinary tract infections etc..
Glycerol：Water lock, moisturizing, moisturizing.
Propylene glycol：Water lock, moisturizing, moisturizing.
Sorbierite：Water lock, moisturizing, moisturizing.
Lauroyl glutamate：Amino acid starting material, as surfactant.
Cocounut oil acyl glutamic acid：Amino acid starting material, as surfactant.
Triethanolamine：Neutralizer is used for saponification.
Sodium hydroxide：Neutralizer is used for saponification.
Dehydrated alcohol：Diluent, placing response process raw material are agglomerating.
Water：Thickener adjusts soap lye consistency and soap body hardness in the reaction.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with example, but those skilled in the art will manage
Solution, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.
Embodiment 1
The amino acid camellia oil handmade soap of embodiment 1, is made of following processing step：
（One）Antibacterial plant extract liquid preparing process is：
（1）Selection：Select color, the normal camellia seed powder 200g of smell, lemon peel 260g, flos caryophylli 150g, dandelion 160g；
（2）It crushes：By step（1）Middle raw material is put in proportion into pulverizer, and is sieved（60 mesh）；
（3）It extracts：By step（2）Gained plant material powder is mixed with 7000g water, is heated to 80 DEG C, after persistently stirring 120min
Cold filtration obtains antibacterial plant extraction liquid.
（Two）Amino acid camellia oil handmade soap preparation process is：
（1）It is prewired：To weigh up antibacterial 2500 g of plant extraction liquid and lauroyl amino acid 2500g, cocoamido acid 2600g and
Moisturizer raw material 1600g（Every 1000g is matched：Glycerol 450g, propylene glycol 250g, sorbierite 300g）, put into slow in reaction kettle
Slow to dissolve by heating, temperature sets 80 DEG C, and mixing speed is 20 revs/min；
（2）Saponification：The 3200g triethanolamine ethanol solution that will be weighed up（Every 1000g is matched：It is triethanolamine 700g, anhydrous
Ethyl alcohol 300g）And 600g sodium hydrate aqueous solution（Every 1000g is matched：Sodium hydroxide 230g, water 770g）, it is slowly added into
In reaction kettle, speed of agitator is set as 30 revs/min, reacts 40 minutes；
（3）Compounding：The 400g camellia oil weighed up, 20g essence are added in reaction kettle, close stirring after continuing stirring 6 minutes, after
80 degrees Celsius of continuation of insurance temperature；
（4）Stand defoaming：80 degrees Celsius of heat preservation stands 1 hour；
（5）It is filling：Material is squeezed into the bottle placer of heat preservation and carries out filling, cooling and shaping after being quantitatively circulated into mold；
（6）Demoulding：It is demoulded after filling 30 minutes, obtains high rigidity easy mold release and moisten mild amino acid camellia oil craft
Soap.
Embodiment 2-7
The amino acid camellia oil handmade soap of embodiment 2-7, preparation process condition substantially with embodiment 1, only reaction raw materials and
The conditions such as proportion scale, temperature, time are slightly different, specifically as listed by table 1- table 5.
The antibacterial plant extraction liquid preparation process condition of 1 embodiment 1-7 of table, comparative example 1-2
。
The moisturizer mixed proportion of 2 embodiment 1-7 of table, comparative example 1-2
。
The triethanolamine ethanol solution mixed proportion of 3 embodiment 1-7 of table, comparative example 1-2
。
The sodium hydrate aqueous solution mixed proportion of 4 embodiment 1-7 of table, comparative example 1
。
The amino acid handmade soap preparing process of 5 embodiment 1-7 of table, comparative example 1-2
。
Comparative example 3
Lemon peel is free of in the antibacterial plant extraction liquid, the dosage of flos caryophylli is 410g, other same as Example 1.
Comparative example 4
Flos caryophylli is free of in the antibacterial plant extraction liquid, the dosage of lemon peel is 410 g, other same as Example 1.
Comparative example 5
The compounding camellia seed oil is changed to soybean oil, other same as Example 1.
Comparative example 6
The antibacterial plant extraction liquid dosage is 4100g, other same as Example 1.
The resulting amino acid camellia oil handmade soap of embodiment 1-7, comparative example 1-6 is tested into its pH value, cold-resistant Heat-resistant stable
Property, foam, rinsing type, moisturizing effect, hardness, fungistatic effect.
The functional attributes test result of amino acid camellia oil handmade soap obtained by 6 embodiment 1-7 of table, comparative example 1-6
。
The functional attributes and physical and chemical index of the resulting amino acid camellia oil handmade soap of embodiment 1-7, comparative example 1-6 are tested
Used test method has：
（1）PH value detection
According to pH value measuring method as defined in GB/T 13531.1.
（2）Cold-resistant heat-resistant stability
The resulting amino acid camellia oil handmade soap of embodiment 1-7, comparative example 1-6 is placed on the insulating box that set temperature is 42 DEG C
In, after placing 30 days, the stability as a result, under test handmade soap high temperature is observed after restoring to room temperature；By embodiment 1-7, comparison
The example resulting amino acid camellia oil handmade soap of 1-2 was placed in the refrigerator that set temperature is -15 DEG C after 30 days, was restored to room temperature
Observation as a result, test handmade soap stability at low temperature, (- indicate unstable ,+indicate that stability is preferable, +++ indicate to stablize
Property is very good).
（4）Foam, rinsability, moisturizing effect, fungistatic effect test method be facial skin test, specific method is such as
Under：
It is uniformly applied after the resulting amino acid camellia oil handmade soap of embodiment 1-7, comparative example 1-6 is got abundant foam with bubble net
It smears in the facial skin drenched, and repeated massage is washed by rubbing with the hands, when foam sufficiently enriches to be further added by, experiences foaming abundancy
Degree, and record（Indicate almost without ,+indicate it is a small amount of, ++ indicate it is more, +++ indicate very more）, then rinsed with clear water dry
Only, record was rinsed to the clean time, until not glutinous soapy feeling, with clean towel water purification beads, used moisture after 30 minutes
Tester tests face's moisture value, is sampled with the cotton swab to sterilize in the case where face smears 5 after 2 hours, does the inspection of face's total number of bacteria
Test is tested（Note：Facial sample is taken before washing one's face using handmade soap, carry out the detection of face's total number of bacteria）.
Statistical result such as table 3：
The resulting amino acid camellia oil handmade soap trial effect mean scores table of 7 embodiment 1-7 of table, comparative example 1-6
。
From table 6,7, amino acid camellia oil handmade soap Low-foam and easily cleaning of the present invention effectively can inhibit bacterium to increase, moisten
Property is good.From the point of view of comparative example 2, the foaming abundancy degree of the amino acid soap of sodium hydrate aqueous solution, stability, rinsing type are not added all
It is relatively poor, but the opposite meeting of pH value is weakly acidic；Amino acid soap is determined from the addition of 1,3,4,6 Traditional Chinese medicine bacteriostatic liquid of comparative example
Fungistatic effect, is not added or single component does not compound can all influence its fungistatic effect, and Use out of range can reduce antibacterial effect instead
Fruit；And comparative example 5 reflects the moisturizing effect that tea oil plays in formula and gets well than other plant oil.
Embodiment 1-7, the amino acid camellia oil handmade soap hardness measuring method of comparative example 1-6 are as follows：
The amino acid camellia oil handmade soap of embodiment 1-7, comparative example 1-6 are placed on certain altitude, record its height with ruler,
Hand unclamps, and soap body is made to do the movement of falling object, counts the indeformable height of highest, situation such as table 8.
The amino acid camellia oil handmade soap hardness test result statistical form of 8 embodiment 1-7 of table, comparative example 1-6
。
From table 6,8, amino acid camellia oil handmade soap hardness of the present invention is good, combines triethanolamine ethanol solution and hydroxide
Sodium water solution can greatly improve soap body hardness, be unlikely to deform soap body, more stable under high temperature.
Amino acid camellia oil handmade soap toxicology test of the present invention：Skin irritation test（Multiple skin irritation test）
Test objective：Observe rabbit intact skin long-time multiple-contact tested material（The facial cleanser of the embodiment of the present invention）Afterwards
Generated skin irritation reaction, provides safety foundation for the amino acid camellia oil handmade soap of the embodiment of the present invention.
Test basis：《Cosmetics safety technical specification》Version in 2015.
Test method：White New Zealand rabbits 8 are selected, is randomly divided into 2 groups, every group 4.A group:Experimental group, B group:Go from
Sub- water control group.Family's rabbit back backbone two sides coat is cut for 24 hours before test, skin surface, unhairing range are not damaged in cropping
For 3cm × 3cm, application area is 2.5cm × 2.5cm., amino acid camellia oil hand of the tested material group to various embodiments of the present invention
Work soap, takes tested material 0.5ml to be coated directly on the side of back backbone, and the other side applies 0.5ml control group deionized water, smears daily
1 time, continuously smear 14d.Since second day, cropping when smearing every time removed residual tested material with deionized water.One hour
Afterwards observation as a result, according to《Cosmetics safety technical specification》（Version in 2015）Skin irritation test table scoring, check plot and
Trial zone is equally handled.
Evaluation of result：Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observes other toxic effects in addition to irritation.
。
Test result：Tested material is carrying out giving various embodiments of the present invention in the multiple skin irritation test observation period
Amino acid camellia oil handmade soap after, rabbit has no erythema, oedema.Have no systemic toxicity profiles performance and death condition, the weight of animals
Increase, on breathing, circulation, central nervous system, four limbs activity etc. without influence.
Conclusion (of pressure testing)：The amino acid camellia oil handmade soap of various embodiments of the present invention to white New Zealand rabbits intact skin without
Irritation.
Claims (7)
1. a kind of amino acid camellia handmade soap is prepared from the following raw materials according to mass fraction meter：Lauroyl glutamate 20-30
Part, 20-30 parts of cocounut oil acyl glutamic acid, 10-18 parts of moisturizer, 28-35 parts of triethanolamine ethanol solution, sodium hydrate aqueous solution 5-
10 parts, plant extraction liquid 20-30 parts antibacterial, 3-8 parts of camellia oil, 0.1-0.3 parts of essence.
2. amino acid camellia handmade soap according to claim 1, it is characterised in that：The antibacterial plant extraction liquid includes
The following raw material：20-30 parts of camellia seed powder, 20-30 parts of lemon peel, 10-20 parts of flos caryophylli, 10-20 parts of dandelion.
3. amino acid camellia handmade soap according to claim 1, it is characterised in that：The moisturizer is by following raw material
It mixes：40-50 parts of glycerol, 20-30 parts of sorbierite, 20-30 parts of propylene glycol.
4. amino acid camellia handmade soap according to claim 1, it is characterised in that：The triethanolamine ethanol solution by
Following raw material mixes：60-80 parts of triethanolamine, 20-40 parts of dehydrated alcohol.
5. amino acid camellia handmade soap according to claim 1, it is characterised in that：The sodium hydrate aqueous solution be by
Following raw material mixes：20-25 parts of sodium hydroxide, 75-80 parts of deionized water.
6. amino acid camellia handmade soap according to claim 1 or 2, it is characterised in that：The antibacterial plant extraction liquid
Preparation process is：
（1）Selection：Select camellia seed shell, lemon peel, flos caryophylli, dandelion；
（2）It crushes：By step（1）Middle raw material is put in proportion into pulverizer, and is sieved, and obtains plant material powder；
（3）It extracts：By step（2）Gained plant material powder is according to 1:The ratio of 5-10 is mixed with water, is heated to 70-90 DEG C, is held
Cold filtration after continuous stirring 1-3 hours, obtains antibacterial plant extraction liquid.
7. the preparation method of amino acid camellia handmade soap according to claim 1, it is characterised in that in turn include the following steps：
（1）It is prewired：Antibacterial plant extraction liquid and lauroyl amino acid, cocoamido acid and moisturizer raw material are put into reaction kettle
Middle heating for dissolving, temperature set 70-90 DEG C, and mixing speed is 10-30 revs/min；
（2）Saponification：The triethanolamine ethanol solution, the sodium hydrate aqueous solution that weigh up are slowly added into reaction kettle, stirring turns
Speed is set as 25-35 revs/min, reacts 30-50 minutes；
（3）Compounding：The camellia oil weighed up, essence are added in reaction kettle, stirring is closed after continuing stirring 5-10 minutes, after continuation of insurance
Warm 70-90 DEG C；
（4）Stand defoaming：70-90 DEG C of heat preservation stands 1-2 hours, obtains Material；
（5）It is filling：Material is squeezed into the bottle placer of heat preservation and carries out filling, cooling and shaping after being quantitatively circulated into mold；
（6）Demoulding：It is demoulded after 30-40 minutes filling, obtains amino acid camellia oil handmade soap.
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|---|---|---|---|
| CN201810984848.0A CN108823013A (en) | 2018-08-28 | 2018-08-28 | amino acid camellia handmade soap and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810984848.0A CN108823013A (en) | 2018-08-28 | 2018-08-28 | amino acid camellia handmade soap and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100792040B1 (en) * | 2006-11-01 | 2008-01-04 | 하인숙 | Cleansing soap |
| CN105907501A (en) * | 2016-04-29 | 2016-08-31 | 佛山市芊茹化妆品有限公司 | Transparent amino acid compound soap and preparation method thereof |
| CN107746761A (en) * | 2017-11-27 | 2018-03-02 | 上海清轩生物科技有限公司 | A kind of amino acid composite transparent soap containing camellia seed oil and preparation method thereof |
-
2018
- 2018-08-28 CN CN201810984848.0A patent/CN108823013A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100792040B1 (en) * | 2006-11-01 | 2008-01-04 | 하인숙 | Cleansing soap |
| CN105907501A (en) * | 2016-04-29 | 2016-08-31 | 佛山市芊茹化妆品有限公司 | Transparent amino acid compound soap and preparation method thereof |
| CN107746761A (en) * | 2017-11-27 | 2018-03-02 | 上海清轩生物科技有限公司 | A kind of amino acid composite transparent soap containing camellia seed oil and preparation method thereof |
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Application publication date: 20181116 |