CN102178617B - Protein skin care products having function of skin repair and care - Google Patents
Protein skin care products having function of skin repair and care Download PDFInfo
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- CN102178617B CN102178617B CN201110118721A CN201110118721A CN102178617B CN 102178617 B CN102178617 B CN 102178617B CN 201110118721 A CN201110118721 A CN 201110118721A CN 201110118721 A CN201110118721 A CN 201110118721A CN 102178617 B CN102178617 B CN 102178617B
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Abstract
The invention discloses a protein skin care product having the function of skin repair and care, which contains a protein composition with 0.3% to 5% of mass fraction, wherein the protein composition is composed of keratin and collagen with the mass ratio of the keratin to the collagen being 1: 0.2 to 2. The protein skin care product of the invention having the function of skin repair and care includes mask liquid, cream and cleansing emulsion.
Description
Technical field
The invention belongs to skin care field, particularly have the skin care item of skin repair and care action.
Background technology
Skin is the maximum organ of human body, 5%～15% of gross weight percentage of liveweight, and the gross area is 1.5～2 square metres.Skin has the barrier action of two aspects: prevent on the one hand moisture in the body, the losing of electrolyte and other materials; Stop the intrusion of extraneous harmful substance on the other hand, keep the stable of human internal environment, on physiology, play important defencive function.With advancing age, skin receives the effect of ultraviolet and airborne pollutant, lacks nutrition easily, and then makes the skin dehydration, destroys the keratin of skin, causes pachylosis, follows the string.For skin nutrition, prevent pachylosis, people explore the skin care item prescription, have worked out multiple skin care item to skin moisture-keeping and nutrition; For example: application number is that the one Chinese patent application of 02148919.X discloses a kind of polynary compound paste skin care item of preserving moisture, and its prescription is: wild mountain ginseng 10-20 gram, Flos Hibisci Mutabilis 2-3 gram, Poria 2-3 gram; Radix Angelicae Dahuricae (Radix Heraclei Scabridi) 10-20 gram, Herba Leonuri 2-3 gram, Rhizoma Chuanxiong 10-20 gram, Radix Angelicae Sinensis 2-3 gram; Radix Scutellariae 1-2 gram, paraffin 50-100 gram, glycerol 50-100 gram.The patent No. is that the Chinese patent of ZL200310111505.7 discloses a kind of skin care item, and its prescription is: Dead Sea salt 15-40, Dead Sea mud 35-55, Radix Ginseng 5-10; Hydrolytic collagen 3-5 adds following several kinds or a kind of raw material, propolis 3, bamboo charcoal 7 in above-mentioned prescription; Sea snake bile 3, soybean isoflavone 5, the Rhizoma Atractylodis Macrocephalae 10, Pseudobulbus Bletillae (Rhizoma Bletillae) 10; Poria 10, papain 5, Margarita powder 10.Application number is that 200710020371.6 one Chinese patent application discloses a kind of protective skin cream with skin nutrition, and its prescription is: vitamin e1-10, stearic acid 40-100, white vaseline 10-60; Liquid paraffin 20-70, octadecanol 20-70, methyl-silicone oil 80-150; Glycerol 150-200, alkylaryl gather ethanol ether 8-20, fatty alcohol-polyoxyethylene ether 8-20; Tween 80 5-15, ethyl hydroxybenzoate 0.5-1.5, all the other are distilled water.But the prescription of various skin care item is different, and effect is difference to some extent also, develops the skin care item of more different formulations, remains people's expectation.
Summary of the invention
The object of the present invention is to provide a kind of protein skin care item with skin repair and care action, this kind skin care item can effectively promote the cell protein metabolism, promote skin-nourishing, keep skin moisture, repair skin, recover the natural elasticity of skin.
Technical scheme of the present invention: in the prescription of skin care item, add the protein compositions of mass fraction 0.3%～5%, said protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2～2.Test shows that the keratin preferred molecular weight is 20000～80000 daltonian keratin.Said keratin and collagen protein both can be bought through market, also can prepare voluntarily.
Protein skin care item with skin repair and care action according to the invention comprise facial mask liquid, cream frost and cleanser liquid, and the mass fraction of their component and each component is distinguished as follows:
One, the mass fraction of the component of facial mask liquid and each component
Said nourishing additive agent is at least a in vitamin e acetate, D-panthenol, the allantoin; Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000～80000 daltonian keratin.
Above-mentioned facial mask liquid also can contain essence and antiseptic, and the mass fraction of essence is 0.05%～0.6%, and the mass fraction of antiseptic is 0.01%～0.3%.
In the above-mentioned facial mask liquid, said oils and fats is at least a in cetearyl alcohol, different n-nonanoic acid cetyl, cetin, polyglycereol-4 laurate, the citric acid bilaurate; Wetting agent is at least a in glycerol, propylene glycol, hyaluronic acid and salt thereof, the ceramide; Emulsifying agent is at least a in spermaceti alcohol ether-20, spermaceti alcohol ether-12, glyceryl stearate, polyglycereol-4 laurate, the citric acid bilaurate; Thickening agent is at least a in HANSHENGJIAO, guar gum and derivant thereof, alginic acid ester, hydroxyethyl-cellulose, hydroxypropyl emthylcellulose, cationic hydroxyethyl cellulose, carbomer, the acrylic ester/C10-30 alkyl acrylate cross-linked polymer.
In the above-mentioned facial mask liquid, antiseptic is at least a in methyl hydroxybenzoate, ethyl hydroxybenzoate, propylparaben, the butoben.
Two, the component of cream frost and the mass fraction of each component
Said nourishing additive agent is vitamin e acetate, D-panthenol, plant at least a in sterol, the allantoin; Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000～80000 daltonian keratin.
Above-mentioned cream frost also can contain essence and antiseptic, and the mass percent of essence is 0.05%～0.7%, and the mass percent of antiseptic is 0.01%～0.3%.
In the above-mentioned cream frost, oils and fats is at least a in cetearyl alcohol, dicaprylyl carbonate, polydimethylsiloxane, annular dimethyl polysiloxane, C13-15 alkane, shea butter, American Avocado Tree oil, the olive oil; Wetting agent is at least a in glycerol, propylene glycol, aminoacid, hyaluronic acid and salt thereof, the ceramide; Emulsifying agent is glyceryl stearate, Glucate SS, at least a in the PEG-20 Glucate SS; Thickening agent is at least a in HANSHENGJIAO, guar gum and derivant thereof, carbomer, acrylic ester/C10-30 alkyl acrylate cross-linked polymer, the different alkane footpath/polyacrylamide of laureth-7/C13-C14.
In the above-mentioned cream frost, antiseptic is at least a in methyl hydroxybenzoate, ethyl hydroxybenzoate, propylparaben, the butoben.
Three, the mass fraction of the component of cleanser liquid and each component
Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000～80000 daltonian keratin.
Above-mentioned cleanser liquid also can contain essence and antiseptic, and the mass percent of essence is 0.05%～0.6%, and the mass percent of antiseptic is 0.01%～0.3%.
In the above-mentioned cleanser liquid, oils and fats is at least a in cetearyl alcohol, No. 26 white oils, cetin, carbonic acid ethylhexyl, isopropyl myristate, annular dimethyl polysiloxane, C13-15 alkane, shea butter, the American Avocado Tree oil; Surfactant is at least a in alkyl-glutamic acid salt, N-acyl glutamic acid, N-acyl sarcosine, Tryfac 5573 potassium, the C9-C15-monoalkyl phosphoric acid esters potassium; Wetting agent is at least a in glycerol, aminoacid, hyaluronic acid and the salt thereof; Emulsifying agent is at least a in spermaceti alcohol ether-20, glyceryl stearate, the hard ester acid alcohol of spermaceti ether-25, the citric acid bilaurate; Thickening agent is at least a in HANSHENGJIAO, guar gum and derivant thereof, the carbomer.
In the above-mentioned cleanser liquid, antiseptic is at least a in methyl hydroxybenzoate, ethyl hydroxybenzoate, propylparaben, the butoben.
The method for preparing of facial mask liquid according to the invention, protective skin cream, cleanser liquid: raw materials such as oils and fats are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; In the water pot, add emulsifying agent, wetting agent, nourishing additive agent, surfactant, turn on agitator is stirred to dissolving and mix homogeneously fully, is warming up to 85 ℃ then, and keeps this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions or protein compositions, essence and antiseptic, after the material that is added and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
The present invention has following beneficial effect:
1, owing to contain protein compositions in the skin care item according to the invention, experiment shows to have the physiologically active of obvious promotion keratinocyte growth and breeding, can repair skin, strengthens the compactibility and the elasticity of skin, anti aging effect.
2, because protein compositions contains a large amount of polar groups, be NMF, thereby have the tyrosine that stops in the skin and be converted into melanic effect, make skin moisture-keeping, whiten.
3, through check, skin care item according to the invention meet sanitary index, and concrete data see the following form:
Sanitary index
The specific embodiment
Through embodiment the protein skin care item with skin repair and care action according to the invention are described further below.
Embodiment 1: the preparation keratin
Pilus Caprae seu Ovis is cleaned up, pulverizes, use that pH value is 11, the TGA sodium solution (sodium hydroxide is regulated pH) of concentration 0.5mol/L normal pressure, room temperature (20 ℃～30 ℃) pretreatment 3 hours, adds carbamide then in solution; The addition of carbamide reaches 7mol/L for concentration in solution, continue after normal pressure, room temperature (20 ℃～30 ℃) reduction reaction 25 hours, after the response time expires; Splash into pH value to 6～8 of acetic acid conditioned reaction liquid, then aerating oxygen in solution reacted 0.5 hour in room temperature (20 ℃～30 ℃); After response time expires; Normal pressure filters, and filtrating is carried out dialysis with the dialysis bag of holding back relative molecular weight 20～80kD, and it is 20000～80000 daltonian keratin solution first products that centrifugalize obtains molecular weight; The keratin solution first product saltoutd obtain the keratin solid; Through the vacuum drying at room temperature, promptly obtain the natural wool keratin, yield 42%.
Embodiment 2: the preparation collagen protein
With depilation chopping behind the clean removal of fresh porcine skin (or the fresh Corii Bovis seu Bubali) subcutaneous fat; With the NaCl solution soaking 12h of mass concentration 10%, removing the solubility impurity that desalts, soak time at the expiration after; With deionized water wash 2～3 times, add deionized water making beating mixing then and obtain slip.In above-mentioned slip, add HAc and the pepsin of concentration 0.5mol/L, the addition of HAc is 5% of a slip volume, and pepsic addition is 5% of a slip weight, and the pH value of control slip is handled 72h at normal pressure, room temperature enzyme then 2～3.Enzyme processing time at the expiration after, the supernatant is got in centrifugalize (3000r/min), in the supernatant, adds NaCl and carries out collagen protein and saltout, NaCl concentration is 2mol/L, centrifugalize (8000r/min), deposition is collagen protein.Continue after collagen protein is dissolved among the Hac of concentration 0.5mol/L again, repeat to saltout twice with NaCl, again collagen protein is dissolved among the HAc of 0.5mol/L, with the Na of concentration 0.02mol/L
2HPO
4(pH8.8) dialysis 2d～3d, every 8h changes dialysis solution one time, and after dialysis time expired, centrifugalize (8000r/min) promptly obtained required collagen protein with the collagen deposition lyophilization that obtains.
Keratin that uses among the following embodiment and collagen protein are the keratin and the natural wool keratin of embodiment 1, embodiment 2 said method preparations
Embodiment 3: the preparation of facial mask liquid
In the present embodiment, component of facial mask liquid (raw material) and mass fraction thereof are following:
Protein compositions 0.5%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2;
Oils and fats 3%: polyglycereol-4 laurate 1%, citric acid bilaurate 2%;
Emulsifying agent 1%: glyceryl stearate;
Wetting agent 4%: glycerol 3%, propylene glycol 1%;
Thickening agent 0.12%: acrylic ester/C10-30 alkyl acrylate cross-linked polymer;
Nourishing additive agent 0.5%: vitamin e acetate 0.4%, allantoin 0.1%;
Deionized water 90.88%.
The method for preparing of facial mask liquid is following:
Raw material polyglycereol-4 laurate, citric acid bilaurate, acrylic ester/C10-30 alkyl acrylate cross-linked polymer, vitamin e acetate, allantoin are dropped into the oil phase pot; Under agitation be heated to 60 ℃ in normal pressure; After said raw material dissolves fully; Be warming up to 85 ℃, and keep this temperature; Raw material glyceryl stearate, glycerol, propylene glycol are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, after protein compositions and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 4: the preparation of facial mask liquid
In the present embodiment, component of facial mask liquid (raw material) and mass fraction thereof are following:
Protein compositions 2%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.5;
Oils and fats 10%: cetearyl alcohol 6%, different n-nonanoic acid cetyl 4%;
Emulsifying agent 3%: spermaceti alcohol ether-20 1.5%, spermaceti alcohol ether-12 1.5%;
Wetting agent 0.5%: hyaluronic acid;
Thickening agent 1%: hydroxyethyl-cellulose 0.5%, hydroxypropyl emthylcellulose 0.5%;
Nourishing additive agent 4%:D-pantothenylol;
Antiseptic 0.1%: ethyl hydroxybenzoate;
Essence 0.05%;
Distilled water 79.35%.
The method for preparing of facial mask liquid is following:
Raw material cetearyl alcohol, different n-nonanoic acid cetyl, hyaluronic acid, D-panthenol are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material spermaceti alcohol ether-20, spermaceti alcohol ether-12, hydroxyethyl-cellulose, hydroxypropyl emthylcellulose are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, antiseptic and essence, after protein compositions, antiseptic and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 5: the preparation of facial mask liquid
In the present embodiment, component of facial mask liquid (raw material) and mass fraction thereof are following:
Protein compositions 5%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 2;
Oils and fats 1%: polyglycereol-4 laurate;
Emulsifying agent 2%: spermaceti alcohol ether-20 1%, glyceryl stearate 1%;
Wetting agent 0.1%: glycerol;
Thickening agent 0.8%: alginic acid ester 0.4%, cationic hydroxyethyl cellulose 0.4%;
Nourishing additive agent 5%: vitamin e acetate 2%, allantoin 3%;
Antiseptic 0.3%: methyl hydroxybenzoate;
Essence 0.6%;
Distilled water 85.2%.
The method for preparing of facial mask liquid is following:
Raw material polyglycereol-4 laurate, alginic acid ester, cationic hydroxyethyl cellulose, vitamin e acetate, allantoin are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material spermaceti alcohol ether-20, glyceryl stearate, glycerol are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, and opened and stir, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, antiseptic and essence, after protein compositions, antiseptic and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 6: the preparation of facial mask liquid
In the present embodiment, component of facial mask liquid (raw material) and mass fraction thereof are following:
Protein compositions 1.5%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 1;
Oils and fats 6%: polyglycereol-4 laurate 4%, cetin 2%;
Emulsifying agent 5%: spermaceti alcohol ether-124%, glyceryl stearate 1%;
Wetting agent 10%: glycerol 6%, ceramide 4%;
Thickening agent 2%: HANSHENGJIAO 1.4%, guar gum 0.6%;
Nourishing additive agent 1%: vitamin e acetate;
Antiseptic 0.02%: propylparaben;
Essence 0.1%;
Deionized water 74.38%.
The method for preparing of facial mask liquid is following:
Raw material polyglycereol-4 laurate, cetin, HANSHENGJIAO, guar gum, vitamin e acetate are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material spermaceti alcohol ether-12, glyceryl stearate, glycerol are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, ceramide, antiseptic and essence; When protein compositions, ceramide, antiseptic and essence and other mixing of materials evenly after, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 7: the preparation of cream
In the present embodiment, component of cream (raw material) and mass fraction thereof are following:
Protein compositions 1%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2;
Oils and fats 30%: cetearyl alcohol 10%, C13-15 alkane 5%, dicaprylyl carbonate 3%, shea butter 6%, polydimethylsiloxane 6%;
Emulsifying agent 2.5%: glyceryl stearate 0.5%, Glucate SS 0.8%, PEG-20 Glucate SS glyceryl stearate 1.2%;
Wetting agent 3%: propylene glycol;
The different alkane footpath/polyacrylamide of thickening agent 1%: laureth-7/C13-C14;
Nourishing additive agent 0.5%: vitamin e acetate 0.2%, allantoin 0.3%
Deionized water 62%.
The method for preparing of cream is following:
Raw material cetearyl alcohol, C13-15 alkane, dicaprylyl carbonate, shea butter, polydimethylsiloxane, the different alkane footpath/polyacrylamide of laureth-7/C13-C14, vitamin e acetate, allantoin are dropped into the oil phase pot; Under agitation be heated to 60 ℃ in normal pressure; After said raw material dissolves fully; Be warming up to 85 ℃, and keep this temperature; Raw material glyceryl stearate, Glucate SS, PEG-20 Glucate SS glyceryl stearate, propylene glycol are added in the water pot; Turn on agitator; Under normal pressure, be stirred to dissolving (about 20 minutes) and mix homogeneously fully; Be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, after protein compositions and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 8: the preparation of cream
In the present embodiment, component of cream (raw material) and mass fraction thereof are following:
Protein compositions 2.5%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 1.5;
Oils and fats 10%: annular dimethyl polysiloxane 6%, American Avocado Tree oil 1%, olive oil 3%;
Emulsifying agent 1%: glyceryl stearate 0.5%, Glucate SS 0.5%;
Wetting agent 5%: glycerol 3%, aminoacid 2%;
Thickening agent 0.3%: carbomer 0.2%, HANSHENGJIAO 0.1%;
Nourishing additive agent 2%:D-pantothenylol 1%, plant sterol 1%;
Antiseptic 0.01%: butoben;
Essence 0.1%;
Distilled water 79.09%.
The method for preparing of cream is following:
With raw material annular dimethyl polysiloxane, American Avocado Tree oil, olive oil, carbomer, HANSHENGJIAO, D-panthenol, plant sterol and drop into the oil phase pot, under agitation be heated to 60 ℃ in normal pressure, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature; Raw material glyceryl stearate, Glucate SS, glycerol are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, aminoacid, antiseptic and essence, after protein compositions, aminoacid, antiseptic and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 9: the preparation of cream
In the present embodiment, component of cream (raw material) and mass fraction thereof are following:
Protein compositions 0.5%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 1;
Oils and fats 5%: dicaprylyl carbonate 2%, polydimethylsiloxane 3%; ,
Emulsifying agent 5%: Glucate SS;
Wetting agent 10%: hyaluronic acid 3%, ceramide 7%;
Thickening agent 2%: acrylic ester/C10-30 alkyl acrylate cross-linked polymer;
Nourishing additive agent 3%:D-pantothenylol 1%, vitamin e acetate 2%;
Antiseptic 0.1%: methyl hydroxybenzoate;
Essence 0.05%;
Deionized water 74.35%.
The method for preparing of cream is following:
Material carbon dioctyl phthalate, polydimethylsiloxane, hyaluronic acid, acrylic ester/C10-30 alkyl acrylate cross-linked polymer, D-panthenol, vitamin e acetate are dropped into the oil phase pot; Under agitation be heated to 60 ℃ in normal pressure; After said raw material dissolves fully; Be warming up to 85 ℃, and keep this temperature; The raw material Glucate SS is added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, antiseptic and essence, after protein compositions, antiseptic, ceramide and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 10: the preparation of cream
In the present embodiment, component of cream (raw material) and mass fraction thereof are following:
Protein compositions 5%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 2;
Oils and fats 14%: annular dimethyl polysiloxane 6%, C13-15 alkane 5%, olive oil 3%;
Emulsifying agent 3%: Glucate SS;
Wetting agent 0.1%: propylene glycol;
Thickening agent 0.1%: HANSHENGJIAO;
Nourishing additive agent 5%:D-pantothenylol 2%, allantoin 3%;
Antiseptic 0.3%: ethyl hydroxybenzoate;
Essence 0.7%;
Distilled water 71.8%.
The method for preparing of cream is following:
Raw material annular dimethyl polysiloxane, C13-15 alkane, olive oil, HANSHENGJIAO, D-panthenol, allantoin are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material Glucate SS, propylene glycol are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, antiseptic and essence, after protein compositions, antiseptic and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 11: the preparation of cleanser liquid
In the present embodiment, component of cleanser liquid (raw material) and mass fraction thereof are following:
Protein compositions 0.3%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.6;
Oils and fats 11.5%:26 white oil 6%, cetearyl alcohol 3%, isopropyl myristate 2.5%;
Surfactant 10%: Tryfac 5573 potassium 5%, C9-C15-monoalkyl phosphoric acid esters potassium 5%;
Emulsifying agent 2.5%: the hard ester acid alcohol of spermaceti ether-251%, glyceryl stearate 1.5%;
Wetting agent 2%: glycerol 1%, amino acid/11 %;
Thickening agent 0.3%: carbomer;
Deionized water 73.4%.
The method for preparing of cleanser liquid is following:
No. 26 white oils of raw material, cetearyl alcohol, isopropyl myristate, carbomer are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material Tryfac 5573 potassium, C9-C15-monoalkyl phosphoric acid esters potassium, glycerol, the hard ester acid alcohol of spermaceti ether-25, glyceryl stearate are added in the water pot; Turn on agitator; Under normal pressure, be stirred to dissolving (about 20 minutes) and mix homogeneously fully, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions and aminoacid, after protein compositions, aminoacid and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 12: the preparation of cleanser liquid
In the present embodiment, component of cleanser liquid (raw material) and mass fraction thereof are following:
Protein compositions 0.6%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 1.2;
Oils and fats 15%: shea butter 5%, American Avocado Tree oil 6%, cetin 4%;
Surfactant 3%: alkyl-glutamic acid salt 2%, N-acyl glutamic acid 1%; ,,
Emulsifying agent 1%: citric acid bilaurate; ,
Wetting agent 6%: hyaluronic acid 4%, aminoacid 2%;
Thickening agent 0.8%: guar gum;
Antiseptic 0.1%: methyl hydroxybenzoate;
Essence 0.05%;
Deionized water 73.45%.
The method for preparing of cleanser liquid is following:
Raw material shea butter, American Avocado Tree oil, cetin, hyaluronic acid, guar gum are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material alkyl-glutamic acid salt, N-acyl glutamic acid, citric acid bilaurate are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, antiseptic, aminoacid and essence, after protein compositions, antiseptic, aminoacid and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 13: the preparation of cleanser liquid
In the present embodiment, component of cleanser liquid (raw material) and mass fraction thereof are following:
Protein compositions 5%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2;
Oils and fats 5%: carbonic acid ethylhexyl 3%, C13-15 alkane 2%;
Surfactant 6%:N-acyl sarcosine 3%, Tryfac 5573 potassium 3%; ,
Emulsifying agent 5%: spermaceti alcohol ether-20 3%, citric acid bilaurate 2%;
Wetting agent 0.1%: glycerol;
Thickening agent 1.2%: carbomer 0.5%, HANSHENGJIAO 0.7%;
Antiseptic 0.01%: propylparaben;
Essence 0.6%;
Distilled water 77.09%.
The method for preparing of cleanser liquid is following:
Raw material carbonic acid ethylhexyl, C13-15 alkane, carbomer, HANSHENGJIAO are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material N-acyl sarcosine, Tryfac 5573 potassium, spermaceti alcohol ether-20, citric acid bilaurate, glycerol are added in the water pot; Turn on agitator; Under normal pressure, be stirred to dissolving (about 20 minutes) and mix homogeneously fully, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, antiseptic and essence, after protein compositions, antiseptic and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 14: the preparation of cleanser liquid
In the present embodiment, component of cleanser liquid (raw material) and mass fraction thereof are following:
Protein compositions 3%: protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 2;
Oils and fats 7%: annular dimethyl polysiloxane 6%, cetearyl alcohol 1%;
Surfactant 4%: alkyl-glutamic acid salt 2%, N-acyl glutamic acid 2%;
Emulsifying agent 3%: glyceryl stearate;
Wetting agent 10%: glycerol 2%, aminoacid 2%, hyaluronic acid 6%;
Thickening agent 2%: carbomer 1%, guar gum 1%;
Antiseptic 0.3%: propylparaben;
Essence 0.2%;
Deionized water 70.5%.
The method for preparing of cleanser liquid is following:
Raw material annular dimethyl polysiloxane, cetearyl alcohol, hyaluronic acid, carbomer, guar gum are dropped into the oil phase pot, under agitation be heated to 60 ℃, after said raw material dissolves fully, be warming up to 85 ℃, and keep this temperature in normal pressure; Raw material alkyl-glutamic acid salt, N-acyl glutamic acid, glyceryl stearate, glycerol are added in the water pot, and turn on agitator is stirred to dissolving (about 20 minutes) and mix homogeneously fully under normal pressure, be warming up to 85 ℃ then, and keep this temperature.The emulsifying pot is evacuated to the 100mmHg post; Then successively with the input of 3/4 water material in water pot emulsifying pot, with the whole oil phase material input emulsifying pots in the oil phase pot, with 1/4 water material input emulsifying pot remaining in the water pot; Open and stir homogenizer; Beat homogenizing 15 minutes, turn on agitator, deaeration.Continue after the mixed material in the emulsifying pot be cooled to 50 ℃ add protein compositions, antiseptic, aminoacid and essence, after protein compositions, antiseptic, aminoacid and essence and other mixing of materials are even, be cooled to 40 ℃ of dischargings to clean container.
Embodiment 15: the test skin care item
1, test sample
(1) the foregoing description 6 prepared facial mask liquid
(2) the foregoing description 9 prepared cream
(3) the foregoing description 12 prepared cleanser liquids
(4) with reference to sample, said is to press the facial mask liquid that the foregoing description 6 is removed protein compositions with reference to sample, and the mass percent of its component and each component is following:
Oils and fats 6%: polyglycereol-4 laurate 4%, cetin 2%;
Emulsifying agent 5%: spermaceti alcohol ether-12 4%, glyceryl stearate 1%;
Wetting agent 10%: glycerol 6%, ceramide 4%;
Thickening agent 2%: HANSHENGJIAO 1.4%, guar gum 0.6%;
Nourishing additive agent 1%: vitamin e acetate;
Antiseptic 0.02%: propylparaben;
Essence 0.1%;
Deionized water 75.88%.
2, tested object
40 healthy no dermopathic women between 30 years old～50 years old are divided into four groups at random with 40 tested objects, called after A group respectively, and the B group, C group and D organize every group 10 people.
3, method of testing
(1) before four groups of tested objects left and right, confirm test zone on the arm, the area of test zone is 5cm * 5cm;
(2) with SKICON 200 type keratodermatitis water content measuring instruments the skin hydration effect of four groups of tested object test zones is tested; Survey the inspection appearance with SEM575 type skin elasticity the skin elasticity of four groups of tested object test zones is tested, this test result is called as initial value.
(3) A group tested object uses the prepared facial mask liquid of the foregoing description 6; B group tested object uses the prepared cream of the foregoing description 9; C group tested object uses the prepared cleanser liquid of the foregoing description 12, and D group tested object uses said with reference to sample, uses continuously seven days; Every day, each used once sooner or later, and each consumption is 0.5 gram.
(4) A; B; C, the continuous use test sample of D group tested object tested the skin hydration effect of each group tested object test zone with SKICON 200 type keratodermatitis water content measuring instruments after seven days; Survey the inspection appearance with SEM575 type skin elasticity the skin elasticity of each group tested object test zone is tested, this test result is called as test value.
4, result of the test
(1) result of the test of A group
Test value is compared with initial value, and experimenter's skin average capacitance increases by 36%, and experimenter's skin average elasticity increases by 16.6%, and the average compactibility of experimenter's skin increases by 11.8%.
(1) result of the test of B group
Test value is compared with initial value, and experimenter's skin average capacitance increases by 39.2%, and experimenter's skin average elasticity increases by 19.6%, and the average compactibility of experimenter's skin increases by 15.4%.
(1) result of the test of C group
Test value is compared with initial value, and experimenter's skin average capacitance increases by 26.3%, and experimenter's skin average elasticity increases by 13.7%, and the average compactibility of experimenter's skin increases by 9.4%.
(2) result of the test of D group
Test value is compared with initial value, and experimenter's skin average capacitance increases by 1.9%, and experimenter's skin average elasticity increases by 1.1%, and the average compactibility of experimenter's skin increases by 2.8%.
Claims (8)
1. protein skin care item with skin repair and care action is characterized in that said skin care item are facial mask liquid, are made up of the component of following mass fraction:
Said protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2 ~ 2; Said nourishing additive agent is at least a in vitamin e acetate, D-panthenol, the allantoin; Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000 ~ 80000 daltonian keratin.
2. the protein skin care item with skin repair and care action according to claim 1 is characterized in that said oils and fats is at least a in cetearyl alcohol, different n-nonanoic acid cetyl, cetin, polyglycereol-4 laurate, the citric acid bilaurate; Wetting agent is at least a in glycerol, propylene glycol, hyaluronic acid and salt thereof, the ceramide; Emulsifying agent is at least a in spermaceti alcohol ether-20, spermaceti alcohol ether-12, the glyceryl stearate; Thickening agent is at least a in HANSHENGJIAO, guar gum and derivant thereof, alginic acid ester, hydroxyethyl-cellulose, hydroxypropyl emthylcellulose, cationic hydroxyethyl cellulose, carbomer, the acrylic ester/C10-30 alkyl acrylate cross-linked polymer.
3. protein skin care item with skin repair and care action is characterized in that said skin care item are the cream frost, are made up of the component of following mass fraction:
Said protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2 ~ 2; Said nourishing additive agent is vitamin e acetate, D-panthenol, plant at least a in sterol, the allantoin; Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000 ~ 80000 daltonian keratin.
4. protein skin care item with skin repair and care action is characterized in that said skin care item are the cream frost, are made up of the component of following mass fraction:
Said protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2 ~ 2; Said nourishing additive agent is vitamin e acetate, D-panthenol, plant at least a in sterol, the allantoin; Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000 ~ 80000 daltonian keratin.
5. according to claim 3 or 4 described protein skin care item, it is characterized in that oils and fats is at least a in cetearyl alcohol, dicaprylyl carbonate, polydimethylsiloxane, C13-15 alkane, shea butter, American Avocado Tree oil, the olive oil with skin repair and care action; Wetting agent is at least a in glycerol, propylene glycol, aminoacid, hyaluronic acid and salt thereof, the ceramide; Emulsifying agent is glyceryl stearate, Glucate SS, at least a in the PEG-20 Glucate SS; Thickening agent is at least a in HANSHENGJIAO, guar gum and derivant thereof, carbomer, acrylic ester/C10-30 alkyl acrylate cross-linked polymer, the different alkane footpath/polyacrylamide of laureth-7/C13-C14.
6. protein skin care item with skin repair and care action is characterized in that said skin care item are cleanser liquid, are made up of the component of following mass fraction:
Said protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2 ~ 2; Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000 ~ 80000 daltonian keratin.
7. protein skin care item with skin repair and care action is characterized in that said skin care item are cleanser liquid, are made up of the component of following mass fraction:
Said protein compositions is made up of keratin and collagen protein, and the mass ratio of keratin and collagen protein is 1: 0.2 ~ 2; Said pure water is deionized water or distilled water; Said keratin is molecular weight 20000 ~ 80000 daltonian keratin.
8. according to claim 6 or 7 described protein skin care item, it is characterized in that oils and fats is at least a in cetearyl alcohol, No. 26 white oils, cetin, carbonic acid ethylhexyl, isopropyl myristate, annular dimethyl polysiloxane, C13-15 alkane, shea butter, the American Avocado Tree oil with skin repair and care action; Surfactant is at least a in alkyl-glutamic acid salt, N-acyl glutamic acid, N-acyl sarcosine, the C9-C15-monoalkyl phosphoric acid esters potassium; Wetting agent is at least a in glycerol, aminoacid, hyaluronic acid and the salt thereof; Emulsifying agent is at least a in spermaceti alcohol ether-20, glyceryl stearate, the hard ester acid alcohol of spermaceti ether-25, the citric acid bilaurate; Thickening agent is at least a in HANSHENGJIAO, guar gum and derivant thereof, the carbomer.
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| CN201110118721A CN102178617B (en) | 2011-05-09 | 2011-05-09 | Protein skin care products having function of skin repair and care |
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| CN201110118721A CN102178617B (en) | 2011-05-09 | 2011-05-09 | Protein skin care products having function of skin repair and care |
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| CN106811502A (en) * | 2015-12-01 | 2017-06-09 | 江南大学 | The preparation method of the skincare product containing almond polypeptide |
| CN105310945A (en) * | 2015-12-15 | 2016-02-10 | 钟苏 | Skin repair mask cream and preparation method thereof |
| CN106473945A (en) * | 2016-07-21 | 2017-03-08 | 北京东方艾美生物技术股份有限公司 | A kind of preparation method of keratin facial mask |
| US9993578B1 (en) * | 2017-01-12 | 2018-06-12 | Lorstan Pharmaceutical, LLC | Silicone oil-in-water composition useful as an injectable filler and as a scaffold for collagen growth |
| CN107260571A (en) * | 2017-06-08 | 2017-10-20 | 刘佩华 | Protein skin care item with skin repair and care action |
| CN108283617A (en) * | 2018-04-24 | 2018-07-17 | 上海上水和肌化妆品有限公司 | A kind of composition and forming method of skin basement membrane maintenance |
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| CN108524402A (en) * | 2018-07-09 | 2018-09-14 | 福建省海乐威生物工程有限公司 | A kind of face cream for having effects that cutin and repairing |
| CN109700998B (en) * | 2019-02-25 | 2022-02-08 | 曾湘红 | Compound skin injury regeneration repairing agent and preparation method thereof |
| CN112370410A (en) * | 2020-12-29 | 2021-02-19 | 石狮市蓝思婷鸟化妆品科技有限公司 | Preparation method of whitening and moisturizing mask |
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