CN103908415B - A kind of facial film and preparation method thereof - Google Patents
A kind of facial film and preparation method thereof Download PDFInfo
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- CN103908415B CN103908415B CN201410157889.4A CN201410157889A CN103908415B CN 103908415 B CN103908415 B CN 103908415B CN 201410157889 A CN201410157889 A CN 201410157889A CN 103908415 B CN103908415 B CN 103908415B
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Abstract
The invention discloses a kind of facial film, described facial film includes film bag A and film bag B, equipped with mask in described film bag A, equipped with adding heat posted in described film bag B, the inner side of the inner side of described film bag A and described film bag B is close together, the outside of described film bag B is air-vent face, and described air-vent face is by airtight film phonograph seal.Skin barrier structure repaired by facial film in this facial film, fundamentally solves skin barrier poor effect and causes moisture of skin to scatter and disappear too fast problem, reduces the noninductive of moisture of skin and scatter and disappear, can long-acting raising moisture content of skin, moisturizing is more effective；This facial film avoids the interpolation of nerve stimulation exothermic mixture, reduces the zest of product, makes product milder；This facial film contains and adds heat posted, and use in winter facial film warm is comfortable, blood circulation promoting, improves the assimilation effect of effect material, improves the comfortable experience of user；And facial film heating and temperature control is suitable for, it is possible to effectively keep stablizing of product efficacy thing.
Description
Technical field
The invention belongs to household chemicals field, be specifically related to a kind of warm moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof.
Background technology
What existing facial film market circulation was sold is general facial film, and more is show individual character on the formula of essence, carries out the market segments but without the warm facial film used for the winter.
Market circulation moisture saver mask present situation:
(1) moisturizing approach one: only add hygroscopic agent (such as: glycerol, propylene glycol, butanediol) in cosmetics and make horny layer form steam gradient from inside to outside, supplements the loss that surface moisture evaporates to dry environment.Skin ambient relative humidity is at least up to 70%, and hygroscopic agent could absorb moisture from external environment, and when in reality, relative humidity is to reach, the hygroscopic agent of major part external is to absorb moisture from corium in non-ambient.
(2) moisturizing approach two: add epidermis closing composition (such as: wax class, silicone oil, vaseline) in cosmetics and reduce moisture evaporation.By reaching to suppress cuticular water loss for the closing of skin, and protection skin is not disturbed by external substance.The feature of this kind of wetting agent is to be absorbed by the skin, and can form one layer of oil film, and the moisture of isolation skin is to air evaporation thus reaching to reduce cuticular water loss.
Market circulation heating facial film present situation:
(1) the neurostimulating materials such as capsaicin, Rhizoma Zingiberis Recens extract, Vanillyl butyl ether, cephrol butyl ether, vanillyl alcohol isopropyl ether are added.
This sentences capsaicin and the neurostimulating mechanism of action is sketched: capsaicin activates VR1, calcium is from channel opener, flow of calcium ions, in kytoplasm, calcium ion concentration raises, cause neuron and fiber release neuropeptide thereof, as: Arg-Pro-Lys-Pro-Gln-Gln-Phe-Phe-Gly-Leu-Met-NH2, neurokinin A, calcitonin-gene-related peptide, vasoactive intestinal peptide and excitatory amino acid, such as glutamic acid, aspartic acid.But the concrete machine causing neurocyte release Arg-Pro-Lys-Pro-Gln-Gln-Phe-Phe-Gly-Leu-Met-NH2 still imperfectly understands, Purkiss etc. isolated culture dorsal root ganglion neurons it was found that, capsaicin cause Arg-Pro-Lys-Pro-Gln-Gln-Phe-Phe-Gly-Leu-Met-NH2 discharge possibly through two kinds of mechanism: one depends on extracellular calcium and synaptosome coupling protein 25Kpa (SNAP-25);Another kind, when acellular outer calcium ion, it is not necessary to SNAP-25, capsaicin also can successfully stimulate ganglionic cell to release Arg-Pro-Lys-Pro-Gln-Gln-Phe-Phe-Gly-Leu-Met-NH2.
(2) with the material of massaging heating for declaring, there is no real heating effect.
Market moisture saver mask shortcoming:
Moistening effect is instant, and long-acting moistening effect is not good.
Market heating facial film shortcoming:
(1) skin irritation is big, it is easy to cause allergy.
(2) falseness is declared, without real warm sensation, customer experience feedback is not good.
Cause the reason of disadvantage mentioned above:
(1) do not pay attention to the skin self structure integrity importance to skin moisture-keeping, it does not have start with from skin moisture-keeping mechanism, start with from repairing skin barrier structure, fundamentally solve skin water loss problem.
(2) capsaicin, cephrol butyl ether, Vanillyl butyl ether, the heat sensitizer such as vanillyl alcohol isopropyl ether, it is by stimulating neuron, promotes human body to make stress, increase veins beneath the skin blood circulation amount, so that human body skin is rubescent, heating.The commonly used normal physiological mechanism that can upset human body skin, causes allergy, and subcutaneous red blood streak is expanded.
(3) with publicity for amusement, without real warm sensation.
Summary of the invention
The weak point that it is an object of the invention to overcome prior art to exist and provide and a kind of be possible to prevent moisture of skin loss, long-acting moisturizing and there is the facial film of warm effect；Meanwhile, the preparation method that present invention also offers described facial film.
For achieving the above object, the technical scheme that the present invention takes: a kind of facial film, described facial film includes film bag A and film bag B, equipped with mask in described film bag A, equipped with adding heat posted in described film bag B, the inner side of the inner side of described film bag A and described film bag B is close together, and the outside of described film bag B is air-vent face, and described air-vent face is by airtight film phonograph seal.
Preferred implementation as facial film of the present invention, described mask includes facial mask liquid and face paper, described facial mask liquid comprises the component of following weight portion: deionized water 31-94 part, emulsifying agent 0.2-5 part, skin closure agent 0.01-10 part, skin-nourishing agent 1-5 part, hygroscopic agent 1.1-13 part, cutin moisture-binding agent 0.55-10.5 part, skin repair factor 0.5-20 part, skin nature moisturizing factor 2-5 part, preservative 0.1-0.5 part.
When the facial mask liquid of described mask contains the combination of components of the above weight portion, " the skin repair factor " therein, " the skin moisture-keeping factor ", " skin closure agent " and other nutritional labeling have synergism, formula system is made to play lipid between reparation horn cell, increase keratodermatitis water content, improving horny layer Bound moisture ratio, nutritive maintenance skin etc. acts on.
The present invention sets about from repairing skin physiology structure, coordinate the effect of skin closure agent, skin-nourishing agent, the skin repair factor and skin nature moisturizing factor again, hygroscopic agent can draw large quantity of moisture and in combination from corium, no matter at low humidity or under high humidity conditions, all there is identical high-hygroscopicity, thus allowing the moisture within skin better be deposited in inside skin, reduce the lost degree of moisture of skin.
As the preferred implementation of facial film of the present invention, described emulsifying agent is at least one in cetearyl Fructus Canarii albi grease and Olivem 1000；Described skin closure agent is at least one in vaseline, ceramide and liquid paraffin；Described skin-nourishing agent is at least one in Semen pruni armeniacae oil, Butyrospermum parkii fruit ester and Vitamin E acetate；Described hygroscopic agent is at least one in sorbitol, 1,3 butylene glycol, trehalose and glycerol；Described cutin moisture-binding agent is at least one in reed fragrant plant oil and hyaluronic acid；The described skin repair factor is at least one in glycine, alanine, valine, isoleucine, leucine, proline, arginine, aspartic acid, glutamic acid, L-threonine, citric acid and glycine betaine；Described skin nature moisturizing factor is at least one in serine, sodium lactate, pyrrolidone sodium carboxylate, carbamide, potassium salt aqueous solution and magnesium chloride brine；Described preservative is at least one in double; two imidazolidinyl urea and phenoxyethanol.
In the selection of skin closure agent described above; vaseline is a kind of mineral wax; it will not be absorbed by the skin; one protecting film can be formed in skin surface; the moisture making skin not easily evaporates lost, and it is largely insoluble in water, can be attached on skin for a long time; therefore there is good moistening effect, be very suitable for dry skin and use；Liquid paraffin has low irritability and good closure due to mineral oil, so there being the effect of the moisture evaporation intercepting skin.
In the selection of skin-nourishing agent described above, Semen pruni armeniacae oil is a kind of natural wetting agent, rich in mineral substances, protein and various vitamin, is a kind of skin care and the splendid vegetable oil of moisturizing effect, and it can effectively facilitate cell turnover；Vitamin E acetate has osmosis, the protection to xerosis cutis and ultraviolet injury, and reducing lipid peroxidation has good effect.
In the selection of hygroscopic agent described above, sorbitol can absorb less moisture from air；1,3 butylene glycol 5 DEG C, humidity 50% time hydroscopicity be 25%, 25 DEG C, humidity 75% time hydroscopicity be 35%；Trehalose can be dissolved in water becomes thick colloidal liquid, has certain hygroscopicity, can absorb moisture from the external world, increases water content of stratum corneum；The water absorbing properties of glycerol is the 39% of weight, has stronger absorbability.
In the selection of cutin moisture-binding agent described above, reed fragrant plant oil forms the cagelike structure of uniqueness because of polyglycerolmethacrylate, reed fragrant plant oil is made to have water-soluble skin emollient and the strong point of glossy skin emollient concurrently, multi-functional moisturizing substrate, increase skinfeel and lubricity, improve moisture retention, there is lock outlet capacity；Hyaluronic acid is a kind of acid mucopolysaccharide, and it is the important foundation material that skin water is tender, itself is also a kind of composition of human body, and it has special water retention, 100 times of deal more up to itself weight, thus improving horny layer Bound moisture ratio.
In the selection of the skin repair factor described above, glycine is the main component of collagen protein；Alanine is the ultimate unit constituting protein, is one of 21 seed amino acids forming human body protein；Valine, isoleucine, leucic effect are the metabolism controlling protein；Proline is high moisturizing composition in water-soluble amino acid, and the synergism mainly by PCA and lactic acid produces；Arginic effect is moisturizing and horny layer softening layer；The effect of aspartic acid is to promote skin metabolism；The effect of glutamic acid is to promote skin moisture-keeping and smooth；The effect of L-threonine is that human body skin is had water holding ability, can promote phospholipid synthesis and fatty acid oxidation；The effect of citric acid is to improve stratum corneum；The effect of glycine betaine is moistening, moisturizing, has certain antibacterial anti-inflammatory effect.
In the selection of skin nature moisturizing factor described above, serine is present in the protein-Si polymeric protein (Filaggrin) in human epidermal layer, bears the vital task of skin moisture-keeping；The effect of pyrrolidone sodium carboxylate is available to moisture content and the elasticity of skin；Carbamide is a kind of useful moisturizing ingredient, and it is present in the middle of the horny layer of skin, belongs to the main component of skin nature moisturizing factor, and for skin, carbamide has moisturizing and effect of soft cutin, so also being able to prevent horny layer from blocking pore；The effect of potassium salt aqueous solution and magnesium chloride brine is that electrolyte balance regulates, and supplements mineral salt.
Preferred implementation as facial film of the present invention, described hygroscopic agent is the mixture of sorbitol, 1,3 butylene glycol, trehalose and glycerol, sorbitol in described hygroscopic agent, 1, the total weight parts of 3-butanediol and trehalose is 0.1-10 part, and in described hygroscopic agent, the weight portion of glycerol is 1-3 part；Cutin moisture-binding agent of the present invention is the oily and hyaluronic mixture of reed fragrant plant, and in described cutin moisture-binding agent, the weight portion of reed fragrant plant oil is 0.5-10 part, and in described cutin moisture-binding agent, hyaluronic weight portion is 0.05-0.5 part.
According to the different mechanism of action, wetting agent is divided into 4 classes:
1. the oils and fats moisturizing of water evaporates is prevented.Grease on skin, forms moisture barrier, does not allow water evaporates, be called closure moisturizing.
2. the moisture-absorbing moisture-keeping of outside moisture is absorbed.
3. in conjunction with the hydration moisturizing of hydration.
4. the reparation moisturizing of horn cell is repaired.
In the selection of hygroscopic agent described above, sorbitol, 1,3-butanediol, trehalose and glycerol belong to the 2nd kind of moisturizing mechanism, in the selection of cutin moisture-binding agent described above, reed fragrant plant oil and hyaluronic acid belong to the 3rd kind of moisturizing mechanism, fit again other material synergism, it is possible to full 4 moisturizing mechanism, thus reaching perfect moisture-keeping efficacy.
As the preferred implementation of facial film of the present invention, described in add heat posted and include exothermic material, gelatin layer and non-woven bag, described exothermic material is positioned in described non-woven bag, and described non-woven bag adheres to the inner side of described film bag B by gelatin layer.
As the preferred implementation of facial film of the present invention, when, after the closing membrane torn on described air-vent face, the temperature adding heat posted brings up to 45 ± 3 DEG C.There is corresponding pore quantity how many and hole diameter size adjustment according to adding heat posted surface area with the ventilative situation of non-woven bag, control heating layer heating stability contorting at 45 ± 3 DEG C, the stability of the functional component that facial mask essence adds can be kept while heating facial film.In a particular embodiment of the present invention, selecting the surface area adding heat posted is 100-169cm2, air-vent quantity is 100-250, and vent diameter is 5-6mm, thus controlling heating layer heating stability contorting at 45 ± 3 DEG C.
As the preferred implementation of facial film of the present invention, described exothermic material comprises the component of following weight portion: reduced iron powder 20-60 part of 200 orders, activated carbon 5-20 part of 100 orders, sodium chloride 2-7 part, insulation material 30-40 part, wood flour 30-35 part, aluminium powder 1-5 part, magnetic water 5-20 part.
Described exothermic material chooses the combination of each component described above, avoid the interpolation of the heat sensitizers such as pungent such as capsaicin, cephrol butyl ether, Vanillyl butyl ether, vanillyl alcohol isopropyl ether, the normal physiological mechanism of human body skin will not be upset, without there is the problem causing allergy, subcutaneous red blood streak to expand.
Before using, air-vent face is sealed by one layer of airtight film.During use, tearing the airtight film sealing described air-vent face, jiggle bag, air can enter film bag B, then contacts with exothermic material through nonwoven layer, and following chemical reaction occurs:
Negative pole: Fe-2e-=Fe2+Positive pole: O2+2H2O+4e-=4OH-
2Fe+O2+2H2O=2Fe(OH)2
4Fe(OH)2+2H2O+O2=4Fe(OH)3
2Fe(OH)3=Fe2O3+3H2O。
As the preferred implementation of facial film of the present invention, described insulation material is at least one in expanded perlite, Vermiculitum and zeolite.
It addition, the preparation method that the present invention also provides for a kind of facial film described above, the mask prepared, for first preparing mask respectively and adding heat posted, is then put into film bag A by described preparation method, and the heating prepared is placed with into film bag B.
As the preferred implementation of the preparation method of facial film of the present invention, said method comprising the steps of:
One, the preparation of mask
(1) first Water-solubility Material being dissolved with deionized water, heating stirs to 80-85 DEG C；
(2) then with another container, oil-soluble heating material is melted completely to 80 to 85 DEG C, stand-by；
(3) when stirring, oil-soluble material is joined in Water-solubility Material, start homogenizing, homogenizing 10-20 minute, be uniformly dispersed to material body；
(4) stirring 10-20 minute is continued；
(5) stirring cools down finely dispersed material to 45 DEG C；
(6) add low temperature to add materials, stir；
(7) qualified rear discharging, fill sealer are detected；
Described Water-solubility Material includes hygroscopic agent and cutin moisture-binding agent, and described oil-soluble material includes skin closure agent and emulsifying agent, and described low temperature adds materials and includes skin-nourishing agent, the skin repair factor, skin nature moisturizing factor and preservative；
Two, the preparation of heat posted is added
(1) preparation of exothermic material: by the reduced iron powder of 200 orders, the activated carbon of 100 orders, sodium chloride, insulation material, wood flour, aluminium powder, magnetic water, Homogeneous phase mixing, namely obtain exothermic material；
(2) exothermic material prepared is positioned in non-woven bag, and sticks gelatin layer in the side of non-woven bag；
Three, the preparation of facial film
The above-mentioned mask prepared is put in film bag A, the heating prepared is placed with in film bag B.
Described above prepare mask equipment be: use edible-type rustless steel produce, for instance: rustless steel 314L type or 316 types；The yarn core filter using pore radius to be 0.05-0.2 μm.Described above prepare mask environment be: adopt the air cleaner of 1,000,000 grades.In the preparation of mask described above, described qualified finger meets enterprise's acceptance criteria of facial film, and this standard-required is higher than industry standard.
Mask of the present invention, starts with from skin moisture-keeping mechanistic point, apery body skin components structure, repairs skin barrier effect, it is prevented that moisture of skin loses, long-acting moisturizing.Meanwhile, utilize the oxidation heat liberation principle of iron powder, by special package design, control exothermic temperature, on the basis that facial film functional component is constant, preheat facial film, thus releasing the ice-cold difficult problem of winter facial film.Simultaneously because the rising of temperature, be conducive to opening of pore, thus promoting the skin absorption to active substance.
In moisturizing mechanism, additionally it is different from commercially available general MASQUE APAISANT HYDRATANT (usually taking water suction or skin surface to cover single mode), simultaneously without heating composition such as capsaicin, Rhizoma Zingiberis Recens extract, Vanillyl butyl ether, cephrol butyl ether in formula, non-stimulated, safer.Facial film of the present invention is consistent with the market demand, has society's prospect preferably.
The beneficial effects of the present invention is: the invention provides a kind of facial film, skin barrier structure repaired by facial film in this facial film, fundamentally solve skin barrier poor effect and cause moisture of skin to scatter and disappear too fast problem, reduce the noninductive of moisture of skin to scatter and disappear, can long-acting raising moisture content of skin, moisturizing is more effective；This facial film avoids the interpolation of nerve stimulation exothermic mixture, reduces the zest of product, makes product milder；This facial film contains and adds heat posted, and use in winter facial film warm is comfortable, blood circulation promoting, improves the assimilation effect of effect material, improves the comfortable experience of user；And facial film heating and temperature control is suitable for, it is possible to effectively keep stablizing of product efficacy thing.Facial film of the present invention is warming mask product under the premise ensureing facial film functional component effectiveness, cosily use in the winter time with Convenient face membrane, promote the blood circulation of human body facial film, promote the absorption of active substance, realize facial film warm and replenishing water and preserving moisture combines, fill up winter and warm the blank in moisturizing MASQUE APAISANT HYDRATANT market.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of a kind of embodiment of facial film of the present invention；
Fig. 2 is the schematic cross-section of facial film described in Fig. 1；
Fig. 3 is the preparation technology flow chart of a kind of embodiment of mask of the present invention；
Fig. 4 is the change that experimenter uses product forward and backward 1 hour, 4 hours and 8 hours moisture content of skin；
In Fig. 1 and 2: 1 is film bag A, 2 is film bag B, and 3 is air-vent face, and 4 is air-vent, and 5 is airtight film, and 6 is mask, and 7 for adding heat posted；
In Fig. 4: abscissa 1 is for before using product, and abscissa 2 is for using after product 1 hour, and abscissa 3 is for using after product 4 hours, and abscissa 4 is for using after product 8 hours.
Detailed description of the invention
For better illustrating the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
A kind of embodiment of facial film of the present invention, as depicted in figs. 1 and 2, described facial film includes film bag A1 and film bag B2, equipped with mask 6 in described film bag A1, equipped with adding heat posted 7 in described film bag B2, the inner side of the inner side of described film bag A1 and described film bag B2 is close together, and the outside of described film bag B2 is air-vent face 3, and described air-vent face 3 is sealed by airtight film 5.
Described mask includes facial mask liquid and face paper, described facial mask liquid comprises the component of following weight portion: deionized water 31 parts, emulsifying agent 5 parts, skin closure agent 10 parts, skin-nourishing agent 1 part, hygroscopic agent 1.1 parts, cutin moisture-binding agent 10.5 parts, the skin repair factor 0.5 part, skin nature moisturizing factor 5 parts, preservative 0.1 part.Described emulsifying agent is cetearyl Fructus Canarii albi grease；Described skin closure agent is liquid paraffin；Described skin-nourishing agent is Semen pruni armeniacae oil and the mixture of Butyrospermum parkii fruit ester；Described hygroscopic agent is sorbitol；Described cutin moisture-binding agent is the oily and hyaluronic mixture of reed fragrant plant, and the parts by weight of reed fragrant plant oil are 10 parts, and hyaluronic weight portion is 0.5 part；The described skin repair factor is the mixture of glycine and isoleucine；Described skin nature moisturizing factor is carbamide；Described preservative is double; two imidazolidinyl urea.
The described heat posted 7 that adds includes exothermic material, gelatin layer and non-woven bag, and described exothermic material is positioned in non-woven bag, and described non-woven bag adheres to the inner side of described film bag B2 by gelatin layer.Described exothermic material comprises the component of following weight portion: the reduced iron powder of 200 orders 20 parts, the activated carbon of 100 orders 5 parts, 2 parts of sodium chloride, insulation material 30 parts, wood flour 35 parts, aluminium powder 5 parts, magnetic water 20 parts.Described insulation material is expanded perlite.
The preparation method of facial film described in the present embodiment comprises the following steps:
One, the preparation of mask, as shown in Figure 3:
(1) first Water-solubility Material being dissolved with deionized water, heating stirs to 80-85 DEG C；
(2) then with another container, oil-soluble heating material is melted completely to 80 to 85 DEG C, stand-by；
(3) when stirring, oil-soluble material is joined in Water-solubility Material, start homogenizing, homogenizing 10-20 minute, be uniformly dispersed to material body；
(4) stirring 10-20 minute is continued；
(5) stirring cools down finely dispersed material to 45 DEG C；
(6) add low temperature to add materials, stir；
(7) qualified rear discharging, fill sealer are detected；
Described Water-solubility Material includes hygroscopic agent and cutin moisture-binding agent, and described oil-soluble material includes skin closure agent and emulsifying agent, and described low temperature adds materials and includes skin-nourishing agent, the skin repair factor, skin nature moisturizing factor and preservative；
Described qualified finger meets enterprise's acceptance criteria of facial film, and this standard-required is higher than industry standard；
Two, the preparation of heat posted is added
(1) preparation of exothermic material: by the reduced iron powder of 200 orders, the activated carbon of 100 orders, sodium chloride, insulation material, wood flour, aluminium powder, magnetic water, Homogeneous phase mixing, namely obtain exothermic material；
(2) exothermic material prepared is positioned in non-woven bag, and sticks gelatin layer in the side of non-woven bag；
Three, the preparation of facial film
The above-mentioned mask prepared is put in film bag A, the heating prepared is placed with in film bag B, add the non-woven bag in heat posted and adhered to the inner side of described film bag B by gelatin layer.
The Preparation equipment of mask described in the present embodiment is that the rustless steel using edible-type produces, for instance: rustless steel 314L type or 316 types；The yarn core filter using pore radius to be 0.05-0.2 μm；Prepare the air cleaner that environment is employing 1,000,000 grades.
Facial film described in the present embodiment, before using, air-vent face 3 is covered by one layer of airtight film 5；During use, tearing the airtight film 5 that air-vent face 3 covers, jiggle bag, air can enter film bag B2 by air-vent 4, then contacts with exothermic material through nonwoven layer, and following chemical reaction occurs:
Negative pole: Fe-2e-=Fe2+Positive pole: O2+2H2O+4e-=4OH-
2Fe+O2+2H2O=2Fe(OH)2
4Fe(OH)2+2H2O+O2=4Fe(OH)3
2Fe(OH)3=Fe2O3+3H2O；
Producing heat after reaction, after tearing the airtight film 5 on described air-vent face 3, the temperature adding heat posted 7 brings up to 45 ± 3 DEG C, can keep the stability of the functional component that facial mask essence adds while heating facial film.When after the airtight film 5 torn on air-vent face 3, the temperature adding heat posted 7 brings up to how many, main by adding the surface area of heat posted, the ventilative situation of non-woven bag and the quantity of the upper air-vent 4 of described air-vent 3 and diameter decision, the present embodiment selects the surface area adding heat posted to be 100-169cm2, air-vent quantity is 100-250, vent diameter is 5-6mm.
Embodiment 2
A kind of embodiment of facial film of the present invention, facial film described in the present embodiment except the component of facial mask liquid and exothermic material and content different from embodiment 1 except, all the other are all identical with embodiment 1.
In facial film described in the present embodiment, facial mask liquid comprises the component of following weight portion: deionized water 94 parts, emulsifying agent 0.2 part, skin closure agent 0.01 part, skin-nourishing agent 5 parts, hygroscopic agent 13 parts, cutin moisture-binding agent 0.55 part, the skin repair factor 20 parts, skin nature moisturizing factor 2 parts, preservative 0.5 part.Described emulsifying agent is Olivem 1000；Described skin closure agent is vaseline；Described skin-nourishing agent is Vitamin E acetate；Described hygroscopic agent is the mixture of sorbitol, 1,3 butylene glycol, trehalose and glycerol, and the gross weight number of sorbitol, 1,3 butylene glycol and trehalose is 10 parts, and the parts by weight of glycerol are 3 parts；Described cutin moisture-binding agent is the oily and hyaluronic mixture of reed fragrant plant, and the weight portion of reed fragrant plant oil is 0.5 part, and hyaluronic parts by weight are 0.05 part；The described skin repair factor is glycine betaine；Described skin nature moisturizing factor is the mixture of serine and sodium lactate；Described preservative is phenoxyethanol.
Exothermic material described in the present embodiment comprises the component of following weight portion: the reduced iron powder of 200 orders 30 parts, the activated carbon of 100 orders 8 parts, 3 parts of sodium chloride, insulation material 32 parts, wood flour 32 parts, aluminium powder 4 parts, magnetic water 8 parts.Described insulation material is zeolite.
Embodiment 3
A kind of embodiment of facial film of the present invention, facial film described in the present embodiment except the component of facial mask liquid and exothermic material and content different from embodiment 1 except, all the other are all identical with embodiment 1.
In facial film described in the present embodiment, facial mask liquid comprises the component of following weight portion: deionized water 50 parts, emulsifying agent 1 part, skin closure agent 2 parts, skin-nourishing agent 2 parts, hygroscopic agent 2 parts, cutin moisture-binding agent 1 part, the skin repair factor 2 parts, skin nature moisturizing factor 3 parts, preservative 0.4 part.Described emulsifying agent is the mixture of cetearyl Fructus Canarii albi grease and Olivem 1000；Described skin closure agent is the mixture of vaseline and ceramide；Described skin-nourishing agent is Butyrospermum parkii fruit ester；Described hygroscopic agent is the mixture of sorbitol and 1,3 butylene glycol；Described cutin moisture-binding agent is reed fragrant plant oil；The described skin repair factor is glycine, alanine, valine, isoleucine and leucic mixture；Described skin nature moisturizing factor is the mixture of serine, sodium lactate and pyrrolidone sodium carboxylate；Described preservative is the mixture of double; two imidazolidinyl urea and phenoxyethanol.
Exothermic material described in the present embodiment comprises the component of following weight portion: the reduced iron powder of 200 orders 40 parts, the activated carbon of 100 orders 10 parts, 5 parts of sodium chloride, insulation material 35 parts, wood flour 30 parts, aluminium powder 3 parts, magnetic water 15 parts.Described insulation material is Vermiculitum.
Embodiment 4
A kind of embodiment of facial film of the present invention, facial film described in the present embodiment except the component of facial mask liquid and exothermic material and content different from embodiment 1 except, all the other are all identical with embodiment 1.
In facial film described in the present embodiment, facial mask liquid comprises the component of following weight portion: deionized water 60 parts, emulsifying agent 5 parts, skin closure agent 5 parts, skin-nourishing agent 3 parts, hygroscopic agent 5 parts, cutin moisture-binding agent 4 parts, the skin repair factor 10 parts, skin nature moisturizing factor 4 parts, preservative 0.3 part.Described emulsifying agent is cetearyl Fructus Canarii albi grease；Described skin closure agent is ceramide；Described skin-nourishing agent is the mixture of Semen pruni armeniacae oil, Butyrospermum parkii fruit ester and Vitamin E acetate；Described hygroscopic agent is the mixture of sorbitol, 1,3 butylene glycol, trehalose and glycerol, and the gross weight number of sorbitol, 1,3 butylene glycol and trehalose is 4 parts, and the parts by weight of glycerol are 1 part；Described cutin moisture-binding agent is the oily and hyaluronic mixture of reed fragrant plant, and the parts by weight of reed fragrant plant oil are 3.5 parts, and hyaluronic parts by weight are 0.5 part；The described skin repair factor is the mixture of proline, arginine, aspartic acid and glutamic acid；Described skin nature moisturizing factor is the mixture of carbamide, potassium salt aqueous solution and magnesium chloride brine；Described preservative is phenoxyethanol.
Exothermic material described in the present embodiment comprises the component of following weight portion: the reduced iron powder of 200 orders 50 parts, the activated carbon of 100 orders 15 parts, 6 parts of sodium chloride, insulation material 38 parts, wood flour 34 parts, aluminium powder 2 parts, magnetic water 10 parts.Described insulation material is the mixture of expanded perlite and Vermiculitum.
Embodiment 5
A kind of embodiment of facial film of the present invention, facial film described in the present embodiment except the component of facial mask liquid and exothermic material and content different from embodiment 1 except, all the other are all identical with embodiment 1.
In facial film described in the present embodiment, facial mask liquid comprises the component of following weight portion: deionized water 80 parts, emulsifying agent 4 parts, skin closure agent 8 parts, skin-nourishing agent 4 parts, hygroscopic agent 10 parts, cutin moisture-binding agent 7 parts, the skin repair factor 16 parts, skin nature moisturizing factor 4 parts, preservative 0.2 part.Described emulsifying agent is Olivem 1000；Described skin closure agent is the mixture of vaseline, ceramide and liquid paraffin；Described skin-nourishing agent is the mixture of Semen pruni armeniacae oil, Butyrospermum parkii fruit ester and Vitamin E acetate；Described hygroscopic agent is the mixture of sorbitol, 1,3 butylene glycol, trehalose and glycerol, and the gross weight number of described sorbitol, 1,3 butylene glycol and trehalose is 8 parts, and the parts by weight of glycerol are 2 parts；Described cutin moisture-binding agent is hyaluronic acid；The described skin repair factor is the mixture of citric acid and glycine betaine；Described skin nature moisturizing factor is the mixture of potassium salt aqueous solution and magnesium chloride brine；Described preservative is the mixture of double; two imidazolidinyl urea and phenoxyethanol.
Exothermic material described in the present embodiment comprises the component of following weight portion: the reduced iron powder of 200 orders 60 parts, the activated carbon of 100 orders 20 parts, 7 parts of sodium chloride, insulation material 40 parts, wood flour 33 parts, aluminium powder 1 part, magnetic water 20 parts.Described insulation material is the mixture of expanded perlite, Vermiculitum and zeolite.
Embodiment 6
The skin moisture-keeping eficac Clinical test of facial film of the present invention:
1, test objective: observe moisture saver mask of the present invention to the long-acting moisture-keeping efficacy of skin.
2, test method and design
2.1 test methods and number
Adopting the clinical research test of self cross-reference clinic moisture-keeping efficacy open, number 20 people is included in test in.
2.2 experimenters select
2.2.1 the women's health person at 20 to 55 years old ages；
2.2.2 can use test product as requested and complete testing experiment.
2.3 tested products, product using method and pot life
2.3.1 tested products
Tested products is moisture saver mask of the present invention.
2.3.2 product using method and the pot life
Experimenter's only single is bent side 2 place 5cm × 5cm at double; two forearms respectively and is used moisture saver mask, and every square centimeter makes consumption be 1 milligram, smears uniformly, until fully absorbing.
2.4 observing times
Observe 8 hours altogether.After experimenter enters metastable laboratory environment, within the 1st hour, 4 hours and 8 hours, carry out moisture content of skin mensuration (after sitting quietly 30 minutes) and after using product before use.
2.5 skin moisture-keeping effect study on the efficiency
2.5.1 apparatus measures
Use German company produce skin moisture measuring instrument (CM825), experimenter's target site skin being carried out moisture content of skin mensuration, target site is measured 3 times, takes its meansigma methods；Before being used by measurement product, use latter 1 hour, use latter 4 hours and use the change of the moisture content of skin numerical value of latter 8 hours to assess the moisture-keeping efficacy of this product.
2.5.2 apparatus measures requirement
Each experimenter is carried out with point each observing time before use by the mensuration of moisture content of skin by specialty researcher.Each apparatus measures condition keeps self-consistentency, and namely same target site is measured by same researcher, measures environmental condition basically identical.Furthermore, it desired to experimenter sits quietly 30 minutes before first test under metastable measurement environment, quiet under experimental enviroment after use product stay 8 hours.
3, result
3.1 experimenter's ordinary circumstances:
Selected qualified female subjects is 20 people, all completes test.During subject enrollment, the age is between 20 years old to 53 years old, average 29.9 ± 8.9 years old.
The change of 3.2 apparatus measures result moisture content of skin
Experimenter after using before product, using different moisturizer after 1 hour, 4 hours and 8 hours the numerical value of moisture content of skin in Table 1 and Fig. 1.1 see from the table below, experimenter is using after the more commercially available moisture saver mask of moisturizer of the present invention 1st hour, 4 hours and 8 hours measured moisture content of skin are all significantly increased (see table 1 and Fig. 4), and moisture saver mask of the present invention remains within higher level after using product 8 hours.
Table 1 uses different product different time sections moisture content of skin (%) to change
4, brief summary
By the moisture-keeping efficacy clinical trial of the single use of 20 experimenters moisture saver mask of the present invention (sample lot number 20131030A) and commercially available moisture saver mask (sample lot number 20131228A), result shows: experimenter is using 1mg/cm2Moisture saver mask after 1 hour, 4 hours and 8 hours, moisture content of skin substantially increases before all relatively using, and after 8 hours, moisture content of skin remains within higher level, has long lasting skin moisture-keeping efficacy.
5, conclusion
Facial film of the present invention has long lasting skin moisture-keeping efficacy.
Finally be should be noted that; above example is only in order to illustrate technical scheme but not limiting the scope of the invention; although the present invention being explained in detail with reference to preferred embodiment; it will be understood by those within the art that; technical scheme can be modified or equivalent replacement, without deviating from the spirit and scope of technical solution of the present invention.
Claims (7)
1. a facial film, it is characterized in that, described facial film includes film bag A and film bag B, equipped with mask in described film bag A, equipped with adding heat posted in described film bag B, the inner side of the inner side of described film bag A and described film bag B is close together, and the outside of described film bag B is air-vent face, and described air-vent face is by airtight film phonograph seal；
Described mask includes facial mask liquid and face paper, described facial mask liquid comprises the component of following weight portion: deionized water 31-94 part, emulsifying agent 0.2-5 part, skin closure agent 0.01-10 part, skin-nourishing agent 1-5 part, hygroscopic agent 1.1-13 part, cutin moisture-binding agent 0.55-10.5 part, skin repair factor 0.5-20 part, skin nature moisturizing factor 2-5 part, preservative 0.1-0.5 part；
Described emulsifying agent is at least one in cetearyl Fructus Canarii albi grease and Olivem 1000；Described skin closure agent is at least one in vaseline, ceramide and liquid paraffin；Described skin-nourishing agent is at least one in Semen pruni armeniacae oil, Butyrospermum parkii fruit fat and Vitamin E acetate；Described hygroscopic agent is the mixture of sorbitol, 1,3 butylene glycol, trehalose and glycerol, and in described hygroscopic agent, the total weight parts of sorbitol, 1,3 butylene glycol and trehalose is 0.1-10 part, and in described hygroscopic agent, the weight portion of glycerol is 1-3 part；Described cutin moisture-binding agent is the oily and hyaluronic mixture of reed fragrant plant, and in described cutin moisture-binding agent, the weight portion of reed fragrant plant oil is 0.5-10 part, and in described cutin moisture-binding agent, hyaluronic weight portion is 0.05-0.5 part；The described skin repair factor is at least one in glycine, alanine, valine, isoleucine, leucine, proline, arginine, aspartic acid, glutamic acid, L-threonine, citric acid and glycine betaine；Described skin nature moisturizing factor is at least one in serine, sodium lactate, pyrrolidone sodium carboxylate and carbamide；Described preservative is at least one in double; two imidazolidinyl urea and phenoxyethanol.
2. facial film according to claim 1, it is characterised in that described in add heat posted and include exothermic material, gelatin layer and non-woven bag, described exothermic material is positioned in described non-woven bag, and described non-woven bag adheres to the inner side of described film bag B by gelatin layer.
3. facial film according to claim 2, it is characterised in that when, after the airtight film torn on described air-vent face, the temperature adding heat posted brings up to 45 ± 3 DEG C.
4. the facial film according to Claims 2 or 3, it is characterised in that described exothermic material comprises the component of following weight portion: reduced iron powder 20-60 part of 200 orders, activated carbon 5-20 part of 100 orders, sodium chloride 2-7 part, insulation material 30-40 part, wood flour 30-35 part, aluminium powder 1-5 part, magnetic water 5-20 part.
5. facial film according to claim 4, it is characterised in that described insulation material is at least one in expanded perlite, Vermiculitum and zeolite.
6. the preparation method of the facial film as described in any one of claim 1-5, it is characterised in that the mask prepared, for first preparing mask respectively and adding heat posted, is then put into film bag A by described preparation method, and the heating prepared is placed with into film bag B.
7. facial film preparation method as claimed in claim 6, it is characterised in that said method comprising the steps of:
One, the preparation of mask
(1) first Water-solubility Material being dissolved with deionized water, heating stirs to 80-85 DEG C；
(2) then with another container, oil-soluble heating material is melted completely to 80 to 85 DEG C, stand-by；
(3) when stirring, oil-soluble material is joined in Water-solubility Material, start homogenizing, homogenizing 10-20 minute, be uniformly dispersed to material body；
(4) stirring 10-20 minute is continued；
(5) stirring cools down finely dispersed material to 45 DEG C；
(6) add low temperature to add materials, stir；
(7) qualified rear discharging, fill sealer are detected；
Described Water-solubility Material includes hygroscopic agent and cutin moisture-binding agent, and described oil-soluble material includes skin closure agent and emulsifying agent, and described low temperature adds materials and includes skin-nourishing agent, the skin repair factor, skin nature moisturizing factor and preservative；
Two, the preparation of heat posted is added
(1) preparation of exothermic material: by the reduced iron powder of 200 orders, the activated carbon of 100 orders, sodium chloride, insulation material, wood flour, aluminium powder, magnetic water, Homogeneous phase mixing, namely obtain exothermic material；
(2) exothermic material prepared is positioned in non-woven bag, and sticks gelatin layer in the side of non-woven bag；
Three, the preparation of facial film
The above-mentioned mask prepared is put in film bag A, the heating prepared is placed with in film bag B.
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105620921A (en) * | 2014-10-31 | 2016-06-01 | 深圳市小婉牛化妆品有限公司 | Heating device for sheet skin-care beauty mask |
| CN204468398U (en) * | 2014-12-23 | 2015-07-15 | 台州市泰澄电子科技有限公司 | A kind of cold/hot dressing facial mask device with ventilating structure |
| CN105982841A (en) * | 2015-02-06 | 2016-10-05 | 张祈 | Moisturizing and hydrating mask |
| TWI579414B (en) * | 2015-06-04 | 2017-04-21 | 廈門醫學高等專科學校 | Manufacturing method for electrochemically coating polymers in mask |
| CN105662913A (en) * | 2015-12-31 | 2016-06-15 | 杭州心悦化妆品有限公司 | High moisturizing toner |
| CN105832633A (en) * | 2016-04-28 | 2016-08-10 | 福建春伦茶业集团有限公司 | Moisturizing and skin whitening mask for restraining melanin forming |
| CN106474014A (en) * | 2016-12-12 | 2017-03-08 | 珍尔姿（广州）化妆品有限公司 | A kind of facial film with crease-resistant effect |
| CN109573300B (en) * | 2019-01-25 | 2020-01-14 | 湖北创界生物科技有限公司 | Facial mask packaging bag |
| CN110106629B (en) * | 2019-06-11 | 2021-08-17 | 绍兴蓝海纤维科技有限公司 | Hydrogel type alginate fiber non-woven fabric as well as preparation method and application thereof |
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