CN106566728A - Olive oil skincare soap and preparation method thereof - Google Patents

Olive oil skincare soap and preparation method thereof Download PDF

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Publication number
CN106566728A
CN106566728A CN201610936647.4A CN201610936647A CN106566728A CN 106566728 A CN106566728 A CN 106566728A CN 201610936647 A CN201610936647 A CN 201610936647A CN 106566728 A CN106566728 A CN 106566728A
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CN
China
Prior art keywords
olive oil
soap
beaker
soap base
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610936647.4A
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Chinese (zh)
Inventor
赵利霞
闵祥凤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LONGNAN XIANGYU OIL OLIVES DEVELOPMENT Co Ltd
Original Assignee
LONGNAN XIANGYU OIL OLIVES DEVELOPMENT Co Ltd
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Filing date
Publication date
Application filed by LONGNAN XIANGYU OIL OLIVES DEVELOPMENT Co Ltd filed Critical LONGNAN XIANGYU OIL OLIVES DEVELOPMENT Co Ltd
Priority to CN201610936647.4A priority Critical patent/CN106566728A/en
Publication of CN106566728A publication Critical patent/CN106566728A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/005Synthetic soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

Olive oil skincare soap is prepared from, by weight, 400 g of a soap base, 30-50 ml of pepper and moxa leaf water and 5-6 g of olive oil. A preparation method of the olive oil skincare soap comprises the steps that the soap base of 400 g is put into a beaker, the beaker is heated through a water bath method, and the soap base is stirred properly while the beaker is heated over water till the soap base is completely melted; then the 30-50 ml of pepper and moxa leaf water is added, and the mixture is stirred to be even; the 5-6 g of olive oil is added, and the new mixture is stirred to be even; and the liquid mixture is poured into a mold, and the mold is removed after the liquid is completely solidified. The skincare soap has good moistening, mosquito repelling and itching relieving effects; through characteristics of olive oil, bubbles are exquisite and moist; and the soap has abundant squalene extremely friendly to the skin, as well as fatty acid essential to human bodies, and the soap has the functions of cleaning, sterilization and skin protection. The raw materials are natural, no essence needs to be added, and neither irritation nor irritability is caused.

Description

Olive oil skin-protection soap and manufacture method
Technical field
The invention belongs to a kind of skin-protection soap, more particularly to a kind of olive oil skin protection of use castile soap matrix manufacturing Soap, the invention further relates to the manufacture method of olive oil skin-protection soap.
Background technology
Olive oil has the history of thousand of years in Mediterranean country, is described as " liquid golden " in west, " vegetable oil emperor Afterwards ", " Mediterranean manna ", reason are that its splendid natural health effect, beauty functions and preferable cooking use.Can Edible high-grade olive oil is the natural fruit oil extracted by physical cold squeezing process with just ripe or ripe Fructus oleae europaeae fresh fruit Juice, is the xylophyta oil for uniquely being used for the mankind in the form of naturalness in the world.
Olive oil absorbs rapid, effectively keeps rich in the Squalene splendid with skin affinity and essential fatty acid Skin elasticity and moist;Contained abundant monounsaturated fatty acid and Vitamin E, K, A, D etc. and phenols antioxidation in olive oil Material, can eliminate lip wrinkle, it is dry and cracked the effects such as, can be the cosmetics and skincare product of " eating ".
With the progress of society, articles for washing is abundant and more professional, and people wash one's hands, wash one's face and take a shower and are more happy to make With special articles for washing, the articles for washing even more specialty of child.But be added with the personal cleansing articles for use in modern times antibacterial, The adding ingredients such as preservative, synthetic perfume, synthetic dyestuff, synthctic fat and surfactant, are irritating to the skin, and can cause not Good anaphylaxiss.Although adding in Most of children articles for washing has Vitamin E, milk isoreactivity composition and Chinese medicinal ingredients, Being that surface activity raw material therein still more adopts chemically synthesized product.Child skin children is tender, to external world the zest opposing of environment Power is weak, so, it is particularly important the no added natural skin-cleaning articles for use of safety to be provided for child.
The content of the invention
Present invention aim at providing a kind of pure natural oil baby's skin-protection soap of the olive without chemical addition agent, the present invention is also provided The manufacture method of olive oil baby's skin-protection soap.
For achieving the above object, the first technical scheme that the present invention takes is as follows:A kind of olive oil skin-protection soap, by following heavy The raw material of amount number is prepared from:Soap base 400g, 30~50ml of green pepper Ai Shui and 5~6 g of olive oil.
A kind of manufacture method of olive oil skin-protection soap, it is characterised in that:Soap base 400g is put into beaker, is heated using immersion method Beaker, the agitation as appropriate soap base during water proof heating is carried out to beaker, until soap base melts completely;Green pepper Ai Shui is added then 30~50ml is stirred until homogeneous;5~6 g of olive oil is added to be stirred until homogeneous;Mould is poured in the state of liquid, treats to solidify completely The demoulding afterwards.
The soap base is obtained by saponification;The preparation method of soap base is:Weigh olive oil 500g, sodium hydroxide 60.75~64g, 141.5~150g of water;Olive oil is put in rustless steel container and is heated to 40 DEG C;Water is placed in into another container, Sodium hydroxide is added to the water into prepared sodium hydrate aqueous solution;When the temperature of the temperature and sodium hydrate aqueous solution of olive oil is all When 40 DEG C, sodium hydrate aqueous solution is slowly poured in olive oil and mixed, be gently mixed with egg-whisk, continue 20min, often afterwards Every 2~3min, under continuation stirring is several, stir when egg-whisk is lifted, drip the soap lye for going down soap lye surface in a reservoir and stay Under fine vestige, natural cooling is standby.
The saponification value of olive oil is:0.135;Generally the amount of sodium hydroxide is multiplied by its saponification equal to the weight of olive oil Valency.The present invention reduces 5%~10% to ensure that the fancy soap made is gentle to skin, making to retain the oils and fatss of reasonable amount in fancy soap The consumption of sodium hydroxide.
I.e. needed for 500g olive oil, the lower limit of amount of sodium hydroxide is:(500g×0.135)-(500g×0.135×10%) =60.75g;
Needed for 500g olive oil, the upper limit of amount of sodium hydroxide is:(500g×0.135)-(500g×0.135×5%)= 64.125g;
2.33~2.35 times for sodium hydroxide weight of the weight of water;I.e. the lower weight limit of water is 60.75 × 2.33=141.5g; I.e. the upper weight limit of water is 64.125 × 2.35=150.7g.
The preparation method of the green pepper Ai Shui is:By 500ml water, 10~12g Pericarpium Zanthoxylies and 15~18g Folium Artemisiae Argyis boiled rear infusion Obtain green pepper Ai Shui within 15 minutes.
The second technical scheme that the present invention is taken for achieving the above object is as follows:A kind of olive oil skin-protection soap, by following heavy The raw material of amount number is prepared from:Soap base 400g, Folium Artemisiae Argyi fresh 30~40ml of juice and 5~6g of olive oil.
Its manufacture method is:Fresh Folium Artemisiae Argyi squeezes with juice extractor after cleaning up that to obtain the fresh juice of Folium Artemisiae Argyi stand-by;Take soap base 400g is put into beaker, heats beaker using immersion method, the middle agitation as appropriate soap base of water proof heating process is carried out to beaker, until Soap base melts completely;Fresh 30~the 40ml of juice of Folium Artemisiae Argyi is then added to be stirred until homogeneous;5~6 g of olive oil is added to be stirred until homogeneous; The state of liquid pours mould into, the demoulding after solidifying completely.
Pericarpium Zanthoxyli can be used to outer being coated with and resist mosquito bite and skin disease, and Pericarpium Zanthoxyli has functions that anti-inflammation and sterilization;
Folium Artemisiae Argyi also known as Artemisia argyi, Artemisia argyi Levl. et Van. var. argyi cv. Qiai, Radix Artemisia ordosicae, nature and flavor are bitter, pungent, warm, enter spleen, liver and kidney channel.Energy dispelling cold and removing dampness, warming the meridian for stopping bleeding;Folium Artemisiae Argyi There are the effects such as antibacterial, antiviral, antiallergic, enhancing immunologic function.
The olive oil skin-protection soap that the present invention is provided has the advantages that olive oil, rich in the Squalene splendid with skin affinity And essential fatty acid, there is cleaning, sterilization and skin is protected.
As the characteristic of olive oil is so that foam is fine and smooth, moist.With the multiple use that washes one's face, takes a shower, washes one's hands, can expire The needs of the daily skin nursing of sufficient people, raw material need not add any essence from natural, non-stimulated, without anaphylaxis.The present invention It is a kind of moist, anthelmintic, the good skin-protection soap of antipruritic effect, as oils and fatss are remained after saponification, therefore imitates with more preferable moisturizing Really, the more feel of mild and moist, foam are fine and smooth abundant, are particularly suitable for child's use.The skin-protection soap color and luster made of green pepper Ai Shui Shallow brown green, simple and elegant delicate fragrance;The skin-protection soap made of the fresh juice of Folium Artemisiae Argyi is light green color, glittering and translucent, pure and fresh pleasant.
Prevalence has handmade soap in recent years.The present invention is applicable not only to industrialization manufacture, is more suitable for child's handmade soap and all finds pleasure in Portion, allows child oneself to make, teaches through lively activities, provide unlimited imagination space for child, allow child to give full play to oneself Individual character, go out the colourful handmade soap oneself liked with different handmade soap die modelings.
Specific embodiment
Embodiment 1;Step one, prepares soap base:Weigh olive oil 500g, sodium hydroxide 61g, water 142g;Olive oil is put Enter;Water is placed in into another container, sodium hydroxide is added to the water into prepared sodium hydroxide water-soluble Liquid;When the temperature of the temperature and sodium hydrate aqueous solution of olive oil is all 40 DEG C into, sodium hydrate aqueous solution is slowly poured olive Mix in olive oil, be gently mixed with egg-whisk, continue 20min, afterwards every 2~3min, continue stirring it is several under, stir to lifting During egg-whisk, drip the soap lye for going down soap lye surface in a reservoir and leave fine vestige, show that the degree for stirring is fully equal Even, natural cooling is standby.
Step 2, prepares green pepper Ai Shui:500ml water, 12g Pericarpium Zanthoxylies and 16g Folium Artemisiae Argyis boiled rear infusion is obtained into green pepper Chinese mugwort for 15 minutes Water.
Step 3, prepares olive oil skin-protection soap;
(1)Weigh:Soap base 400g, green pepper Ai Shui 40ml, olive oil 5g;
(2)Soap base 400g is put into beaker, heats beaker using immersion method, suitably stirs during water proof heating is carried out to beaker Soap base is mixed, until soap base melts completely to homogeneous;
(3)Green pepper Ai Shui 40ml are added into jar agitation to uniform;
(4)5 g of olive oil is added into jar agitation to uniform;
(5)Pour the liquid in beaker into mould, after 24 hours, solidify the demoulding completely.
Embodiment 2;Step one, prepares soap base:Weigh olive oil 500g, sodium hydroxide 64g, water 150g;Remaining is with enforcement Example 1.
Step 2, prepares green pepper Ai Shui:500ml water, 11g Pericarpium Zanthoxylies and 18g Folium Artemisiae Argyis boiled rear infusion is obtained into green pepper Chinese mugwort for 15 minutes Water.
Step 3, prepares olive oil skin-protection soap;
(1)Weigh:Soap base 400g, green pepper Ai Shui 50ml, olive oil 6g;
(2)Soap base 400g is put into beaker, and remaining is with embodiment 1.
(3)Green pepper Ai Shui 50ml are added into jar agitation to uniform;
(4)6 g of olive oil is added into jar agitation to uniform;
(5)Pour the liquid in beaker into mould, after 24 hours, solidify the demoulding completely.
Embodiment 3;Step one, prepares soap base:Weigh olive oil 500g, sodium hydroxide 64g, water 148g;Remaining is with enforcement Example 1.
Step 2, prepares green pepper Ai Shui:500ml water, 10g Pericarpium Zanthoxylies and 15g Folium Artemisiae Argyis boiled rear infusion is obtained into green pepper Chinese mugwort for 15 minutes Water.
Step 3, prepares olive oil skin-protection soap;
(1)Weigh:Soap base 400g, green pepper Ai Shui 35ml, olive oil 5.5g;
(2)Soap base 400g is put into beaker, and remaining is with embodiment 1.
(3)Green pepper Ai Shui 35ml are added into jar agitation to uniform;
(4)Olive oil 5.5g is added into jar agitation to uniform;
(5)Pour the liquid in beaker into mould, after 24 hours, solidify the demoulding completely.
Embodiment 4;Step one, prepares soap base:With embodiment 1.
Step 2, prepares the fresh juice of Folium Artemisiae Argyi:Fresh Folium Artemisiae Argyi squeezes with juice extractor after cleaning up that to obtain the fresh juice of Folium Artemisiae Argyi stand-by.
Step 3, prepares olive oil skin-protection soap;
(1)Weigh:The fresh juice 40ml of soap base 400g, Folium Artemisiae Argyi, olive oil 5g;
(2)Soap base 400g is put into beaker, and remaining is with embodiment 1.
(3)Folium Artemisiae Argyi fresh juice 45ml is added into jar agitation to uniform;
(4)Olive oil 5g is added into jar agitation to uniform;
(5)Pour the liquid in beaker into mould, after 24 hours, solidify the demoulding completely.
Embodiment 5;Step one, prepares soap base:With embodiment 1.
Step 2, prepares the fresh juice of Folium Artemisiae Argyi:With embodiment 4.
Step 3, prepares olive oil skin-protection soap;
(1)Weigh:The fresh juice 30ml of soap base 400g, Folium Artemisiae Argyi, olive oil 5.5g;
(2)Soap base 400g is put into beaker, and remaining is with embodiment 1.
(3)Folium Artemisiae Argyi fresh juice 35ml is added into jar agitation to uniform;
(4)Olive oil 5.5g is added into jar agitation to uniform;
(5)Pour the liquid in beaker into mould, after 24 hours, solidify the demoulding completely.

Claims (4)

1. a kind of olive oil skin-protection soap, it is characterised in that be prepared from by the raw material of following portions by weight:Soap base 400g, green pepper Ai Shui 30~50ml and 5~6 g of olive oil;Its manufacture method is:Soap base 400g is put into beaker, heats beaker using immersion method, right Beaker carries out agitation as appropriate soap base during water proof heating, until soap base melts completely;Green pepper 30~50ml of Ai Shui are added then It is stirred until homogeneous;5~6 g of olive oil is added to be stirred until homogeneous;Mould is poured in the state of liquid, the demoulding after solidifying completely.
2. olive oil skin-protection soap as claimed in claim 1, it is characterised in that:The preparation method of the green pepper Ai Shui is:Will The boiled rear infusion of 500ml water, 10~12g Pericarpium Zanthoxylies and 15~18g Folium Artemisiae Argyis obtains green pepper Ai Shui in 15 minutes.
3. a kind of olive oil skin-protection soap, it is characterised in that be prepared from by the raw material of following portions by weight:Soap base 400g, Folium Artemisiae Argyi are fresh 30~40ml of juice and 5~6g of olive oil;Its manufacture method is:Fresh Folium Artemisiae Argyi squeezes with juice extractor after cleaning up that to obtain Folium Artemisiae Argyi fresh Juice is stand-by;Take soap base 400g and be put into beaker, beaker is heated using immersion method, beaker is being carried out in water proof heating process suitably Stirring soap base, until soap base melts completely;Fresh 30~the 40ml of juice of Folium Artemisiae Argyi is then added to be stirred until homogeneous;Add 5~6 g of olive oil It is stirred until homogeneous;Mould is poured in the state of liquid, the demoulding after solidifying completely.
4. the olive oil skin-protection soap as described in claim 1,2 or 3, it is characterised in that:The preparation method of the soap base is:Weigh Olive oil 500g, 60.75~64g of sodium hydroxide, 141.5~150g of water;Olive oil is put in rustless steel container and is heated to 40 ℃;Water is placed in into another container, sodium hydroxide is added to the water into prepared sodium hydrate aqueous solution;When the temperature and hydrogen-oxygen of olive oil When the temperature for changing sodium water solution is all 40 DEG C, sodium hydrate aqueous solution is slowly poured in olive oil and mixed, with egg-whisk gently Stirring, continues 20min, afterwards every 2~3min, under continuation stirring is several, stirs when egg-whisk is lifted, drips the soap lye for going down Soap lye surface in a reservoir leaves fine vestige, and natural cooling is standby.
CN201610936647.4A 2016-11-01 2016-11-01 Olive oil skincare soap and preparation method thereof Pending CN106566728A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107779320A (en) * 2017-10-16 2018-03-09 山东师范大学 A kind of green peel of walnut clean skin product and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104419569A (en) * 2013-08-22 2015-03-18 罗伟 Preparation method for household olive-oil soap
CN105219567A (en) * 2015-10-19 2016-01-06 西林县大银子铁皮石斛种销农民专业合作社 A kind of Herba Dendrobii beauty soap and preparation method thereof
CN105219564A (en) * 2015-10-26 2016-01-06 詹俊英 A kind of wormwood shea butter children plant bath soap and preparation method thereof
CN105287324A (en) * 2014-06-09 2016-02-03 刘瑛 Health-care prickly ash liquid soap

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104419569A (en) * 2013-08-22 2015-03-18 罗伟 Preparation method for household olive-oil soap
CN105287324A (en) * 2014-06-09 2016-02-03 刘瑛 Health-care prickly ash liquid soap
CN105219567A (en) * 2015-10-19 2016-01-06 西林县大银子铁皮石斛种销农民专业合作社 A kind of Herba Dendrobii beauty soap and preparation method thereof
CN105219564A (en) * 2015-10-26 2016-01-06 詹俊英 A kind of wormwood shea butter children plant bath soap and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
娜娜妈: "《自己做100%保养级手工皂娜娜妈的30中无毒手工皂》", 31 March 2012, 华夏出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107779320A (en) * 2017-10-16 2018-03-09 山东师范大学 A kind of green peel of walnut clean skin product and preparation method thereof

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Application publication date: 20170419